Structure refinement of the δ1p phase in the Fe–Zn system by single-crystal X-ray diffraction combined with scanning transmission electron microscopy

Okamoto, N.L.; Tanaka, K.; Yasuhara, A.; Inui, H.

doi:10.1107/S2052520613034410

Acta Crystallographica Section B
Acta Crystallographica
Section B STRUCTURAL SCIENCE, CRYSTAL ENGINEERING AND MATERIALS

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Figure 3
(a) HAADF and (b) ABF images simultaneously taken along the [11 $[\overline 2]$ 0] zone axis with the Cs-corrected STEM. The framed area corresponds to the projection of the unit cell. (c) and (d) Magnified images of the parts indicated by a solid frame in (a) and (b). (e) HAADF and (f) ABF images calculated with the structural parameters reported by Belin et al. (Belin & Belin, 2000

). (h) HAADF and (i) ABF images calculated with the structural parameters refined in the present study. The corresponding portion of [11 $[\overline 2]$ 0] projection of the structural models (g) reported by Belin et al. (Belin & Belin, 2000

) and (j) refined in the present study.

STRUCTURAL SCIENCE
CRYSTAL ENGINEERING
MATERIALS

ISSN: 2052-5206

Volume 70| Part 2| March 2014| Pages 275-282

doi:10.1107/S2052520613034410

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