# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared), status flag # data_I _shelx_title ' cu_dm13596_0m in P41212' _shelx_refln_list_code 4 _shelx_F_calc_maximum 1339.91 _exptl_crystal_F_000 3744.00 _reflns_d_resolution_high 0.8220 loop_ _space_group_symop_operation_xyz 'x, y, z' '-y+1/2, x+1/2, z+1/4' '-x, -y, z+1/2' 'y+1/2, -x+1/2, z+3/4' 'x+1/2, -y+1/2, -z+3/4' 'y, x, -z' '-x+1/2, y+1/2, -z+1/4' '-y, -x, -z+1/2' _cell_length_a 13.9016 _cell_length_b 13.9016 _cell_length_c 38.8340 _cell_angle_alpha 90.000 _cell_angle_beta 90.000 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 1 0 152610.89 175615.66 9660.12 o 0 2 0 14.30 69.39 24.53 o 1 2 0 70.90 291.29 17.35 o 2 2 0 13.56 371.74 52.04 o 1 3 0 20.82 45.97 10.97 o 3 3 0 1016.81 997.58 73.60 o 0 4 0 64665.13 70276.38 5516.63 o 1 4 0 345.66 567.20 38.32 o 2 4 0 320.85 333.18 27.54 o 3 4 0 520.54 407.05 370.20 o 4 4 0 1233.85 1266.40 138.78 o 1 5 0 36189.29 39082.45 1530.05 o 2 5 0 2959.18 3897.27 193.47 o 3 5 0 511.07 529.25 61.33 o 4 5 0 8513.64 11072.56 637.52 o 5 5 0 3369.99 3591.31 204.24 o 0 6 0 128243.01 156235.25 12195.58 o 1 6 0 436.06 1223.71 147.46 o 2 6 0 692.95 831.82 121.44 o 3 6 0 4.10 19.83 32.13 o 4 6 0 751.94 1113.08 58.31 o 5 6 0 129.24 234.75 22.88 o 6 6 0 3498.41 4490.77 449.23 o 1 7 0 31442.39 36643.34 1816.68 o 2 7 0 350.16 828.92 58.42 o 3 7 0 3253.21 3814.47 159.66 o 4 7 0 12.20 42.13 19.67 o 5 7 0 18050.84 17811.52 432.01 o 6 7 0 9788.93 10845.28 282.51 o 7 7 0 6323.49 18332.62 584.21 o 0 8 0 198576.39 189789.61 8644.33 o 1 8 0 98.97 304.40 42.71 o 2 8 0 50.29 962.89 73.60 o 3 8 0 7301.74 11460.62 360.28 o 4 8 0 173.34 297.09 33.54 o 5 8 0 7478.94 6445.95 184.87 o 6 8 0 33051.02 37386.44 793.90 o 7 8 0 736.07 2449.94 160.28 o 8 8 0 33728.25 31910.54 725.19 o 1 9 0 309.63 650.41 83.79 o 2 9 0 22.75 450.88 43.37 o 3 9 0 3047.07 2311.59 95.98 o 4 9 0 3697.98 3462.35 121.70 o 5 9 0 15057.13 12900.31 326.32 o 6 9 0 6789.27 6970.46 139.70 o 7 9 0 2441.35 2834.21 68.54 o 8 9 0 12823.43 10268.22 189.53 o 9 9 0 4844.91 4443.34 134.34 o 0 10 0 7119.70 7009.13 386.26 o 1 10 0 12783.76 12294.15 345.31 o 2 10 0 2077.19 2222.71 85.13 o 3 10 0 1792.40 1426.63 62.09 o 4 10 0 1415.80 1387.24 84.48 o 5 10 0 3606.55 3771.46 88.41 o 6 10 0 114.20 157.61 22.68 o 7 