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Figure 9
3D-ΔPDF map of Mn[Co] at different temperatures, the section uv0.17 containing the signal from the Co atom to the nearest zeolitic oxygen: (a) at room temperature the signal is weak and centred near xxx with x = 0.21 which corresponds to (d) a disordered configuration of water; at low temperatures the peak becomes more pronounced and moves to x = 0.17 for a flash-frozen sample, (b), and to x = 0.19 for slowly cooled sample, (c), which corresponds to a better defined position of zeolitic water, (e).

Journal logoSTRUCTURAL SCIENCE
CRYSTAL ENGINEERING
MATERIALS
ISSN: 2052-5206
Volume 78| Part 3| June 2022| Pages 369-375
https://doi.org/10.1107/S2052520622001275
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