A fresh view on the structure and twinning of owyheeite, a rod-polytype and twofold superstructure

Owyheeite [Cu_0.09 (1)Ag_2.77 (4)Pb_10.23 (4)Sb_10.89 (5)S_28.00 (5)] crystallizes as a twofold superstructure with P2₁/n symmetry and pseudo-orthorhombic metrics [a = 8.1882 (3) Å, b = 27.2641 (7) Å, c = 22.8679 (7) Å, β = 90.293 (3)°, V = 5105.0 (3) ų, Z = 4]. Owyheeite is systematically twinned by reflection at (021) or equivalently (021). Twinning is explained by describing a simplified Pmcn archetype structure as polytype built of two kinds of rods, which contact via electron-pair micelles. A procedure of generating hypothetical polytypes by tiling space with partially overlapping equivalent regions is described.

1. Introduction

Owyheeite is a mineral in the class of sulfosalts (Moëlo et al., 2008) and was first described by Shannon (1921). Owing to systematic twinning and faint superstructure reflections, a full structure refinement has not been possible up to now. Laufek et al. (2007) refined the structure from synchrotron powder diffraction data in the space group P2₁/c and the unit-cell parameters a = 4.1035 (1) Å, b = 27.3144 (3) Å, c = 22.9366 (3) Å, β = 90.359 (1)°. They observed, but did not account for, weak reflections with half-integer h values indicating a doubling of the a-axis to a ∼ 8.2 Å. The existence of the twofold superstructure had previously been reported by Robinson (1949). An order–disorder (OD) interpretation (Dornberger-Schiff & Grell-Niemann, 1961) of the systematic twinning has been given by Makovicky & Olsen (2015).

Using a modern diffractometer system with a hybrid photon counting detector and a highly collimated X-ray beam, we finally were able to refine the structure based on intensity data from a tiny needle of owyheeite. Here, a discussion of the twofold superstructure and an interpretation of the twinning based on partial pseudo-symmetry is given.

The material investigated by us is a portion of a specimen (2 × 3 mm) from Hector-Calumet mine, Elsa, Galena Hill, Mayo Mining District, Yukon, Canada given to one co-author (DT) by Mark Mauthner. Owyheeite is associated with boulangerite, zinkenite and sphalerite.

2. Experimental

2.1. Single crystal diffraction

Intensity data from a small needle of owyheeite were collected at room temperature on a Rigaku XtaLAB Synergy-S diffractometer system with finely collimated Mo Kα radiation. Data were processed with the CrysAlisPro software (1.171.42.85a; Rigaku Oxford Diffraction, 2023). Two main domains were identified and frame data reduced to intensity values with overlap information (HKLF5-style reflection file). Intensities were scaled using the multi-scan approach and a Gaussian absorption correction was applied based on crystal faces.

The structure was solved with SHELXT (Sheldrick, 2015a) and refined against |F|² with SHELXL (Sheldrick, 2015b). Data collection and refinement details are compiled in Table 1.

Table 1
Experimental details for owyheeite

Crystal data
Chemical formula	Ag2.80Cu0.20Pb9.77S28Sb11.23
Mr	4604.25
Crystal system, space group	Monoclinic, P21/n
Temperature (K)	298
a, b, c (Å)	8.1882 (3), 27.2641 (7), 22.8679 (7)
β (°)	90.283 (3)
V (Å^3)	5105.0 (3)
Z	4
Radiation type	Mo Kα
μ (mm^−1)	40.20
Crystal size (mm)	0.06 × 0.02 × 0.01
Data collection
Diffractometer	Rigaku XtaLAB Synergy, Dualflex, HyPix-6000 HE
Absorption correction	Multiscan (CrysAlisPRO; Rigaku Oxford Diffraction, 2023). Numerical absorption correction based on Gaussian integration over a multifaceted crystal model. Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.
Tmin, Tmax	0.167, 0.800
No. of measured, independent and observed [I > 2σ(I)] reflections	40130, 22895, 15639
Rint	0.044
(sin θ/λ)max (Å^−1)	0.714
Refinement
R[F^2> 2σ(F^2)], wR(F^2), S	0.066, 0.146, 1.02
No. of reflections	22895
No. of parameters	495
No. of restraints	1
	w = 1/[σ^2(Fo^2) + (0.0506P)^2 + 282.6104P] where P = (Fo^2 + 2Fc^2)/3
Δρmax, Δρmin (e Å^−3)	2.22, −4.45
Additional computer programs: OLEX2 (v. 1.5; Dolomanov et al., 2009).

2.2. Electron microprobe analysis

Ten points analyses on three grains were performed with a Jeol JXA 8530 F field emission electron microprobe in WDS mode at 25 kV, 20 nA, 2 µm beam diameter, using sulfide and metal standards and an online ZAF correction procedure (Fig. 1). The owyheeite empirical formula (52 apfu) is Cu_0.09 (1)Ag_2.77 (4)Pb_10.23 (4)Sb_10.89 (5)S_28.00 (5) with no serious variations among 10 individual analytical points and very close to the published empirical formula for owyheeite (Laufek et al., 2007). The composition is reasonably close to the composition refined from single crystal data, Cu_0.20Ag_2.80Pb_9.77S₂₈Sb_11.23. It must however be noted that the localization of the Cu position in the crystal structure is highly speculative (see below).

Figure 1 (a) Backscattered electron (BSE) image of owyheeite (gray) grains, associated with boulangerite (light gray), small inclusions of galena (white) and quartz (black). (b) Corresponding plane-polarized optical image showing dimensions and random orientation of owyheeite grains.

3. Results and discussion

3.1. Structural overview

Owyheeite is a twofold superstructure that can be derived from a basic structure with P2₁/c symmetry and lattice parameter a_b = a/2 ∼ 4.1 Å. The corresponding basis vector will be called a_b = a/2. By ignoring the superstructure reflections, an average structure with unit-cell parameter a_b is obtained in structure refinements. Note that the basic and average structures are related yet subtly different [for details see, for example, van Smaalen (2007)].

Since this average structure has been described in detail (Laufek et al., 2007; Makovicky & Olsen, 2015), here only a short overview is given. The structure is monoclinic, but possesses pseudo-orthorhombic metrics [β = 90.292 (3)°]. As numerous other members of the sulfosalt family, owyheeite is a modular structure (Ferraris et al., 2008). In the classical interpretation, it is described as being built of two kinds of rods extending along [100], marked by blue and orange backgrounds in Fig. 2. The rods can be considered as an intermediate between the PbS and SnS archetypes. The octahedral coordination is strongly distorted by formation of distinct long (orange background) and short (blue background) electron-pair micelles at the center of the rods, where predominantly Sb is located. The rods connect via predominant Pb positions with capped prismatic coordination and Ag positions with tetrahedral coordination. For a detailed description of the coordination polyhedra, see Laufek et al. (2007).

Figure 2 The crystal structure of owyheeite viewed down [100]. Atoms are represented by gray (S), blue (predominant Pb), red (predominant Sb), green (Ag) and orange (putative Cu) spheres of arbitrary radius. Blue and orange backgrounds mark the two kinds of crystal-chemical rods according to the interpretation of Laufek et al. (2007). Light colors of the background indicates a translational component of a/2. The p-subscript in cp means that the axis is (slightly) out of plane, owing to the slightly obtuse angle β. The n[010] glide reflection planes are indicated by the usual dash-dotted lines.

3.2. Superstructure

In the actual superstructure, a is doubled to a = 2a_b ∼ 8.2 Å, which means that the crystal-chemical rods described above can appear in two positions with respect to the a-axis (origin at x = 0 and ½, respectively). Rods related by the c_[010] glide reflection in the basic structure are additionally translated along a/2 as indicated by different shading of the blue and orange backgrounds in Fig. 2. Owing to the additional intrinsic translational component, the c_[010] glide reflection becomes an n_[010] glide reflection (indicated by the usual graphical symbol in Fig. 2) and the symmetry of the superstructure is accordingly P2₁/n. The symmetry descent from the P2₁/c basic structure to the P2₁/n superstructure is of the klassengleiche type (retention of crystal class) and of index 2. More precisely, it is an isomorphic symmetry descent, since the space groups are of the same type.

Each site in the average structure splits into two sites in the superstructure (ignoring additional occupational disorder). Atoms corresponding to the same position in the average structure are labeled with the same number. Labels of atoms with x-coordinates in the 0–½ range end in an A, those in the ½–1 range with a B. Labels of S-sites start with S, of other sites with M (for metal).

Tables 2 and 3 list the distances of the atoms in the superstructure to those in the average structure. The latter were calculated by transforming into the a_b ∼ 4.1 Å cell and averaging the resulting coordinates. Sites with occupancies <½ were ignored for these considerations.

Table 2
Distance of S atoms in the superstructure to those in the average structure

Atoms	d (Å)	Atoms	d (Å)
S1A/S1B	0.062	S8A/S8B	0.105
S2A/S2B	0.028	S9A/S9B	0.213
S3A/S3B	0.028	S10A/S10B	0.193
S4A/S4B	0.074	S11A/S11B	0.150
S5A/S5B	0.094	S12A/S12B	0.261
S6A/S6B	0.051	S13A/S13B	0.135
S7A/S7B	0.200	S14A/S14B	0.198

Table 3
Distance of M atoms in the superstructure to those in the average structure, whereby sites with occupancies < ½ were ignored

Occupancies of the 0 < x < ½ and x < ½ < 1 sites are listed in the second and third column, respectively.

Sites	d (Å)	occ. 0 < x < ½	occ. ½ < x < 1
M1A/M1B	0.031	Pb	Pb
M2A/M2B	0.026	Pb	Pb
M3A/M3B	0.061	Pb	Pb
M4A/M4B	0.245	76% Pb, 24% Sb	90% Ag, 10% Cu
M5A/M5B	0.079	95% Sb, 5% Pb	97% Sb, 3% Pb
M6A/M6B	0.103	98% Sb, 2% Pb	73% Pb, 27% Sb
M7A/M7B	0.032	Pb	Pb
M8A/M8B	0.109	Sb	Sb
M9A/M9B	0.177	Sb	Sb
M10A/M10B	0.109	Sb	Sb
M11A/M11B	0.136	93% Sb, 7% Pb	97% Sb, 3% Pb
M12A/M12B	0.091	Ag	Ag

The modulation amplitude is color-coded in Fig. 3(a) and the atom-naming scheme given in Figs. 3(b) and 3(c). The largest modulation amplitudes (>0.24 Å from the averaged position) are observed for the S12A/S12B and M4A/M4B sites (red background). Atoms which show less than 0.10 Å modulation amplitude are marked by a yellow background and atoms with an intermediate modulation (0.10–0.24 Å) by a blue background.

Figure 3 (a) The crystal structure of owyheeite viewed down [100]. Atoms are represented by gray (S), blue (predominant Pb), red (predominant Sb), green (Ag) and orange (putative Cu) spheres of arbitrary radius. Background according to modulation amplitude with respect to the average structure (yellow: <0.10 Å, blue: 0.10–0.24 Å, red: >0.24 Å). Numbering schemes of the (b) S- and (c) M-sites. Slightly more than an asymmetric unit is shown for better orientation.

The part of the structure that shows less modulation is the `surface' of the crystal-chemical rods described in the previous section (§3.1), whereas the `center' of the rods feature distinctly more pronounced modulation. This will lead to an alternative rod description below.

Besides positional modulation, formation of a superstructure can also affect occupancies. These are compiled in the two rightmost columns of Table 3 (no occupational modulation occurs for S atoms). The structure features practically no occupational modulation with two exceptions. Firstly, the M4A/M4B sites mentioned previously and secondly the M6A/M6B sites, which are Sb/Pb mixed positions at the midpoint of the `long' electron-pair micelles [see Fig. 3(a) for position]. The M6A position is practically pure (98%) Sb as expected for atoms bordering the micelles. However, perhaps surprisingly, the M6B position is majorly (73%) Pb.

The M4A/M4B site is unique, as it is heavily positionally modulated and occupationally disordered. The M4A/M4B atoms and the coordinating S atoms are depicted in Fig. 4. The M4A site was refined as a Pb (76%) and an Sb (24%) position. Considering Pb⋯S contacts up to 3.6 Å, the Pb4A position is coordinated by a square pyramid [2.572 (8)–3.432 (6) Å]. A further longer contact to S12B [3.664 (6) Å] completes the strongly irregular octahedral coordination. The minor Sb4A sites features four short contacts [2.386 (10)–3.362 (12) Å] and a longer Sb4A⋯S8A contact [3.568 (10) Å]. The irregular polyhedron can be derived from a trigonal bipyramid.

Figure 4 Column of disordered M4A/M4B sites with coordinating S atoms.

On the M4B site three distinct electron-density peaks were observed, which were assigned to two Ag atoms and a Cu atom. However, assignment of the latter is purely speculative and based on the composition determined from microprobe analysis and very short M—S distances, which might however be virtual. The major position (72% Ag) is coordinated by a flattened tetrahedron [2.542 (7)–2.844 (7) Å]. The coordination of the minor Ag position (10%) appears trigonally planar, though local changes of the coordinating S atoms may not be apparent from X-ray diffraction. Likewise, the putative Cu atom (18% occupancy) features two very short apparent contacts [2.26 (3) and 2.34 (3) Å], which may however not be realized.

The pronounced modulation of the electron pair micelles is reflected by a distinct asymmetry of the Sb coordination polyhedra (Fig. 5). Ignoring contacts across the micelles, the coordination can be considered as distorted square pyramidal, or ψ¹-octahedral when including the electron pairs. When (arbitrarily) choosing 3.0 Å as the limit between short and intermediate length Sb—S bonds, the modulation forms characteristic patterns. The contact to the apex of the pyramid (the S atoms obstructed in Fig. 5 by the M atoms) is always short, practically always less than 2.5 Å. Only for the M6B position, which however is mostly Pb, a longer distance of 2.641 (6) Å is observed. In the short micelles [Fig. 5(a)], one row of Sb atoms features alternately 5 (Sb10A) and 3+2 (Sb10B) coordination. In contrast, the second row (Sb11A/Sb11B) features only 4+1 coordination, whereby the intermediate length contact alternates between two positions. In the long micelles [Fig. 5(b)] only an alternating sequence of 5 and 3+2 coordinations are realized, whereby adjacent rows are offset by a/2. In the M6A/M6B row, the position of the 5 coordinated M atom is substituted by ∼73% Pb (see also Table 3).

Figure 5 `Surface' of the (a) short (blue in Fig. 2) and (b) long (orange in Fig. 2) electron-pair micelles. M⋯S contacts are indicated up to 3.0 Å. Minor positions are omitted for clarity.

3.3. Twinning and polytypism

3.3.1. OD Theory

Owyheeite is twinned by reflection at the (021) or equivalently planes. Makovicky & Olsen (2015) have presented an OD interpretation (Dornberger-Schiff & Grell-Niemann, 1961) of the twinning of owyheeite. In such an OD interpretation, partial symmetry, i.e. symmetry that is valid only for a distinct modules, usually diperiodic layers, leads to an ambiguity in the arrangement of the modules. It is only required that adjacent modules form geometrically equivalent pairs, meaning that all possible arrangements are locally equivalent. Thus, OD theory can be considered as a generalization of the concept of crystalline matter to short-range order.

The symmetry of an OD structure is described by a groupoid of partial operations (POs) mapping a module onto itself or onto a different module. These OD groupoids are categorized into OD groupoid families, which correspond to the 230 space group types in classical crystal structures. The linear parts of POs that are not valid for the whole structure often appear as twin operations. Thus, OD groupoid families offer an unified view on a family of polytypes and the potential twin operations or other stacking faults (such as formation of antiphase domains) of its members.

Not all of the POs correspond to full symmetry operations and therefore OD structures typically feature desymmetrization (Ďurovič, 1979) with respect to an idealized model.

Application of the OD theory serves two distinct purposes. Firstly, it allows the concise description and prediction of various forms of stacking disorders. Secondly, on a higher level, it allows for a classification of whole families of polytypic structures. The second may require a higher degree of idealization.

3.3.2. A simplified structure

To keep the OD description simple, we will apply the OD theory to a simplified archetype structure. An application of the OD theory to the owyheeite superstructure would result in numerous different putative twin composition planes, which cannot be differentiated by routine diffraction methods. In fact, Fig. 3 shows that parts of the structure with large modulation are separated by parts with negligible modulation. Since the former feature less translation symmetry, application of the OD theory would predict alternative possible placements of the former with respect to the latter. However, so far there is no evidence of such an ambiguity. Moreover, as we will show below, alternative polytypes possess electron-pair micelles of a different shape, which might possess a different modulation. Instead, here we attempt to develop a model that is as simple as possible, yet complex enough to explain the observed twinning and to provide a building principle that can be applied to related structures with different modulations.

Firstly, we will only consider the basic P2₁/c structure with unit-cell parameter a_b = a/2 ∼ 4.1 Å. Moreover, we will assume reflection symmetry at planes x = ½. The resulting, distinctly simpler, structure has orthorhombic Pmcn symmetry. The full symbol P2₁/m2₁/c2₁/n emphasizes the supergroup relation with P2₁/c. This pseudo-symmetry has already been noted by Makovicky & Olsen (2015). Even though the upcoming discussion will pertain to the simplified Pmcn archetype structure, some figures will show the actual structure to give an impression of the deviation from this idealized symmetry.

3.3.3. A structure of rods

The OD interpretation of Makovicky & Olsen (2015) in terms of OD layers is not entirely satisfying, because the OD groupoids do not contain all operations of the actual polytype and introduction of `accidental' symmetry is required. An analogous phenomenon is observed for the close-packing of spheres, when described as an OD structure of hexagonal layers. For the cubic closest packing, additional `accidental' symmetry operations, namely threefold rotations with an axis inclined to the layer planes, are not contained in the OD groupoid and appear `out of nowhere'. The close-packing of spheres is therefore a poor example of an OD structure.

This shortcoming in the OD description of owyheeite is due to the fact that the twin plane is at an oblique angle to the monoclinic axis of owyheeite. The OD layers were chosen by Makovicky & Olsen (2015) as extending parallel to (021). The symmetry operations in the [010] direction of the actual structure cannot be contained in the OD groupoid because they would map a layer onto a layer extending parallel to , which intersects the original layer. In fact, these layers are a symmetrically equivalent description to the (021) layers. Ultimately, a unified description can only be obtained by modeling the structure in terms of periodic rods extending along [100].

As has already been noted by Makovicky & Olsen (2015), the twin elements form an angle close to 120° with the symmetry elements of the structure. Here, we will assume ideal 120° angles. Deviations therefrom are due to desymmetrization of the actual polytypes.

The first step in an OD interpretation is identifying the modules. Reflection planes encompassing a 120° angle require a threefold rotational symmetry along the plane intersections. In the least modulated parts of the structure (yellow background in Fig. 3), there are suggestive rods of Pb atoms coordinated by bicapped trigonal prisms located around a threefold pseudo-rotation axis, as has already been noted by Laufek et al. (2007). Extending outward from this structural element the atoms that still follow this symmetry are identified. Ultimately, the truncated triangular rods shown in Fig. 6 are obtained, which will be designated as A-rods. The threefold rotation and the x = ½ reflection plane combine to give rod symmetry. Similar trigonal modules have been identified in numerous other sulfosalt minerals (Makovicky, 1985).

Figure 6 The crystal structure of owyheeite viewed down [100]. Atoms are represented by gray (S), blue (predominant Pb), red (predominant Sb), green (Ag) and orange (putative Cu) spheres of arbitrary radius. Lines mark the outline of the A- and B-rods.

By identifying the A-rods, all atoms with the exception of the Ag13 atoms are located either in or at the boundary of the rods. Thus, Ag13 and the coordinating S atoms form a second kind of rod, called B-rods, with symmetry (Fig. 6). The symmetry of both kinds of rods is shown in Fig. 7.

Figure 7 The (left) A- and (right) B-rods viewed (top) along and (bottom) perpendicular to the rod axis. Atoms are represented by gray (S), blue (predominant Pb), red (predominant Sb), green (Ag) and orange (putative Cu) spheres of arbitrary radius. (Pseudo-)symmetry elements are indicated by the usual graphical symbols.

3.3.4. Maximum equivalent regions

The partitioning of the structure into A- and B-rods is clearly not OD in the classical sense, which would mean that equivalent sides of an A-rod connect to adjacent rods in geometrically equivalent ways. However, the A-rods possess three equivalent `short' sides, two of which connect to other A-rods via a shared face and the third to a B-rod via an edge.

Nevertheless, the structure can still be considered to have OD character. In fact, the crucial part of an OD interpretation is that all polytypes of a family are locally equivalent. In classical OD structures, every pair of adjacent modules is part of a maximum equivalent region (MER), which is the largest region that is equivalent in all polytypes of the family (Grell, 1984). Since the structure is fully covered by MERs consisting of at least two modules, every point of a polytype is located at least one module deep in an MER [see Figs. 8(a) and 8(b)].

Figure 8 (a,b) Schematic representation of two members of an OD family of layer structures with MERs of two layers width. (c,d) Schematic representation of two members of a family of non-OD layer structures, where the polytypes are nevertheless fully covered by MERs. Odd-numbered layers can appear in one of two orientations.

However, such a situation can also be constructed with modules contacting in non-equivalent ways as shown in Fig. 8(b). We have named these kinds of structures non-classical OD structures (Stöger & Weil, 2013).

In owyheeite, one can also identify such an MER composed of three A-rods and one B-rod, as schematized in Fig. 9.

Figure 9 Schematic representation of a MER in the archetype structure of owyheeite consisting of three A-rods and one B-rod viewed down [100]. Different levels of gray indicate a translation of ab/2. POs of particular interest (see text) are indicated in red.

To build the structure from MERs, one has to know their partial symmetry. The POs mapping a rod onto itself, called λ-POs in OD theory, correspond to the rod groups of the A- and B-rods as described above. The POs mapping two distinct rods are called σ-POs. Since rod groups are infinite, there is also an infinite number of σ-POs relating two given rods of the same type. Since all rods possess the same translation group it is convenient to consider σ-POs only up to translation. Then two A-rods are related by = 6 and two B-rods by = 4 classes of σ-POs.

The two adjacent A-rods of the MER sharing a face are mapped by a reflection and a twofold rotation as in indicated in Fig. 9 (top of figure). The linear parts of these two operations remain as twin law. Their symmetry elements (reflection plane and rotation axis) coincide with those of the B-rod. This is an important fact, as it means that the B-rod can only be placed in one way with respect to the A-rods. The remaining four classes of σ-POs relating adjacent A-rods are glide reflections and screw rotations, which are not indicated in Fig. 9 for clarity.

The top-left and bottom A-rods in Fig. 9 are mapped by an inversion, which remains as a total operation of the owyheeite structure. It is located at x = ¼ which means that the origins of the rods are shifted along a_b/2, which is indicated by a different shade of gray in Fig. 9. The other classes of σ-POs are two- and sixfold screw rotations and threefold rotoinversions.

The top-right and bottom A-rods in Fig. 9 are mapped by twofold screw rotations and glide reflections. The screw axis indicated in Fig. 9 is a symmetry operation of the archetype structure.

3.3.5. Polytypes

In analogy to OD structures of layers, the whole polytype can be grown by applying the λ- or σ-POs described in the previous section to the MER. Since the POs are valid for individual A-rods, but not the whole MER, non-equivalent fragments are thus obtained. For example, Fig. 10 shows three non-equivalent ways of applying λ- or σ-POs to the MER shown in Fig. 9. All three cases are partial overlays of two MERs sharing a common A-rod.

Figure 10 Three geometrically non-equivalent ways of extending the MER of Fig. 9 with another MER, such that they share the top-left A-rod of Fig. 9. A representative operation mapping the first MER to the second is indicated by the graphical symbol of the corresponding symmetry element (note that graphical symbols are defined for full symmetry elements, not single symmetry operations).

By repeated extension of the newly generated fragment with MERs, full polytypes can be grown. Here, a significantly increased complexity of rod polytypes manifests itself, as not all combinations of MERs lead to valid structures. Thus, whereas enumerating all layer polytypes is generally trivial, doing the same for rod polytypes may be a challenging combinatorial problem. Examples of possible polytypes are schematized in Fig. 11. Note that every A-rod belongs to three MERs.

Figure 11 Schematic representation of three distinct polytypes obtained by combining MERs: (a) Pmcn archetype owyheeite, (b) isomorphic Pmcn symmetry, (c) a putative polytype. Light colors indicate a translation along a/2.

Fig. 11(a) shows the Pmcn archetype owyheeite structure. Fig. 11(b) gives an alternative polytype with isomorphic Pmcn symmetry, but a different shape of the unit cell. These two polytypes are constructed of equivalent layers (extending horizontally in Fig. 11). They are members of the OD family of layers suggested by Makovicky & Olsen (2015), if one ignores the issue of `accidental' symmetry. An example of a putative polytype that cannot be derived from the layer model is schematized in Fig. 11(c). It has hexagonal symmetry and is the simplest representative of a whole family of polytypes, since every A-rod with a dark shade in Fig. 11(c) can appear in one of two orientations.