10 0 19.37 229.52 24.27 o 8 10 0 111.58 167.94 24.79 o 9 10 0 308.86 334.14 26.13 o 10 10 0 2679.81 2637.04 91.05 o 1 11 0 1467.17 2196.47 97.04 o 2 11 0 102.31 550.30 36.20 o 3 11 0 13.33 142.66 26.59 o 4 11 0 1374.13 1460.14 47.06 o 5 11 0 888.01 1012.11 38.88 o 6 11 0 275.56 831.15 35.55 o 7 11 0 631.94 1427.18 58.03 o 8 11 0 194.90 185.11 25.38 o 9 11 0 268.16 187.58 23.57 o 10 11 0 191.35 426.38 28.49 o 11 11 0 14.00 -9.05 33.54 o 0 12 0 9159.04 8744.59 271.86 o 1 12 0 2465.40 2724.54 77.74 o 2 12 0 10.28 489.22 37.05 o 3 12 0 8414.67 10403.23 206.76 o 4 12 0 16.57 184.77 25.84 o 5 12 0 3425.37 2833.35 67.76 o 6 12 0 828.69 1654.89 50.64 o 7 12 0 2403.85 3261.26 74.77 o 8 12 0 3908.45 4417.28 96.64 o 9 12 0 8831.13 7816.55 163.44 o 10 12 0 146.05 151.31 24.78 o 11 12 0 81.25 226.15 27.69 o 1 13 0 26369.25 26327.41 487.42 o 2 13 0 2000.25 3401.49 94.85 o 3 13 0 1500.06 1460.46 58.74 o 4 13 0 3869.60 3333.14 93.45 o 5 13 0 20456.13 18136.84 320.55 o 6 13 0 6062.37 5287.80 116.52 o 7 13 0 10060.84 13386.74 280.98 o 8 13 0 9670.03 7995.56 166.21 o 9 13 0 4777.69 3683.31 90.10 o 10 13 0 241.65 477.58 38.79 o 0 14 0 29299.73 25649.53 701.04 o 1 14 0 127.84 609.76 54.76 o 2 14 0 1729.27 2047.94 86.35 o 3 14 0 1401.40 1187.51 60.49 o 4 14 0 1386.36 1208.63 53.70 o 5 14 0 971.74 999.58 51.24 o 6 14 0 3843.15 4473.13 123.87 o 7 14 0 3139.10 2695.95 83.42 o 8 14 0 5884.08 4826.45 121.74 o 9 14 0 505.63 426.66 45.96 o 1 15 0 176.29 626.50 49.06 o 2 15 0 0.14 426.58 37.74 o 3 15 0 59.51 153.76 38.27 o 4 15 0 2673.60 1842.39 73.50 o 5 15 0 409.79 982.01 123.85 o 6 15 0 304.32 494.25 46.67 o 7 15 0 16.63 147.06 29.44 o 0 16 0 67.63 -0.64 93.89 o 1 16 0 12.25 110.65 35.89 o 2 16 0 0.67 712.80 54.43 o 3 16 0 64.13 171.67 41.09 o 4 16 0 315.64 305.18 35.18 o 5 16 0 373.45 585.39 69.39 o 0 1 1 479.23 492.48 30.05 o 1 1 1 142622.25 130895.19 15604.44 o -1 2 1 92.44 198.73 15.02 o 0 2 1 48658.66 59844.77 2694.26 o 1 2 1 23.64 115.65 43.37 o 2 2 1 425.84 471.11 41.63 o -2 3 1 46254.87 48059.86 2190.07 o -1 3 1 71.60 34.70 13.11 o 0 3 1 42.80 127.74 20.03 o 1 3 1 55.89 46.26 20.03 o 2 3 1 46432.66 49035.79 1897.33 o 3 3 1 2604.13 2109.85 126.59 o -3 4 1 5250.73 4639.53 667.89 o -2 4 1 253.54 458.34 58.97 o -1 4 1 11666.97 13226.45 509.55 o 0 4 1 