Figure 10
The 2:1 adduct between 1,1-DMTU and dioxane. The hydrogen bond within the asymmetric unit is indicated by a dashed line. The morpholine molecule has been completed by symmetry; only the asymmetric unit is numbered. Selected molecular dimensions (Å, °): S1—C2 1.7111 (10), N3—C2 1.3405 (14), N1—C2 1.3396 (13), N1—C11 1.4624 (14), N1—C12 1.4656 (13), O1—C3 1.4364 (13), O1—C4 1.4369 (13), C2—N1—C11 122.18 (9), C2—N1—C12 120.77 (9), C11—N1—C12 117.00 (8), N1—C2—N3 117.60 (9), N1—C2—S1 122.74 (8), N3—C2—S1 119.66 (8), C3—O1—C4 110.17 (8). |