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Figure 5
LeBail-fit of the powder pattern acquired for the sample prepared at 1250°C (Co Kα1 radiation) at ambient conditions. Observed step intensities are represented by small circles. Calculated step intensities (solid line) have been modeled based on a mixture of the two polytypes of SFCA-III. Tick marks for the Bragg peaks of each phase are given (first row: triclinic SFCA-III; second row: monoclinic SFCA-III). The lower line represents the difference curve between observed and calculated step intensities. 2θ given in °.

Journal logoSTRUCTURAL SCIENCE
CRYSTAL ENGINEERING
MATERIALS
ISSN: 2052-5206
Volume 75| Part 6| December 2019| Pages 1126-1136
https://doi.org/10.1107/S2052520619014380
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