Twins of the owyheeite archetype can be formed as shown in Fig. 12(a), where a fragment of the polytype of Fig. 11(b) is located between both twin domains. The orientations of the twin individuals are related by the linear part of a reflection σ-PO (see Fig. 9). Owing to the threefold symmetry of the A-rods, the composition plane can also occur in other directions. The possible twin orientation states of the owyheeite archetype structure can be derived by coset decomposition of the point group of the structure in the point group of the groupoid of all POs. These are the point groups generated by the linear parts of all symmetry operations and all POs, respectively. Thus, there are |6/mmm|/|mmm| = 3 possible orientation states, with a threefold axis as twin element.

Figure 12 Schematic representation of (a) a twin and (b) a trill (a twin with three orientation states) of the owyheeite archetype structure. Gray, red and blue represent different twin domains. Parts of the structure that can be attributed to two or three domains are colored in yellow. Light colors indicate a translation along a/2.

For example, Fig. 12(b) gives an example of a trill (twin with three orientation states) meeting in a single rod. As before, the interface between two domains are sheet-like fragments of the polytype in Fig. 11(b). Where all three domains meet, a rod-like fragment of the Fig. 11(c) polytype is realized. As noted by Makovicky & Olsen (2015), such a trill might not be stable in actual owyheeite owing to strong metric distortions of the bulk domains.

3.3.6. Electron-pair micelles

The schemes in Figs. 11 and 12 feature white areas, which represent regions of non-interaction between the A- and B-rods that have been ignored so far. In general, the possibility of empty space between rods is a further complication compared to layer polytypes and may appear for example in zeolites or metal–organic frameworks (MOFs). For owyheeite, these regions are not empty, but correspond to the electron-pair micelles discussed in §3.1. The model above assumed that these are not structure directing, i.e. the rods can contact in arbitrary ways. Evidently, this is a strong idealization, as there will be interactions across the electron-pair micelles.

If the micelles are considered as individual modules, the polytypes cease having OD character. To show this, we increase the level of abstraction and represent the arrangement of the A- and B-rods by oriented equilateral triangles, whereby the A-rod triangles have a tripled side length compared to the B-rod triangles. The triangles can then be placed on a trigonal net as shown in Fig. 13. The electron-pair micelles are the remaining space, i.e. small unshaded triangles. In the owyheeite archetype [Fig. 13(a)], two kinds of micelles exist, a long and a short one marked by red and blue arrows, respectively. These correspond to the short and long rods marked in Fig. 2. In the polytype schematized in Fig. 13(b) [corresponding to Fig. 11(b)], a third intermediate-length micelle exists, marked by a yellow arrow. Such micelles are therefore expected to exist at the interface between two twin domains. The micelle differs from the previous ones in that the adjacent B-rods are at the same x-coordinates (note the shading of the B-rods at the long end of the micelles). The hypothetical P6/m and related polytypes of Fig. 11(c) only possess micelles of this kind [see Fig. 13(c)].

Figure 13 Schematic representation of the polytypes from Fig. 11 by triangles placed on a triangular net. The orientation of the A-rods is given by circular arrows. Different kinds of electron-pair micelles are indicated by colored arrows.

Thus, when considering the electron-pair micelles as building blocks, the structure family does not have OD character, since the A- and B-rods connect to different micelles. Ultimately, one might even consider the structures as not being polytypes, but rather members of a merotype family (Ferraris et al., 2008), since they may contain different types of electron-pair micelles. Despite the varying spatial distribution of A- and B-rods, in all polytypes there are as many A-rods as B-rods.

Note that the modulation of atoms in the actual owyheeite superstructure is distinctly more pronounced for the electron-pair micelles and the strongest modulation (M4A/M4B position) is precisely located at the transition from short to long micelles (see Fig. 3). Standard diffraction methods do not allow a structural characterization of the twin interface. Therefore, the exact nature of the intermediate electron-pair micelle is unknown. It might feature a different modulation period or a different chemistry, which substantiates the choice of basing the model on a simplified archetype structure. The latter could mean the twin interface is allochemical.

3.3.7. Relationship to the OD interpretation in terms of layers

The rod interpretation given above was derived by combining the OD interpretation of Makovicky & Olsen (2015) with the space group symmetry of the archetype structure. The model should therefore reduce to the original OD model if only a single twin-plane is considered. This is in fact the case, as schematized in Fig. 14. Makovicky & Olsen (2015) proposed an alternating sequence of two kinds of OD layers. Thick layers, which we designate as L1, feature reflection planes perpendicular to the layer planes and which correspond to the reflection planes indicated in Fig. 9. The thinner L2-layers do not possess such a symmetry. Note that application of the reflection plane of an L1-layer onto the adjacent L2-layer changes the connectivity of the A- and B-rods and generates an alternative electron-pair micelle at the twin interface that does not exist in the twin individuals as described in the previous section.

Figure 14 The twin interface schematized in Fig. 12(a) interpreted in terms of an OD structure of layers. Horizontal lines indicate the layer boundaries. Layer types are indicated to the right. Color codes as in Fig. 12.

3.3.8. An alternative three-rod model

A characteristic feature of the owyheeite structure is the M4 column (Fig. 4), which is located at the `corner' of the A-rods close to the contact point of the B-rods. In the actual polytype [Fig. 11(a)], there is one such M4 column per A-rod. In the polytypes of Figs. 11(b) and 11(c) one might also expect none, two or three M4 columns, according to the number of connected B-rods. In a strict sense, these different kinds A-rods could therefore be considered as non-equivalent. When allowing for less idealization the corners of the A-rods have to be omitted, resulting in smaller C-rods, marked by a blue background in Fig. 15. Two of the three corners of the A-rods are then attributed to the B-rods, giving a new D-rod (red in Fig. 15). The third corner, which features the M4 column, becomes a third kind of rod, designated as E (yellow in Fig. 15). The resulting three-rod model is equivalent to the two-rod model with MERs being built of three C-rods, one D-rod and one E-rod. It is a common phenomenon in OD structures that varying levels of idealization lead to equivalent models with a different number of kinds of layers. The interface between modules can be considered as its own module. Here, we focused on a more general model with fewer modules to emphasize the general building principle of the structure family and not the actual chemistry of this particular member.

Figure 15 The crystal structure of owyheeite viewed down [100]. Atoms are represented by gray (S), blue (predominant Pb), red (predominant Sb), green (Ag) and orange (putative Cu) spheres of arbitrary radius. Background colors according to a three-rod interpretation with less idealization.

4. Conclusion and outlook

A description of modular structures is incomplete without consideration of partial symmetry. Only a rod-model allows for a comprehensive symmetry description from which the symmetry of the owyheeite (archetype) structure and the twin operations can be derived. The model also provides a deeper understanding of the nature of the twin domain, notably the different electron-pair micelles located at the twin interface. A theory of polytypes of rods is significantly harder to achieve than for layers and therefore only a little work has been performed in this direction.

A second point of note is that the OD character of a structure is perhaps not ideally expressed by decomposing the structure into disjoint modules. Instead, we suggest considering MERs as the basic building blocks of the structure. The operations relating MERs are likewise partial operations that form groupoids. In this case however, the domains and codomains of the operations do partially overlap. These types of groupoids will allow for a finer classification of modular structures.

Finally, the rod interpretation given here has been derived indirectly from twinning. Alternative arrangements are realized at the twin interface. The ultimate proof of the interpretation's validity will, however, require finding macroscopic polytypes.

Supporting information

Computing details

Program(s) used to refine structure: SHELXL 2014/7 (Sheldrick, 2015); molecular graphics: Olex2 1.5 (Dolomanov et al., 2009); software used to prepare material for publication: Olex2 1.5 (Dolomanov et al., 2009).

(I)

Crystal data

Ag2.802Cu0.198Pb9.773S28Sb11.227	F(000) = 7838
Mr = 4604.25	Dx = 5.991 Mg m^−3
Monoclinic, P21/n	Mo Kα radiation, λ = 0.71073 Å
a = 8.1882 (3) Å	Cell parameters from 10665 reflections
b = 27.2641 (7) Å	θ = 2.6–30.3°
c = 22.8679 (7) Å	µ = 40.20 mm^−1
β = 90.283 (3)°	T = 298 K
V = 5105.0 (3) Å^3	Needle, black
Z = 4	0.06 × 0.02 × 0.01 mm

Data collection

XtaLAB Synergy, Dualflex, HyPix-6000 HE diffractometer	22895 independent reflections
Radiation source: micro-focus sealed X-ray tube, PhotonJet (Mo) X-ray Source	15639 reflections with I > 2σ(I)
Mirror monochromator	Rint = 0.044
Detector resolution: 10.0000 pixels mm^-1	θmax = 30.5°, θmin = 2.6°
Absorption correction: gaussian CrysAlisPro 1.171.42.85a (Rigaku Oxford Diffraction, 2023) Numerical absorption correction based on gaussian integration over a multifaceted crystal model Empirical absorption correction using spherical harmonics, implemented in SCALE3 ABSPACK scaling algorithm.	h = −10→10
Tmin = 0.167, Tmax = 0.800	k = −37→37
40130 measured reflections	l = −31→28

Refinement

Refinement on F^2	495 parameters
Least-squares matrix: full	1 restraint
R[F^2 > 2σ(F^2)] = 0.066	w = 1/[σ^2(Fo^2) + (0.0506P)^2 + 282.6104P] where P = (Fo^2 + 2Fc^2)/3
wR(F^2) = 0.146	(Δ/σ)max = 0.001
S = 1.02	Δρmax = 2.22 e Å^−3
22895 reflections	Δρmin = −4.45 e Å^−3

Special details

Geometry. All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes.

Refinement. Refined as a 2-component twin.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Ų)

	x	y	z	Uiso*/Ueq	Occ. (<1)
Pb1A	0.13809 (14)	0.54196 (3)	0.71129 (5)	0.0267 (2)
Pb1B	0.63907 (14)	0.53999 (3)	0.71251 (5)	0.0273 (2)
Pb2A	0.13200 (13)	0.63842 (4)	0.86531 (4)	0.0249 (2)
Pb2B	0.63777 (13)	0.63931 (4)	0.86509 (4)	0.0249 (2)
Pb3A	0.13610 (13)	0.70101 (4)	0.68425 (5)	0.0249 (2)
Pb3B	0.63427 (13)	0.69841 (4)	0.67996 (5)	0.0257 (2)
Pb4A	0.1431 (2)	0.39576 (5)	0.70156 (7)	0.0402 (5)	0.761 (3)
Sb4A	0.3230 (12)	0.3828 (3)	0.7082 (4)	0.0402 (5)	0.239 (3)
Ag4B	0.6988 (8)	0.39629 (16)	0.70960 (19)	0.0678 (17)	0.700 (4)
Cu4B	0.872 (5)	0.3813 (11)	0.7059 (15)	0.079 (8)*	0.198 (4)
Ag4B'	0.771 (7)	0.3833 (16)	0.693 (2)	0.079 (8)*	0.103 (4)
Sb5A	0.3837 (2)	0.49705 (5)	0.86726 (7)	0.0213 (7)	0.954 (12)
Pb5A	0.3837 (2)	0.49705 (5)	0.86726 (7)	0.0213 (7)	0.046 (12)
Sb5B	0.8769 (2)	0.49291 (5)	0.86305 (7)	0.0186 (6)	0.965 (12)
Pb5B	0.8769 (2)	0.49291 (5)	0.86305 (7)	0.0186 (6)	0.035 (12)
Sb6A	0.3836 (2)	0.57521 (5)	1.00794 (7)	0.0165 (6)	0.980 (12)
Pb6A	0.3836 (2)	0.57521 (5)	1.00794 (7)	0.0165 (6)	0.020 (12)
Pb6B	0.88437 (14)	0.57752 (4)	1.01651 (5)	0.0212 (4)	0.736 (12)
Sb6B	0.88437 (14)	0.57752 (4)	1.01651 (5)	0.0212 (4)	0.264 (12)
Pb7A	0.12978 (12)	0.71549 (3)	1.02526 (4)	0.0203 (2)
Pb7B	0.63621 (12)	0.71459 (3)	1.02407 (4)	0.0213 (2)
Sb8A	0.3895 (2)	0.77114 (5)	0.82949 (7)	0.0176 (3)
Sb8B	0.8947 (2)	0.77516 (6)	0.82143 (7)	0.0187 (4)
Sb9A	0.3874 (2)	0.84421 (5)	0.65815 (7)	0.0164 (3)
Sb9B	0.8867 (2)	0.83625 (5)	0.67042 (7)	0.0170 (3)
Sb10A	0.3874 (2)	0.61028 (6)	0.55911 (7)	0.0207 (7)	0.954 (12)
Pb10A	0.3874 (2)	0.61028 (6)	0.55911 (7)	0.0207 (7)	0.046 (12)
Sb10B	0.8952 (2)	0.60293 (6)	0.56180 (7)	0.0226 (7)	0.960 (12)
Pb10B	0.8952 (2)	0.60293 (6)	0.56180 (7)	0.0226 (7)	0.040 (12)
Sb11A	0.4120 (3)	0.45100 (7)	0.57928 (9)	0.0401 (9)	0.936 (15)
Pb11A	0.4120 (3)	0.45100 (7)	0.57928 (9)	0.0401 (9)	0.064 (15)
Sb11B	0.8894 (5)	0.46416 (9)	0.57591 (9)	0.0215 (5)	0.976 (7)
Pb11B	0.827 (10)	0.456 (2)	0.580 (2)	0.0215 (5)	0.024 (7)
Ag12A	0.3758 (4)	0.33132 (9)	0.56007 (12)	0.0511 (7)
Ag12B	0.8683 (4)	0.33751 (8)	0.56187 (10)	0.0435 (6)
S1A	0.3856 (7)	0.56964 (19)	0.8064 (3)	0.0156 (12)
S1B	0.8821 (7)	0.57118 (19)	0.8113 (3)	0.0154 (12)
S2A	0.3881 (8)	0.6922 (2)	0.7799 (3)	0.0169 (12)
S2B	0.8864 (8)	0.6921 (2)	0.7823 (3)	0.0173 (12)
S3A	0.8848 (8)	0.6178 (2)	0.6661 (3)	0.0161 (12)
S3B	0.3870 (7)	0.61604 (19)	0.6655 (2)	0.0149 (12)
S4A	0.3794 (8)	0.4667 (2)	0.6853 (3)	0.0213 (13)
S4B	0.8959 (9)	0.4648 (2)	0.6842 (3)	0.0215 (13)
S5A	0.3835 (8)	0.65743 (19)	0.9630 (3)	0.0158 (12)
S5B	0.8842 (8)	0.6596 (2)	0.9552 (2)	0.0159 (12)
S6A	0.3849 (7)	0.76088 (19)	0.6179 (3)	0.0145 (12)
S6B	0.8835 (8)	0.7591 (2)	0.6139 (3)	0.0167 (12)
S7A	0.1390 (11)	0.3845 (3)	0.5897 (4)	0.0408 (19)
S7B	0.6039 (9)	0.3821 (2)	0.6017 (3)	0.0303 (16)
S8A	0.1215 (8)	0.4613 (2)	0.8100 (3)	0.0182 (13)
S8B	0.6441 (8)	0.4595 (2)	0.8063 (3)	0.0201 (13)
S9A	0.1620 (9)	0.5455 (2)	0.9434 (3)	0.0222 (14)
S9B	0.6103 (8)	0.5455 (2)	0.9457 (3)	0.0202 (13)
S10A	0.1143 (8)	0.6279 (2)	1.0926 (3)	0.0181 (12)
S10B	0.6612 (8)	0.6276 (2)	1.0905 (3)	0.0195 (13)
S11A	0.1570 (9)	0.7517 (2)	0.8942 (3)	0.0237 (14)
S11B	0.6209 (8)	0.7522 (2)	0.8947 (3)	0.0195 (13)
S12A	0.1089 (8)	0.8062 (2)	0.7409 (3)	0.0192 (13)
S12B	0.6700 (8)	0.8120 (2)	0.7425 (3)	0.0248 (14)
S13A	0.1422 (8)	0.6660 (2)	0.5494 (3)	0.0186 (13)
S13B	0.6125 (9)	0.6698 (2)	0.5465 (3)	0.0231 (14)
S14A	0.6493 (9)	0.5254 (2)	0.5771 (3)	0.0255 (15)
S14B	0.1048 (8)	0.5295 (2)	0.5723 (3)	0.0205 (13)

Atomic displacement parameters (Ų)

	U^11	U^22	U^33	U^12	U^13	U^23
Pb1A	0.0237 (6)	0.0257 (6)	0.0308 (6)	0.0011 (4)	−0.0005 (5)	−0.0025 (4)
Pb1B	0.0247 (6)	0.0254 (6)	0.0318 (6)	−0.0014 (4)	0.0012 (5)	−0.0043 (4)
Pb2A	0.0220 (6)	0.0325 (6)	0.0204 (5)	−0.0016 (4)	0.0005 (4)	−0.0016 (4)
Pb2B	0.0230 (6)	0.0302 (5)	0.0214 (5)	0.0029 (4)	−0.0003 (4)	−0.0014 (4)
Pb3A	0.0225 (6)	0.0259 (5)	0.0262 (5)	−0.0012 (4)	0.0002 (4)	0.0071 (4)
Pb3B	0.0227 (6)	0.0257 (5)	0.0287 (6)	−0.0001 (4)	0.0006 (5)	0.0071 (4)
Pb4A	0.0491 (11)	0.0328 (8)	0.0389 (9)	0.0000 (7)	0.0007 (8)	−0.0077 (6)
Sb4A	0.0491 (11)	0.0328 (8)	0.0389 (9)	0.0000 (7)	0.0007 (8)	−0.0077 (6)
Ag4B	0.128 (5)	0.036 (2)	0.039 (2)	−0.032 (3)	0.007 (3)	0.0076 (17)
Sb5A	0.0313 (12)	0.0166 (9)	0.0161 (10)	−0.0012 (6)	0.0013 (7)	0.0008 (6)
Pb5A	0.0313 (12)	0.0166 (9)	0.0161 (10)	−0.0012 (6)	0.0013 (7)	0.0008 (6)
Sb5B	0.0202 (11)	0.0201 (9)	0.0156 (10)	0.0016 (6)	−0.0001 (7)	0.0021 (6)
Pb5B	0.0202 (11)	0.0201 (9)	0.0156 (10)	0.0016 (6)	−0.0001 (7)	0.0021 (6)
Sb6A	0.0167 (10)	0.0180 (9)	0.0149 (9)	−0.0004 (6)	−0.0004 (6)	−0.0005 (5)
Pb6A	0.0167 (10)	0.0180 (9)	0.0149 (9)	−0.0004 (6)	−0.0004 (6)	−0.0005 (5)
Pb6B	0.0188 (7)	0.0261 (6)	0.0188 (6)	−0.0012 (4)	0.0018 (4)	−0.0027 (4)
Sb6B	0.0188 (7)	0.0261 (6)	0.0188 (6)	−0.0012 (4)	0.0018 (4)	−0.0027 (4)
Pb7A	0.0198 (6)	0.0221 (5)	0.0191 (5)	−0.0004 (4)	0.0011 (4)	0.0028 (3)
Pb7B	0.0206 (6)	0.0219 (5)	0.0214 (5)	−0.0004 (4)	0.0011 (4)	0.0025 (3)
Sb8A	0.0217 (10)	0.0130 (7)	0.0181 (8)	−0.0011 (6)	0.0016 (7)	0.0016 (6)
Sb8B	0.0251 (10)	0.0167 (8)	0.0142 (8)	0.0012 (6)	−0.0003 (7)	−0.0014 (6)
Sb9A	0.0178 (9)	0.0164 (8)	0.0151 (8)	0.0012 (6)	0.0018 (6)	−0.0003 (6)
Sb9B	0.0186 (9)	0.0152 (8)	0.0173 (8)	−0.0010 (6)	0.0024 (7)	0.0013 (6)
Sb10A	0.0237 (11)	0.0191 (9)	0.0193 (10)	−0.0007 (6)	0.0005 (7)	−0.0027 (6)
Pb10A	0.0237 (11)	0.0191 (9)	0.0193 (10)	−0.0007 (6)	0.0005 (7)	−0.0027 (6)
Sb10B	0.0309 (12)	0.0210 (10)	0.0159 (10)	−0.0006 (7)	0.0008 (7)	0.0000 (6)
Pb10B	0.0309 (12)	0.0210 (10)	0.0159 (10)	−0.0006 (7)	0.0008 (7)	0.0000 (6)
Sb11A	0.0493 (17)	0.0412 (13)	0.0299 (13)	0.0166 (9)	−0.0002 (9)	−0.0050 (8)
Pb11A	0.0493 (17)	0.0412 (13)	0.0299 (13)	0.0166 (9)	−0.0002 (9)	−0.0050 (8)
Sb11B	0.0218 (15)	0.0203 (9)	0.0223 (10)	−0.0049 (10)	0.0038 (9)	−0.0030 (7)
Pb11B	0.0218 (15)	0.0203 (9)	0.0223 (10)	−0.0049 (10)	0.0038 (9)	−0.0030 (7)
Ag12A	0.070 (2)	0.0429 (14)	0.0404 (15)	−0.0033 (13)	0.0044 (14)	0.0079 (10)
Ag12B	0.070 (2)	0.0317 (12)	0.0283 (12)	−0.0042 (11)	−0.0016 (12)	0.0055 (9)
S1A	0.015 (3)	0.012 (3)	0.019 (3)	−0.001 (2)	−0.004 (2)	−0.001 (2)
S1B	0.013 (3)	0.013 (3)	0.020 (3)	0.002 (2)	0.000 (2)	0.000 (2)
S2A	0.021 (4)	0.016 (3)	0.014 (3)	−0.001 (2)	0.000 (2)	−0.004 (2)
S2B	0.017 (3)	0.016 (3)	0.019 (3)	−0.003 (2)	0.001 (2)	0.000 (2)
S3A	0.017 (3)	0.015 (3)	0.016 (3)	−0.001 (2)	0.004 (2)	0.000 (2)
S3B	0.016 (3)	0.015 (3)	0.014 (3)	0.001 (2)	0.001 (2)	0.000 (2)
S4A	0.021 (4)	0.022 (3)	0.021 (3)	−0.003 (2)	0.001 (3)	0.000 (2)
S4B	0.028 (4)	0.021 (3)	0.015 (3)	0.001 (3)	0.001 (3)	0.000 (2)
S5A	0.014 (3)	0.012 (3)	0.022 (3)	0.000 (2)	0.000 (2)	0.000 (2)
S5B	0.014 (3)	0.021 (3)	0.012 (3)	0.004 (2)	0.001 (2)	−0.002 (2)
S6A	0.011 (3)	0.015 (3)	0.018 (3)	0.002 (2)	−0.001 (2)	0.001 (2)
S6B	0.023 (4)	0.013 (3)	0.014 (3)	0.003 (2)	−0.002 (2)	−0.001 (2)
S7A	0.039 (5)	0.029 (4)	0.054 (5)	−0.001 (3)	0.010 (4)	−0.004 (3)
S7B	0.020 (4)	0.024 (3)	0.047 (4)	0.002 (3)	0.003 (3)	−0.007 (3)
S8A	0.023 (4)	0.014 (3)	0.017 (3)	−0.002 (2)	0.001 (2)	−0.001 (2)
S8B	0.020 (4)	0.020 (3)	0.020 (3)	0.000 (2)	0.000 (3)	0.001 (2)
S9A	0.026 (4)	0.022 (3)	0.019 (3)	−0.001 (2)	−0.007 (3)	0.000 (2)
S9B	0.021 (4)	0.022 (3)	0.018 (3)	0.002 (2)	−0.002 (3)	−0.004 (2)
S10A	0.017 (3)	0.017 (3)	0.020 (3)	0.001 (2)	−0.002 (2)	−0.002 (2)
S10B	0.017 (3)	0.021 (3)	0.021 (3)	−0.001 (2)	−0.001 (3)	0.002 (2)
S11A	0.028 (4)	0.024 (3)	0.019 (3)	0.003 (3)	0.004 (3)	0.005 (2)
S11B	0.028 (4)	0.016 (3)	0.015 (3)	−0.002 (2)	−0.002 (3)	0.000 (2)
S12A	0.019 (4)	0.021 (3)	0.017 (3)	−0.003 (2)	−0.002 (3)	0.004 (2)
S12B	0.016 (4)	0.034 (4)	0.024 (3)	0.004 (3)	0.007 (3)	0.004 (3)
S13A	0.020 (4)	0.018 (3)	0.018 (3)	0.003 (2)	0.002 (3)	−0.001 (2)
S13B	0.024 (4)	0.019 (3)	0.026 (3)	−0.003 (2)	0.009 (3)	0.003 (2)
S14A	0.020 (4)	0.027 (3)	0.029 (4)	0.011 (3)	−0.004 (3)	−0.005 (3)
S14B	0.019 (3)	0.016 (3)	0.027 (3)	−0.002 (2)	−0.003 (3)	0.002 (2)

Geometric parameters (Å, º)

