Journal of Synchrotron Radiation

Volume 21, Part 1 (January 2014)



[Issue Author Index][Volume Author Index]
[Cover illustration] Cover illustration: X-ray scattering diagrams of [W/Si]10 multilayers deposited at Ar pressures of 1, 3, 5 and 7 mTorr were measured at beamline BL16B1 at the Shanghai Synchrotron Radiation Facility (see Li, Zhu, Wang, Chen, Wang and Wang, pages 97-103). Larger scattering spots reveal rougher interfaces in multilayers grown at higher Ar pressure.

research papers


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J. Synchrotron Rad. (2014). 21, 1-4  [ doi:10.1107/S1600577513023205 ]

Pinhole-type two-dimensional ultra-small-angle X-ray scattering on the micrometer scale

H. Kishimoto, Y. Shinohara, Y. Suzuki, A. Takeuchi, N. Yagi and Y. Amemiya

Synopsis: A pinhole-type ultra-small-angle X-ray scattering set-up that enlarges the accessible q-range to 0.25 µm-1 is described.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 5-15  [ doi:10.1107/S1600577513023850 ]

Coherence properties of focused X-ray beams at high-brilliance synchrotron sources

A. Singer and I. A. Vartanyants

Synopsis: An analytical approach describing properties of focused partially coherent X-ray beams is presented.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 16-23  [ doi:10.1107/S1600577513024077 ]

Tests and characterization of a laterally graded multilayer Montel mirror

K. Mundboth, J. Sutter, D. Laundy, S. Collins, S. Stoupin and Y. Shvyd'ko

Synopsis: A laterally graded multilayer Montel mirror with a parabolic figure has been tested and characterized. It exhibits excellent reflectivity and focusing/collimating properties.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 24-31  [ doi:10.1107/S1600577513024715 ]

Synchrotron X-ray footprinting on tour

J. Bohon, R. D'Mello, C. Ralston, S. Gupta and M. R. Chance

Synopsis: Synchrotron X-ray footprinting resources were investigated at a variety of beamlines and synchrotron facilities to understand their potential for a mobile general user. Results indicate that viable resources exist at each synchrotron investigated such that a prospective user need only provide a simple flow apparatus and sample handling accessories to perform this technique.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 32-44  [ doi:10.1107/S1600577513019085 ]

Soft-X-ray ARPES facility at the ADRESS beamline of the SLS: concepts, technical realisation and scientific applications

V. N. Strocov, X. Wang, M. Shi, M. Kobayashi, J. Krempasky, C. Hess, T. Schmitt and L. Patthey

Synopsis: Concepts and technical realization of the soft-X-ray ARPES facility at the Swiss Light Source are described. Its performance is illustrated by a few scientific applications ranging from three-dimensional materials to buried interfaces and impurities.

Online 7 November 2013


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J. Synchrotron Rad. (2014). 21, 45-56  [ doi:10.1107/S1600577513026192 ]

A novel X-ray diffractometer for studies of liquid-liquid interfaces

B. M. Murphy, M. Greve, B. Runge, C. T. Koops, A. Elsen, J. Stettner, O. H. Seeck and O. M. Magnussen

Synopsis: A dedicated liquid surface diffractometer employing a tilting double-crystal monochromator in Bragg geometry has been designed. This diffractometer allows reflectivity and grazing-incidence scattering measurements of an immobile mechanical completely decoupled liquid sample from 6.4 to 29.4 keV.

Online 29 November 2013


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J. Synchrotron Rad. (2014). 21, 57-60  [ doi:10.1107/S1600577513026593 ]

A planar parabolic refractive nickel lens for high-energy X-rays

A. Andrejczuk, M. Nagamine, Y. Sakurai and M. Itou

Synopsis: A compound refractive nickel lens focusing 174 keV X-rays to 5 µm with a gain of 4 is presented.