7203.28 7790.16 360.57 o 1 4 1 10702.41 11926.85 723.74 o 2 4 1 266.45 371.60 29.44 o 3 4 1 5192.39 4978.85 399.00 o 4 4 1 72.92 55.51 28.87 o -4 5 1 4975.45 4431.78 275.80 o -3 5 1 592.13 546.60 61.33 o -2 5 1 18899.56 21940.29 998.21 o -1 5 1 13635.63 14547.47 653.05 o 0 5 1 2412.29 2455.45 152.97 o 1 5 1 13466.81 13540.27 639.95 o 2 5 1 18843.48 21746.88 994.87 o 3 5 1 597.20 582.32 61.33 o 4 5 1 4972.18 4437.30 269.87 o 5 5 1 3037.18 2222.47 95.61 o -5 6 1 4613.39 4470.80 121.16 o -4 6 1 2154.25 2596.18 109.89 o -3 6 1 1059.00 1326.53 81.69 o -2 6 1 9204.18 9870.96 832.70 o -1 6 1 2061.18 2777.40 196.27 o 0 6 1 499863.50 596642.75 32862.82 o 1 6 1 1957.35 3129.20 166.10 o 2 6 1 9198.60 10384.82 588.81 o 3 6 1 1115.32 1381.47 136.43 o 4 6 1 2274.97 2519.75 110.60 o 5 6 1 4599.09 4542.15 122.10 o 6 6 1 26909.76 36582.64 1130.89 o -6 7 1 14639.66 13715.78 353.36 o -5 7 1 22770.85 24463.90 601.19 o -4 7 1 347.59 405.90 30.77 o -3 7 1 7297.59 8069.07 295.40 o -2 7 1 2084.35 2531.47 105.08 o -1 7 1 104266.95 107781.53 3642.61 o 0 7 1 1609.58 1842.22 191.39 o 1 7 1 102870.16 105253.25 5265.73 o 2 7 1 1904.25 2325.74 121.73 o 3 7 1 7477.16 8044.44 304.71 o 4 7 1 355.52 389.73 27.87 o 5 7 1 22561.74 23530.87 573.10 o 6 7 1 14637.80 13692.88 354.38 o 7 7 1 57169.43 56938.45 1203.17 o -7 8 1 15107.56 13477.85 275.55 o -6 8 1 45193.95 42026.62 939.03 o -5 8 1 3215.86 3915.78 119.98 o -4 8 1 190.48 301.29 35.05 o -3 8 1 40401.68 39999.48 1185.18 o -2 8 1 14446.83 13862.62 425.34 o -1 8 1 3516.19 3410.12 166.72 o 0 8 1 19856.92 24911.59 1682.75 o 1 8 1 3915.84 3799.20 151.60 o 2 8 1 14164.59 13592.95 458.13 o 3 8 1 39567.27 39073.71 1185.18 o 4 8 1 183.74 258.80 33.54 o 5 8 1 3293.51 3602.70 111.14 o 6 8 1 45631.92 41588.44 844.36 o 7 8 1 15365.51 13682.32 263.53 o 8 8 1 12504.65 13933.20 218.96 o -8 9 1 226.56 1087.15 36.70 o -7 9 1 7090.92 6828.55 122.75 o -6 9 1 8416.34 8302.02 162.21 o -5 9 1 96.76 607.53 86.63 o -4 9 1 1205.75 1349.43 63.96 o -3 9 1 19.61 240.02 34.20 o -2 9 1 4581.53 4610.20 252.90 o -1 9 1 5787.91 5578.20 246.08 o 0 9 1 289.00 323.05 61.33 o 1 9 1 5910.08 5930.96 246.08 o 2 9 1 4567.11 4948.37 188.67 o 3 9 1 9.85 202.31 32.21 o 4 9 1 1218.17 1324.40 65.14 o 5 9 1 96.39 567.18 69.03 o 6 9 1 8581.53 8236.46 175.67 o 7 9 1 