Pb1A—Pb1B	4.1024 (17)	Sb9A—S8A^ix	3.275 (6)
Pb1A—Pb1B^i	4.0866 (17)	Sb9A—S10A^xii	2.511 (7)
Pb1A—Pb4A	3.9924 (17)	Sb9A—S10B^xi	2.527 (6)
Pb1A—Sb11B^i	4.263 (3)	Sb9A—S12A	3.146 (7)
Pb1A—S1A	3.061 (6)	Sb9A—S12B	3.131 (7)
Pb1A—S1B^i	3.210 (6)	Sb9B—Sb4A^x	3.860 (10)
Pb1A—S3A^i	3.102 (6)	Sb9B—Ag4B^x	3.274 (4)
Pb1A—S3B	3.058 (6)	Sb9B—Cu4B^x	3.75 (3)
Pb1A—S4A	2.912 (7)	Sb9B—Ag4B'^x	3.63 (5)
Pb1A—S4B^i	2.955 (7)	Sb9B—S6B	2.467 (6)
Pb1A—S8A	3.155 (6)	Sb9B—S8B^x	3.413 (6)
Pb1A—S14B	3.207 (6)	Sb9B—S10A^xii	3.009 (6)
Pb1B—Pb1A^ii	4.0866 (17)	Sb9B—S10B^xii	3.067 (7)
Pb1B—Ag4B	3.949 (5)	Sb9B—S12A^ii	2.559 (6)
Pb1B—Pb11B	4.09 (6)	Sb9B—S12B	2.516 (7)
Pb1B—S1A	3.101 (6)	Sb10A—Sb10B^i	4.037 (3)
Pb1B—S1B	3.121 (6)	Sb10A—Pb10B^i	4.037 (3)
Pb1B—S3A	3.114 (6)	Sb10A—Sb11A^xiii	3.944 (3)
Pb1B—S3B	3.114 (6)	Sb10A—Pb11A^xiii	3.944 (3)
Pb1B—S4A	2.981 (6)	Sb10A—Ag12A^xiii	3.711 (3)
Pb1B—S4B	3.010 (7)	Sb10A—Ag12B^xiii	3.743 (3)
Pb1B—S8B	3.067 (6)	Sb10A—S3B	2.437 (6)
Pb1B—S14A	3.123 (7)	Sb10A—S7B^xiii	3.684 (8)
Pb2A—Pb2B	4.1414 (16)	Sb10A—S13A	2.527 (6)
Pb2A—Pb2B^i	4.0469 (16)	Sb10A—S13B	2.473 (7)
Pb2A—Sb6A	4.2173 (18)	Sb10A—S14A	3.181 (6)
Pb2A—S1A	3.110 (6)	Sb10A—S14B	3.210 (6)
Pb2A—S1B^i	3.008 (6)	Sb10B—Sb10A^ii	4.037 (3)
Pb2A—S2A	3.226 (6)	Sb10B—Pb10A^ii	4.037 (3)
Pb2A—S2B^i	3.123 (6)	Sb10B—Sb11B^xiv	4.054 (3)
Pb2A—S5A	3.075 (6)	Sb10B—Sb11B	3.798 (3)
Pb2A—S5B^i	2.952 (6)	Sb10B—Ag12A^xiii	3.980 (3)
Pb2A—S9A	3.109 (6)	Sb10B—Ag12B^xiv	3.800 (3)
Pb2A—S11A	3.165 (6)	Sb10B—S3A	2.421 (6)
Pb2B—Pb2A^ii	4.0470 (16)	Sb10B—S7A^xiii	3.492 (9)
Pb2B—Pb7B	4.1749 (14)	Sb10B—S13A^ii	2.672 (7)
Pb2B—Sb8A	4.2068 (18)	Sb10B—S13B	2.966 (7)
Pb2B—S1A	3.105 (6)	Sb10B—S14A	2.941 (8)
Pb2B—S1B	2.999 (6)	Sb10B—S14B^ii	2.647 (6)
Pb2B—S2A	3.165 (6)	Sb11A—Pb10A^xiii	3.944 (3)
Pb2B—S2B	3.136 (6)	Sb11A—Sb11B	3.927 (5)
Pb2B—S5A	3.104 (6)	Sb11A—Pb11B	3.40 (8)
Pb2B—S5B	2.929 (6)	Sb11A—Ag12A	3.306 (3)
Pb2B—S9B	3.162 (6)	Sb11A—S4A	2.478 (7)
Pb2B—S11B	3.156 (6)	Sb11A—S7A	2.890 (8)
Pb3A—Pb3B^i	4.1103 (17)	Sb11A—S7B	2.501 (7)
Pb3A—Pb3B	4.0814 (17)	Sb11A—S14A	2.809 (8)
Pb3A—Sb8B^i	4.2305 (19)	Sb11A—S14A^xiii	3.666 (7)
Pb3A—Sb9B^i	4.2259 (18)	Sb11A—S14B	3.306 (7)
Pb3A—S2A	3.009 (6)	Sb11B—Pb11B	0.57 (8)
Pb3A—S2B^i	3.052 (6)	Sb11B—Ag12B	3.472 (3)
Pb3A—S3A^i	3.089 (6)	Sb11B—S4B	2.477 (6)
Pb3A—S3B	3.127 (6)	Sb11B—S7A^ii	2.999 (8)
Pb3A—S6A	3.025 (6)	Sb11B—S7B	3.291 (8)
Pb3A—S6B^i	3.057 (6)	Sb11B—S14A	2.579 (7)
Pb3A—S12A	3.155 (6)	Sb11B—S14B^xiii	3.394 (7)
Pb3A—S13A	3.229 (6)	Sb11B—S14B^ii	2.509 (7)
Pb3B—Pb3A^ii	4.1103 (17)	Pb11B—Ag12B	3.28 (5)
Pb3B—Sb10A	4.1761 (19)	Pb11B—S4B	2.45 (5)
Pb3B—S2A	3.059 (6)	Pb11B—S7A^ii	3.23 (7)
Pb3B—S2B	3.118 (6)	Pb11B—S7B	2.77 (8)
Pb3B—S3A	3.024 (6)	Pb11B—S14A	2.38 (6)
Pb3B—S3B	3.041 (6)	Pb11B—S14B^ii	3.04 (8)
Pb3B—S6A	3.009 (6)	Ag12A—Pb7A^iii	3.712 (3)
Pb3B—S6B	3.036 (6)	Ag12A—Sb8A^iii	3.721 (3)
Pb3B—S12B	3.423 (7)	Ag12A—Sb8B^iv	3.629 (3)
Pb3B—S13B	3.155 (7)	Ag12A—Sb10A^xiii	3.711 (3)
Pb4A—Sb4A	1.522 (10)	Ag12A—Pb10A^xiii	3.711 (3)
Pb4A—Ag4B^i	3.643 (7)	Ag12A—S7A	2.517 (9)
Pb4A—Cu4B^i	2.25 (4)	Ag12A—S7B	2.508 (8)
Pb4A—Ag4B'^i	3.07 (6)	Ag12A—S11A^iii	2.424 (7)
Pb4A—Sb8A^iii	3.481 (2)	Ag12A—S13B^xiii	2.439 (7)
Pb4A—Sb9A^iii	3.513 (2)	Ag12B—Sb8A^iv	3.651 (3)
Pb4A—S4A	2.763 (7)	Ag12B—Sb10A^xiii	3.743 (3)
Pb4A—S4B^i	2.790 (7)	Ag12B—Pb10A^xiii	3.743 (3)
Pb4A—S7A	2.576 (9)	Ag12B—Pb10B^xiv	3.800 (3)
Pb4A—S8A	3.061 (6)	Ag12B—S7A^ii	2.635 (9)
Pb4A—S12A^iii	3.434 (6)	Ag12B—S7B	2.647 (8)
Pb4A—S12B^iii	3.669 (7)	Ag12B—S11B^iv	2.529 (6)
Sb4A—Ag4B	3.099 (12)	Ag12B—S13A^xiii	2.547 (6)
Sb4A—Ag4B'	3.69 (6)	S1A—Sb5B^i	4.843 (6)
Sb4A—Sb8A^iii	3.609 (9)	S1A—Pb5B^i	4.843 (6)
Sb4A—Sb9A^iii	3.670 (10)	S1B—Pb1A^ii	3.210 (6)
Sb4A—Sb11A	3.564 (10)	S1B—Pb2A^ii	3.008 (6)
Sb4A—S4A	2.392 (11)	S1B—Sb5A^ii	4.748 (6)
Sb4A—S7A	3.094 (13)	S1B—Pb5A^ii	4.748 (6)
Sb4A—S7B	3.359 (13)	S2A—Sb8B^i	4.730 (7)
Sb4A—S8A	3.571 (11)	S2B—Pb1A^ii	4.866 (6)
Sb4A—S12A^iii	2.454 (11)	S2B—Pb2A^ii	3.123 (6)
Ag4B—Pb4A^ii	3.643 (7)	S2B—Pb3A^ii	3.052 (6)
Ag4B—Cu4B	1.48 (4)	S2B—Ag4B'^x	5.40 (5)
Ag4B—Ag4B'	0.79 (5)	S2B—Sb8A^ii	4.768 (6)
Ag4B—Sb8B^iv	3.463 (4)	S3A—Pb1A^ii	3.102 (6)
Ag4B—Sb9B^iv	3.274 (4)	S3A—Pb3A^ii	3.089 (6)
Ag4B—Pb11B	3.54 (7)	S3A—Sb10A^ii	4.802 (6)
Ag4B—S4A	3.290 (10)	S3A—Pb10A^ii	4.802 (6)
Ag4B—S4B	2.537 (8)	S3B—Sb10B^i	4.677 (6)
Ag4B—S7B	2.613 (9)	S3B—Pb10B^i	4.677 (6)
Ag4B—S8B	2.841 (8)	S4B—Pb1A^ii	2.955 (7)
Ag4B—S12B^iv	2.761 (9)	S4B—Pb4A^ii	2.790 (7)
Cu4B—Pb4A^ii	2.25 (4)	S4B—Sb4A^ii	4.184 (12)
Cu4B—Sb4A^ii	3.69 (4)	S5A—Pb6B^i	4.796 (6)
Cu4B—Ag4B'	0.88 (5)	S5A—Sb6B^i	4.796 (6)
Cu4B—Sb8A^iv	3.67 (3)	S5A—Sb9B^viii	4.747 (6)
Cu4B—Sb8B^iv	3.68 (3)	S5B—Pb2A^ii	2.952 (6)
Cu4B—Sb9B^iv	3.75 (3)	S5B—Sb6A^ii	4.839 (6)
Cu4B—Sb11B	3.74 (3)	S5B—Pb6A^ii	4.839 (6)
Cu4B—Pb11B	3.54 (7)	S5B—Pb7A^ii	2.985 (6)
Cu4B—Ag12B	3.50 (3)	S5B—Sb9A^vii	4.643 (6)
Cu4B—S4B	2.34 (3)	S6A—Pb6B^xi	4.978 (5)
Cu4B—S12B^iv	2.26 (3)	S6A—Sb6B^xi	4.978 (5)
Ag4B'—Pb4A^ii	3.07 (6)	S6A—Pb7A^xii	2.994 (6)
Ag4B'—Sb8B^iv	3.26 (5)	S6A—Pb7B^xi	3.026 (6)
Ag4B'—Sb9B^iv	3.63 (5)	S6A—Sb9B^i	4.728 (6)
Ag4B'—Sb11B	3.60 (5)	S6B—Pb3A^ii	3.057 (6)
Ag4B'—Pb11B	3.28 (8)	S6B—Sb6A^xii	5.125 (6)
Ag4B'—Ag12B	3.34 (5)	S6B—Pb6A^xii	5.125 (6)
Ag4B'—S4B	2.45 (5)	S6B—Pb7A^xii	2.977 (6)
Ag4B'—S7B	2.49 (5)	S6B—Pb7B^xii	3.010 (6)
Ag4B'—S8B	3.49 (5)	S6B—Sb9A^ii	4.835 (6)
Ag4B'—S12B^iv	2.49 (5)	S7A—Ag4B'^i	3.83 (5)
Sb5A—Sb6A^v	3.950 (2)	S7A—Sb8A^iii	3.607 (8)
Sb5A—Sb6A	3.859 (2)	S7A—Sb10B^xiii	3.492 (9)
Sb5A—Pb6A^v	3.950 (2)	S7A—Pb10B^xiii	3.492 (9)
Sb5A—Pb6B^v	4.009 (2)	S7A—Sb11B^i	2.999 (8)
Sb5A—Sb6B^v	4.009 (2)	S7A—Pb11B^i	3.23 (7)
Sb5A—S1A	2.419 (6)	S7A—Ag12B^i	2.635 (9)
Sb5A—S8A	2.692 (7)	S7B—Sb8B^iv	3.404 (7)
Sb5A—S8B	2.750 (7)	S7B—Sb10A^xiii	3.684 (8)
Sb5A—S9A	2.846 (7)	S7B—Pb10A^xiii	3.684 (8)
Sb5A—S9B	2.894 (6)	S8A—Ag4B^i	4.507 (8)
Sb5A—S10B^v	3.552 (6)	S8A—Ag4B'^i	4.46 (5)
Sb5B—Sb6A^v	4.094 (2)	S8A—Sb5B^i	2.501 (7)
Sb5B—Pb6A^v	4.094 (2)	S8A—Pb5B^i	2.501 (7)
Sb5B—Pb6B^vi	3.8783 (19)	S8A—Pb6B^v	4.107 (6)
Sb5B—Sb6B^vi	3.8783 (19)	S8A—Sb6B^v	4.107 (6)
Sb5B—S1B	2.441 (6)	S8A—Sb9A^iii	3.275 (6)
Sb5B—S8A^ii	2.501 (7)	S8B—Sb6A^v	4.360 (6)
Sb5B—S8B	2.474 (7)	S8B—Pb6A^v	4.360 (6)
Sb5B—S9A^ii	3.292 (7)	S8B—Sb9A^iv	5.024 (7)
Sb5B—S9B	3.231 (7)	S8B—Sb9B^iv	3.413 (6)
Sb5B—S10A^v	3.446 (6)	S9A—Sb5B^i	3.292 (7)
Sb6A—Sb5A^v	3.950 (2)	S9A—Sb5B^v	4.562 (7)
Sb6A—Pb5A^v	3.950 (2)	S9A—Pb5B^i	3.292 (7)
Sb6A—Pb6B^i	4.094 (2)	S9A—Pb6B^i	2.961 (7)
Sb6A—Sb6B^i	4.094 (2)	S9A—Pb6B^v	3.498 (6)
Sb6A—S5A	2.466 (6)	S9A—Sb6B^i	2.961 (7)
Sb6A—S9A	2.471 (7)	S9A—Sb6B^v	3.498 (6)
Sb6A—S9B^v	3.458 (6)	S9B—Pb5A^v	4.431 (6)
Sb6A—S9B	2.480 (7)	S9B—Sb6A^v	3.458 (6)
Sb6A—S10A	3.274 (7)	S9B—Pb6A^v	3.458 (6)
Sb6A—S10B	3.276 (6)	S10A—Ag4B^v	4.812 (8)
Pb6B—Sb5A^v	4.009 (2)	S10A—Ag4B'^v	5.00 (5)
Pb6B—Pb5A^v	4.009 (2)	S10A—Sb5B^v	3.446 (6)
Pb6B—Sb5B^vi	3.8783 (19)	S10A—Pb5B^v	3.446 (6)
Pb6B—Pb5B^vi	3.8783 (19)	S10A—Pb6B^i	2.903 (6)
Pb6B—Pb6A^ii	4.094 (2)	S10A—Sb6B^i	2.903 (6)
Pb6B—Sb9A^vii	3.8788 (18)	S10A—Pb7B^i	4.828 (6)
Pb6B—S5B	2.641 (6)	S10A—Sb9A^viii	2.511 (7)
Pb6B—S9A^ii	2.961 (7)	S10A—Sb9B^viii	3.009 (6)
Pb6B—S9A^v	3.498 (6)	S10B—Pb4A^v	5.050 (6)
Pb6B—S9B	2.895 (6)	S10B—Sb4A^v	4.612 (11)
Pb6B—S10A^ii	2.903 (6)	S10B—Sb5A^v	3.552 (6)
Pb6B—S10B	2.845 (7)	S10B—Pb5A^v	3.552 (6)
Pb7A—Pb7B^i	4.0415 (15)	S10B—Pb7A^ii	4.769 (6)
Pb7A—Pb7B	4.1470 (15)	S10B—Sb9A^vii	2.527 (6)
Pb7A—Sb9A^viii	3.9853 (18)	S10B—Sb9B^viii	3.067 (7)
Pb7A—Sb9B^viii	4.1671 (18)	S11A—Pb4A^ix	4.789 (6)
Pb7A—Ag12A^ix	3.712 (3)	S11A—Sb4A^ix	4.277 (10)
Pb7A—S5A	2.980 (6)	S11A—Sb8B^i	2.786 (7)
Pb7A—S5B^i	2.985 (6)	S11A—Ag12A^ix	2.424 (7)
Pb7A—S6A^viii	2.994 (6)	S11A—Ag12B^x	4.642 (8)
Pb7A—S6B^viii	2.977 (6)	S11A—Ag12B^ix	5.002 (7)
Pb7A—S10A	2.845 (6)	S11B—Pb4A^ix	4.978 (6)
Pb7A—S11A	3.164 (6)	S11B—Ag4B^x	4.830 (8)
Pb7A—S13B^viii	3.168 (6)	S11B—Ag4B'^x	4.19 (5)
Pb7B—Pb7A^ii	4.0414 (15)	S11B—Ag12A^ix	4.723 (7)
Pb7B—Sb9A^vii	4.0172 (18)	S11B—Ag12A^x	4.760 (7)
Pb7B—Sb9B^viii	4.1669 (19)	S11B—Ag12B^x	2.529 (6)
Pb7B—Ag12B^x	3.885 (2)	S12A—Pb3B^i	5.062 (6)
Pb7B—S5A	2.938 (6)	S12A—Pb4A^ix	3.434 (6)
Pb7B—S5B	2.981 (6)	S12A—Sb4A^ix	2.454 (11)
Pb7B—S6A^vii	3.026 (6)	S12A—Ag4B^ix	3.700 (8)
Pb7B—S6B^viii	3.010 (7)	S12A—Ag4B'^ix	4.06 (5)
Pb7B—S10B	2.824 (6)	S12A—Pb7B^xi	4.997 (6)
Pb7B—S11B	3.133 (6)	S12A—Sb8B^i	2.686 (7)
Pb7B—S13A^vii	3.307 (6)	S12A—Sb9B^i	2.559 (6)
Sb8A—Pb4A^ix	3.481 (2)	S12A—Ag12A^ix	4.603 (7)
Sb8A—Sb4A^ix	3.609 (9)	S12B—Pb4A^ix	3.669 (7)
Sb8A—Cu4B^x	3.67 (3)	S12B—Sb4A^ix	4.620 (12)
Sb8A—Sb8B^i	4.057 (3)	S12B—Sb4A^x	4.710 (12)
Sb8A—Ag12A^ix	3.721 (3)	S12B—Ag4B^x	2.761 (9)
Sb8A—Ag12B^x	3.651 (3)	S12B—Cu4B^x	2.26 (3)
Sb8A—S2A	2.432 (6)	S12B—Ag4B'^x	2.49 (5)
Sb8A—S7A^ix	3.608 (8)	S12B—Ag12B^x	4.540 (7)
Sb8A—S11A	2.475 (7)	S13A—Pb7B^xi	3.307 (6)
Sb8A—S11B	2.460 (6)	S13A—Sb10B^i	2.672 (7)
Sb8A—S12A	3.202 (6)	S13A—Pb10B^i	2.672 (7)
Sb8A—S12B	3.244 (7)	S13A—Sb11B^xiii	4.568 (6)
Sb8B—Sb4A^x	3.799 (9)	S13A—Pb11B^xiii	4.47 (5)
Sb8B—Ag4B^x	3.463 (4)	S13A—Ag12A^xv	4.915 (7)
Sb8B—Cu4B^x	3.68 (3)	S13A—Ag12A^xiii	4.684 (7)
Sb8B—Ag4B'^x	3.26 (5)	S13A—Ag12B^xiii	2.547 (6)
Sb8B—Sb9B	3.834 (2)	S13B—Pb7A^xii	3.168 (6)
Sb8B—Ag12A^x	3.629 (3)	S13B—Pb7B^xi	5.038 (7)
Sb8B—S2B	2.435 (6)	S13B—Sb11A^xiii	4.376 (7)
Sb8B—S7B^x	3.404 (7)	S13B—Pb11A^xiii	4.376 (7)
Sb8B—S11A^ii	2.785 (7)	S13B—Ag12A^xiii	2.439 (7)
Sb8B—S11B	2.874 (7)	S13B—Ag12B^xiii	4.645 (8)
Sb8B—S12A^ii	2.686 (7)	S13B—Ag12B^xiv	4.936 (7)
Sb8B—S12B	2.760 (7)	S14A—Sb11A^xiii	3.666 (7)
Sb9A—Pb4A^ix	3.512 (2)	S14A—Pb11A^xiii	3.666 (7)
Sb9A—Sb4A^ix	3.670 (10)	S14B—Sb10B^i	2.647 (6)
Sb9A—Cu4B^x	3.81 (4)	S14B—Pb10B^i	2.647 (6)
Sb9A—Pb6B^xi	3.8787 (18)	S14B—Sb11B^i	2.509 (7)
Sb9A—Sb6B^xi	3.8787 (18)	S14B—Sb11B^xiii	3.394 (7)
Sb9A—Pb7A^xii	3.9853 (18)	S14B—Pb11B^xiii	3.56 (6)
Sb9A—S6A	2.451 (6)	S14B—Pb11B^i	3.04 (8)
Pb1B^i—Pb1A—Pb1B	178.31 (4)	S14B^ii—Sb11B—Sb10B	43.99 (15)
Pb1B—Pb1A—Sb11B^i	118.20 (6)	S14B^xiii—Sb11B—Sb10B	82.20 (11)
Pb1B^i—Pb1A—Sb11B^i	61.59 (5)	S14B^ii—Sb11B—Ag12B	137.6 (2)
Pb4A—Pb1A—Pb1B	88.67 (4)	S14B^xiii—Sb11B—Ag12B	87.66 (11)
Pb4A—Pb1A—Pb1B^i	89.87 (4)	S14B^ii—Sb11B—S7A^ii	92.3 (2)
Pb4A—Pb1A—Sb11B^i	57.83 (4)	S14B^ii—Sb11B—S7B	171.4 (2)
S1A—Pb1A—Pb1B^i	131.07 (12)	S14B^ii—Sb11B—S14A	94.4 (2)
S1A—Pb1A—Pb1B	48.68 (12)	S14B^ii—Sb11B—S14B^xiii	85.3 (2)
S1A—Pb1A—Pb4A	106.19 (11)	Ag4B—Pb11B—Cu4B	24.2 (7)
S1A—Pb1A—Sb11B^i	162.05 (11)	Ag4B'—Pb11B—Ag4B	12.6 (9)
S1A—Pb1A—S1B^i	82.24 (16)	Ag4B'—Pb11B—Cu4B	14.2 (10)
S1A—Pb1A—S3A^i	120.79 (15)	Ag4B'—Pb11B—Sb11A	81 (2)
S1A—Pb1A—S8A	72.18 (15)	Ag4B'—Pb11B—Ag12B	61.2 (13)
S1A—Pb1A—S14B	141.57 (17)	Sb11A—Pb11B—Ag4B	71.8 (16)
S1B^i—Pb1A—Pb1B	130.91 (11)	Sb11A—Pb11B—Cu4B	95 (2)
S1B^i—Pb1A—Pb1B^i	48.85 (11)	Sb11B—Pb11B—Ag4B	127 (6)
S1B^i—Pb1A—Pb4A	107.12 (10)	Sb11B—Pb11B—Cu4B	106 (6)
S1B^i—Pb1A—Sb11B^i	109.24 (12)	Sb11B—Pb11B—Ag4B'	120 (7)
S3A^i—Pb1A—Pb1B^i	49.03 (11)	Sb11B—Pb11B—Sb11A	157 (7)
S3A^i—Pb1A—Pb1B	132.67 (12)	Sb11B—Pb11B—Ag12B	105 (6)
S3A^i—Pb1A—Pb4A	130.83 (11)	Sb11B—Pb11B—S4B	86 (6)
S3A^i—Pb1A—Sb11B^i	76.90 (11)	Sb11B—Pb11B—S7A^ii	62 (6)
S3A^i—Pb1A—S1B^i	68.55 (15)	Sb11B—Pb11B—S7B	155 (7)
