Acta Crystallographica Section E

Structure Reports Online

Volume 70, Part 5 (May 2014)

organic compounds

zp2013 scheme

Acta Cryst. (2014). E70, o556-o557    [ doi:10.1107/S1600536814007521 ]

(E)-tert-Butyl 2-(5-{[4-(dimethylamino)phenyl]diazenyl}-2,6-dioxo-1H-pyrimid­in-3-yl)acetate dichloromethane monosolvate

R. H. E. Hudson, M. E. Moustafa and P. D. Boyle

Abstract: In the title compound, C18H23N5O4·CH2Cl2, the di­chloro­methane solvent mol­ecule is disordered over two sets of sites in a 0.630 (13):0.370 (13) ratio. The dihedral angle between the uracil and phenyl rings is 30.2 (1)°. In the crystal, the principal inter­actions are N-H...O hydrogen bonds, which link uracil units across centres of symmetry, forming eight-membered rings with an R22(8) graph-set motif. The structure also displays C-H...O and C-H...Cl hydrogen bonds. Intra­molecular C-H...O short contacts are also observed.

CCDC reference: 995390

htmldisplay filedownload file

Hyper-Text Markup Language (HTML) file (88.7 kbytes)
[ doi:10.1107/S1600536814007521/zp2013sup0.html ]
Supplementary materials

cmldisplay filedownload file

Chemical Markup Language (CML) file (7.4 kbytes)
[ doi:10.1107/S1600536814007521/zp2013Isup3.cml ]
Supplementary material


To open or display or play some files, you may need to set your browser up to use the appropriate software. See the full list of file types for an explanation of the different file types and their related mime types and, where available links to sites from where the appropriate software may be obtained.

The download button will force most browsers to prompt for a file name to store the data on your hard disk.

Where possible, images are represented by thumbnails.

 bibliographic record in  format

  Find reference:   Volume   Page   
  Search:     From   to      Advanced search

Copyright © International Union of Crystallography
IUCr Webmaster