7151.79 7009.08 134.54 o 8 9 1 200.33 1049.50 39.88 o 9 9 1 1070.47 1295.00 45.16 o -9 10 1 711.61 706.57 34.50 o -8 10 1 48.20 58.39 21.73 o -7 10 1 2056.40 1981.20 54.96 o -6 10 1 467.74 627.93 30.61 o -5 10 1 3216.21 3537.91 79.88 o -4 10 1 1130.29 1099.72 56.06 o -3 10 1 524.59 746.02 44.63 o -2 10 1 1876.43 2024.44 79.86 o -1 10 1 5542.34 6091.22 189.34 o 0 10 1 1243.53 1557.06 81.78 o 1 10 1 5646.00 6245.03 190.43 o 2 10 1 1788.00 2104.07 98.61 o 3 10 1 572.13 884.22 51.93 o 4 10 1 1215.22 1154.13 55.08 o 5 10 1 3184.35 3368.00 86.53 o 6 10 1 481.38 595.61 29.27 o 7 10 1 2019.24 1909.67 53.09 o 8 10 1 53.44 72.16 21.88 o 9 10 1 705.05 741.00 33.48 o 10 10 1 603.08 624.39 31.80 o -10 11 1 953.24 937.87 39.26 o -9 11 1 290.35 421.24 27.45 o -8 11 1 62.48 165.45 23.73 o -7 11 1 4081.83 4110.04 82.24 o -6 11 1 824.68 1002.58 37.75 o -5 11 1 258.79 337.09 27.84 o -4 11 1 1563.51 1892.98 53.39 o -3 11 1 258.48 211.30 26.87 o -2 11 1 3309.27 2960.41 79.86 o -1 11 1 1334.63 1472.80 79.02 o 0 11 1 138.88 253.63 36.49 o 1 11 1 1188.13 1155.29 64.36 o 2 11 1 3245.72 2862.15 86.46 o 3 11 1 280.39 197.53 30.76 o 4 11 1 1579.96 1773.94 53.74 o 5 11 1 299.47 426.00 29.33 o 6 11 1 780.82 902.88 35.86 o 7 11 1 4252.66 4200.80 83.89 o 8 11 1 73.12 190.16 25.59 o 9 11 1 286.76 380.44 29.58 o 10 11 1 966.25 905.28 38.78 o 11 11 1 103.48 164.81 26.01 o -11 12 1 976.52 816.23 44.51 o -10 12 1 733.31 816.54 43.06 o -9 12 1 1227.55 2281.12 88.53 o -8 12 1 4771.06 4998.34 106.03 o -7 12 1 6320.36 5764.37 111.46 o -6 12 1 3603.18 4097.46 87.28 o -5 12 1 134.29 496.05 30.52 o -4 12 1 1905.61 1968.80 53.51 o -3 12 1 17792.17 17534.24 306.08 o -2 12 1 2767.88 2549.88 69.80 o -1 12 1 2179.30 2809.78 79.44 o 0 12 1 7365.75 7546.74 170.94 o 1 12 1 2063.21 2574.60 75.61 o 2 12 1 2747.11 2503.63 75.88 o 3 12 1 18031.58 17721.25 344.35 o 4 12 1 1943.76 1975.22 60.54 o 5 12 1 171.29 496.18 32.11 o 6 12 1 3776.60 4133.97 89.37 o 7 12 1 6308.56 5812.17 115.79 o 8 12 1 4678.04 5110.88 115.64 o 9 12 1 1257.95 2346.92 99.75 o 10 12 1 724.73 788.25 34.93 o 11 12 1 969.16 746.08 42.50 o -10 13 1 1221.04 1238.28 57.05 o -9 13 1 707.41 963.19 57.83 o -8 13 1 543.43 1470.49 73.23 o -7 13 1 19234.28 18591.52 348.17 o -6 13 1 172.65 976.10 48.16 o -5 13 1 1840.28 3607.68 