Figure 1
Part of the 2kl plane of the diffraction pattern of HMT–resorcinol reconstructed from the area-detector images: (a) at room temperature and (b) at 120 K. For the data collection parameters of (a) see Table 1; parameters for (b): Kuma four-circle diffractometer, Sapphire II CCD detector, Mo K radiation, sample–detector distance 65.25 mm, scans, width 0.5°/frame, exposure time 50 s/frame. |