Temperature-resolved study of three [M(M′O4)4(TBPO)4] complexes (MM′ = URe, ThRe, ThTc)

Helliwell, M.; Collison, D.; John, G.H.; May, I.; Sarsfield, M.J.; Sharrad, C.A.; Sutton, A.D.

doi:10.1107/S0108768105036931

Acta Crystallographica Section B
Acta Crystallographica
Section B STRUCTURAL SCIENCE, CRYSTAL ENGINEERING AND MATERIALS

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Figure 3
Diffraction patterns showing the differing lattice types at different temperatures [at identical setting for (a) and (b), and for (c), (d) and (e)]. (a) (I) at 293 K, showing the body-centred tetragonal lattice; (b) (I) at 230 K, where the lattice has become C-centred orthorhombic; (c) (III) at 260 K, showing the body-centred cubic lattice; (d) (III) at 230 K, where the lattice has become C-centred orthorhombic; (e) (III) at 205 K, where the lattice has become primitive orthorhombic.

STRUCTURAL SCIENCE
CRYSTAL ENGINEERING
MATERIALS

ISSN: 2052-5206

Volume 62| Part 1| January 2006| Pages 68-85

doi:10.1107/S0108768105036931

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