137.48 o -4 13 1 940.07 1099.96 49.25 o -3 13 1 932.89 1047.26 48.60 o -2 13 1 8706.60 8256.32 166.98 o -1 13 1 16504.83 17404.91 325.00 o 0 13 1 4172.50 4499.18 119.18 o 1 13 1 16232.55 16737.62 324.26 o 2 13 1 8941.57 8313.22 180.42 o 3 13 1 981.36 1157.06 55.45 o 4 13 1 951.25 1156.17 51.25 o 5 13 1 1746.63 3518.33 118.83 o 6 13 1 182.55 976.60 71.05 o 7 13 1 19221.55 18425.58 382.10 o 8 13 1 614.31 1831.49 107.56 o 9 13 1 741.31 1048.11 49.54 o 10 13 1 1157.09 1195.93 57.05 o -9 14 1 545.10 387.57 45.96 o -8 14 1 1377.38 2137.72 67.58 o -7 14 1 945.84 1255.80 53.63 o -6 14 1 6463.06 7734.50 181.47 o -5 14 1 877.39 889.36 50.21 o -4 14 1 1586.06 1491.55 60.61 o -3 14 1 121.56 92.53 32.37 o -2 14 1 3692.37 4422.12 110.23 o -1 14 1 2593.02 2665.21 83.84 o 0 14 1 11698.29 13291.28 269.93 o 1 14 1 2557.20 2656.09 85.55 o 2 14 1 3674.55 4357.66 139.05 o 3 14 1 128.95 88.16 37.04 o 4 14 1 1650.30 1466.21 61.68 o 5 14 1 903.89 948.68 51.61 o 6 14 1 6405.22 7710.32 193.36 o 7 14 1 928.87 1269.71 49.06 o 8 14 1 1474.71 2297.60 70.82 o 9 14 1 562.65 501.95 38.32 o -7 15 1 178.90 447.82 39.13 o -6 15 1 993.88 1030.09 61.21 o -5 15 1 3775.86 3139.59 105.43 o -4 15 1 430.21 746.22 63.09 o -3 15 1 695.11 519.39 44.80 o -2 15 1 2106.61 2116.22 72.23 o -1 15 1 714.29 1254.82 57.67 o 0 15 1 63.30 61.18 36.33 o 1 15 1 795.51 1355.59 62.52 o 2 15 1 2047.06 1996.47 70.30 o 3 15 1 733.02 566.88 47.60 o 4 15 1 396.42 517.91 46.24 o 5 15 1 3771.85 3246.25 113.32 o 6 15 1 1059.56 1193.37 61.72 o 7 15 1 165.56 523.82 38.32 o -5 16 1 1978.00 1474.57 138.78 o -4 16 1 600.55 692.22 52.84 o -3 16 1 666.47 644.15 52.81 o -2 16 1 2341.59 2098.36 78.71 o -1 16 1 872.56 779.97 50.35 o 0 16 1 71.75 123.66 35.89 o 1 16 1 905.83 725.62 49.86 o 2 16 1 2213.56 1911.08 88.33 o 3 16 1 750.05 725.88 48.43 o 4 16 1 575.66 734.26 49.40 o 5 16 1 1996.15 1526.62 156.13 o 0 1 2 858.87 703.81 40.06 o 1 1 2 112681.88 109862.76 10590.89 o -1 2 2 3463.13 3378.79 150.24 o 0 2 2 666.75 824.95 59.51 o 1 2 2 3020.51 2758.51 135.97 o 2 2 2 15658.87 17784.96 2116.45 o -2 3 2 69162.20 77212.02 6800.38 o -1 3 2 1269.56 1512.45 115.24 o 0 3 2 23.00 43.37 24.53 o 1 3 2 1261.83 1594.30 80.13 o 2 3 2 68697.36 77696.38 3022.53 o 3 3 2 237.44 375.80 66.80 o -3 4 2 1189.54 988.83 121.44 o -2 