S3A^i—Pb1A—S8A	132.23 (17)	Sb11B—Pb11B—S14A	104 (6)
S3A^i—Pb1A—S14B	71.74 (16)	Sb11B—Pb11B—S14B^ii	19 (5)
S3B—Pb1A—Pb1B^i	132.77 (11)	Ag12B—Pb11B—Ag4B	71.6 (12)
S3B—Pb1A—Pb1B	48.92 (11)	Ag12B—Pb11B—Cu4B	61.7 (11)
S3B—Pb1A—Pb4A	129.29 (11)	Ag12B—Pb11B—Sb11A	93.6 (19)
S3B—Pb1A—Sb11B^i	113.37 (12)	S4B—Pb11B—Ag4B	45.8 (11)
S3B—Pb1A—S1A	68.94 (15)	S4B—Pb11B—Cu4B	41.1 (10)
S3B—Pb1A—S1B^i	121.25 (15)	S4B—Pb11B—Ag4B'	48.0 (14)
S3B—Pb1A—S3A^i	83.75 (16)	S4B—Pb11B—Sb11A	104 (2)
S3B—Pb1A—S8A	137.45 (17)	S4B—Pb11B—Ag12B	101.3 (18)
S3B—Pb1A—S14B	77.51 (15)	S4B—Pb11B—S7A^ii	79.3 (17)
S4A—Pb1A—Pb1B	46.57 (13)	S4B—Pb11B—S7B	93 (2)
S4A—Pb1A—Pb1B^i	132.20 (13)	S4B—Pb11B—S14B^ii	80.0 (19)
S4A—Pb1A—Pb4A	43.79 (13)	S7A^ii—Pb11B—Ag4B	84.4 (13)
S4A—Pb1A—Sb11B^i	79.83 (13)	S7A^ii—Pb11B—Cu4B	61.1 (12)
S4A—Pb1A—S1A	82.60 (17)	S7A^ii—Pb11B—Ag4B'	72.2 (15)
S4A—Pb1A—S1B^i	140.04 (16)	S7A^ii—Pb11B—Sb11A	140 (2)
S4A—Pb1A—S3A^i	148.73 (17)	S7A^ii—Pb11B—Ag12B	47.8 (8)
S4A—Pb1A—S3B	86.63 (17)	S7B—Pb11B—Ag4B	47.0 (11)
S4A—Pb1A—S4B^i	84.89 (19)	S7B—Pb11B—Cu4B	60.2 (13)
S4A—Pb1A—S8A	71.72 (17)	S7B—Pb11B—Ag4B'	47.7 (14)
S4A—Pb1A—S14B	77.15 (17)	S7B—Pb11B—Sb11A	46.5 (13)
S4B^i—Pb1A—Pb1B^i	47.32 (13)	S7B—Pb11B—Ag12B	51.1 (10)
S4B^i—Pb1A—Pb1B	131.46 (13)	S7B—Pb11B—S7A^ii	93.9 (16)
S4B^i—Pb1A—Pb4A	44.30 (13)	S7B—Pb11B—S14B^ii	171 (2)
S4B^i—Pb1A—Sb11B^i	34.49 (13)	S14A—Pb11B—Ag4B	102 (2)
S4B^i—Pb1A—S1A	139.98 (16)	S14A—Pb11B—Cu4B	123 (2)
S4B^i—Pb1A—S1B^i	83.46 (17)	S14A—Pb11B—Ag4B'	115 (3)
S4B^i—Pb1A—S3A^i	87.60 (17)	S14A—Pb11B—Sb11A	54.8 (16)
S4B^i—Pb1A—S3B	147.81 (16)	S14A—Pb11B—Ag12B	147 (3)
S4B^i—Pb1A—S8A	67.79 (16)	S14A—Pb11B—S4B	95.4 (19)
S4B^i—Pb1A—S14B	70.33 (16)	S14A—Pb11B—S7A^ii	165 (3)
S8A—Pb1A—Pb1B^i	86.53 (13)	S14A—Pb11B—S7B	100 (3)
S8A—Pb1A—Pb1B	91.86 (13)	S14A—Pb11B—S14B^ii	86.2 (18)
S8A—Pb1A—Pb4A	49.02 (11)	S14B^ii—Pb11B—Ag4B	125.5 (18)
S8A—Pb1A—Sb11B^i	98.65 (12)	S14B^ii—Pb11B—Cu4B	111 (2)
S8A—Pb1A—S1B^i	68.47 (15)	S14B^ii—Pb11B—Ag4B'	124 (2)
S8A—Pb1A—S14B	129.16 (15)	S14B^ii—Pb11B—Sb11A	140.9 (19)
S14B—Pb1A—Pb1B	94.90 (12)	S14B^ii—Pb11B—Ag12B	124 (2)
S14B—Pb1A—Pb1B^i	85.71 (12)	S14B^ii—Pb11B—S7A^ii	79.0 (19)
S14B—Pb1A—Pb4A	80.80 (11)	Sb4A—Ag12A—Pb7A^iii	143.52 (16)
S14B—Pb1A—Sb11B^i	35.86 (12)	Sb4A—Ag12A—Sb8A^iii	58.25 (15)
S14B—Pb1A—S1B^i	132.82 (16)	Sb4A—Ag12A—Sb10A^xiii	125.05 (16)
Pb1A^ii—Pb1B—Pb1A	178.30 (4)	Sb4A—Ag12A—Pb10A^xiii	125.05 (16)
Pb1A^ii—Pb1B—Pb11B	67.9 (11)	Pb7A^iii—Ag12A—Sb8A^iii	88.62 (6)
Ag4B—Pb1B—Pb1A	97.87 (10)	Sb8B^iv—Ag12A—Sb4A	62.49 (15)
Ag4B—Pb1B—Pb1A^ii	83.63 (10)	Sb8B^iv—Ag12A—Pb7A^iii	92.22 (7)
Ag4B—Pb1B—Pb11B	52.2 (9)	Sb8B^iv—Ag12A—Sb8A^iii	66.99 (6)
Pb11B—Pb1B—Pb1A	112.4 (11)	Sb8B^iv—Ag12A—Sb10A^xiii	117.32 (9)
S1A—Pb1B—Pb1A	47.84 (11)	Sb8B^iv—Ag12A—Pb10A^xiii	117.32 (9)
S1A—Pb1B—Pb1A^ii	132.36 (11)	Sb10A^xiii—Ag12A—Pb7A^iii	89.09 (7)
S1A—Pb1B—Ag4B	110.71 (13)	Sb10A^xiii—Ag12A—Sb8A^iii	175.20 (10)
S1A—Pb1B—Pb11B	155.7 (12)	Pb10A^xiii—Ag12A—Pb7A^iii	89.09 (7)
S1A—Pb1B—S1B	81.61 (16)	Pb10A^xiii—Ag12A—Sb8A^iii	175.20 (10)
S1A—Pb1B—S3A	119.62 (15)	Pb10A^xiii—Ag12A—Sb10A^xiii	0.0
S1A—Pb1B—S3B	67.73 (15)	Sb11A—Ag12A—Sb4A	60.91 (15)
S1A—Pb1B—S14A	137.84 (17)	Sb11A—Ag12A—Pb7A^iii	155.56 (9)
S1B—Pb1B—Pb1A^ii	50.76 (11)	Sb11A—Ag12A—Sb8A^iii	113.41 (9)
S1B—Pb1B—Pb1A	129.44 (12)	Sb11A—Ag12A—Sb8B^iv	105.76 (9)
S1B—Pb1B—Ag4B	101.77 (13)	Sb11A—Ag12A—Sb10A^xiii	68.12 (7)
S1B—Pb1B—Pb11B	116.5 (11)	Sb11A—Ag12A—Pb10A^xiii	68.12 (7)
S1B—Pb1B—S14A	137.05 (18)	S7A—Ag12A—Sb4A	56.0 (3)
S3A—Pb1B—Pb1A	129.53 (12)	S7A—Ag12A—Pb7A^iii	128.6 (2)
S3A—Pb1B—Pb1A^ii	48.77 (11)	S7A—Ag12A—Sb8A^iii	67.5 (2)
S3A—Pb1B—Ag4B	126.14 (15)	S7A—Ag12A—Sb8B^iv	116.0 (2)
S3A—Pb1B—Pb11B	83.3 (11)	S7A—Ag12A—Sb10A^xiii	110.9 (2)
S3A—Pb1B—S1B	69.53 (15)	S7A—Ag12A—Pb10A^xiii	110.9 (2)
S3A—Pb1B—S14A	74.23 (17)	S7A—Ag12A—Sb11A	57.63 (19)
S3B—Pb1B—Pb1A	47.76 (11)	S7B—Ag12A—Sb4A	62.2 (2)
S3B—Pb1B—Pb1A^ii	130.54 (11)	S7B—Ag12A—Pb7A^iii	132.53 (19)
S3B—Pb1B—Ag4B	137.47 (14)	S7B—Ag12A—Sb8A^iii	115.0 (2)
S3B—Pb1B—Pb11B	111.6 (8)	S7B—Ag12A—Sb8B^iv	64.38 (18)
S3B—Pb1B—S1B	119.19 (15)	S7B—Ag12A—Sb10A^xiii	69.59 (19)
S3B—Pb1B—S3A	81.77 (16)	S7B—Ag12A—Pb10A^xiii	69.59 (19)
S3B—Pb1B—S14A	76.32 (16)	S7B—Ag12A—Sb11A	48.62 (17)
S4A—Pb1B—Pb1A	45.19 (13)	S7B—Ag12A—S7A	98.8 (3)
S4A—Pb1B—Pb1A^ii	136.02 (13)	S11A^iii—Ag12A—Sb4A	86.1 (2)
S4A—Pb1B—Ag4B	54.54 (16)	S11A^iii—Ag12A—Pb7A^iii	57.59 (15)
S4A—Pb1B—Pb11B	75.0 (12)	S11A^iii—Ag12A—Sb8A^iii	41.09 (17)
S4A—Pb1B—S1A	80.81 (17)	S11A^iii—Ag12A—Sb8B^iv	50.10 (17)
S4A—Pb1B—S1B	141.75 (16)	S11A^iii—Ag12A—Sb10A^xiii	139.47 (19)
S4A—Pb1B—S3A	147.87 (16)	S11A^iii—Ag12A—Pb10A^xiii	139.47 (19)
S4A—Pb1B—S3B	84.45 (17)	S11A^iii—Ag12A—Sb11A	146.77 (18)
S4A—Pb1B—S4B	89.82 (18)	S11A^iii—Ag12A—S7A	108.2 (3)
S4A—Pb1B—S8B	70.96 (17)	S11A^iii—Ag12A—S7B	114.5 (3)
S4A—Pb1B—S14A	74.35 (19)	S11A^iii—Ag12A—S13B^xiii	115.1 (2)
S4B—Pb1B—Pb1A^ii	46.21 (13)	S13B^xiii—Ag12A—Sb4A	157.8 (2)
S4B—Pb1B—Pb1A	135.00 (13)	S13B^xiii—Ag12A—Pb7A^iii	57.64 (15)
S4B—Pb1B—Ag4B	39.97 (16)	S13B^xiii—Ag12A—Sb8A^iii	134.31 (19)
S4B—Pb1B—Pb11B	36.5 (9)	S13B^xiii—Ag12A—Sb8B^iv	135.9 (2)
S4B—Pb1B—S1A	142.84 (16)	S13B^xiii—Ag12A—Sb10A^xiii	41.28 (16)
S4B—Pb1B—S1B	84.12 (16)	S13B^xiii—Ag12A—Pb10A^xiii	41.28 (16)
S4B—Pb1B—S3A	86.43 (17)	S13B^xiii—Ag12A—Sb11A	98.11 (16)
S4B—Pb1B—S3B	147.37 (16)	S13B^xiii—Ag12A—S7A	108.1 (3)
S4B—Pb1B—S8B	69.88 (17)	S13B^xiii—Ag12A—S7B	110.7 (3)
S4B—Pb1B—S14A	71.21 (16)	Cu4B—Ag12B—Sb8A^iv	61.7 (6)
S8B—Pb1B—Pb1A	91.37 (13)	Cu4B—Ag12B—Sb10A^xiii	124.6 (6)
S8B—Pb1B—Pb1A^ii	90.25 (13)	Cu4B—Ag12B—Pb10A^xiii	124.6 (6)
S8B—Pb1B—Ag4B	45.67 (13)	Cu4B—Ag12B—Pb10B^xiv	123.5 (6)
S8B—Pb1B—Pb11B	96.5 (8)	Ag4B'—Ag12B—Cu4B	14.5 (9)
S8B—Pb1B—S1A	73.07 (16)	Ag4B'—Ag12B—Sb8A^iv	72.9 (9)
S8B—Pb1B—S1B	71.50 (16)	Ag4B'—Ag12B—Sb10A^xiii	112.7 (9)
S8B—Pb1B—S3A	135.97 (17)	Ag4B'—Ag12B—Pb10A^xiii	112.7 (9)
S8B—Pb1B—S3B	136.40 (18)	Ag4B'—Ag12B—Pb10B^xiv	129.1 (8)
S8B—Pb1B—S14A	126.98 (17)	Ag4B'—Ag12B—Sb11B	63.8 (8)
S14A—Pb1B—Pb1A	91.54 (13)	Sb8A^iv—Ag12B—Sb10A^xiii	172.53 (8)
S14A—Pb1B—Pb1A^ii	87.89 (13)	Sb8A^iv—Ag12B—Pb10A^xiii	172.53 (8)
S14A—Pb1B—Ag4B	81.54 (14)	Sb8A^iv—Ag12B—Pb10B^xiv	116.16 (9)
S14A—Pb1B—Pb11B	35.4 (8)	Sb10A^xiii—Ag12B—Pb10B^xiv	64.71 (5)
Pb2B^i—Pb2A—Pb2B	179.30 (4)	Pb10A^xiii—Ag12B—Sb10A^xiii	0.0
Pb2B^i—Pb2A—Sb6A	119.21 (4)	Pb10A^xiii—Ag12B—Pb10B^xiv	64.71 (5)
Pb2B—Pb2A—Sb6A	61.23 (3)	Sb11B—Ag12B—Cu4B	64.8 (5)
S1A—Pb2A—Pb2B^i	132.30 (11)	Sb11B—Ag12B—Sb8A^iv	113.78 (8)
S1A—Pb2A—Pb2B	48.17 (11)	Sb11B—Ag12B—Sb10A^xiii	73.59 (6)
S1A—Pb2A—Sb6A	76.33 (11)	Sb11B—Ag12B—Pb10A^xiii	73.59 (6)
S1A—Pb2A—S2A	64.83 (15)	Sb11B—Ag12B—Pb10B^xiv	67.58 (7)
S1A—Pb2A—S2B^i	116.69 (16)	Pb11B—Ag12B—Cu4B	62.8 (11)
S1A—Pb2A—S11A	129.52 (17)	Pb11B—Ag12B—Ag4B'	59.4 (13)
S1B^i—Pb2A—Pb2B	132.94 (12)	Pb11B—Ag12B—Sb8A^iv	117.2 (11)
S1B^i—Pb2A—Pb2B^i	47.54 (11)	Pb11B—Ag12B—Sb10A^xiii	70.3 (11)
S1B^i—Pb2A—Sb6A	113.41 (11)	Pb11B—Ag12B—Pb10A^xiii	70.3 (11)
S1B^i—Pb2A—S1A	84.78 (16)	Pb11B—Ag12B—Pb10B^xiv	74.3 (13)
S1B^i—Pb2A—S2A	118.12 (15)	Pb11B—Ag12B—Sb11B	9.1 (14)
S1B^i—Pb2A—S2B^i	66.51 (15)	S7A^ii—Ag12B—Cu4B	66.6 (6)
S1B^i—Pb2A—S5A	148.53 (15)	S7A^ii—Ag12B—Ag4B'	78.8 (10)
S1B^i—Pb2A—S9A	77.92 (16)	S7A^ii—Ag12B—Sb8A^iv	67.84 (19)
S1B^i—Pb2A—S11A	136.36 (17)	S7A^ii—Ag12B—Sb10A^xiii	117.4 (2)
S2A—Pb2A—Pb2B^i	130.50 (12)	S7A^ii—Ag12B—Pb10A^xiii	117.4 (2)
S2A—Pb2A—Pb2B	48.98 (11)	S7A^ii—Ag12B—Pb10B^xiv	62.7 (2)
S2A—Pb2A—Sb6A	109.74 (12)	S7A^ii—Ag12B—Sb11B	56.85 (18)
S2B^i—Pb2A—Pb2B	129.61 (12)	S7A^ii—Ag12B—Pb11B	65.0 (14)
S2B^i—Pb2A—Pb2B^i	49.86 (12)	S7A^ii—Ag12B—S7B	112.5 (2)
S2B^i—Pb2A—Sb6A	166.46 (12)	S7B—Ag12B—Cu4B	61.6 (6)
S2B^i—Pb2A—S2A	80.64 (16)	S7B—Ag12B—Ag4B'	47.4 (10)
S2B^i—Pb2A—S11A	73.15 (16)	S7B—Ag12B—Sb8A^iv	115.84 (19)
S5A—Pb2A—Pb2B^i	131.77 (12)	S7B—Ag12B—Sb10A^xiii	67.93 (18)
S5A—Pb2A—Pb2B	48.21 (12)	S7B—Ag12B—Pb10A^xiii	67.93 (18)
S5A—Pb2A—Sb6A	35.33 (10)	S7B—Ag12B—Pb10B^xiv	118.71 (18)
S5A—Pb2A—S1A	88.27 (15)	S7B—Ag12B—Sb11B	63.39 (17)
S5A—Pb2A—S2A	85.88 (16)	S7B—Ag12B—Pb11B	54.4 (15)
S5A—Pb2A—S2B^i	142.13 (15)	S11B^iv—Ag12B—Cu4B	86.8 (5)
S5A—Pb2A—S9A	70.70 (16)	S11B^iv—Ag12B—Ag4B'	90.0 (8)
S5A—Pb2A—S11A	68.98 (16)	S11B^iv—Ag12B—Sb8A^iv	42.24 (15)
S5B^i—Pb2A—Pb2B^i	46.27 (12)	S11B^iv—Ag12B—Sb10A^xiii	131.15 (16)
S5B^i—Pb2A—Pb2B	133.68 (12)	S11B^iv—Ag12B—Pb10A^xiii	131.15 (16)
S5B^i—Pb2A—Sb6A	82.90 (12)	S11B^iv—Ag12B—Pb10B^xiv	131.90 (18)
S5B^i—Pb2A—S1A	151.89 (15)	S11B^iv—Ag12B—Sb11B	151.19 (16)
S5B^i—Pb2A—S1B^i	86.35 (17)	S11B^iv—Ag12B—Pb11B	149.2 (10)
S5B^i—Pb2A—S2A	141.61 (15)	S11B^iv—Ag12B—S7A^ii	108.9 (3)
S5B^i—Pb2A—S2B^i	83.60 (16)	S11B^iv—Ag12B—S7B	108.3 (2)
S5B^i—Pb2A—S5A	85.52 (17)	S11B^iv—Ag12B—S13A^xiii	111.0 (2)
S5B^i—Pb2A—S9A	79.18 (17)	S13A^xiii—Ag12B—Cu4B	162.2 (5)
S5B^i—Pb2A—S11A	73.02 (17)	S13A^xiii—Ag12B—Ag4B'	154.4 (9)
S9A—Pb2A—Pb2B	85.94 (14)	S13A^xiii—Ag12B—Sb8A^iv	132.57 (17)
S9A—Pb2A—Pb2B^i	94.70 (14)	S13A^xiii—Ag12B—Sb10A^xiii	42.27 (15)
S9A—Pb2A—Sb6A	35.50 (12)	S13A^xiii—Ag12B—Pb10A^xiii	42.27 (15)
S9A—Pb2A—S1A	72.89 (17)	S13A^xiii—Ag12B—Pb10B^xiv	44.57 (15)
S9A—Pb2A—S2A	131.97 (18)	S13A^xiii—Ag12B—Sb11B	97.55 (15)
S9A—Pb2A—S2B^i	141.26 (17)	S13A^xiii—Ag12B—Pb11B	99.4 (10)
S9A—Pb2A—S11A	132.12 (16)	S13A^xiii—Ag12B—S7A^ii	106.5 (3)
S11A—Pb2A—Pb2B^i	93.32 (14)	S13A^xiii—Ag12B—S7B	109.7 (2)
S11A—Pb2A—Pb2B	86.04 (13)	Pb1A—S1A—Pb1B	83.48 (15)
S11A—Pb2A—Sb6A	101.91 (12)	Pb1A—S1A—Pb2A	90.87 (16)
S11A—Pb2A—S2A	68.97 (16)	Pb1A—S1A—Pb2B	153.4 (2)
Pb2A^ii—Pb2B—Pb2A	179.30 (4)	Pb1A—S1A—Sb5B	130.36 (16)
Pb2A^ii—Pb2B—Pb7B	90.53 (3)	Pb1A—S1A—Sb5B^i	61.06 (10)
Pb2A—Pb2B—Pb7B	89.68 (3)	Pb1A—S1A—Pb5B^i	61.06 (10)
Pb2A—Pb2B—Sb8A	61.51 (3)	Pb1A—S1A—Sb6A	135.48 (18)
Pb2A^ii—Pb2B—Sb8A	119.19 (4)	Pb1B—S1A—Pb2A	155.2 (2)
Pb7B—Pb2B—Sb8A	75.22 (3)	Pb1B—S1A—Pb2B	90.74 (16)
S1A—Pb2B—Pb2A^ii	131.27 (12)	Pb1B—S1A—Sb5B	60.07 (10)
S1A—Pb2B—Pb2A	48.26 (11)	Pb1B—S1A—Sb5B^i	130.69 (15)
S1A—Pb2B—Pb7B	132.22 (12)	Pb1B—S1A—Pb5B^i	130.69 (15)
S1A—Pb2B—Sb8A	96.86 (11)	Pb1B—S1A—Sb6A	134.95 (17)
S1A—Pb2B—S2A	65.61 (14)	Pb2A—S1A—Sb5B^i	64.38 (11)
S1A—Pb2B—S2B	116.90 (16)	Pb2A—S1A—Sb5B	136.07 (16)
S1A—Pb2B—S9B	73.03 (15)	Pb2A—S1A—Pb5B^i	64.38 (11)
S1A—Pb2B—S11B	131.30 (16)	Pb2A—S1A—Sb6A	62.72 (10)
S1B—Pb2B—Pb2A	131.76 (12)	Pb2B—S1A—Pb2A	83.58 (14)
S1B—Pb2B—Pb2A^ii	47.75 (11)	Pb2B—S1A—Sb5B	65.66 (11)
S1B—Pb2B—Pb7B	131.82 (12)	Pb2B—S1A—Sb5B^i	136.03 (17)
S1B—Pb2B—Sb8A	140.59 (12)	Pb2B—S1A—Pb5B^i	136.03 (17)
S1B—Pb2B—S1A	83.53 (16)	Pb2B—S1A—Sb6A	63.50 (10)
S1B—Pb2B—S2A	117.39 (15)	Sb5A—S1A—Pb1A	101.59 (19)
S1B—Pb2B—S2B	66.45 (15)	Sb5A—S1A—Pb1B	101.02 (19)
S1B—Pb2B—S5A	147.75 (15)	Sb5A—S1A—Pb2A	103.8 (2)
S1B—Pb2B—S9B	77.75 (16)	Sb5A—S1A—Pb2B	105.0 (2)
S1B—Pb2B—S11B	136.26 (18)	Sb5A—S1A—Sb5B^i	59.01 (13)
S2A—Pb2B—Pb2A^ii	130.27 (12)	Sb5A—S1A—Sb5B	59.10 (13)
S2A—Pb2B—Pb2A	50.25 (12)	Sb5A—S1A—Pb5B^i	59.01 (13)
S2A—Pb2B—Pb7B	107.89 (10)	Sb5A—S1A—Sb6A	56.79 (12)
S2A—Pb2B—Sb8A	35.05 (10)	Sb5B—S1A—Sb5B^i	117.99 (12)
S2B—Pb2B—Pb2A^ii	49.57 (11)	Sb5B—S1A—Pb5B^i	118.0
S2B—Pb2B—Pb2A	130.96 (12)	Pb5B^i—S1A—Sb5B^i	0.0
S2B—Pb2B—Pb7B	107.73 (11)	Sb6A—S1A—Sb5B^i	74.91 (10)
S2B—Pb2B—Sb8A	78.78 (11)	Sb6A—S1A—Sb5B	75.36 (9)
