Structure analysis of titanate nanorods by automated electron diffraction tomography

Andrusenko, I.; Mugnaioli, E.; Gorelik, T.E.; Koll, D.; Panthöfer, M.; Tremel, W.; Kolb, U.

doi:10.1107/S0108768111014534

Acta Crystallographica Section B
Acta Crystallographica
Section B STRUCTURAL SCIENCE, CRYSTAL ENGINEERING AND MATERIALS

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Figure 6
Zonal diffraction patterns and HRTEM micrographs of NaTi₃O₆(OH)·2H₂O nanorods along the [010] direction. (a) Simulated zonal diffraction pattern in [010]; (b) experimental zonal diffraction pattern in [010] with weak diffuse scattered intensities; (c) HRTEM of a nanorod in the [010] projection and (d) its Fourier transform; (e)–(f) Fourier filtered images of (d) using 001 and 200 reflections; (g) nanorod seen in the [010] projection with two highlighted areas in the correspondence of dislocation-like defects: one defect consists of two separated edge dislocations, the other consists of two dislocations with a merged core.

STRUCTURAL SCIENCE
CRYSTAL ENGINEERING
MATERIALS

ISSN: 2052-5206

Volume 67| Part 3| May 2011| Pages 218-225

doi:10.1107/S0108768111014534

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