4 2 749.97 949.42 66.24 o -1 4 2 56515.89 62775.25 2864.42 o 0 4 2 34930.25 40206.89 2152.09 o 1 4 2 57259.57 64098.23 2857.77 o 2 4 2 809.05 1139.54 66.24 o 3 4 2 1277.54 924.38 64.26 o 4 4 2 2.92 34.70 36.80 o -4 5 2 9570.62 10823.19 630.94 o -3 5 2 2413.67 2556.56 177.55 o -2 5 2 10351.80 11428.87 650.14 o -1 5 2 4395.14 5197.08 312.62 o 0 5 2 743.22 1076.99 66.24 o 1 5 2 4861.86 5933.65 275.05 o 2 5 2 10407.25 11342.73 527.44 o 3 5 2 2495.64 2763.70 177.55 o 4 5 2 9668.49 11027.51 630.94 o 5 5 2 1143.44 1761.62 74.96 o -5 6 2 270.43 502.03 31.02 o -4 6 2 768.02 1250.03 132.71 o -3 6 2 24441.37 26350.09 1301.67 o -2 6 2 66384.72 72983.86 4035.78 o -1 6 2 40395.04 47095.71 2643.48 o 0 6 2 10716.46 24963.64 1977.66 o 1 6 2 40546.63 47486.45 2133.23 o 2 6 2 65980.42 71305.62 3953.64 o 3 6 2 24139.67 25943.17 1095.71 o 4 6 2 867.19 1398.34 80.48 o 5 6 2 220.51 479.24 27.94 o 6 6 2 237014.91 214915.55 5261.24 o -6 7 2 3956.74 4607.27 138.99 o -5 7 2 5719.49 6906.60 199.77 o -4 7 2 1640.31 1894.34 65.62 o -3 7 2 11380.52 11147.62 400.50 o -2 7 2 13413.72 13954.77 502.52 o -1 7 2 147382.11 144295.45 6116.43 o 0 7 2 19854.30 20704.76 1081.53 o 1 7 2 149158.64 146944.48 8539.52 o 2 7 2 13216.60 14464.07 513.54 o 3 7 2 11264.61 11294.90 367.18 o 4 7 2 1649.11 1817.30 61.37 o 5 7 2 6023.86 6809.35 205.72 o 6 7 2 3961.54 4340.27 138.99 o 7 7 2 160385.19 151378.16 3174.48 o -7 8 2 1031.58 1559.62 52.82 o -6 8 2 9433.99 12162.71 282.49 o -5 8 2 5790.99 6451.48 167.47 o -4 8 2 607.98 807.19 46.40 o -3 8 2 8601.32 9589.65 303.97 o -2 8 2 8480.99 7698.98 251.06 o -1 8 2 6538.82 7207.66 283.30 o 0 8 2 3929.77 4958.41 202.66 o 1 8 2 5880.40 6688.03 256.73 o 2 8 2 8708.71 8083.99 274.70 o 3 8 2 8880.88 9650.67 394.63 o 4 8 2 594.28 719.72 47.82 o 5 8 2 5713.35 5886.13 166.64 o 6 8 2 9283.30 11729.98 267.60 o 7 8 2 1144.37 1757.22 52.30 o 8 8 2 524.26 961.71 36.15 o -8 9 2 1820.27 2058.91 53.53 o -7 9 2 2964.32 3519.64 73.93 o -6 9 2 1272.38 2008.96 78.98 o -5 9 2 8109.57 7917.39 212.04 o -4 9 2 11072.37 10667.18 258.34 o -3 9 2 1502.02 1488.63 71.50 o -2 9 2 844.07 2156.40 260.22 o -1 9 2 2061.56 2845.62 139.16 o 0 9 2 229.11 511.91 73.60 o 1 9 2 1939.64 2683.47 135.97 o 2 9 2 920.08 2295.84 268.89 o 3 9 2 1557.51 1511.08 83.70 o 4 9 2 10957.74 