S2B—Pb2B—S2A	80.71 (17)	Sb6A—S1A—Pb5B^i	74.91 (10)
S2B—Pb2B—S9B	140.49 (17)	Pb1A^ii—S1B—Sb5A	130.78 (15)
S2B—Pb2B—S11B	73.19 (16)	Pb1A^ii—S1B—Sb5A^ii	61.27 (10)
S5A—Pb2B—Pb2A^ii	132.39 (12)	Pb1A^ii—S1B—Pb5A^ii	61.27 (10)
S5A—Pb2B—Pb2A	47.61 (11)	Pb1A^ii—S1B—Pb6B	136.18 (16)
S5A—Pb2B—Pb7B	44.67 (11)	Pb1B—S1B—Pb1A^ii	80.39 (14)
S5A—Pb2B—Sb8A	71.25 (11)	Pb1B—S1B—Sb5A	62.10 (10)
S5A—Pb2B—S1A	87.82 (16)	Pb1B—S1B—Sb5A^ii	128.81 (15)
S5A—Pb2B—S2A	86.44 (16)	Pb1B—S1B—Pb5A^ii	128.81 (15)
S5A—Pb2B—S2B	143.29 (15)	Pb1B—S1B—Pb6B	137.10 (18)
S5A—Pb2B—S9B	70.01 (16)	Pb2A^ii—S1B—Pb1A^ii	89.92 (16)
S5A—Pb2B—S11B	70.11 (16)	Pb2A^ii—S1B—Pb1B	153.3 (2)
S5B—Pb2B—Pb2A	133.29 (12)	Pb2A^ii—S1B—Sb5A	137.25 (18)
S5B—Pb2B—Pb2A^ii	46.75 (12)	Pb2A^ii—S1B—Sb5A^ii	64.08 (11)
S5B—Pb2B—Pb7B	45.57 (12)	Pb2A^ii—S1B—Pb5A^ii	64.08 (11)
S5B—Pb2B—Sb8A	107.80 (11)	Pb2A^ii—S1B—Pb6B	64.39 (11)
S5B—Pb2B—S1A	150.85 (15)	Pb2B—S1B—Pb1A^ii	152.3 (2)
S5B—Pb2B—S1B	86.94 (16)	Pb2B—S1B—Pb1B	92.38 (16)
S5B—Pb2B—S2A	141.96 (15)	Pb2B—S1B—Pb2A^ii	84.71 (14)
S5B—Pb2B—S2B	83.73 (17)	Pb2B—S1B—Sb5A	64.91 (11)
S5B—Pb2B—S5A	85.70 (17)	Pb2B—S1B—Sb5A^ii	136.98 (17)
S5B—Pb2B—S9B	78.05 (16)	Pb2B—S1B—Pb5A^ii	136.98 (17)
S5B—Pb2B—S11B	72.29 (16)	Pb2B—S1B—Pb6B	64.31 (11)
S9B—Pb2B—Pb2A^ii	93.92 (13)	Sb5A—S1B—Sb5A^ii	119.39 (12)
S9B—Pb2B—Pb2A	85.44 (13)	Sb5A—S1B—Pb5A^ii	119.4
S9B—Pb2B—Pb7B	83.63 (11)	Pb5A^ii—S1B—Sb5A^ii	0.0
S9B—Pb2B—Sb8A	140.20 (13)	Sb5B—S1B—Pb1A^ii	98.14 (18)
S9B—Pb2B—S2A	132.86 (17)	Sb5B—S1B—Pb1B	95.75 (18)
S11B—Pb2B—Pb2A	87.75 (13)	Sb5B—S1B—Pb2A^ii	110.3 (2)
S11B—Pb2B—Pb2A^ii	92.89 (13)	Sb5B—S1B—Pb2B	109.2 (2)
S11B—Pb2B—Pb7B	48.17 (11)	Sb5B—S1B—Sb5A	58.57 (13)
S11B—Pb2B—Sb8A	35.55 (12)	Sb5B—S1B—Sb5A^ii	60.94 (13)
S11B—Pb2B—S2A	70.04 (15)	Sb5B—S1B—Pb5A^ii	60.94 (13)
S11B—Pb2B—S9B	131.34 (16)	Sb5B—S1B—Pb6B	63.09 (13)
Pb3B—Pb3A—Pb3B^i	176.61 (4)	Pb6B—S1B—Sb5A	75.21 (9)
Pb3B^i—Pb3A—Sb8B^i	63.59 (3)	Pb6B—S1B—Sb5A^ii	75.35 (9)
Pb3B—Pb3A—Sb8B^i	119.79 (4)	Pb6B—S1B—Pb5A^ii	75.35 (9)
Pb3B—Pb3A—Sb9B^i	119.74 (4)	Pb1A—S2A—Pb1B	49.91 (6)
Pb3B^i—Pb3A—Sb9B^i	62.01 (3)	Pb1A—S2A—Sb9A	121.52 (12)
Sb9B^i—Pb3A—Sb8B^i	53.92 (3)	Pb1B—S2A—Sb9A	121.92 (12)
S2A—Pb3A—Pb3B^i	134.25 (13)	Pb2A—S2A—Pb1A	62.35 (9)
S2A—Pb3A—Pb3B	48.26 (12)	Pb2A—S2A—Pb1B	94.60 (12)
S2A—Pb3A—Sb8B^i	79.64 (12)	Pb2A—S2A—Sb8B^i	62.45 (11)
S2A—Pb3A—Sb9B^i	116.94 (11)	Pb2A—S2A—Sb8B	131.00 (16)
S2A—Pb3A—S2B^i	85.35 (17)	Pb2A—S2A—Sb9A	135.76 (17)
S2A—Pb3A—S3A^i	119.55 (16)	Pb2B—S2A—Pb1A	94.84 (12)
S2A—Pb3A—S3B	65.95 (15)	Pb2B—S2A—Pb1B	62.31 (10)
S2A—Pb3A—S6A	86.93 (16)	Pb2B—S2A—Pb2A	80.77 (14)
S2A—Pb3A—S6B^i	152.06 (15)	Pb2B—S2A—Sb8B	62.57 (11)
S2A—Pb3A—S12A	79.82 (15)	Pb2B—S2A—Sb8B^i	130.09 (16)
S2A—Pb3A—S13A	131.07 (17)	Pb2B—S2A—Sb9A	136.11 (17)
S2B^i—Pb3A—Pb3B	133.59 (12)	Pb3A—S2A—Pb1A	62.88 (10)
S2B^i—Pb3A—Pb3B^i	48.92 (12)	Pb3A—S2A—Pb1B	97.26 (13)
S2B^i—Pb3A—Sb8B^i	34.49 (11)	Pb3A—S2A—Pb2A	91.77 (17)
S2B^i—Pb3A—Sb9B^i	78.40 (11)	Pb3A—S2A—Pb2B	157.2 (2)
S2B^i—Pb3A—S3A^i	65.96 (15)	Pb3A—S2A—Pb3B	84.53 (15)
S2B^i—Pb3A—S3B	119.02 (15)	Pb3A—S2A—Sb8B^i	61.62 (11)
S2B^i—Pb3A—S6B^i	88.49 (17)	Pb3A—S2A—Sb8B	133.88 (17)
S2B^i—Pb3A—S12A	73.82 (16)	Pb3A—S2A—Sb9A	61.95 (10)
S2B^i—Pb3A—S13A	133.80 (17)	Pb3B—S2A—Pb1A	94.80 (13)
S3A^i—Pb3A—Pb3B	130.46 (12)	Pb3B—S2A—Pb1B	62.05 (10)
S3A^i—Pb3A—Pb3B^i	47.09 (11)	Pb3B—S2A—Pb2A	155.50 (19)
S3A^i—Pb3A—Sb8B^i	97.90 (11)	Pb3B—S2A—Pb2B	93.37 (17)
S3A^i—Pb3A—Sb9B^i	108.03 (12)	Pb3B—S2A—Sb8B^i	133.66 (17)
S3A^i—Pb3A—S3B	82.82 (16)	Pb3B—S2A—Sb8B	63.34 (11)
S3A^i—Pb3A—S12A	132.41 (17)	Pb3B—S2A—Sb9A	62.41 (10)
S3A^i—Pb3A—S13A	70.61 (16)	Sb8A—S2A—Pb1A	154.3 (2)
S3B—Pb3A—Pb3B^i	129.88 (11)	Sb8A—S2A—Pb1B	153.9 (2)
S3B—Pb3A—Pb3B	47.66 (11)	Sb8A—S2A—Pb2A	96.98 (19)
S3B—Pb3A—Sb8B^i	139.95 (11)	Sb8A—S2A—Pb2B	96.57 (18)
S3B—Pb3A—Sb9B^i	162.47 (11)	Sb8A—S2A—Pb3A	105.7 (2)
S3B—Pb3A—S12A	141.03 (16)	Sb8A—S2A—Pb3B	107.3 (2)
S3B—Pb3A—S13A	68.69 (15)	Sb8A—S2A—Sb8B^i	59.05 (14)
S6A—Pb3A—Pb3B^i	132.31 (11)	Sb8A—S2A—Sb8B	59.36 (13)
S6A—Pb3A—Pb3B	47.28 (11)	Sb8A—S2A—Sb9A	61.70 (12)
S6A—Pb3A—Sb8B^i	115.63 (11)	Sb8B—S2A—Pb1A	145.52 (14)
S6A—Pb3A—Sb9B^i	79.51 (11)	Sb8B^i—S2A—Pb1A	96.29 (11)
S6A—Pb3A—S2B^i	150.09 (15)	Sb8B^i—S2A—Pb1B	146.17 (14)
S6A—Pb3A—S3A^i	141.13 (16)	Sb8B—S2A—Pb1B	95.61 (11)
S6A—Pb3A—S3B	83.47 (15)	Sb8B^i—S2A—Sb8B	118.15 (11)
S6A—Pb3A—S6B^i	84.95 (17)	Sb8B^i—S2A—Sb9A	73.54 (9)
S6A—Pb3A—S12A	76.39 (16)	Sb8B—S2A—Sb9A	73.68 (9)
S6A—Pb3A—S13A	70.53 (16)	Pb1A^ii—S2B—Pb1B	49.57 (6)
S6B^i—Pb3A—Pb3B^i	47.36 (12)	Pb1A^ii—S2B—Ag4B'^x	161.6 (6)
S6B^i—Pb3A—Pb3B	132.08 (13)	Pb1B—S2B—Ag4B'^x	139.1 (6)
S6B^i—Pb3A—Sb8B^i	79.91 (12)	Pb2A^ii—S2B—Pb1A^ii	62.34 (10)
S6B^i—Pb3A—Sb9B^i	35.19 (11)	Pb2A^ii—S2B—Pb1B	93.74 (12)
S6B^i—Pb3A—S3A^i	82.04 (16)	Pb2A^ii—S2B—Pb2B	80.56 (14)
S6B^i—Pb3A—S3B	139.04 (15)	Pb2A^ii—S2B—Ag4B'^x	122.8 (6)
S6B^i—Pb3A—S12A	72.28 (15)	Pb2A^ii—S2B—Sb8A^ii	61.40 (10)
S6B^i—Pb3A—S13A	70.39 (15)	Pb2A^ii—S2B—Sb8A	128.81 (17)
S12A—Pb3A—Pb3B^i	87.30 (12)	Pb2A^ii—S2B—Sb9B	136.26 (17)
S12A—Pb3A—Pb3B	95.64 (12)	Pb2B—S2B—Pb1A^ii	95.30 (13)
S12A—Pb3A—Sb8B^i	39.37 (12)	Pb2B—S2B—Pb1B	62.47 (10)
S12A—Pb3A—Sb9B^i	37.12 (11)	Pb2B—S2B—Ag4B'^x	102.9 (6)
S12A—Pb3A—S13A	131.47 (15)	Pb2B—S2B—Sb8A	60.67 (11)
S13A—Pb3A—Pb3B^i	89.56 (12)	Pb2B—S2B—Sb8A^ii	129.32 (17)
S13A—Pb3A—Pb3B	87.23 (12)	Pb2B—S2B—Sb9B	135.73 (18)
S13A—Pb3A—Sb8B^i	149.20 (12)	Pb3A^ii—S2B—Pb1A^ii	62.29 (10)
S13A—Pb3A—Sb9B^i	101.31 (11)	Pb3A^ii—S2B—Pb1B	96.05 (14)
Pb3A—Pb3B—Pb3A^ii	176.61 (4)	Pb3A^ii—S2B—Pb2A^ii	92.98 (17)
Pb3A^ii—Pb3B—Sb10A	120.41 (4)	Pb3A^ii—S2B—Pb2B	156.8 (2)
Pb3A—Pb3B—Sb10A	62.96 (3)	Pb3A^ii—S2B—Pb3B	83.53 (15)
S2A—Pb3B—Pb3A^ii	130.20 (12)	Pb3A^ii—S2B—Ag4B'^x	99.3 (6)
S2A—Pb3B—Pb3A	47.21 (12)	Pb3A^ii—S2B—Sb8A^ii	63.20 (11)
S2A—Pb3B—Sb10A	98.29 (11)	Pb3A^ii—S2B—Sb8A	135.32 (17)
S2A—Pb3B—S2B	82.67 (17)	Pb3A^ii—S2B—Sb9B	61.98 (10)
S2A—Pb3B—S12B	78.06 (15)	Pb3B—S2B—Pb1A^ii	94.33 (13)
S2A—Pb3B—S13B	132.44 (17)	Pb3B—S2B—Pb1B	61.90 (10)
S2B—Pb3B—Pb3A^ii	47.55 (12)	Pb3B—S2B—Pb2A^ii	154.7 (2)
S2B—Pb3B—Pb3A	129.86 (12)	Pb3B—S2B—Pb2B	92.80 (17)
S2B—Pb3B—Sb10A	141.41 (11)	Pb3B—S2B—Ag4B'^x	82.4 (6)
S2B—Pb3B—S12B	71.41 (15)	Pb3B—S2B—Sb8A^ii	135.49 (16)
S2B—Pb3B—S13B	138.33 (18)	Pb3B—S2B—Sb8A	65.13 (11)
S3A—Pb3B—Pb3A	133.93 (12)	Pb3B—S2B—Sb9B	63.03 (10)
S3A—Pb3B—Pb3A^ii	48.43 (11)	Sb8A^ii—S2B—Pb1A^ii	95.09 (11)
S3A—Pb3B—Sb10A	80.72 (12)	Sb8A—S2B—Pb1A^ii	145.58 (13)
S3A—Pb3B—S2A	119.23 (16)	Sb8A^ii—S2B—Pb1B	144.55 (14)
S3A—Pb3B—S2B	65.92 (16)	Sb8A—S2B—Pb1B	96.06 (11)
S3A—Pb3B—S3B	84.47 (16)	Sb8A^ii—S2B—Ag4B'^x	75.3 (6)
S3A—Pb3B—S6B	83.46 (16)	Sb8A—S2B—Ag4B'^x	48.0 (6)
S3A—Pb3B—S12B	130.14 (17)	Sb8A—S2B—Sb8A^ii	119.05 (12)
S3A—Pb3B—S13B	75.76 (17)	Sb8B—S2B—Pb1A^ii	153.3 (2)
S3B—Pb3B—Pb3A	49.49 (11)	Sb8B—S2B—Pb1B	157.1 (2)
S3B—Pb3B—Pb3A^ii	132.88 (11)	Sb8B—S2B—Pb2A^ii	101.3 (2)
S3B—Pb3B—Sb10A	35.23 (11)	Sb8B—S2B—Pb2B	102.8 (2)
S3B—Pb3B—S2A	66.42 (15)	Sb8B—S2B—Pb3A^ii	100.29 (19)
S3B—Pb3B—S2B	118.64 (15)	Sb8B—S2B—Pb3B	104.0 (2)
S3B—Pb3B—S12B	140.29 (16)	Sb8B—S2B—Ag4B'^x	21.6 (6)
S3B—Pb3B—S13B	71.19 (16)	Sb8B—S2B—Sb8A	61.02 (14)
S6A—Pb3B—Pb3A	47.59 (12)	Sb8B—S2B—Sb8A^ii	58.29 (13)
S6A—Pb3B—Pb3A^ii	132.64 (12)	Sb8B—S2B—Sb9B	54.64 (12)
S6A—Pb3B—Sb10A	71.85 (11)	Sb9B—S2B—Pb1A^ii	121.43 (13)
S6A—Pb3B—S2A	86.29 (16)	Sb9B—S2B—Pb1B	122.34 (13)
S6A—Pb3B—S2B	146.13 (15)	Sb9B—S2B—Ag4B'^x	41.4 (5)
S6A—Pb3B—S3A	145.17 (16)	Sb9B—S2B—Sb8A^ii	75.05 (9)
S6A—Pb3B—S3B	85.22 (16)	Sb9B—S2B—Sb8A	75.27 (9)
S6A—Pb3B—S6B	85.00 (17)	Pb1A^ii—S3A—Pb1B	82.20 (14)
S6A—Pb3B—S12B	75.01 (16)	Pb1A^ii—S3A—Sb10A^ii	64.42 (11)
S6A—Pb3B—S13B	69.42 (17)	Pb1A^ii—S3A—Sb10A	135.53 (16)
S6B—Pb3B—Pb3A^ii	47.78 (11)	Pb1A^ii—S3A—Pb10A^ii	64.42 (11)
S6B—Pb3B—Pb3A	132.60 (12)	Pb1A^ii—S3A—Sb11B	62.77 (10)
S6B—Pb3B—Sb10A	108.00 (11)	Pb1A^ii—S3A—Pb11B	66.0 (8)
S6B—Pb3B—S2A	148.05 (15)	Pb1B—S3A—Sb10A^ii	134.54 (16)
S6B—Pb3B—S2B	87.66 (16)	Pb1B—S3A—Sb10A	65.91 (11)
S6B—Pb3B—S3B	142.89 (15)	Pb1B—S3A—Pb10A^ii	134.54 (16)
S6B—Pb3B—S12B	70.00 (15)	Pb1B—S3A—Sb11B	63.00 (10)
S6B—Pb3B—S13B	71.85 (16)	Pb1B—S3A—Pb11B	57.0 (9)
S12B—Pb3B—Pb3A	93.30 (12)	Pb3A^ii—S3A—Pb1A^ii	90.06 (17)
S12B—Pb3B—Pb3A^ii	83.74 (12)	Pb3A^ii—S3A—Pb1B	152.3 (2)
S12B—Pb3B—Sb10A	146.83 (12)	Pb3A^ii—S3A—Sb10A^ii	61.84 (11)
S13B—Pb3B—Pb3A	88.61 (13)	Pb3A^ii—S3A—Sb10A	132.10 (16)
S13B—Pb3B—Pb3A^ii	94.54 (13)	Pb3A^ii—S3A—Pb10A^ii	61.84 (11)
S13B—Pb3B—Sb10A	36.16 (12)	Pb3A^ii—S3A—Sb11B	135.36 (18)
S13B—Pb3B—S12B	129.20 (16)	Pb3A^ii—S3A—Pb11B	141.9 (10)
Sb4A—Pb4A—Ag4B^i	164.2 (4)	Pb3B—S3A—Pb1A^ii	154.4 (2)
Sb4A—Pb4A—Cu4B^i	155.0 (9)	Pb3B—S3A—Pb1B	91.11 (17)
Sb4A—Pb4A—Ag4B'^i	160.1 (9)	Pb3B—S3A—Pb3A^ii	84.49 (14)
Sb4A—Pb4A—Sb8A^iii	82.4 (3)	Pb3B—S3A—Sb10A^ii	131.92 (16)
Sb4A—Pb4A—Sb9A^iii	83.6 (4)	Pb3B—S3A—Sb10A	60.30 (11)
Sb4A—Pb4A—S4A	59.8 (4)	Pb3B—S3A—Pb10A^ii	131.92 (16)
Sb4A—Pb4A—S4B^i	150.7 (4)	Pb3B—S3A—Sb11B	134.84 (18)
Sb4A—Pb4A—S7A	94.6 (4)	Pb3B—S3A—Pb11B	129.6 (10)
Sb4A—Pb4A—S8A	96.5 (4)	Sb10A—S3A—Sb10A^ii	118.11 (12)
Sb4A—Pb4A—S12A^iii	39.3 (4)	Sb10A—S3A—Pb10A^ii	118.1
Sb4A—Pb4A—S12B^iii	119.9 (4)	Sb10A—S3A—Pb11B	70.7 (9)
Ag4B^i—Pb4A—S12B^iii	44.37 (13)	Sb10A^ii—S3A—Pb11B	80.7 (10)
Cu4B^i—Pb4A—Ag4B^i	10.3 (8)	Pb10A^ii—S3A—Sb10A^ii	0.0
Cu4B^i—Pb4A—Ag4B'^i	7.3 (13)	Pb10A^ii—S3A—Pb11B	80.7 (10)
Cu4B^i—Pb4A—Sb8A^iii	76.3 (8)	Sb10B—S3A—Pb1A^ii	100.97 (19)
Cu4B^i—Pb4A—Sb9A^iii	79.4 (8)	Sb10B—S3A—Pb1B	104.33 (19)
Cu4B^i—Pb4A—S4A	144.9 (8)	Sb10B—S3A—Pb3A^ii	103.2 (2)
Cu4B^i—Pb4A—S4B^i	54.0 (8)	Sb10B—S3A—Pb3B	104.6 (2)
Cu4B^i—Pb4A—S7A	90.8 (9)	Sb10B—S3A—Sb10A^ii	57.11 (13)
Cu4B^i—Pb4A—S8A	90.4 (8)	Sb10B—S3A—Sb10A	61.25 (14)
Cu4B^i—Pb4A—S12A^iii	116.0 (8)	Sb10B—S3A—Pb10A^ii	57.11 (13)
Cu4B^i—Pb4A—S12B^iii	35.6 (8)	Sb10B—S3A—Sb11B	54.15 (11)
Ag4B'^i—Pb4A—Ag4B^i	9.4 (8)	Sb10B—S3A—Pb11B	56.9 (7)
Ag4B'^i—Pb4A—Sb8A^iii	78.7 (8)	Sb11B—S3A—Sb10A^ii	74.22 (10)
Ag4B'^i—Pb4A—Sb9A^iii	86.6 (9)	Sb11B—S3A—Sb10A	75.06 (10)
Ag4B'^i—Pb4A—S12A^iii	122.1 (9)	Sb11B—S3A—Pb10A^ii	74.22 (10)
Ag4B'^i—Pb4A—S12B^iii	42.2 (9)	Sb11B—S3A—Pb11B	6.5 (9)
Sb8A^iii—Pb4A—Ag4B^i	86.48 (8)	Pb1A—S3B—Pb1B	83.31 (14)
Sb8A^iii—Pb4A—Sb9A^iii	77.88 (5)	Pb1A—S3B—Pb3A	90.16 (16)
Sb8A^iii—Pb4A—S12B^iii	53.88 (11)	Pb1A—S3B—Sb10B	134.35 (16)
Sb9A^iii—Pb4A—Ag4B^i	83.12 (8)	Pb1A—S3B—Sb10B^i	63.23 (11)
Sb9A^iii—Pb4A—S12B^iii	51.64 (11)	Pb1A—S3B—Pb10B^i	63.23 (11)
S4A—Pb4A—Ag4B^i	134.77 (16)	Pb1A—S3B—Sb11A	64.03 (10)
S4A—Pb4A—Ag4B'^i	139.8 (9)	Pb1B—S3B—Pb3A	151.7 (2)
S4A—Pb4A—Sb8A^iii	135.15 (15)	Pb1B—S3B—Sb10B^i	133.78 (16)
S4A—Pb4A—Sb9A^iii	117.13 (14)	Pb1B—S3B—Sb10B	63.09 (11)
S4A—Pb4A—S4B^i	91.0 (2)	Pb1B—S3B—Pb10B^i	133.78 (16)
S4A—Pb4A—S8A	75.15 (18)	Pb1B—S3B—Sb11A	60.02 (9)
S4A—Pb4A—S12A^iii	97.82 (18)	Pb3A—S3B—Sb10B	133.86 (16)
S4A—Pb4A—S12B^iii	166.91 (18)	Pb3A—S3B—Sb10B^i	64.00 (11)
S4B^i—Pb4A—Ag4B^i	44.00 (15)	Pb3A—S3B—Pb10B^i	64.00 (11)
S4B^i—Pb4A—Ag4B'^i	49.2 (9)	Pb3A—S3B—Sb11A	139.60 (17)
S4B^i—Pb4A—Sb8A^iii	125.05 (15)	Pb3B—S3B—Pb1A	153.5 (2)
S4B^i—Pb4A—Sb9A^iii	110.17 (14)	Pb3B—S3B—Pb1B	90.82 (16)
S4B^i—Pb4A—S8A	71.15 (18)	Pb3B—S3B—Pb3A	82.85 (13)
S4B^i—Pb4A—S12A^iii	163.98 (18)	Pb3B—S3B—Sb10B^i	133.08 (16)