Online 27 November 2013


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J. Synchrotron Rad. (2014). 21, 61-65  [ doi:10.1107/S1600577513029706 ]

Controlling X-ray beam trajectory with a flexible hollow glass fibre

Y. Tanaka, T. Nakatani, R. Onitsuka, K. Sawada and I. Takahashi

Synopsis: X-ray beam trajectory control has been performed by using a 1.5 m-long flexible hollow glass fibre. A two-dimensional scan of a synchrotron radiation beam was demonstrated for X-ray absorption mapping.

Online 10 December 2013


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J. Synchrotron Rad. (2014). 21, 66-75  [ doi:10.1107/S1600577513029676 ]

The Bionanoprobe: hard X-ray fluorescence nanoprobe with cryogenic capabilities

S. Chen, J. Deng, Y. Yuan, C. Flachenecker, R. Mak, B. Hornberger, Q. Jin, D. Shu, B. Lai, J. Maser, C. Roehrig, T. Paunesku, S. C. Gleber, D. J. Vine, L. Finney, J. VonOsinski, M. Bolbat, I. Spink, Z. Chen, J. Steele, D. Trapp, J. Irwin, M. Feser, E. Snyder, K. Brister, C. Jacobsen, G. Woloschak and S. Vogt

Synopsis: The Bionanoprobe has been developed to study trace elements in frozen-hydrated biological systems with sub-100 nm spatial resolution. Here its performance is demonstrated and first results reported.

Online 12 December 2013


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J. Synchrotron Rad. (2014). 21, 76-81  [ doi:10.1107/S1600577513021516 ]

X-ray reflectivity measurements of liquid/solid interfaces under high hydrostatic pressure conditions

F. J. Wirkert, M. Paulus, J. Nase, J. Möller, S. Kujawski, C. Sternemann and M. Tolan

Synopsis: A high hydrostatic pressure cell for X-ray reflectivity measurements at the solid/liquid interface is presented.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 82-88  [ doi:10.1107/S1600577513025162 ]

Polymer electrolyte fuel cell performance degradation at different synchrotron beam intensities

J. Eller and F. N. Büchi

Synopsis: The dependency of beam intensity on the performance degradation of polymer electrolyte fuel cells during X-ray imaging experiments at the Tomcat beamline of the Swiss Light Source is reported and the underlying degradation mechanisms are identified.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 89-96  [ doi:10.1107/S1600577513027434 ]

Strategies for in situ laser heating in the diamond anvil cell at an X-ray diffraction beamline

S. Petitgirard, A. Salamat, P. Beck, G. Weck and P. Bouvier

Synopsis: An overview of several innovations regarding in situ laser-heating techniques in the diamond anvil cell at the high-pressure beamline ID27 of the European Synchrotron Radiation Facility is presented.

Online 8 November 2013


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J. Synchrotron Rad. (2014). 21, 97-103  [ doi:10.1107/S1600577513024296 ]

Integration method for directly analyzing interface statistics of periodic multilayers from X-ray scattering

H. Li, J. Zhu, Z. Wang, H. Chen, Y. Wang and J. Wang

Synopsis: An integration method is demonstrated for directly determining the average interface statistics or, more specifically, power spectral density of periodic multilayers from the X-ray scattering diagram.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 104-110  [ doi:10.1107/S160057751302242X ]

Study on the reflectivity properties of spherically bent analyser crystals

A.-P. Honkanen, R. Verbeni, L. Simonelli, M. Moretti Sala, G. Monaco and S. Huotari

Synopsis: A treatment is presented to explain reflectivity curves of finite-size elastically bent analyser crystals for X-ray spectrometry.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 111-118  [ doi:10.1107/S1600577513025459 ]

Scanning X-ray strain microscopy of inhomogeneously strained Ge micro-bridges

T. Etzelstorfer, M. J. Süess, G. L. Schiefler, V. L. R. Jacques, D. Carbone, D. Chrastina, G. Isella, R. Spolenak, J. Stangl, H. Sigg and A. Diaz

