Figure 11
Diffractograms of the Nd0.9 sample during the reduction with wet H2 at increasing temperatures. The material was completely stable up to a temperature of 625 °C. However, after holding the temperature at 650 °C for 5 h, a peak (green border) corresponding to an elemental Fe phase could be observed, while the perovskite structure (peaks labelled `P'; for the respective hkl indices, cf. Fig. 2) remained intact. |