Figure 1
A view of the DAC high-pressure chamber with the pressure-frozen polycrystalline (CH3)3SiCl at 0.23 GPa (a); (b) the single-crystal subsequently obtained under isochoric conditions at the initial stage of its growth. The ruby chip for pressure calibration has moved in the process of crystallization from the top-left (a) to the top (b) part of the pressure chamber. The Miller indices of the crystal in phase β have been given. |