Synopsis: A scanning X-ray strain microscopy technique using a micro-focused beam is demonstrated.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 119-126  [ doi:10.1107/S1600577513028269 ]

Model-independent structure factors from powder X-ray diffraction: a novel approach

T. Straasø, A.-C. Dippel, J. Becker and J. Als-Nielsen

Synopsis: Using a high-energy high-resolution synchrotron X-ray beam for powder X-ray diffraction simplifies the analysis of the diffraction pattern to the extent that fitting of any parameter becomes superfluous. A diamond powder pattern has been used as an experimental illustration.

Online 7 December 2013


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J. Synchrotron Rad. (2014). 21, 127-130  [ doi:10.1107/S1600577513029317 ]

Numerical reconstruction of an object image using an X-ray dynamical diffraction Fraunhofer hologram

M. K. Balyan

Synopsis: A numerical method of reconstruction of an object image using a dynamical diffraction Fraunhofer hologram is discussed.

Online 7 December 2013


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J. Synchrotron Rad. (2014). 21, 131-135  [ doi:10.1107/S1600577513028944 ]

Momentum-resolved resonant inelastic X-ray scattering on a single crystal under high pressure

M. Yoshida, K. Ishii, I. Jarrige, T. Watanuki, K. Kudo, Y. Koike, K. Kumagai, N. Hiraoka, H. Ishii, K.-D. Tsuei and J. Mizuki

Synopsis: The development of resonant inelastic X-ray scattering under high pressure is presented. The pressure evolution of momentum-resolved electronic excitations was obtained in single-crystalline Sr2.5Ca11.5Cu24O41.

Online 7 December 2013


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J. Synchrotron Rad. (2014). 21, 136-142  [ doi:10.1107/S1600577513023771 ]

The status of strontium in biological apatites: an XANES/EXAFS investigation

D. Bazin, A. Dessombz, C. Nguyen, H. K. Ea, F. Lioté, J. Rehr, C. Chappard, S. Rouzière, D. Thiaudière, S. Reguer and M. Daudon

Synopsis: Biological apatites have been investigated through XANES-EXAFS spectroscopy and a set of numerical simulations, taking into account local lattice distortion, Ca2+/Sr2+ substitution or the presence of cationic vacancies, have been performed.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 143-148  [ doi:10.1107/S1600577513025708 ]

Influence of co-dopant in the europium reduction in SrAl2O4 host

M. V. S. Rezende, P. J. R. Montes, F. M. S. Soares, C. Santos and M. E. G. Valerio

Synopsis: The effect of the Ln3+ (Ln = Gd, Dy, Er or Y) co-dopant ions on the reduction of the Eu3+ ions using dispersive X-ray absorption spectroscopy is shown. The measurements around the Eu LIII-edge in SrO:Al2O3:Eu,Ln were used to propose a mechanism for the Eu reduction and stabilization within the samples.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 149-160  [ doi:10.1107/S1600577513025228 ]

Study of fossil bones by synchrotron radiation micro-spectroscopic techniques and scanning electron microscopy

I. M. Zougrou, M. Katsikini, F. Pinakidou, E. C. Paloura, L. Papadopoulou and E. Tsoukala

Synopsis: Morphological and structural characterization of the alterations induced by fossilization processes in Earlymost Villafranchian fossil bones by means of X-ray absorption and fluorescence micro-spectroscopies and optical and scanning electron microscopies.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 161-164  [ doi:10.1107/S1600577513026088 ]

Grazing-incidence small-angle X-ray scattering from Ge nanodots self-organized on Si(001) examined with soft X-rays

T. Yamamoto, H. Okuda, K. Takeshita, N. Usami, Y. Kitajima and H. Ogawa

Synopsis: Grazing-incidence small-angle scattering patterns of Ge nanodots self-organized on Si(001) with soft X-rays showed a strongly anisotropic scattering profile, although the patterns with hard X-rays are symmetric. This apparent difference is explained in terms of the curvature of the Ewald sphere and anisotropic structure factors.

