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[Contents scheme]

Acta Cryst. (2014). E70, m194
[ doi:10.1107/S1600536814009052 ]

Tetrakis[[mu]3-2-(piperidin-1-yl)ethanolato]tetrakis[chloridocopper(II)]

M. Luo, Y.-H. Huang and J.-C. Zhang


Key indicators

checkCIF/PLATON results

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Alert level A PLAT015_ALERT_5_A No _shelx_hkl_file record in SHELXL20xy CIF ... Please Do !
Alert level B PLAT934_ALERT_3_B Number of (Iobs-Icalc)/SigmaW > 10 Outliers .... 3 Check
Alert level C PLAT234_ALERT_4_C Large Hirshfeld Difference N2 -- C10 .. 0.17 Ang. PLAT234_ALERT_4_C Large Hirshfeld Difference C15 -- C16 .. 0.16 Ang. PLAT341_ALERT_3_C Low Bond Precision on C-C Bonds ............... 0.0147 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H2B .. CL4 .. 2.97 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H7A .. CL2 .. 2.87 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H23A .. CL2 .. 2.94 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H28A .. CL4 .. 2.84 Ang. PLAT601_ALERT_2_C Structure Contains Solvent Accessible VOIDS of . 36 Ang3 PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 2.868 Check PLAT911_ALERT_3_C Missing # FCF Refl Between THmin & STh/L= 0.600 2 Why ?
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT033_ALERT_4_G Flack x Value Deviates > 2*sigma from Zero ..... 0.180 PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT Unusually Large. 55.91 Why ? PLAT199_ALERT_1_G Reported _cell_measurement_temperature ..... (K) 293 Check PLAT200_ALERT_1_G Reported _diffrn_ambient_temperature ..... (K) 293 Check PLAT232_ALERT_2_G Hirshfeld Test Diff (M-X) Cu1 -- O3 .. 6.0 su PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 79 Do ! CL2 -CU2 -O1 -C1 -82.00 1.50 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 83 Do ! CL2 -CU2 -O1 -CU1 49.20 1.50 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 100 Do ! CL1 -CU1 -O2 -C8 -93.10 1.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 104 Do ! CL1 -CU1 -O2 -CU2 39.40 1.60 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 107 Do ! CL3 -CU3 -O3 -C15 79.00 1.50 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 111 Do ! CL3 -CU3 -O3 -CU4 -52.40 1.50 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 121 Do ! CL4 -CU4 -O4 -C22 82.00 1.70 1.555 1.555 1.555 1.555 PLAT710_ALERT_4_G Delete 1-2-3 or 2-3-4 Linear Torsion Angle ... # 125 Do ! CL4 -CU4 -O4 -CU3 -47.10 1.70 1.555 1.555 1.555 1.555 PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 38 Note
1 ALERT level A = Most likely a serious problem - resolve or explain 1 ALERT level B = A potentially serious problem, consider carefully 10 ALERT level C = Check. Ensure it is not caused by an omission or oversight 15 ALERT level G = General information/check it is not something unexpected 2 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 3 ALERT type 2 Indicator that the structure model may be wrong or deficient 4 ALERT type 3 Indicator that the structure quality may be low 16 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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