[Open access]

[Contents scheme]

Acta Cryst. (2014). E70, o556-o557
[ doi:10.1107/S1600536814007521 ]

(E)-tert-Butyl 2-(5-{[4-(dimethylamino)phenyl]diazenyl}-2,6-dioxo-1H-pyrimid­in-3-yl)acetate dichloromethane monosolvate

R. H. E. Hudson, M. E. Moustafa and P. D. Boyle


Key indicators

checkCIF/PLATON results

No syntax errors found



Alert level A PLAT015_ALERT_5_A No _shelx_hkl_file record in SHELXL20xy CIF ... Please Do !
Alert level C PLAT480_ALERT_4_C Long H...A H-Bond Reported H2C .. O1 .. 2.62 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H4 .. CL2X .. 2.98 Ang. PLAT480_ALERT_4_C Long H...A H-Bond Reported H13B .. CL2X .. 2.99 Ang. PLAT906_ALERT_3_C Large K value in the Analysis of Variance ...... 3.797 Check
Alert level G PLAT005_ALERT_5_G No _iucr_refine_instructions_details in the CIF Please Do ! PLAT302_ALERT_4_G Anion/Solvent Disorder ............ Percentage = 100 Note PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels .......... 4 Note PLAT860_ALERT_3_G Number of Least-Squares Restraints ............. 12 Note PLAT910_ALERT_3_G Missing # of FCF Reflections Below Th(Min) ..... 1 Why ? PLAT912_ALERT_4_G Missing # of FCF Reflections Above STh/L= 0.600 453 Note
1 ALERT level A = Most likely a serious problem - resolve or explain 0 ALERT level B = A potentially serious problem, consider carefully 4 ALERT level C = Check. Ensure it is not caused by an omission or oversight 6 ALERT level G = General information/check it is not something unexpected 0 ALERT type 1 CIF construction/syntax error, inconsistent or missing data 0 ALERT type 2 Indicator that the structure model may be wrong or deficient 3 ALERT type 3 Indicator that the structure quality may be low 6 ALERT type 4 Improvement, methodology, query or suggestion 2 ALERT type 5 Informative message, check

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