Online 5 November 2013


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J. Synchrotron Rad. (2014). 21, 165-169  [ doi:10.1107/S1600577513026921 ]

A facile heating cell for in situ transmittance and fluorescence X-ray absorption spectroscopy investigations

P. An, C. Hong, J. Zhang, W. Xu and T. Hu

Synopsis: A facile heating cell for in situ transmittance and fluorescence X-ray absorption spectroscopy is described. It provides a novel approach to the design of an in situ cell for synchrotron radiation applications.

Online 6 November 2013


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J. Synchrotron Rad. (2014). 21, 170-176  [ doi:10.1107/S1600577513026696 ]

Scanning transmission X-ray microscopy probe for in situ mechanism study of graphene-oxide-based resistive random access memory

H. W. Nho, J. Y. Kim, J. Wang, H.-J. Shin, S.-Y. Choi and T. H. Yoon

Synopsis: An in situ probe for scanning transmission X-ray microscopy has been developed and applied to the study of the bipolar resistive switching mechanism in an Al/graphene oxide/Al resistive random access memory device.

Online 28 November 2013


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J. Synchrotron Rad. (2014). 21, 177-182  [ doi:10.1107/S1600577513026544 ]

Liquid X-ray scattering with a pink-spectrum undulator

S. Bratos, J.-Cl. Leicknam, M. Wulff and D. Khakhulin

Synopsis: The diffraction of non-monochromatic X-rays by liquids id described.

Online 3 December 2013


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J. Synchrotron Rad. (2014). 21, 183-192  [ doi:10.1107/S1600577513028233 ]

Development of a single-shot CCD-based data acquisition system for time-resolved X-ray photoelectron spectroscopy at an X-ray free-electron laser facility

M. Oura, T. Wagai, A. Chainani, J. Miyawaki, H. Sato, M. Matsunami, R. Eguchi, T. Kiss, T. Yamaguchi, Y. Nakatani, T. Togashi, T. Katayama, K. Ogawa, M. Yabashi, Y. Tanaka, Y. Kohmura, K. Tamasaku, S. Shin and T. Ishikawa

Synopsis: A single-shot CCD-based data acquisition system for time-resolved photoelectron spectroscopy using an X-ray free-electron laser has been developed. The basic performance of the system is demonstrated using XFEL-induced and synchrotron-radiation-induced Ti 1s core-level spectroscopy.

Online 10 December 2013


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J. Synchrotron Rad. (2014). 21, 193-202  [ doi:10.1107/S1600577513027951 ]

Thorough small-angle X-ray scattering analysis of the instability of liquid micro-jets in air

B. Marmiroli, F. Cacho-Nerin, B. Sartori, J. Pérez and H. Amenitsch

Synopsis: The reliability and effectiveness of small-angle X-ray scattering in detecting liquid jet instability is demonstrated by measuring the jet break-up length for different liquids, flow rates and jet diameter.

Online 11 December 2013


 

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J. Synchrotron Rad. (2014). 21, 203-208  [ doi:10.1107/S1600577513030117 ]

SAXS Merge: an automated statistical method to merge SAXS profiles using Gaussian processes

Y. G. Spill, S. J. Kim, D. Schneidman-Duhovny, D. Russel, B. Webb, A. Sali and M. Nilges

Synopsis: A statistical method to merge SAXS profiles using Gaussian processes is presented.

Online 14 December 2013


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J. Synchrotron Rad. (2014). 21, 209-214  [ doi:10.1107/S1600577513030026 ]

X-ray absorption near-edge structure anomalous behaviour in structures with buried layers containing silicon nanocrystals

V. A. Terekhov, D. I. Tetelbaum, D. E. Spirin, K. N. Pankov, A. N. Mikhailov, A. I. Belov, A. V. Ershov and S. Yu. Turishchev

Synopsis: X-ray absorption near-edge structure anomalous behaviour of silicon suboxide layers with silicon and silicon carbide nanocrystals is reported.

