view article
Figure 3
Overall diffracted intensities of reflections hkl for l = 3n, 3n + 1 and 3n + 2 as a function of temperature. Indexing is based on the low-temperature super-cell matrix and temperatures given are the instrumental setting temperatures. The sum of the averaged intensities within the three classes has been normalized to 1000. (a) KappaCCD data; (b) SMART APEX data. Note that a calibration of the Bruker Kryoflex showed a 1.0–2.0 K gap, compared with the actual temperature at the crystal (see §2.2[link]).

Journal logoJOURNAL OF
APPLIED
CRYSTALLOGRAPHY
ISSN: 1600-5767
Volume 36| Part 1| February 2003| Pages 141-145
https://doi.org/10.1107/S0021889802021878
Follow J. Appl. Cryst.
Sign up for e-alerts
E-alerts
Follow J. Appl. Cryst. on Twitter
Twitter
Follow us on facebook
Facebook
Sign up for RSS feeds
RSS