Figure 3
Precession electron-diffraction patterns of (a)–(c) ∊6 and (d)–(f) ∊16, and (g)–(i) the simulated precession electron-diffraction patterns from the derived structure model of ∊16. The kinematical simulation conditions are: voltage 200 kV, precession angle 1.1°, and crystal thicknesses (g) 400 Å, (h) 500 Å and (i) 400 Å. The intensity distributions in reciprocal space are similar for ∊6 and ∊16. The corresponding reflections have the same h and k, but l(∊16) ≃ τ2 l(∊6), such that the very strong reflection (006) in ∊6 corresponds to (0016) in ∊16. |