Structure, thermal expansion and incompressibility of MgSO4·9H2O, its relationship to meridianiite (MgSO4·11H2O) and possible natural occurrences

Fortes, A.D.; Knight, K.S.; Wood, I.G.

doi:10.1107/S2052520616018266

Acta Crystallographica Section B
Acta Crystallographica
Section B STRUCTURAL SCIENCE, CRYSTAL ENGINEERING AND MATERIALS

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Figure 8
(a) Refined phase fractions of MS9, MS11 and ice as a function of time from X-ray powder diffraction data measured on a Peltier-cooled cold stage with ca 52 cm³ head-space over the sample. The solid line through the symbols for MS11 reports the fit of equation (5)

to the data. The two dashed lines show the expected phase fractions of ice and MS9 concomitant with the observed abundance of MS11 as a function of time. (b) Refined phase fractions of deuterated MS9, MS11 and ice as a function of time from neutron powder diffraction data measured in an indium-sealed container. Lines and symbols have the same meaning as in part (a).

STRUCTURAL SCIENCE
CRYSTAL ENGINEERING
MATERIALS

ISSN: 2052-5206

Volume 73| Part 1| February 2017| Pages 47-64

https://doi.org/10.1107/S2052520616018266

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