An unexpected co-crystal with a variable degree of order: 1:1 rac-1,2-cyclohexanediol/triphenylphos­phine oxide

Siegler, M.A.; Fu, Y.; Simpson, G.H.; King, D.P.; Parkin, S.; Brock, C.P.

doi:10.1107/S0108768107054699

Acta Crystallographica Section B
Acta Crystallographica
Section B STRUCTURAL SCIENCE, CRYSTAL ENGINEERING AND MATERIALS

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Figure 10
Overlays (left) of the TPPO layer of the CHDTPPO structure at 90 K (as determined for a crystal grown from acetone) with the structure of the Pbca polymorph determined at 100 K (Brock et al., 1985

) and (right) of the CHDTPPO structure at 294 K (also for a crystal grown from acetone) with the structure of the second monoclinic polymorph at room temperature (Spek, 1987

). The upper drawings are related to the lower drawings by a rotation of 90° around the vertical axis. Labels for axes that are more than 1° out of the plane of the drawing are shown in parentheses.

STRUCTURAL SCIENCE
CRYSTAL ENGINEERING
MATERIALS

ISSN: 2052-5206

Volume 63| Part 6| November 2007| Pages 912-925

doi:10.1107/S0108768107054699

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