10826.36 279.77 o 5 9 2 8179.48 7915.77 198.76 o 6 9 2 1341.88 2000.03 83.16 o 7 9 2 2919.87 3509.40 73.09 o 8 9 2 1879.01 1993.26 50.88 o 9 9 2 81.70 564.51 29.42 o -9 10 2 3262.60 2811.75 62.89 o -8 10 2 591.94 602.51 29.35 o -7 10 2 71.67 279.18 24.56 o -6 10 2 332.52 498.57 28.01 o -5 10 2 2379.55 2327.21 63.45 o -4 10 2 740.03 908.20 45.84 o -3 10 2 1106.67 1212.30 56.13 o -2 10 2 1761.20 1980.10 79.64 o -1 10 2 6863.91 6714.49 197.67 o 0 10 2 6283.88 5861.65 185.89 o 1 10 2 6583.25 6255.76 184.52 o 2 10 2 1838.37 1995.33 87.93 o 3 10 2 1265.56 1368.49 90.94 o 4 10 2 675.87 765.71 46.54 o 5 10 2 2535.78 2522.47 70.62 o 6 10 2 342.05 502.00 29.56 o 7 10 2 30.23 207.53 22.45 o 8 10 2 622.93 689.92 31.55 o 9 10 2 3161.84 2723.10 64.68 o 10 10 2 6.51 -21.38 21.38 o -10 11 2 966.07 964.49 41.84 o -9 11 2 91.62 252.37 23.67 o -8 11 2 61.15 66.19 21.76 o -7 11 2 2379.65 2896.24 63.12 o -6 11 2 1284.42 1254.10 41.95 o -5 11 2 443.23 545.68 31.52 o -4 11 2 744.86 1182.44 40.80 o -3 11 2 246.17 208.62 26.45 o -2 11 2 2634.91 2713.76 77.40 o -1 11 2 1137.26 1114.77 54.58 o 0 11 2 1463.03 1809.55 65.77 o 1 11 2 1121.76 1041.55 50.59 o 2 11 2 2661.52 2877.13 79.17 o 3 11 2 269.05 239.04 30.14 o 4 11 2 694.62 1043.27 41.44 o 5 11 2 418.37 569.11 32.50 o 6 11 2 1281.06 1231.03 43.16 o 7 11 2 2400.41 2969.97 66.00 o 8 11 2 73.36 102.30 23.57 o 9 11 2 113.26 220.86 26.23 o 10 11 2 928.73 897.88 35.66 o 11 11 2 1690.73 1706.05 54.53 o -11 12 2 49.42 110.88 23.72 o -10 12 2 2075.39 1931.70 56.04 o -9 12 2 2141.04 2409.29 68.44 o -8 12 2 908.67 1416.09 42.77 o -7 12 2 291.71 945.59 34.70 o -6 12 2 7564.51 7176.78 130.38 o -5 12 2 1074.46 1136.24 41.72 o -4 12 2 1260.73 965.57 41.39 o -3 12 2 5231.94 6310.25 121.83 o -2 12 2 996.20 1117.58 43.99 o -1 12 2 2131.28 2358.36 68.36 o 0 12 2 365.48 1101.66 50.31 o 1 12 2 2236.73 2569.19 76.79 o 2 12 2 972.33 1032.08 46.28 o 3 12 2 5136.57 6235.16 133.42 o 4 12 2 1233.59 1008.87 45.01 o 5 12 2 1060.48 1132.02 43.96 o 6 12 2 7391.14 7028.89 148.30 o 7 12 2 320.83 1039.80 47.57 o 8 12 2 919.90 1424.01 56.02 o 9 12 2 2298.41 2493.04 70.84 o 10 12 2 2072.61 1923.74 60.45 o 11 12 2 46.92 117.49 24.88 o -10 13 2 547.70 688.35 49.14 o -9 13 2 68.78 467.86 29.95 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