S4B^i—Pb4A—S12B^iii	87.80 (18)	Pb3B—S3B—Sb10B	62.07 (11)
S7A—Pb4A—Ag4B^i	92.4 (2)	Pb3B—S3B—Pb10B^i	133.08 (16)
S7A—Pb4A—Ag4B'^i	85.0 (9)	Pb3B—S3B—Sb11A	133.67 (17)
S7A—Pb4A—Sb8A^iii	71.34 (17)	Sb10A—S3B—Pb1A	107.7 (2)
S7A—Pb4A—Sb9A^iii	149.12 (17)	Sb10A—S3B—Pb1B	107.3 (2)
S7A—Pb4A—S4A	87.5 (2)	Sb10A—S3B—Pb3A	100.90 (19)
S7A—Pb4A—S4B^i	86.2 (2)	Sb10A—S3B—Pb3B	98.75 (19)
S7A—Pb4A—S8A	150.8 (2)	Sb10A—S3B—Sb10B	59.87 (13)
S7A—Pb4A—S12A^iii	107.5 (2)	Sb10A—S3B—Sb10B^i	59.65 (13)
S7A—Pb4A—S12B^iii	105.4 (2)	Sb10A—S3B—Pb10B^i	59.65 (13)
S8A—Pb4A—Ag4B^i	83.99 (16)	Sb10A—S3B—Sb11A	62.66 (12)
S8A—Pb4A—Ag4B'^i	93.2 (9)	Sb10B^i—S3B—Sb10B	119.28 (12)
S8A—Pb4A—Sb8A^iii	136.89 (12)	Sb10B—S3B—Sb11A	72.35 (9)
S8A—Pb4A—Sb9A^iii	59.29 (11)	Sb10B^i—S3B—Sb11A	76.37 (9)
S8A—Pb4A—S12A^iii	98.11 (16)	Pb10B^i—S3B—Sb10B^i	0.0
S8A—Pb4A—S12B^iii	92.15 (16)	Pb10B^i—S3B—Sb10B	119.3
S12A^iii—Pb4A—Ag4B^i	124.91 (14)	Pb10B^i—S3B—Sb11A	76.37 (9)
S12A^iii—Pb4A—Sb8A^iii	55.16 (10)	Pb1A—S4A—Pb1B	88.24 (17)
S12A^iii—Pb4A—Sb9A^iii	53.85 (11)	Pb1A—S4A—Ag4B	156.4 (2)
S12A^iii—Pb4A—S12B^iii	80.60 (15)	Pb1A—S4A—Ag4B'	162.2 (7)
Pb4A—Sb4A—Ag4B	159.1 (5)	Pb1A—S4A—Sb5A	70.42 (13)
Pb4A—Sb4A—Ag4B'	162.3 (9)	Pb1A—S4A—Pb11B	136.5 (8)
Pb4A—Sb4A—Sb8A^iii	72.9 (3)	Pb1A—S4A—Ag12A	132.8 (2)
Pb4A—Sb4A—Sb9A^iii	72.0 (4)	Pb1B—S4A—Ag4B	77.89 (18)
Pb4A—Sb4A—Sb11A	89.9 (4)	Pb1B—S4A—Ag4B'	78.3 (7)
Pb4A—Sb4A—S4A	86.8 (4)	Pb1B—S4A—Sb5A	70.25 (12)
Pb4A—Sb4A—S7A	56.1 (3)	Pb1B—S4A—Pb11B	64.1 (8)
Pb4A—Sb4A—S7B	126.5 (5)	Pb1B—S4A—Ag12A	131.3 (2)
Pb4A—Sb4A—S8A	58.4 (3)	Pb4A—S4A—Pb1A	89.4 (2)
Pb4A—Sb4A—S12A^iii	117.6 (5)	Pb4A—S4A—Pb1B	160.1 (2)
Ag4B—Sb4A—Ag4B'	9.0 (7)	Pb4A—S4A—Ag4B	97.2 (2)
Ag4B—Sb4A—Sb8A^iii	125.4 (3)	Pb4A—S4A—Ag4B'	99.3 (7)
Ag4B—Sb4A—Sb9A^iii	119.7 (3)	Pb4A—S4A—Sb5A	90.40 (16)
Ag4B—Sb4A—Sb11A	74.9 (2)	Pb4A—S4A—Pb11B	127.8 (8)
Ag4B—Sb4A—S7B	47.5 (2)	Pb4A—S4A—Ag12A	61.77 (12)
Ag4B—Sb4A—S8A	112.6 (3)	Sb4A—S4A—Pb1A	119.8 (4)
Sb8A^iii—Sb4A—Ag4B'	117.3 (7)	Sb4A—S4A—Pb1B	137.2 (4)
Sb8A^iii—Sb4A—Sb9A^iii	74.29 (18)	Sb4A—S4A—Pb4A	33.4 (3)
Sb9A^iii—Sb4A—Ag4B'	123.5 (8)	Sb4A—S4A—Ag4B	63.8 (3)
Sb11A—Sb4A—Ag4B'	73.2 (8)	Sb4A—S4A—Ag4B'	66.2 (8)
Sb11A—Sb4A—Sb8A^iii	110.0 (2)	Sb4A—S4A—Sb5A	88.4 (3)
Sb11A—Sb4A—Sb9A^iii	159.6 (3)	Sb4A—S4A—Sb11A	94.1 (3)
Sb11A—Sb4A—S8A	108.9 (2)	Sb4A—S4A—Pb11B	102.7 (8)
S4A—Sb4A—Ag4B	72.3 (3)	Sb4A—S4A—Ag12A	51.5 (2)
S4A—Sb4A—Ag4B'	77.4 (8)	Ag4B—S4A—Ag4B'	7.3 (7)
S4A—Sb4A—Sb8A^iii	148.0 (4)	Ag4B—S4A—Sb5A	86.87 (16)
S4A—Sb4A—Sb9A^iii	123.3 (3)	Ag4B—S4A—Pb11B	52.4 (8)
S4A—Sb4A—Sb11A	43.9 (2)	Ag4B—S4A—Ag12A	69.20 (14)
S4A—Sb4A—S7A	83.6 (3)	Ag4B'—S4A—Sb5A	93.9 (7)
S4A—Sb4A—S7B	73.3 (3)	Ag4B'—S4A—Pb11B	46.0 (10)
S4A—Sb4A—S8A	70.1 (3)	Ag4B'—S4A—Ag12A	64.7 (7)
S4A—Sb4A—S12A^iii	150.9 (5)	Sb5A—S4A—Pb11B	123.0 (8)
S7A—Sb4A—Ag4B	119.1 (4)	Sb5A—S4A—Ag12A	139.04 (15)
S7A—Sb4A—Ag4B'	113.4 (8)	Sb11A—S4A—Pb1A	113.5 (2)
S7A—Sb4A—Sb8A^iii	64.6 (2)	Sb11A—S4A—Pb1B	103.9 (2)
S7A—Sb4A—Sb9A^iii	120.3 (3)	Sb11A—S4A—Pb4A	95.1 (2)
S7A—Sb4A—Sb11A	50.9 (2)	Sb11A—S4A—Ag4B	88.6 (2)
S7A—Sb4A—S7B	72.4 (3)	Sb11A—S4A—Ag4B'	81.4 (7)
S7A—Sb4A—S8A	109.7 (3)	Sb11A—S4A—Sb5A	173.2 (3)
S7B—Sb4A—Ag4B'	41.0 (8)	Sb11A—S4A—Pb11B	50.3 (8)
S7B—Sb4A—Sb8A^iii	98.8 (2)	Sb11A—S4A—Ag12A	42.61 (12)
S7B—Sb4A—Sb9A^iii	158.2 (3)	Pb11B—S4A—Ag12A	67.5 (8)
S7B—Sb4A—Sb11A	42.23 (17)	Pb1A^ii—S4B—Pb1B	86.48 (16)
S7B—Sb4A—S8A	142.8 (3)	Pb1A^ii—S4B—Sb4A^ii	78.06 (19)
S8A—Sb4A—Ag4B'	121.6 (8)	Pb1A^ii—S4B—Sb5B	72.03 (12)
S8A—Sb4A—Sb8A^iii	115.9 (3)	Pb1A^ii—S4B—Ag12B	135.8 (2)
S8A—Sb4A—Sb9A^iii	53.77 (17)	Pb1B—S4B—Sb4A^ii	156.9 (2)
S12A^iii—Sb4A—Ag4B	82.7 (3)	Pb1B—S4B—Sb5B	68.53 (12)
S12A^iii—Sb4A—Ag4B'	79.9 (8)	Pb1B—S4B—Ag12B	129.1 (2)
S12A^iii—Sb4A—Sb8A^iii	60.2 (2)	Pb4A^ii—S4B—Pb1A^ii	88.0 (2)
S12A^iii—Sb4A—Sb9A^iii	57.8 (2)	Pb4A^ii—S4B—Pb1B	159.4 (2)
S12A^iii—Sb4A—Sb11A	142.1 (4)	Pb4A^ii—S4B—Sb4A^ii	10.26 (14)
S12A^iii—Sb4A—S7A	122.4 (4)	Pb4A^ii—S4B—Sb5B	90.88 (16)
S12A^iii—Sb4A—S7B	100.6 (4)	Pb4A^ii—S4B—Ag12B	66.38 (13)
S12A^iii—Sb4A—S8A	107.8 (3)	Sb4A^ii—S4B—Ag12B	72.95 (16)
Sb4A—Ag4B—Pb4A^ii	172.2 (2)	Ag4B—S4B—Pb1A^ii	154.6 (3)
Sb4A—Ag4B—Sb8B^iv	70.51 (18)	Ag4B—S4B—Pb1B	90.4 (3)
Sb4A—Ag4B—Sb9B^iv	74.5 (2)	Ag4B—S4B—Pb4A^ii	86.2 (2)
Sb4A—Ag4B—Pb11B	110.1 (13)	Ag4B—S4B—Sb4A^ii	96.3 (3)
Sb4A—Ag4B—S4A	43.9 (2)	Ag4B—S4B—Sb5B	83.35 (19)
Cu4B—Ag4B—Pb4A^ii	15.8 (12)	Ag4B—S4B—Ag12B	62.67 (18)
Cu4B—Ag4B—Sb4A	156.8 (13)	Cu4B—S4B—Pb1A^ii	134.8 (10)
Cu4B—Ag4B—Sb8B^iv	86.3 (12)	Cu4B—S4B—Pb1B	124.0 (9)
Cu4B—Ag4B—Sb9B^iv	96.8 (13)	Cu4B—S4B—Pb4A^ii	51.2 (10)
Cu4B—Ag4B—Pb11B	78.0 (18)	Cu4B—S4B—Sb4A^ii	61.4 (10)
Cu4B—Ag4B—S4A	156.0 (12)	Cu4B—S4B—Ag4B	35.1 (9)
Cu4B—Ag4B—S4B	65.1 (12)	Cu4B—S4B—Ag4B'	21.0 (12)
Cu4B—Ag4B—S7B	100.7 (14)	Cu4B—S4B—Sb5B	88.2 (8)
Cu4B—Ag4B—S8B	111.6 (13)	Cu4B—S4B—Sb11B	101.8 (8)
Cu4B—Ag4B—S12B^iv	54.7 (12)	Cu4B—S4B—Pb11B	95.3 (16)
Ag4B'—Ag4B—Pb4A^ii	39 (4)	Cu4B—S4B—Ag12B	51.1 (8)
Ag4B'—Ag4B—Sb4A	133 (4)	Ag4B'—S4B—Pb1A^ii	155.1 (13)
Ag4B'—Ag4B—Cu4B	29 (4)	Ag4B'—S4B—Pb1B	108.0 (13)
Ag4B'—Ag4B—Sb8B^iv	69 (4)	Ag4B'—S4B—Pb4A^ii	71.3 (13)
Ag4B'—Ag4B—Sb9B^iv	110 (4)	Ag4B'—S4B—Sb4A^ii	81.6 (13)
Ag4B'—Ag4B—Pb11B	65 (4)	Ag4B'—S4B—Ag4B	18.2 (12)
Ag4B'—Ag4B—S4A	141 (4)	Ag4B'—S4B—Sb5B	94.1 (11)
Ag4B'—Ag4B—S4B	75 (4)	Ag4B'—S4B—Sb11B	93.8 (11)
Ag4B'—Ag4B—S7B	72 (4)	Ag4B'—S4B—Ag12B	47.6 (11)
Ag4B'—Ag4B—S8B	140 (4)	Sb5B—S4B—Sb4A^ii	90.28 (17)
Ag4B'—Ag4B—S12B^iv	62 (3)	Sb5B—S4B—Ag12B	139.20 (15)
Sb8B^iv—Ag4B—Pb4A^ii	101.87 (17)	Sb11B—S4B—Pb1A^ii	103.0 (2)
Sb8B^iv—Ag4B—Pb11B	109.6 (9)	Sb11B—S4B—Pb1B	102.0 (2)
Sb9B^iv—Ag4B—Pb4A^ii	104.95 (16)	Sb11B—S4B—Pb4A^ii	98.6 (2)
Sb9B^iv—Ag4B—Sb8B^iv	69.32 (8)	Sb11B—S4B—Sb4A^ii	98.1 (2)
Sb9B^iv—Ag4B—Pb11B	174.8 (12)	Sb11B—S4B—Ag4B	102.3 (3)
Sb9B^iv—Ag4B—S4A	105.1 (2)	Sb11B—S4B—Sb5B	169.2 (2)
Pb11B—Ag4B—Pb4A^ii	70.1 (13)	Sb11B—S4B—Ag12B	50.73 (13)
S4A—Ag4B—Pb4A^ii	141.91 (16)	Pb11B—S4B—Pb1A^ii	115.0 (18)
S4A—Ag4B—Sb8B^iv	110.3 (2)	Pb11B—S4B—Pb1B	96.6 (15)
S4A—Ag4B—Pb11B	80.1 (12)	Pb11B—S4B—Pb4A^ii	103.7 (15)
S4B—Ag4B—Pb4A^ii	49.83 (19)	Pb11B—S4B—Sb4A^ii	105.4 (16)
S4B—Ag4B—Sb4A	135.9 (3)	Pb11B—S4B—Ag4B	90.4 (18)
S4B—Ag4B—Sb8B^iv	142.7 (3)	Pb11B—S4B—Ag4B'	84 (2)
S4B—Ag4B—Sb9B^iv	134.3 (2)	Pb11B—S4B—Sb5B	163.7 (18)
S4B—Ag4B—Pb11B	43.8 (11)	Pb11B—S4B—Sb11B	13.2 (19)
S4B—Ag4B—S4A	92.2 (2)	Pb11B—S4B—Ag12B	46.1 (13)
S4B—Ag4B—S7B	94.6 (3)	Pb2A—S5A—Pb2B	84.17 (15)
S4B—Ag4B—S8B	80.5 (2)	Pb2A—S5A—Pb6B	132.65 (16)
S4B—Ag4B—S12B^iv	117.2 (3)	Pb2A—S5A—Pb6B^i	62.62 (10)
S7B—Ag4B—Pb4A^ii	104.1 (2)	Pb2A—S5A—Sb6B^i	62.62 (10)
S7B—Ag4B—Sb4A	71.5 (3)	Pb2A—S5A—Sb8A	67.68 (11)
S7B—Ag4B—Sb8B^iv	66.46 (18)	Pb2A—S5A—Sb9B^viii	137.09 (18)
S7B—Ag4B—Sb9B^iv	130.8 (2)	Pb2B—S5A—Pb6B	62.37 (10)
S7B—Ag4B—Pb11B	50.8 (11)	Pb2B—S5A—Pb6B^i	133.41 (15)
S7B—Ag4B—S4A	72.2 (2)	Pb2B—S5A—Sb6B^i	133.41 (15)
S7B—Ag4B—S8B	141.1 (3)	Pb2B—S5A—Sb8A	66.27 (11)
S7B—Ag4B—S12B^iv	111.4 (3)	Pb2B—S5A—Sb9B^viii	136.57 (17)
S8B—Ag4B—Pb4A^ii	101.7 (2)	Sb6A—S5A—Pb2A	98.53 (18)
S8B—Ag4B—Sb4A	85.4 (3)	Sb6A—S5A—Pb2B	99.06 (18)
S8B—Ag4B—Sb8B^iv	134.6 (2)	Sb6A—S5A—Pb6B	58.83 (13)
S8B—Ag4B—Sb9B^iv	67.42 (16)	Sb6A—S5A—Pb6B^i	58.60 (13)
S8B—Ag4B—Pb11B	114.7 (9)	Sb6A—S5A—Sb6B^i	58.60 (13)
S8B—Ag4B—S4A	69.4 (2)	Sb6A—S5A—Pb7A	106.4 (2)
S12B^iv—Ag4B—Pb4A^ii	68.3 (2)	Sb6A—S5A—Pb7B	106.6 (2)
S12B^iv—Ag4B—Sb4A	106.8 (3)	Sb6A—S5A—Sb8A	160.1 (2)
S12B^iv—Ag4B—Sb8B^iv	51.15 (15)	Sb6A—S5A—Sb9B^viii	67.44 (14)
S12B^iv—Ag4B—Sb9B^iv	48.36 (15)	Pb6B^i—S5A—Pb6B	117.20 (11)
S12B^iv—Ag4B—Pb11B	126.8 (11)	Sb6B^i—S5A—Pb6B	117.2
S12B^iv—Ag4B—S4A	149.3 (3)	Sb6B^i—S5A—Pb6B^i	0.0
S12B^iv—Ag4B—S8B	105.0 (2)	Pb7A—S5A—Pb2A	88.31 (16)
Pb4A^ii—Cu4B—Sb4A^ii	10.0 (4)	Pb7A—S5A—Pb2B	154.3 (2)
Pb4A^ii—Cu4B—Sb8A^iv	67.1 (8)	Pb7A—S5A—Pb6B	135.77 (17)
Pb4A^ii—Cu4B—Sb8B^iv	135.6 (12)	Pb7A—S5A—Pb6B^i	61.46 (11)
Pb4A^ii—Cu4B—Sb9B^iv	130.6 (13)	Pb7A—S5A—Sb6B^i	61.46 (11)
Pb4A^ii—Cu4B—Sb11B	79.6 (9)	Pb7A—S5A—Sb8A	88.11 (13)
Pb4A^ii—Cu4B—Pb11B	87.9 (17)	Pb7A—S5A—Sb9B^viii	60.23 (11)
Pb4A^ii—Cu4B—Ag12B	91.4 (10)	Pb7B—S5A—Pb2A	154.5 (2)
Pb4A^ii—Cu4B—S4B	74.8 (10)	Pb7B—S5A—Pb2B	87.37 (16)
Pb4A^ii—Cu4B—S12B^iv	108.9 (15)	Pb7B—S5A—Pb6B^i	135.94 (18)
Sb4A^ii—Cu4B—Sb9B^iv	124.2 (10)	Pb7B—S5A—Pb6B	61.35 (11)
Sb4A^ii—Cu4B—Sb11B	87.9 (8)	Pb7B—S5A—Sb6B^i	135.94 (18)
Ag4B—Cu4B—Pb4A^ii	153.8 (19)	Pb7B—S5A—Pb7A	88.97 (15)
Ag4B—Cu4B—Sb4A^ii	162.8 (17)	Pb7B—S5A—Sb8A	86.86 (13)
Ag4B—Cu4B—Sb8A^iv	138.5 (17)	Pb7B—S5A—Sb9B^viii	60.35 (11)
Ag4B—Cu4B—Sb8B^iv	70.0 (13)	Sb8A—S5A—Pb6B^i	121.01 (13)
Ag4B—Cu4B—Sb9B^iv	60.1 (11)	Sb8A—S5A—Pb6B	119.35 (14)
Ag4B—Cu4B—Sb11B	85.3 (14)	Sb8A—S5A—Sb6B^i	121.01 (13)
Ag4B—Cu4B—Pb11B	77.8 (18)	Sb8A—S5A—Sb9B^viii	132.47 (13)
Ag4B—Cu4B—Ag12B	98.3 (16)	Sb9B^viii—S5A—Pb6B	76.18 (9)
Ag4B—Cu4B—S4B	79.8 (13)	Sb9B^viii—S5A—Pb6B^i	76.22 (9)
Ag4B—Cu4B—S12B^iv	92.9 (16)	Sb9B^viii—S5A—Sb6B^i	76.22 (9)
Ag4B'—Cu4B—Pb4A^ii	154 (5)	Pb2A^ii—S5B—Sb6A^ii	59.86 (10)
Ag4B'—Cu4B—Sb4A^ii	160 (5)	Pb2A^ii—S5B—Sb6A	131.64 (16)
Ag4B'—Cu4B—Ag4B	26 (3)	Pb2A^ii—S5B—Pb6A^ii	59.86 (10)
Ag4B'—Cu4B—Sb8A^iv	118 (4)	Pb2A^ii—S5B—Pb7A^ii	90.57 (18)
Ag4B'—Cu4B—Sb8B^iv	56 (4)	Pb2A^ii—S5B—Pb7B	159.8 (2)
Ag4B'—Cu4B—Sb9B^iv	75 (4)	Pb2A^ii—S5B—Sb8B	68.88 (11)
Ag4B'—Cu4B—Sb11B	74 (4)	Pb2A^ii—S5B—Sb9A^vii	133.72 (18)
Ag4B'—Cu4B—Pb11B	66 (4)	Pb2B—S5B—Pb2A^ii	86.98 (15)
Ag4B'—Cu4B—Ag12B	72 (4)	Pb2B—S5B—Sb6A	60.41 (11)
Ag4B'—Cu4B—S4B	87 (4)	Pb2B—S5B—Sb6A^ii	131.62 (16)
Ag4B'—Cu4B—S12B^iv	95 (4)	Pb2B—S5B—Pb6A^ii	131.62 (16)
Sb8A^iv—Cu4B—Sb4A^ii	58.7 (6)	Pb2B—S5B—Pb7A^ii	159.1 (2)
Sb8A^iv—Cu4B—Sb8B^iv	68.6 (5)	Pb2B—S5B—Pb7B	89.88 (17)
Sb8A^iv—Cu4B—Sb9B^iv	101.6 (7)	Pb2B—S5B—Sb8B	70.21 (11)
Sb8A^iv—Cu4B—Sb11B	107.3 (8)	Pb2B—S5B—Sb9A^vii	134.38 (19)
Sb8B^iv—Cu4B—Sb4A^ii	127.2 (9)	Sb6A^ii—S5B—Sb6A	115.22 (12)
Sb8B^iv—Cu4B—Sb9B^iv	62.1 (5)	Pb6A^ii—S5B—Sb6A^ii	0.0
Sb8B^iv—Cu4B—Sb11B	111.4 (9)	Pb6A^ii—S5B—Sb6A	115.2
Sb11B—Cu4B—Sb9B^iv	145.2 (11)	Pb6B—S5B—Pb2A^ii	101.88 (18)
Pb11B—Cu4B—Sb4A^ii	96.1 (16)	Pb6B—S5B—Pb2B	102.28 (19)
Pb11B—Cu4B—Sb8A^iv	110.3 (13)	Pb6B—S5B—Sb6A^ii	57.76 (11)
Pb11B—Cu4B—Sb8B^iv	104.8 (15)	Pb6B—S5B—Sb6A	57.67 (12)
Pb11B—Cu4B—Sb9B^iv	137.9 (17)	Pb6B—S5B—Pb6A^ii	57.76 (11)
Pb11B—Cu4B—Sb11B	8.4 (13)	Pb6B—S5B—Pb7A^ii	98.55 (18)
Ag12B—Cu4B—Sb4A^ii	91.3 (8)	Pb6B—S5B—Pb7B	98.28 (19)
Ag12B—Cu4B—Sb8A^iv	61.1 (5)	Pb6B—S5B—Sb8B	167.91 (19)
Ag12B—Cu4B—Sb8B^iv	64.5 (6)	Pb6B—S5B—Sb9A^vii	56.63 (11)
Ag12B—Cu4B—Sb9B^iv	126.5 (10)	Pb7A^ii—S5B—Sb6A^ii	62.77 (11)
Ag12B—Cu4B—Sb11B	57.2 (5)	Pb7A^ii—S5B—Sb6A	132.49 (17)
Ag12B—Cu4B—Pb11B	55.5 (10)	Pb7A^ii—S5B—Pb6A^ii	62.77 (11)
S4B—Cu4B—Sb4A^ii	84.8 (10)	Pb7A^ii—S5B—Sb8B	89.54 (14)
S4B—Cu4B—Sb8A^iv	134.8 (13)	Pb7A^ii—S5B—Sb9A^vii	58.25 (10)
S4B—Cu4B—Sb8B^iv	141.2 (14)	Pb7B—S5B—Sb6A^ii	133.17 (16)
S4B—Cu4B—Sb9B^iv	121.7 (12)	Pb7B—S5B—Sb6A	61.91 (11)
S4B—Cu4B—Sb11B	40.5 (6)	Pb7B—S5B—Pb6A^ii	133.17 (16)
S4B—Cu4B—Pb11B	43.5 (11)	Pb7B—S5B—Pb7A^ii	85.28 (15)
S4B—Cu4B—Ag12B	97.7 (10)	Pb7B—S5B—Sb8B	91.30 (13)
S12B^iv—Cu4B—Sb4A^ii	99.1 (12)	Pb7B—S5B—Sb9A^vii	58.88 (10)
S12B^iv—Cu4B—Sb8A^iv	60.9 (7)	Sb8B—S5B—Sb6A^ii	119.69 (14)
S12B^iv—Cu4B—Sb8B^iv	48.5 (7)	Sb8B—S5B—Sb6A	122.15 (13)
S12B^iv—Cu4B—Sb9B^iv	40.7 (6)	Sb8B—S5B—Pb6A^ii	119.69 (14)
S12B^iv—Cu4B—Sb11B	158.4 (13)	Sb8B—S5B—Sb9A^vii	135.39 (13)