Online 17 December 2013


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J. Synchrotron Rad. (2014). 21, 215-222  [ doi:10.1107/S1600577513023862 ]

Propagation-based phase-contrast X-ray microtomography of a cerebral protection device retrieved after carotid artery stenting

S. W. Youn, H. K. Kim, H. T. Kim, S. M. Han, J. K. Do, Y. R. Do, H. J. Lee, J. Lee and J. H. Lim

Synopsis: Phase-contrast synchrotron X-ray microtomography of a cerebral protection device is presented.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 223-228  [ doi:10.1107/S1600577513024892 ]

High-resolution thermal imaging with a combination of nano-focus X-ray diffraction and ultra-fast chip calorimetry

M. Rosenthal, D. Doblas, J. J. Hernandez, Y. I. Odarchenko, M. Burghammer, E. Di Cola, D. Spitzer, A. E. Antipov, L. S. Aldoshin and D. A. Ivanov

Synopsis: A custom-designed nanocalorimeter is implemented on a nano-focus X-ray beamline. The accessory enables measurements of X-ray-induced heating for high-resolution thermal imaging of single microparticles.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 229-234  [ doi:10.1107/S1600577513029512 ]

Alignment of low-dose X-ray fluorescence tomography images using differential phase contrast

Y. P. Hong, S.-C. Gleber, T. V. O'Halloran, E. L. Que, R. Bleher, S. Vogt, T. K. Woodruff and C. Jacobsen

Synopsis: Differential phase contrast images acquired simultaneously with fluorescence images offer a robust method for alignment in low-dose X-ray nanotomography data acquisition.

Online 12 December 2013


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J. Synchrotron Rad. (2014). 21, 235-241  [ doi:10.1107/S160057751303083X ]

Combining µXANES and µXRD mapping to analyse the heterogeneity in calcium carbonate granules excreted by the earthworm Lumbricus terrestris

L. Brinza, P. F. Schofield, M. E. Hodson, S. Weller, K. Ignatyev, K. Geraki, P. D. Quinn and J. F. W. Mosselmans

Synopsis: A new experimental set-up enabling microfocus fluorescence XANES mapping and microfocus XRD mapping on the same sample at beamline I18 at Diamond Light Source is described. To demonstrate this set-up the heterogeneous mineralogy in calcium carbonate granules excreted by the earthworm Lumbricus terrestris has been analysed. Data analysis methods have been developed which enable µXRD and µXANES two-dimensional maps to be compared.

Online 12 December 2013


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J. Synchrotron Rad. (2014). 21, 242-250  [ doi:10.1107/S1600577513029007 ]

Single-cell resolution in high-resolution synchrotron X-ray CT imaging with gold nanoparticles

E. Schültke, R. Menk, B. Pinzer, A. Astolfo, M. Stampanoni, F. Arfelli, L.-A. Harsan and G. Nikkhah

Synopsis: It is demonstrated that single-cell resolution can be obtained ex vivo in the brain of small animals using gold nanoparticles with the synchrotron-based computed tomography technique.

Online 11 December 2013


short communications


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J. Synchrotron Rad. (2014). 21, 251-253  [ doi:10.1107/S1600577513026969 ]

A low-cost X-ray-transparent experimental cell for synchrotron-based X-ray microtomography studies under geological reservoir conditions

F. Fusseis, H. Steeb, X. Xiao, W. Zhu, I. B. Butler, S. Elphick and U. Mäder

Synopsis: An X-ray-transparent experimental environment that allows time-resolved studies of porous rocks under geological reservoir conditions using high-energy synchrotron X-ray microtomography is presented.

