Journal of Synchrotron Radiation

Volume 13, Part 3 (May 2006)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: The prism array X-ray lens clessidra developed at ELETTRA (Sincrotrone Trieste), see Jark, Pérennès and Matteucci, pages 239-252. Top: micrograph of the lens produced using deep X-ray lithography at the DXRL beamline at ELETTRA. The lens is made of pmma (polymethylmethacrylate = plexiglass) and consists of small prisms of height 25.67 µm and width 77.33 µm. The overall structure is 1.51 mm high, 2.6 mm wide and ~0.65 mm deep. Bottom: radiographs taken 30 mm downstream of the lens during the tilt alignment with a photon energy of 10 keV (tilt increment 1°). A CCD camera with 3.85 µm equivalent pixel size was used at the SYRMEP beamline at ELETTRA at a source distance of 22.6 m. In this lens the resist thickness varied in the beam direction.

research papers


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J. Synchrotron Rad. (2006). 13, 227-238  [ doi:10.1107/S0909049506004341 ]

The ID23-1 structural biology beamline at the ESRF

D. Nurizzo, T. Mairs, M. Guijarro, V. Rey, J. Meyer, P. Fajardo, J. Chavanne, J.-C. Biasci, S. McSweeney and E. Mitchell

Synopsis: A detailed description of the ID23-1 structural biology beamline at the ESRF is given, with a description of the automated hardware and software environments for beamline staff and user community.

Online 13 April 2006


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J. Synchrotron Rad. (2006). 13, 239-252  [ doi:10.1107/S0909049506004936 ]

On the feasibility of large-aperture Fresnel lenses for the microfocusing of hard X-rays

W. Jark, F. Pérennès and M. Matteucci

Synopsis: The limitations of the aperture of highly regular Fresnel X-rays lenses due to absorption, chromatic aberrations and the `thin lens' approximation are discussed. Experimental data for the refraction efficiency are interpreted.

Online 13 April 2006


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J. Synchrotron Rad. (2006). 13, 253-259  [ doi:10.1107/S0909049506006789 ]

Optimizing the signal-to-noise ratio for X-ray photon correlation spectroscopy

P. Falus, L. B. Lurio and S. G. J. Mochrie

Synopsis: A calculation is presented to maximize the signal-to-noise ratio of an X-ray photon correlation spectroscopy beamline by finding the optimum detector pixel size, optimum collimation and optimum X-ray energy.

Online 13 April 2006


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J. Synchrotron Rad. (2006). 13, 260-270  [ doi:10.1107/S0909049506008983 ]

Evaluation of imaging performance of a taper optics CCD `FReLoN' camera designed for medical imaging

P. Coan, A. Peterzol, S. Fiedler, C. Ponchut, J. C. Labiche and A. Bravin

Synopsis: Full characterization in terms of modulation transfer function, normalized noise power spectrum and detective quantum efficiency of a fast-readout low-noise (FReLoN) CCD camera coupled to a fiberoptical taper, a detector developed at the European Synchrotron Radiation Facility.

Online 13 April 2006


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J. Synchrotron Rad. (2006). 13, 271-274  [ doi:10.1107/S0909049506006972 ]

X-ray diffractometer combining synchrotron radiation and pulsed magnetic fields up to 40 T

Y. Narumi, K. Kindo, K. Katsumata, M. Kawauchi, C. Broennimann, U. Staub, H. Toyokawa, Y. Tanaka, A. Kikkawa, T. Yamamoto, M. Hagiwara, T. Ishikawa and H. Kitamura

Synopsis: A synchrotron X-ray diffractometer incorporating a pulsed field magnet for high fields up to 40 T has been developed and a detailed description of this instrument is reported.

Online 13 April 2006


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J. Synchrotron Rad. (2006). 13, 275-277  [ doi:10.1107/S0909049506009058 ]

Temperature-resolved in situ X-ray absorption spectroscopic study on the reduction of nanostructured Fe2O3 within the pore system of mesoporous carbon CMK-1

H. Huwe and M. Fröba

Synopsis: First results on the reduction of iron oxide nanoparticles within a mesoporous carbon CMK-1 host structure are given. The thermochemical behaviour was monitored by temperature-dependent in situ X-ray absorption spectroscopic measurements. In summary, one can say that the kinetics of the reduction steps Fe2O3 [rightwards arrow] Fe3O4 [rightwards arrow] Fe1-xO [rightwards arrow] Fe0 are mainly affected by the particle size, as well as the spatial and chemical environment.

Online 13 April 2006


short communications


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J. Synchrotron Rad. (2006). 13, 278-280  [ doi:10.1107/S0909049506003888 ]

Nearly perfect large-area quartz: 4 meV resolution for 10 keV photons over 10 cm2

J. P. Sutter, A. Q. R. Baron, D. Miwa, Y. Nishino, K. Tamasaku and T. Ishikawa

Synopsis: Bragg backscattering of 10 keV X-rays from large commercial quartz crystals has shown low defect concentrations and experimental energy widths of 4.0 meV. Quartz thus appears to be a useful X-ray optical material, particularly for meV-resolution energy analyzers of X-rays with energy 12 keV or less.

Online 13 April 2006


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J. Synchrotron Rad. (2006). 13, 281-284  [ doi:10.1107/S0909049506004766 ]

High-resolution powder diffraction study of purple membrane with a large Guinier-type camera

T. Oka, K. Miura, K. Inoue, T. Ueki and N. Yagi

Synopsis: X-ray diffraction patterns from a film of oriented purple membranes, which comprise two-dimensional crystals of bacteriorhodopsin trimers, were recorded with a 1 m-pathlength Guinier-type camera at SPring-8 BL40B2. Diffraction peaks were observed up to a resolution of 2.3 Å and a projected electron density map was calculated with intensities up to a spacing of 4.2 Å.

Online 13 April 2006


letters to the editor


 

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J. Synchrotron Rad. (2006). 13, 285  [ doi:10.1107/S0909049506008958 ]

Comments on A new model for statistical error analysis in XAS: about the distribution function of the absorption coefficient by E. Curis & S. Bénazeth (2001). J. Synchrotron Rad. 8, 264-266

S. Nadarajah and S. Kotz

Synopsis: Comment on Curis & Bénazeth [J. Synchrotron Rad. (2001), 8, 264-266].

Online 13 April 2006


 

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J. Synchrotron Rad. (2006). 13, 286  [ doi:10.1107/S090904950600896X ]

Response to S. Nadarajah & S. Kotz's Comments on A new model for statistical error analysis in XAS: about the distribution function of the absorption coefficient by E. Curis & S. Bénazeth (2001). J. Synchrotron Rad. 8, 264-266

E. Curis and S. Bénazeth

Synopsis: Response to Nadarajah & Kotz's comments in the previous paper.

Online 13 April 2006


book reviews


 

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J. Synchrotron Rad. (2006). 13, 287  [ doi:10.1107/S0909049506008910 ]

Structure Determination by X-ray Crystallography

Online 13 April 2006


new commercial products


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J. Synchrotron Rad. (2006). 13, 288  [ doi:10.1107/S0909049506009861 ]

Multiple-pass monochromators

Online 13 April 2006


current events


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J. Synchrotron Rad. (2006). 13, 289-290  [ doi:10.1107/S0909049506012969 ]

Current events

Online 13 April 2006


 

J. Synchrotron Rad. (2006). 13, 291

forthcoming meetings and short courses


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