S12B^iv—Cu4B—Pb11B	153.1 (18)	Sb9A^vii—S5B—Sb6A	75.03 (9)
S12B^iv—Cu4B—Ag12B	101.9 (10)	Sb9A^vii—S5B—Sb6A^ii	74.90 (9)
S12B^iv—Cu4B—S4B	159.9 (16)	Sb9A^vii—S5B—Pb6A^ii	74.90 (9)
Pb4A^ii—Ag4B'—Sb8B^iv	121.3 (16)	Pb3A—S6A—Pb6B^xi	135.41 (16)
Pb4A^ii—Ag4B'—Sb9B^iv	109.9 (14)	Pb3A—S6A—Sb6B^xi	135.41 (16)
Pb4A^ii—Ag4B'—Sb11B	73.2 (11)	Pb3A—S6A—Pb7B^xi	91.28 (16)
Pb4A^ii—Ag4B'—Pb11B	81.0 (19)	Pb3A—S6A—Sb8A	62.11 (10)
Pb4A^ii—Ag4B'—Ag12B	82.0 (13)	Pb3A—S6A—Sb9B^i	61.51 (11)
Pb4A^ii—Ag4B'—S8B	100.7 (13)	Pb3A—S6A—Sb9B	133.75 (16)
Ag4B—Ag4B'—Pb4A^ii	132 (4)	Pb3A—S6A—Sb10A	69.36 (11)
Ag4B—Ag4B'—Cu4B	125 (7)	Pb3B—S6A—Pb3A	85.13 (14)
Ag4B—Ag4B'—Sb8B^iv	98 (4)	Pb3B—S6A—Pb6B^xi	136.02 (17)
Ag4B—Ag4B'—Sb9B^iv	58 (3)	Pb3B—S6A—Sb6B^xi	136.02 (17)
Ag4B—Ag4B'—Sb11B	107 (4)	Pb3B—S6A—Pb7B^xi	155.8 (2)
Ag4B—Ag4B'—Pb11B	102 (4)	Pb3B—S6A—Sb8A	63.89 (10)
Ag4B—Ag4B'—Ag12B	142 (5)	Pb3B—S6A—Sb9B	62.67 (10)
Ag4B—Ag4B'—S4B	87 (3)	Pb3B—S6A—Sb9B^i	135.27 (17)
Ag4B—Ag4B'—S7B	90 (4)	Pb3B—S6A—Sb10A	66.70 (10)
Ag4B—Ag4B'—S8B	31 (3)	Pb6B^xi—S6A—Sb6B^xi	0.00 (3)
Ag4B—Ag4B'—S12B^iv	102 (4)	Pb7A^xii—S6A—Pb3A	157.8 (2)
Cu4B—Ag4B'—Pb4A^ii	19 (3)	Pb7A^xii—S6A—Pb3B	90.01 (16)
Cu4B—Ag4B'—Sb8B^iv	112 (4)	Pb7A^xii—S6A—Pb6B^xi	58.61 (9)
Cu4B—Ag4B'—Sb9B^iv	91 (4)	Pb7A^xii—S6A—Sb6B^xi	58.61 (9)
Cu4B—Ag4B'—Sb11B	92 (4)	Pb7A^xii—S6A—Pb7B^xi	84.35 (15)
Cu4B—Ag4B'—Pb11B	100 (5)	Pb7A^xii—S6A—Sb8A	133.79 (17)
Cu4B—Ag4B'—Ag12B	93 (4)	Pb7A^xii—S6A—Sb9B^i	131.91 (16)
Cu4B—Ag4B'—S4B	72 (4)	Pb7A^xii—S6A—Sb9B	60.24 (10)
Cu4B—Ag4B'—S7B	143 (5)	Pb7A^xii—S6A—Sb10A	88.86 (14)
Cu4B—Ag4B'—S8B	94 (4)	Pb7B^xi—S6A—Pb6B^xi	58.34 (9)
Cu4B—Ag4B'—S12B^iv	65 (4)	Pb7B^xi—S6A—Sb6B^xi	58.34 (9)
Sb8B^iv—Ag4B'—Sb9B^iv	67.4 (9)	Pb7B^xi—S6A—Sb8A	134.19 (17)
Sb8B^iv—Ag4B'—Sb11B	126.4 (14)	Pb7B^xi—S6A—Sb9B	131.53 (16)
Sb8B^iv—Ag4B'—Pb11B	121.9 (18)	Pb7B^xi—S6A—Sb9B^i	60.37 (10)
Sb8B^iv—Ag4B'—Ag12B	71.0 (9)	Pb7B^xi—S6A—Sb10A	89.64 (13)
Sb8B^iv—Ag4B'—S8B	119.1 (15)	Sb8A—S6A—Pb6B^xi	114.44 (11)
Sb11B—Ag4B'—Sb9B^iv	162.8 (15)	Sb8A—S6A—Sb6B^xi	114.44 (11)
Pb11B—Ag4B'—Sb9B^iv	160 (2)	Sb9A—S6A—Pb3A	108.4 (2)
Pb11B—Ag4B'—Sb11B	7.8 (14)	Sb9A—S6A—Pb3B	110.1 (2)
Pb11B—Ag4B'—Ag12B	59.4 (12)	Sb9A—S6A—Pb6B^xi	49.81 (11)
Pb11B—Ag4B'—S8B	105.3 (15)	Sb9A—S6A—Sb6B^xi	49.81 (11)
Ag12B—Ag4B'—Sb9B^iv	136.7 (14)	Sb9A—S6A—Pb7A^xii	93.56 (18)
Ag12B—Ag4B'—Sb11B	59.9 (8)	Sb9A—S6A—Pb7B^xi	93.77 (17)
Ag12B—Ag4B'—S8B	164.1 (16)	Sb9A—S6A—Sb8A	64.63 (13)
S4B—Ag4B'—Pb4A^ii	59.5 (12)	Sb9A—S6A—Sb9B	59.86 (13)
S4B—Ag4B'—Sb8B^iv	169.7 (19)	Sb9A—S6A—Sb9B^i	60.48 (13)
S4B—Ag4B'—Sb9B^iv	122.6 (16)	Sb9A—S6A—Sb10A	176.0 (2)
S4B—Ag4B'—Sb11B	43.4 (8)	Sb9B—S6A—Pb6B^xi	74.53 (8)
S4B—Ag4B'—Pb11B	47.9 (13)	Sb9B^i—S6A—Pb6B^xi	74.63 (8)
S4B—Ag4B'—Ag12B	99.6 (15)	Sb9B^i—S6A—Sb6B^xi	74.63 (8)
S4B—Ag4B'—S7B	99.9 (17)	Sb9B—S6A—Sb6B^xi	74.53 (8)
S4B—Ag4B'—S8B	69.2 (11)	Sb9B—S6A—Sb8A	73.72 (9)
S4B—Ag4B'—S12B^iv	133 (2)	Sb9B^i—S6A—Sb8A	73.96 (9)
S7B—Ag4B'—Pb4A^ii	126.8 (19)	Sb9B^i—S6A—Sb9B	119.66 (12)
S7B—Ag4B'—Sb8B^iv	71.2 (12)	Sb10A—S6A—Pb6B^xi	134.12 (13)
S7B—Ag4B'—Sb9B^iv	121.3 (19)	Sb10A—S6A—Sb6B^xi	134.12 (13)
S7B—Ag4B'—Sb11B	62.3 (10)	Sb10A—S6A—Sb8A	111.43 (12)
S7B—Ag4B'—Pb11B	55.3 (16)	Sb10A—S6A—Sb9B	119.01 (13)
S7B—Ag4B'—Ag12B	51.5 (9)	Sb10A—S6A—Sb9B^i	119.84 (13)
S7B—Ag4B'—S8B	117.7 (18)	Pb3A^ii—S6B—Sb6A^xii	134.75 (18)
S7B—Ag4B'—S12B^iv	126.3 (19)	Pb3A^ii—S6B—Pb6A^xii	134.75 (18)
S8B—Ag4B'—Sb9B^iv	57.3 (8)	Pb3A^ii—S6B—Sb8B	60.93 (10)
S8B—Ag4B'—Sb11B	105.6 (12)	Pb3A^ii—S6B—Sb9A	135.43 (17)
S12B^iv—Ag4B'—Pb4A^ii	81.9 (15)	Pb3A^ii—S6B—Sb9A^ii	64.16 (11)
S12B^iv—Ag4B'—Sb8B^iv	55.4 (9)	Pb3A^ii—S6B—Sb10B	68.11 (10)
S12B^iv—Ag4B'—Sb9B^iv	43.9 (8)	Pb3B—S6B—Pb3A^ii	84.86 (14)
S12B^iv—Ag4B'—Sb11B	150 (2)	Pb3B—S6B—Sb6A^xii	135.84 (17)
S12B^iv—Ag4B'—Pb11B	156 (2)	Pb3B—S6B—Pb6A^xii	135.84 (17)
S12B^iv—Ag4B'—Ag12B	101.3 (15)	Pb3B—S6B—Sb8B	64.18 (11)
S12B^iv—Ag4B'—S8B	94.6 (14)	Pb3B—S6B—Sb9A^ii	137.10 (17)
Sb6A—Sb5A—Sb6A^v	71.05 (5)	Pb3B—S6B—Sb9A	65.56 (12)
Sb6A—Sb5A—Pb6A^v	71.1	Pb3B—S6B—Sb10B	67.94 (10)
Sb6A^v—Sb5A—Pb6B^v	62.09 (4)	Sb6A^xii—S6B—Pb6A^xii	0.00 (5)
Sb6A—Sb5A—Pb6B^v	74.03 (4)	Pb7A^xii—S6B—Pb3A^ii	161.2 (2)
Sb6A—Sb5A—Sb6B^v	74.03 (4)	Pb7A^xii—S6B—Pb3B	89.82 (18)
Sb6A^v—Sb5A—Sb6B^v	62.09 (4)	Pb7A^xii—S6B—Sb6A^xii	58.33 (9)
Pb6A^v—Sb5A—Sb6A^v	0.0	Pb7A^xii—S6B—Pb6A^xii	58.33 (9)
Pb6A^v—Sb5A—Pb6B^v	62.09 (4)	Pb7A^xii—S6B—Pb7B^xii	87.68 (16)
Pb6A^v—Sb5A—Sb6B^v	62.09 (4)	Pb7A^xii—S6B—Sb8B	131.82 (18)
Sb6B^v—Sb5A—Pb6B^v	0.0	Pb7A^xii—S6B—Sb9A	56.06 (10)
S1A—Sb5A—Sb6A	91.58 (14)	Pb7A^xii—S6B—Sb9A^ii	128.52 (16)
S1A—Sb5A—Sb6A^v	144.99 (15)	Pb7A^xii—S6B—Sb10B	93.21 (14)
S1A—Sb5A—Pb6A^v	144.99 (15)	Pb7B^xii—S6B—Pb3A^ii	90.96 (18)
S1A—Sb5A—Pb6B^v	143.23 (16)	Pb7B^xii—S6B—Pb3B	159.3 (2)
S1A—Sb5A—Sb6B^v	143.23 (16)	Pb7B^xii—S6B—Sb6A^xii	57.71 (9)
S1A—Sb5A—S8A	91.37 (19)	Pb7B^xii—S6B—Pb6A^xii	57.71 (9)
S1A—Sb5A—S8B	90.3 (2)	Pb7B^xii—S6B—Sb8B	130.40 (17)
S1A—Sb5A—S9A	88.7 (2)	Pb7B^xii—S6B—Sb9A^ii	55.94 (10)
S1A—Sb5A—S9B	88.69 (18)	Pb7B^xii—S6B—Sb9A	127.99 (15)
S1A—Sb5A—S10B^v	160.03 (18)	Pb7B^xii—S6B—Sb10B	91.67 (14)
S8A—Sb5A—Sb6A	127.02 (15)	Sb8B—S6B—Sb6A^xii	112.96 (11)
S8A—Sb5A—Sb6A^v	123.47 (13)	Sb8B—S6B—Pb6A^xii	112.96 (11)
S8A—Sb5A—Pb6A^v	123.47 (13)	Sb8B—S6B—Sb9A	75.97 (9)
S8A—Sb5A—Pb6B^v	72.60 (13)	Sb8B—S6B—Sb9A^ii	74.67 (9)
S8A—Sb5A—Sb6B^v	72.60 (13)	Sb9A^ii—S6B—Sb6A^xii	70.98 (8)
S8A—Sb5A—S8B	103.7 (2)	Sb9A—S6B—Sb6A^xii	71.05 (8)
S8A—Sb5A—S9A	87.47 (19)	Sb9A—S6B—Pb6A^xii	71.05 (8)
S8A—Sb5A—S9B	167.0 (2)	Sb9A^ii—S6B—Pb6A^xii	70.98 (8)
S8A—Sb5A—S10B^v	72.68 (16)	Sb9A—S6B—Sb9A^ii	116.57 (11)
S8B—Sb5A—Sb6A^v	78.97 (13)	Sb9B—S6B—Pb3A^ii	99.26 (19)
S8B—Sb5A—Sb6A	129.17 (15)	Sb9B—S6B—Pb3B	102.1 (2)
S8B—Sb5A—Pb6A^v	78.97 (13)	Sb9B—S6B—Sb6A^xii	59.79 (12)
S8B—Sb5A—Pb6B^v	125.17 (13)	Sb9B—S6B—Pb6A^xii	59.79 (12)
S8B—Sb5A—Sb6B^v	125.17 (13)	Sb9B—S6B—Pb7A^xii	99.45 (19)
S8B—Sb5A—S9A	168.8 (2)	Sb9B—S6B—Pb7B^xii	98.6 (2)
S8B—Sb5A—S9B	89.32 (19)	Sb9B—S6B—Sb8B	53.17 (11)
S8B—Sb5A—S10B^v	82.17 (17)	Sb9B—S6B—Sb9A^ii	58.34 (13)
S9A—Sb5A—Sb6A	39.75 (13)	Sb9B—S6B—Sb9A	58.92 (13)
S9A—Sb5A—Sb6A^v	95.53 (13)	Sb9B—S6B—Sb10B	164.0 (2)
S9A—Sb5A—Pb6A^v	95.53 (13)	Sb10B—S6B—Sb6A^xii	136.12 (13)
S9A—Sb5A—Pb6B^v	58.45 (13)	Sb10B—S6B—Pb6A^xii	136.12 (13)
S9A—Sb5A—Sb6B^v	58.45 (13)	Sb10B—S6B—Sb8B	110.87 (12)
S9A—Sb5A—S9B	79.51 (18)	Sb10B—S6B—Sb9A	122.85 (14)
S9A—Sb5A—S10B^v	102.13 (17)	Sb10B—S6B—Sb9A^ii	119.91 (14)
S9B—Sb5A—Sb6A^v	58.28 (12)	Pb4A—S7A—Sb4A	29.4 (2)
S9B—Sb5A—Sb6A	39.98 (14)	Pb4A—S7A—Ag4B'^i	52.9 (8)
S9B—Sb5A—Pb6A^v	58.28 (12)	Pb4A—S7A—Sb8A^iii	66.09 (18)
S9B—Sb5A—Pb6B^v	99.89 (14)	Pb4A—S7A—Sb10B^xiii	166.9 (3)
S9B—Sb5A—Sb6B^v	99.89 (14)	Pb4A—S7A—Pb10B^xiii	166.9 (3)
S9B—Sb5A—S10B^v	109.58 (16)	Pb4A—S7A—Sb11A	90.0 (3)
S10B^v—Sb5A—Sb6A^v	51.44 (10)	Pb4A—S7A—Sb11B^i	91.3 (2)
S10B^v—Sb5A—Sb6A	107.53 (11)	Pb4A—S7A—Pb11B^i	90.0 (10)
S10B^v—Sb5A—Pb6A^v	51.44 (10)	Pb4A—S7A—Ag12B^i	107.8 (3)
S10B^v—Sb5A—Pb6B^v	43.69 (11)	Sb4A—S7A—Ag4B'^i	80.9 (8)
S10B^v—Sb5A—Sb6B^v	43.69 (11)	Sb4A—S7A—Sb8A^iii	64.6 (2)
Sb5A—Sb5B—Sb6A^v	58.09 (4)	Sb4A—S7A—Sb10B^xiii	155.0 (3)
Sb5A—Sb5B—Pb6A^v	58.09 (4)	Sb4A—S7A—Pb10B^xiii	155.0 (3)
Pb6A^v—Sb5B—Sb6A^v	0.0	Sb4A—S7A—Pb11B^i	116.7 (10)
Pb6B^vi—Sb5B—Sb5A	119.81 (5)	Sb8A^iii—S7A—Ag4B'^i	68.0 (7)
Pb6B^vi—Sb5B—Sb6A^v	61.72 (4)	Sb10B^xiii—S7A—Ag4B'^i	123.5 (8)
Pb6B^vi—Sb5B—Pb6A^v	61.72 (4)	Sb10B^xiii—S7A—Sb8A^iii	126.0 (2)
Sb6B^vi—Sb5B—Sb5A	119.81 (5)	Pb10B^xiii—S7A—Ag4B'^i	123.5 (8)
Sb6B^vi—Sb5B—Sb6A^v	61.72 (4)	Pb10B^xiii—S7A—Sb8A^iii	126.0 (2)
Sb6B^vi—Sb5B—Pb6A^v	61.72 (4)	Pb10B^xiii—S7A—Sb10B^xiii	0.0
Sb6B^vi—Sb5B—Pb6B^vi	0.0	Sb11A—S7A—Sb4A	73.0 (3)
S1B—Sb5B—Sb5A	90.40 (15)	Sb11A—S7A—Ag4B'^i	131.8 (7)
S1B—Sb5B—Sb6A^v	139.16 (15)	Sb11A—S7A—Sb8A^iii	129.2 (3)
S1B—Sb5B—Pb6A^v	139.16 (15)	Sb11A—S7A—Sb10B^xiii	85.1 (2)
S1B—Sb5B—Pb6B^vi	140.12 (15)	Sb11A—S7A—Pb10B^xiii	85.1 (2)
S1B—Sb5B—Sb6B^vi	140.12 (15)	Sb11A—S7A—Sb11B^i	93.6 (2)
S1B—Sb5B—S8A^ii	92.9 (2)	Sb11A—S7A—Pb11B^i	103.1 (14)
S1B—Sb5B—S8B	94.7 (2)	Sb11B^i—S7A—Sb4A	115.6 (3)
S1B—Sb5B—S9A^ii	82.87 (17)	Sb11B^i—S7A—Ag4B'^i	62.2 (7)
S1B—Sb5B—S9B	84.79 (18)	Sb11B^i—S7A—Sb8A^iii	129.0 (3)
S1B—Sb5B—S10A^v	167.87 (18)	Sb11B^i—S7A—Sb10B^xiii	76.9 (2)
S8A^ii—Sb5B—Sb5A	145.50 (15)	Sb11B^i—S7A—Pb10B^xiii	76.9 (2)
S8A^ii—Sb5B—Sb6A^v	127.93 (14)	Sb11B^i—S7A—Pb11B^i	9.6 (13)
S8A^ii—Sb5B—Pb6A^v	127.93 (14)	Pb11B^i—S7A—Ag4B'^i	54.6 (14)
S8A^ii—Sb5B—Pb6B^vi	76.81 (14)	Pb11B^i—S7A—Sb8A^iii	120.0 (13)
S8A^ii—Sb5B—Sb6B^vi	76.81 (14)	Pb11B^i—S7A—Sb10B^xiii	79.4 (10)
S8A^ii—Sb5B—S9A^ii	81.56 (19)	Pb11B^i—S7A—Pb10B^xiii	79.4 (10)
S8A^ii—Sb5B—S9B	169.20 (19)	Ag12A—S7A—Pb4A	109.3 (3)
S8A^ii—Sb5B—S10A^v	78.32 (17)	Ag12A—S7A—Sb4A	81.7 (3)
S8B—Sb5B—Sb5A	41.88 (16)	Ag12A—S7A—Ag4B'^i	140.3 (8)
S8B—Sb5B—Sb6A^v	78.97 (15)	Ag12A—S7A—Sb8A^iii	72.36 (19)
S8B—Sb5B—Pb6A^v	78.97 (15)	Ag12A—S7A—Sb10B^xiii	81.2 (2)
S8B—Sb5B—Pb6B^vi	125.09 (14)	Ag12A—S7A—Pb10B^xiii	81.2 (2)
S8B—Sb5B—Sb6B^vi	125.09 (14)	Ag12A—S7A—Sb11A	75.0 (2)
S8B—Sb5B—S8A^ii	103.6 (2)	Ag12A—S7A—Sb11B^i	156.1 (4)
S8B—Sb5B—S9A^ii	174.4 (2)	Ag12A—S7A—Pb11B^i	160.6 (11)
S8B—Sb5B—S9B	87.10 (19)	Ag12A—S7A—Ag12B^i	107.7 (3)
S8B—Sb5B—S10A^v	79.51 (17)	Ag12B^i—S7A—Sb4A	127.6 (4)
S9A^ii—Sb5B—Sb5A	132.89 (14)	Ag12B^i—S7A—Ag4B'^i	58.8 (8)
S9A^ii—Sb5B—Sb6A^v	99.56 (13)	Ag12B^i—S7A—Sb8A^iii	69.60 (18)
S9A^ii—Sb5B—Pb6A^v	99.56 (13)	Ag12B^i—S7A—Sb10B^xiii	75.2 (2)
S9A^ii—Sb5B—Pb6B^vi	57.70 (11)	Ag12B^i—S7A—Pb10B^xiii	75.2 (2)
S9A^ii—Sb5B—Sb6B^vi	57.70 (11)	Ag12B^i—S7A—Sb11A	159.2 (4)
S9A^ii—Sb5B—S10A^v	103.78 (15)	Ag12B^i—S7A—Sb11B^i	75.8 (2)
S9B—Sb5B—Sb5A	45.22 (12)	Ag12B^i—S7A—Pb11B^i	67.2 (13)
S9B—Sb5B—Sb6A^v	54.82 (11)	Sb4A—S7B—Sb8B^iv	68.3 (2)
S9B—Sb5B—Pb6A^v	54.82 (11)	Sb4A—S7B—Sb10A^xiii	137.7 (3)
S9B—Sb5B—Pb6B^vi	98.26 (12)	Sb4A—S7B—Pb10A^xiii	137.7 (3)
S9B—Sb5B—Sb6B^vi	98.26 (12)	Ag4B—S7B—Sb4A	61.0 (3)
S9B—Sb5B—S9A^ii	87.68 (16)	Ag4B—S7B—Sb8B^iv	68.8 (2)
S9B—Sb5B—S10A^v	105.39 (16)	Ag4B—S7B—Sb10A^xiii	158.0 (3)
S10A^v—Sb5B—Sb5A	92.24 (12)	Ag4B—S7B—Pb10A^xiii	158.0 (3)
S10A^v—Sb5B—Sb6A^v	50.57 (11)	Ag4B—S7B—Sb11B	82.0 (2)
S10A^v—Sb5B—Pb6A^v	50.57 (11)	Ag4B—S7B—Pb11B	82.2 (12)
S10A^v—Sb5B—Pb6B^vi	46.24 (10)	Ag4B—S7B—Ag12B	98.8 (3)
S10A^v—Sb5B—Sb6B^vi	46.24 (10)	Ag4B'—S7B—Sb4A	76.6 (13)
Sb5A—Sb6A—Sb5A^v	108.95 (4)	Ag4B'—S7B—Ag4B	17.7 (12)
Sb5A—Sb6A—Pb5A^v	109.0	Ag4B'—S7B—Sb8B^iv	65.1 (11)
Sb5A—Sb6A—Pb6B^i	93.03 (4)	Ag4B'—S7B—Sb10A^xiii	145.3 (13)
Sb5A^v—Sb6A—Pb6B^i	116.82 (5)	Ag4B'—S7B—Pb10A^xiii	145.3 (13)
Sb5A^v—Sb6A—Sb6B^i	116.82 (5)	Ag4B'—S7B—Sb11A	120.3 (11)
Sb5A—Sb6A—Sb6B^i	93.03 (4)	Ag4B'—S7B—Sb11B	75.7 (12)
Pb5A^v—Sb6A—Sb5A^v	0.0	Ag4B'—S7B—Pb11B	77.1 (17)
Pb5A^v—Sb6A—Pb6B^i	116.82 (5)	Ag4B'—S7B—Ag12A	137.0 (12)
Pb5A^v—Sb6A—Sb6B^i	116.82 (5)	Ag4B'—S7B—Ag12B	81.1 (12)
Sb6B^i—Sb6A—Pb6B^i	0.0	Sb8B^iv—S7B—Sb10A^xiii	124.33 (19)
S5A—Sb6A—Sb5A	98.88 (14)	Sb8B^iv—S7B—Pb10A^xiii	124.33 (19)
S5A—Sb6A—Sb5A^v	138.91 (15)	Pb10A^xiii—S7B—Sb10A^xiii	0.0
S5A—Sb6A—Pb5A^v	138.91 (15)	Sb11A—S7B—Sb4A	73.3 (2)
S5A—Sb6A—Pb6B^i	90.46 (15)	Sb11A—S7B—Ag4B	105.4 (3)
S5A—Sb6A—Sb6B^i	90.46 (15)	Sb11A—S7B—Sb8B^iv	138.6 (3)
