Figure 2
The stages of ZnAsp2·1.5H2O single-crystal growth from aqueous solution under isochoric conditions in the DAC chamber. (a) Spontaneous powder precipitation at 433 K, and one seed at (b) 443 K, (c) 343 K and (d) 0.49 GPa/296 K. The ruby chip for pressure calibration lies near the middle of the chamber. |