Acta Crystallographica Section E

Structure Reports Online

Volume 70, Part 5 (May 2014)

organic compounds

wm5018 scheme

Acta Cryst. (2014). E70, o558    [ doi:10.1107/S1600536814007971 ]

2,8,15,18,21,24,31,37,44,47,50,53-Dodeca­oxahepta­cyclo­[,35.06,33.09,14.025,30.038,43]octa­penta­conta-1(54),4,6(33),9(14),10,12,25(30),26,28,34,38(43),39,41,55,57-penta­deca­ene di­chloro­methane disolvate

J. Y. Yun, S. W. Ahn, D. H. Kim, W. Sim and J. Y. Lee

Abstract: In the title compound, C46H50O12·2CH2Cl2, each dual 20-crown-6 unit crystallizes with two di­chloro­methane solvent mol­ecules. The crown unit mol­ecule lies about an inversion centre located at the central benzene ring. The two crown ring groups adopt an anti conformation, stabilized by weak intra­molecular C-H...O inter­actions. In the crystal, the crown unit mol­ecules and the solvent mol­ecules are linked by C-H...O inter­actions into a three-dimensional network.

CCDC reference: 996417

htmldisplay filedownload file

Hyper-Text Markup Language (HTML) file (91.9 kbytes)
[ doi:10.1107/S1600536814007971/wm5018sup0.html ]
Supplementary materials


To open or display or play some files, you may need to set your browser up to use the appropriate software. See the full list of file types for an explanation of the different file types and their related mime types and, where available links to sites from where the appropriate software may be obtained.

The download button will force most browsers to prompt for a file name to store the data on your hard disk.

Where possible, images are represented by thumbnails.

 bibliographic record in  format

  Find reference:   Volume   Page   
  Search:     From   to      Advanced search

Copyright © International Union of Crystallography
IUCr Webmaster