Online 5 December 2013


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J. Synchrotron Rad. (2014). 21, 254-258  [ doi:10.1107/S1600577513028786 ]

A reaction cell for time-resolved in situ XAS studies during wet chemical synthesis: the Cu2(OH)3Cl case

J. Boita, M. do Carmo Martins Alves and J. Morais

Synopsis: A reaction cell designed for in situ X-ray absorption experiments on liquid samples and wet chemical synthesis is presented.

Online 28 November 2013


beamlines


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J. Synchrotron Rad. (2014). 21, 259-263  [ doi:10.1107/S1600577513024934 ]

Beamline BL-07 at Indus-2: a facility for microfabrication research

V. P. Dhamgaye, G. S. Lodha, B. Gowri Sankar and C. Kant

Synopsis: Details of the X-ray lithography beamline on Indus-2 are presented.

Online 2 November 2013


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J. Synchrotron Rad. (2014). 21, 264-267  [ doi:10.1107/S1600577513025629 ]

Coherent X-ray scattering beamline at port 9C of Pohang Light Source II

C.-J. Yu, H. C. Lee, C. Kim, W. Cha, J. Carnis, Y. Kim, D. Y. Noh and H. Kim

Synopsis: The coherent X-ray scattering beamline at PLS-II at Pohang Accelerator Laboratory, Korea, is introduced.

Online 5 November 2013


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J. Synchrotron Rad. (2014). 21, 268-272  [ doi:10.1107/S1600577513025733 ]

RISING beamline (BL28XU) for rechargeable battery analysis

H. Tanida, K. Fukuda, H. Murayama, Y. Orikasa, H. Arai, Y. Uchimoto, E. Matsubara, T. Uruga, K. Takeshita, S. Takahashi, M. Sano, H. Aoyagi, A. Watanabe, N. Nariyama, H. Ohashi, H. Yumoto, T. Koyama, Y. Senba, T. Takeuchi, Y. Furukawa, T. Ohata, T. Matsushita, Y. Ishizawa, T. Kudo, H. Kimura, H. Yamazaki, T. Tanaka, T. Bizen, T. Seike, S. Goto, H. Ohno, M. Takata, H. Kitamura, T. Ishikawa, T. Ohta and Z. Ogumi

Synopsis: The BL28XU beamline, dedicated to rechargeable battery analysis, is described.

Online 28 November 2013


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J. Synchrotron Rad. (2014). 21, 273-279  [ doi:10.1107/S1600577513029093 ]

Design of an ultrahigh-energy-resolution and wide-energy-range soft X-ray beamline

L. Xue, R. Reininger, Y.-Q. Wu, Y. Zou, Z.-M. Xu, Y.-B. Shi, J. Dong, H. Ding, J.-L. Sun, F.-Z. Guo, Y. Wang and R.-Z. Tai

Synopsis: A new ultrahigh-energy-resolution and wide-energy-range soft X-ray beamline has been designed at the Shanghai Synchrotron Radiation Facility. The expected energy resolution is approximately 10 meV at 1000 eV.

Online 11 December 2013


meeting reports


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J. Synchrotron Rad. (2014). 21, 280-282  [ doi:10.1107/S1600577513030609 ]

The 11th International Conference on Biology and Synchrotron Radiation

M. Wilmanns and D. I. Svergun

Synopsis: A report on the 11th International Conference on Biology and Synchrotron Radiation which took place on 8-11 September 2013, in Hamburg, Germany, is presented.

Online 3 December 2013


current events


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J. Synchrotron Rad. (2014). 21, 283-284  [ doi:10.1107/S1600577513032840 ]

Current events

Online 6 December 2013


international union of crystallography


 

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J. Synchrotron Rad. (2014). 21, 285-288  [ doi:10.1107/S1600577513022935 ]

Notes for authors

Online 20 December 2014


 

J. Synchrotron Rad. (2014). 21,

forthcoming meetings and short courses


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