Figure 12
Naphthazarin C: the variation of the integrated intensity as a function of temperature of the 070 reflection, which distinguishes between the disordered phase [stable above 110 K; space group P21/c, (070) absent] and the ordered phase [Pc, (070) allowed]... Neutron diffraction measurements (λ = 0.895 Å) were made for 15 min periods on the D9 reactor at ILL Grenoble. There was no indication of hysteresis. Comparison of Figs. 11 and 12 shows the different behavior of distinguishing reflections in first- and second-order transitions. Reproduced with permission from Herbstein et al. (1985). |