Hidden superlattice in Tl2(SC6H4S) and Tl2(SeC6H4Se) solved from powder X-ray diffraction

Stone, K.H.; Turner, D.L.; Singh, M.P.; Vaid, T.P.; Stephens, P.W.

doi:10.1107/S0108768111030692

Acta Crystallographica Section B
Acta Crystallographica
Section B STRUCTURAL SCIENCE, CRYSTAL ENGINEERING AND MATERIALS

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Figure 3
Rietveld plot of Tl₂(SC₆H₄S). The lower panel is refinement to supercell (2) of data taken in capillary with the sample diluted with cork. Data, fit and difference curve above 14° are multiplied by a factor of five. The upper panel shows visible peaks allowed by supercell (2), from data taken in flat-plate geometry.

STRUCTURAL SCIENCE
CRYSTAL ENGINEERING
MATERIALS

ISSN: 2052-5206

Volume 67| Part 5| September 2011| Pages 409-415

doi:10.1107/S0108768111030692

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