S5A—Sb6A—S9A	92.9 (2)	Sb11A—S7B—Sb10A^xiii	76.6 (2)
S5A—Sb6A—S9B	93.2 (2)	Sb11A—S7B—Pb10A^xiii	76.6 (2)
S5A—Sb6A—S9B^v	173.14 (18)	Sb11A—S7B—Sb11B	84.2 (2)
S5A—Sb6A—S10A	81.33 (18)	Sb11A—S7B—Pb11B	80.2 (14)
S5A—Sb6A—S10B	80.96 (18)	Sb11A—S7B—Ag12A	82.6 (2)
S9A—Sb6A—Sb5A	47.44 (17)	Sb11A—S7B—Ag12B	142.0 (3)
S9A—Sb6A—Sb5A^v	128.19 (15)	Sb11B—S7B—Sb4A	128.0 (3)
S9A—Sb6A—Pb5A^v	128.19 (15)	Sb11B—S7B—Sb8B^iv	132.4 (2)
S9A—Sb6A—Pb6B^i	45.83 (17)	Sb11B—S7B—Sb10A^xiii	76.45 (17)
S9A—Sb6A—Sb6B^i	45.83 (17)	Sb11B—S7B—Pb10A^xiii	76.45 (17)
S9A—Sb6A—S9B^v	83.11 (18)	Pb11B—S7B—Sb4A	125.3 (12)
S9A—Sb6A—S9B	95.7 (2)	Pb11B—S7B—Sb8B^iv	135.7 (13)
S9A—Sb6A—S10A	90.2 (2)	Pb11B—S7B—Sb10A^xiii	76.6 (11)
S9A—Sb6A—S10B	173.30 (18)	Pb11B—S7B—Pb10A^xiii	76.6 (11)
S9B—Sb6A—Sb5A^v	83.79 (15)	Pb11B—S7B—Sb11B	4.1 (13)
S9B^v—Sb6A—Sb5A^v	45.39 (11)	Ag12A—S7B—Sb4A	76.5 (3)
S9B—Sb6A—Sb5A	48.57 (15)	Ag12A—S7B—Ag4B	131.1 (3)
S9B^v—Sb6A—Sb5A	74.31 (11)	Ag12A—S7B—Sb8B^iv	73.98 (18)
S9B^v—Sb6A—Pb5A^v	45.39 (11)	Ag12A—S7B—Sb10A^xiii	70.76 (19)
S9B—Sb6A—Pb5A^v	83.79 (15)	Ag12A—S7B—Pb10A^xiii	70.76 (19)
S9B^v—Sb6A—Pb6B^i	90.74 (12)	Ag12A—S7B—Sb11B	146.7 (3)
S9B—Sb6A—Pb6B^i	141.53 (16)	Ag12A—S7B—Pb11B	145.8 (12)
S9B^v—Sb6A—Sb6B^i	90.74 (12)	Ag12A—S7B—Ag12B	103.0 (2)
S9B—Sb6A—Sb6B^i	141.53 (16)	Ag12B—S7B—Sb4A	144.7 (3)
S9B—Sb6A—S9B^v	81.7 (2)	Ag12B—S7B—Sb8B^iv	77.52 (17)
S9B—Sb6A—S10A	172.19 (19)	Ag12B—S7B—Sb10A^xiii	70.31 (18)
S9B—Sb6A—S10B	87.33 (19)	Ag12B—S7B—Pb10A^xiii	70.31 (18)
S10A—Sb6A—Sb5A^v	96.61 (11)	Ag12B—S7B—Sb11B	70.61 (18)
S10A—Sb6A—Sb5A	137.60 (12)	Ag12B—S7B—Pb11B	74.6 (13)
S10A—Sb6A—Pb5A^v	96.61 (11)	Pb1A—S8A—Sb4A	86.0 (2)
S10A—Sb6A—Pb6B^i	44.71 (11)	Pb1A—S8A—Ag4B^i	86.87 (14)
S10A—Sb6A—Sb6B^i	44.71 (11)	Pb1A—S8A—Ag4B'^i	86.1 (6)
S10A—Sb6A—S9B^v	104.19 (16)	Pb1A—S8A—Pb6B^v	150.63 (17)
S10A—Sb6A—S10B	86.29 (16)	Pb1A—S8A—Sb6B^v	150.63 (17)
S10B—Sb6A—Sb5A^v	57.99 (11)	Pb1A—S8A—Sb9A^iii	147.1 (2)
S10B—Sb6A—Sb5A	135.90 (13)	Pb4A—S8A—Pb1A	79.91 (14)
S10B—Sb6A—Pb5A^v	57.99 (11)	Pb4A—S8A—Sb4A	25.05 (17)
S10B—Sb6A—Pb6B^i	131.00 (13)	Pb4A—S8A—Ag4B^i	53.51 (13)
S10B—Sb6A—Sb6B^i	131.00 (13)	Pb4A—S8A—Ag4B'^i	43.4 (7)
S10B—Sb6A—S9B^v	103.26 (15)	Pb4A—S8A—Pb6B^v	129.28 (16)
Sb5A^v—Pb6B—Pb6A^ii	125.04 (4)	Pb4A—S8A—Sb6B^v	129.28 (16)
Pb5A^v—Pb6B—Sb5A^v	0.0	Pb4A—S8A—Sb9A^iii	67.23 (12)
Pb5A^v—Pb6B—Pb6A^ii	125.04 (4)	Sb4A—S8A—Ag4B^i	77.8 (2)
Sb5B^vi—Pb6B—Sb5A^v	63.51 (4)	Sb4A—S8A—Ag4B'^i	67.7 (7)
Sb5B^vi—Pb6B—Pb5A^v	63.51 (4)	Sb4A—S8A—Pb6B^v	118.9 (2)
Sb5B^vi—Pb6B—Pb6A^ii	61.74 (4)	Sb4A—S8A—Sb6B^v	118.9 (2)
Sb5B^vi—Pb6B—Sb9A^vii	71.24 (4)	Ag4B'^i—S8A—Ag4B^i	10.1 (7)
Pb5B^vi—Pb6B—Sb5A^v	63.51 (4)	Sb5A—S8A—Pb1A	93.36 (17)
Pb5B^vi—Pb6B—Pb5A^v	63.51 (4)	Sb5A—S8A—Pb4A	123.8 (2)
Pb5B^vi—Pb6B—Sb5B^vi	0.0	Sb5A—S8A—Sb4A	99.4 (3)
Pb5B^vi—Pb6B—Pb6A^ii	61.74 (4)	Sb5A—S8A—Ag4B^i	177.2 (2)
Pb5B^vi—Pb6B—Sb9A^vii	71.24 (4)	Sb5A—S8A—Ag4B'^i	167.1 (7)
Sb9A^vii—Pb6B—Sb5A^v	74.14 (4)	Sb5A—S8A—Pb6B^v	68.68 (13)
Sb9A^vii—Pb6B—Pb5A^v	74.14 (4)	Sb5A—S8A—Sb6B^v	68.68 (13)
Sb9A^vii—Pb6B—Pb6A^ii	92.65 (4)	Sb5A—S8A—Sb9A^iii	105.26 (19)
S5B—Pb6B—Sb5A^v	141.53 (14)	Sb5B^i—S8A—Pb1A	98.29 (19)
S5B—Pb6B—Pb5A^v	141.53 (14)	Sb5B^i—S8A—Pb4A	130.1 (2)
S5B—Pb6B—Sb5B^vi	142.73 (14)	Sb5B^i—S8A—Sb4A	153.7 (3)
S5B—Pb6B—Pb5B^vi	142.73 (14)	Sb5B^i—S8A—Ag4B^i	76.57 (18)
S5B—Pb6B—Pb6A^ii	89.17 (14)	Sb5B^i—S8A—Ag4B'^i	86.7 (7)
S5B—Pb6B—Sb9A^vii	88.72 (12)	Sb5B^i—S8A—Sb5A	106.1 (2)
S5B—Pb6B—S9A^ii	87.03 (18)	Sb5B^i—S8A—Pb6B^v	66.84 (14)
S5B—Pb6B—S9A^v	162.13 (16)	Sb5B^i—S8A—Sb6B^v	66.84 (14)
S5B—Pb6B—S9B	87.70 (18)	Sb5B^i—S8A—Sb9A^iii	102.1 (2)
S5B—Pb6B—S10A^ii	85.22 (17)	Pb5B^i—S8A—Pb1A	98.29 (19)
S5B—Pb6B—S10B	84.90 (18)	Pb5B^i—S8A—Pb4A	130.1 (2)
S9A^v—Pb6B—Sb5A^v	43.90 (12)	Pb5B^i—S8A—Sb4A	153.7 (3)
S9A^ii—Pb6B—Sb5A^v	130.49 (12)	Pb5B^i—S8A—Ag4B^i	76.57 (18)
S9A^ii—Pb6B—Pb5A^v	130.49 (12)	Pb5B^i—S8A—Ag4B'^i	86.7 (7)
S9A^v—Pb6B—Pb5A^v	43.90 (12)	Pb5B^i—S8A—Sb5A	106.1 (2)
S9A^ii—Pb6B—Sb5B^vi	82.49 (12)	Pb5B^i—S8A—Sb5B^i	0.0
S9A^v—Pb6B—Sb5B^vi	52.70 (11)	Pb5B^i—S8A—Pb6B^v	66.84 (14)
S9A^ii—Pb6B—Pb5B^vi	82.49 (12)	Pb5B^i—S8A—Sb6B^v	66.84 (14)
S9A^v—Pb6B—Pb5B^vi	52.70 (11)	Pb5B^i—S8A—Sb9A^iii	102.1 (2)
S9A^ii—Pb6B—Pb6A^ii	36.76 (12)	Pb6B^v—S8A—Ag4B^i	112.22 (15)
S9A^v—Pb6B—Pb6A^ii	96.18 (12)	Pb6B^v—S8A—Ag4B'^i	116.6 (6)
S9A^ii—Pb6B—Sb9A^vii	129.23 (13)	Sb6B^v—S8A—Ag4B^i	112.22 (15)
S9A^v—Pb6B—Sb9A^vii	107.98 (11)	Sb6B^v—S8A—Ag4B'^i	116.6 (6)
S9A^ii—Pb6B—S9A^v	87.13 (18)	Sb6B^v—S8A—Pb6B^v	0.0
S9B—Pb6B—Sb5A^v	78.01 (13)	Sb9A^iii—S8A—Sb4A	64.66 (18)
S9B—Pb6B—Pb5A^v	78.01 (13)	Sb9A^iii—S8A—Ag4B^i	73.28 (13)
S9B—Pb6B—Sb5B^vi	129.38 (13)	Sb9A^iii—S8A—Ag4B'^i	69.7 (6)
S9B—Pb6B—Pb5B^vi	129.38 (13)	Sb9A^iii—S8A—Pb6B^v	62.19 (10)
S9B—Pb6B—Pb6A^ii	137.74 (14)	Sb9A^iii—S8A—Sb6B^v	62.19 (10)
S9B—Pb6B—Sb9A^vii	129.37 (14)	Pb1B—S8B—Sb4A	88.6 (2)
S9B—Pb6B—S9A^v	76.87 (16)	Pb1B—S8B—Ag4B'	84.8 (8)
S9B—Pb6B—S9A^ii	100.98 (17)	Pb1B—S8B—Sb6A^v	146.72 (18)
S9B—Pb6B—S10A^ii	167.53 (17)	Pb1B—S8B—Pb6A^v	146.72 (18)
S10A^ii—Pb6B—Sb5A^v	101.42 (13)	Pb1B—S8B—Sb9A^iv	124.63 (18)
S10A^ii—Pb6B—Pb5A^v	101.42 (13)	Pb1B—S8B—Sb9B^iv	144.4 (2)
S10A^ii—Pb6B—Sb5B^vi	59.02 (12)	Sb4A—S8B—Sb6A^v	113.1 (2)
S10A^ii—Pb6B—Pb5B^vi	59.02 (12)	Sb4A—S8B—Pb6A^v	113.1 (2)
S10A^ii—Pb6B—Pb6A^ii	52.50 (13)	Sb4A—S8B—Sb9A^iv	105.11 (18)
S10A^ii—Pb6B—Sb9A^vii	40.33 (13)	Ag4B—S8B—Pb1B	83.78 (18)
S10A^ii—Pb6B—S9A^ii	88.91 (18)	Ag4B—S8B—Sb4A	50.0 (2)
S10A^ii—Pb6B—S9A^v	111.54 (15)	Ag4B—S8B—Ag4B'	8.3 (9)
S10B—Pb6B—Sb5A^v	59.57 (12)	Ag4B—S8B—Sb6A^v	129.46 (19)
S10B—Pb6B—Pb5A^v	59.57 (12)	Ag4B—S8B—Pb6A^v	129.46 (19)
S10B—Pb6B—Sb5B^vi	97.93 (13)	Ag4B—S8B—Sb9A^iv	67.84 (18)
S10B—Pb6B—Pb5B^vi	97.93 (13)	Ag4B—S8B—Sb9B^iv	62.34 (14)
S10B—Pb6B—Pb6A^ii	132.85 (13)	Ag4B'—S8B—Sb4A	58.2 (10)
S10B—Pb6B—Sb9A^vii	40.61 (13)	Ag4B'—S8B—Sb6A^v	127.8 (8)
S10B—Pb6B—S9A^v	103.47 (17)	Ag4B'—S8B—Pb6A^v	127.8 (8)
S10B—Pb6B—S9A^ii	167.07 (18)	Ag4B'—S8B—Sb9A^iv	61.1 (9)
S10B—Pb6B—S9B	88.78 (19)	Sb5A—S8B—Pb1B	94.64 (18)
S10B—Pb6B—S10A^ii	80.38 (18)	Sb5A—S8B—Sb4A	88.3 (2)
Pb7B^i—Pb7A—Pb7B	178.97 (4)	Sb5A—S8B—Ag4B	138.2 (3)
Pb7B^i—Pb7A—Sb9B^viii	120.28 (4)	Sb5A—S8B—Ag4B'	146.5 (10)
Pb7B—Pb7A—Sb9B^viii	60.16 (3)	Sb5A—S8B—Sb6A^v	62.78 (12)
Sb9A^viii—Pb7A—Pb7B^i	60.06 (3)	Sb5A—S8B—Pb6A^v	62.78 (12)
Sb9A^viii—Pb7A—Pb7B	120.29 (4)	Sb5A—S8B—Sb9A^iv	138.06 (19)
Sb9A^viii—Pb7A—Sb9B^viii	60.38 (4)	Sb5A—S8B—Sb9B^iv	103.24 (19)
Ag12A^ix—Pb7A—Pb7B	90.65 (6)	Sb5B—S8B—Pb1B	96.40 (19)
Ag12A^ix—Pb7A—Pb7B^i	89.53 (6)	Sb5B—S8B—Sb4A	168.8 (3)
Ag12A^ix—Pb7A—Sb9A^viii	138.01 (6)	Sb5B—S8B—Ag4B	120.5 (3)
Ag12A^ix—Pb7A—Sb9B^viii	135.36 (6)	Sb5B—S8B—Ag4B'	112.2 (10)
S5A—Pb7A—Pb7B^i	133.88 (12)	Sb5B—S8B—Sb5A	101.2 (2)
S5A—Pb7A—Pb7B	45.10 (11)	Sb5B—S8B—Sb6A^v	67.18 (14)
S5A—Pb7A—Sb9A^viii	119.90 (11)	Sb5B—S8B—Pb6A^v	67.18 (14)
S5A—Pb7A—Sb9B^viii	81.40 (12)	Sb5B—S8B—Sb9A^iv	63.86 (14)
S5A—Pb7A—Ag12A^ix	101.98 (12)	Sb5B—S8B—Sb9B^iv	109.7 (2)
S5A—Pb7A—S5B^i	86.64 (17)	Sb6A^v—S8B—Sb9A^iv	75.49 (10)
S5A—Pb7A—S6A^viii	157.42 (15)	Pb6A^v—S8B—Sb6A^v	0.0
S5A—Pb7A—S11A	70.17 (17)	Pb6A^v—S8B—Sb9A^iv	75.49 (10)
S5A—Pb7A—S13B^viii	129.00 (17)	Sb9B^iv—S8B—Sb4A	61.80 (16)
S5B^i—Pb7A—Pb7B	131.65 (12)	Sb9B^iv—S8B—Ag4B'	63.4 (8)
S5B^i—Pb7A—Pb7B^i	47.33 (12)	Sb9B^iv—S8B—Sb6A^v	68.25 (11)
S5B^i—Pb7A—Sb9A^viii	82.19 (12)	Sb9B^iv—S8B—Pb6A^v	68.25 (11)
S5B^i—Pb7A—Sb9B^viii	126.24 (11)	Sb9B^iv—S8B—Sb9A^iv	54.21 (9)
S5B^i—Pb7A—Ag12A^ix	98.37 (12)	Pb2A—S9A—Sb5B^v	137.60 (18)
S5B^i—Pb7A—S6A^viii	92.19 (16)	Pb2A—S9A—Sb5B^i	88.89 (16)
S5B^i—Pb7A—S11A	72.61 (17)	Pb2A—S9A—Pb5B^i	88.89 (16)
S5B^i—Pb7A—S13B^viii	123.78 (17)	Pb2A—S9A—Pb6B^v	157.5 (2)
S6A^viii—Pb7A—Pb7B^i	48.16 (11)	Pb2A—S9A—Sb6B^v	157.5 (2)
S6A^viii—Pb7A—Pb7B	132.77 (11)	Sb5A—S9A—Pb2A	94.35 (19)
S6A^viii—Pb7A—Sb9A^viii	37.87 (11)	Sb5A—S9A—Sb5B^i	84.82 (16)
S6A^viii—Pb7A—Sb9B^viii	81.17 (11)	Sb5A—S9A—Sb5B^v	122.34 (18)
S6A^viii—Pb7A—Ag12A^ix	100.50 (12)	Sb5A—S9A—Pb5B^i	84.82 (16)
S6A^viii—Pb7A—S11A	130.80 (17)	Sb5A—S9A—Pb6B^v	77.65 (14)
S6A^viii—Pb7A—S13B^viii	69.43 (16)	Sb5A—S9A—Pb6B^i	167.5 (2)
S6B^viii—Pb7A—Pb7B^i	134.46 (13)	Sb5A—S9A—Sb6B^i	167.5 (2)
S6B^viii—Pb7A—Pb7B	46.49 (13)	Sb5A—S9A—Sb6B^v	77.65 (14)
S6B^viii—Pb7A—Sb9A^viii	85.64 (12)	Sb5B^i—S9A—Sb5B^v	112.89 (17)
S6B^viii—Pb7A—Sb9B^viii	35.74 (11)	Sb5B^i—S9A—Pb6B^v	69.60 (12)
S6B^viii—Pb7A—Ag12A^ix	99.62 (12)	Sb5B^i—S9A—Sb6B^v	69.60 (12)
S6B^viii—Pb7A—S5A	87.88 (17)	Pb5B^i—S9A—Sb5B^v	112.9
S6B^viii—Pb7A—S5B^i	161.91 (15)	Pb5B^i—S9A—Sb5B^i	0.0
S6B^viii—Pb7A—S6A^viii	86.31 (17)	Pb5B^i—S9A—Pb6B^v	69.60 (12)
S6B^viii—Pb7A—S11A	121.36 (18)	Pb5B^i—S9A—Sb6B^v	69.60 (12)
S6B^viii—Pb7A—S13B^viii	72.42 (17)	Sb6A—S9A—Pb2A	97.55 (19)
S10A—Pb7A—Pb7B	92.63 (13)	Sb6A—S9A—Sb5A	92.8 (2)
S10A—Pb7A—Pb7B^i	87.21 (13)	Sb6A—S9A—Sb5B^i	173.3 (2)
S10A—Pb7A—Sb9A^viii	38.80 (13)	Sb6A—S9A—Sb5B^v	63.24 (14)
S10A—Pb7A—Sb9B^viii	46.23 (13)	Sb6A—S9A—Pb5B^i	173.3 (2)
S10A—Pb7A—Ag12A^ix	176.55 (15)	Sb6A—S9A—Pb6B^i	97.4 (2)
S10A—Pb7A—S5A	81.14 (17)	Sb6A—S9A—Pb6B^v	103.78 (19)
S10A—Pb7A—S5B^i	80.24 (17)	Sb6A—S9A—Sb6B^v	103.78 (19)
S10A—Pb7A—S6A^viii	76.45 (17)	Sb6A—S9A—Sb6B^i	97.4 (2)
S10A—Pb7A—S6B^viii	81.89 (16)	Pb6B^i—S9A—Pb2A	91.43 (17)
S10A—Pb7A—S11A	141.11 (17)	Pb6B^i—S9A—Sb5B^i	84.22 (18)
S10A—Pb7A—S13B^viii	138.04 (17)	Pb6B^i—S9A—Sb5B^v	57.45 (11)
S11A—Pb7A—Pb7B	85.44 (14)	Pb6B^v—S9A—Sb5B^v	61.14 (10)
S11A—Pb7A—Pb7B^i	94.05 (13)	Pb6B^i—S9A—Pb5B^i	84.22 (18)
S11A—Pb7A—Sb9A^viii	152.53 (14)	Pb6B^i—S9A—Pb6B^v	92.87 (18)
S11A—Pb7A—Sb9B^viii	145.33 (14)	Pb6B^i—S9A—Sb6B^v	92.87 (18)
S11A—Pb7A—Ag12A^ix	40.30 (12)	Sb6B^i—S9A—Pb2A	91.43 (17)
S11A—Pb7A—S13B^viii	80.81 (16)	Sb6B^v—S9A—Sb5B^v	61.14 (10)
S13B^viii—Pb7A—Pb7B^i	87.79 (13)	Sb6B^i—S9A—Sb5B^i	84.22 (18)
S13B^viii—Pb7A—Pb7B	93.00 (13)	Sb6B^i—S9A—Sb5B^v	57.45 (11)
S13B^viii—Pb7A—Sb9A^viii	105.28 (12)	Sb6B^i—S9A—Pb5B^i	84.22 (18)
S13B^viii—Pb7A—Sb9B^viii	103.59 (13)	Sb6B^i—S9A—Pb6B^v	92.9
S13B^viii—Pb7A—Ag12A^ix	40.56 (13)	Sb6B^i—S9A—Pb6B^i	0.0
Pb7A^ii—Pb7B—Pb7A	178.97 (4)	Sb6B^v—S9A—Pb6B^v	0.0
Pb7A^ii—Pb7B—Sb9B^viii	119.40 (4)	Sb6B^i—S9A—Sb6B^v	92.87 (18)
Pb7A—Pb7B—Sb9B^viii	60.16 (3)	Pb2B—S9B—Pb5A^v	140.75 (17)
Sb9A^vii—Pb7B—Pb7A^ii	59.28 (3)	Pb2B—S9B—Sb5B	88.13 (17)
Sb9A^vii—Pb7B—Pb7A	120.36 (4)	Pb2B—S9B—Sb6A^v	161.4 (2)
Sb9A^vii—Pb7B—Sb9B^viii	60.36 (4)	Pb2B—S9B—Pb6A^v	161.4 (2)
Ag12B^x—Pb7B—Pb7A	89.50 (5)	Sb5A—S9B—Pb2B	93.14 (17)
Ag12B^x—Pb7B—Pb7A^ii	90.29 (5)	Sb5A—S9B—Pb5A^v	118.9
Ag12B^x—Pb7B—Sb9A^vii	137.21 (5)	Sb5A—S9B—Sb5B	82.37 (15)
Ag12B^x—Pb7B—Sb9B^viii	133.61 (5)	Sb5A—S9B—Sb6A^v	76.32 (14)
S5A—Pb7B—Pb7A	45.93 (12)	Sb5A—S9B—Pb6A^v	76.32 (14)
S5A—Pb7B—Pb7A^ii	135.09 (12)	Sb5A—S9B—Pb6B	167.7 (2)
S5A—Pb7B—Sb9A^vii	120.52 (11)	Sb5B—S9B—Pb5A^v	116.39 (17)
S5A—Pb7B—Sb9B^viii	81.87 (12)	Sb5B—S9B—Sb6A^v	75.40 (13)
S5A—Pb7B—Ag12B^x	102.25 (12)	Sb5B—S9B—Pb6A^v	75.40 (13)
S5A—Pb7B—S5B	87.80 (17)	Sb6A—S9B—Pb2B	97.24 (19)
S5A—Pb7B—S6A^vii	157.56 (15)	Sb6A—S9B—Sb5A	91.5 (2)
S5A—Pb7B—S6B^viii	88.05 (17)	Sb6A^v—S9B—Pb5A^v	56.98 (9)
S5A—Pb7B—S11B	72.55 (16)	Sb6A—S9B—Pb5A^v	62.40 (14)
S5A—Pb7B—S13A^vii	127.98 (16)	Sb6A—S9B—Sb5B	172.0 (3)
S5B—Pb7B—Pb7A^ii	47.39 (12)	Sb6A—S9B—Sb6A^v	98.3 (2)
S5B—Pb7B—Pb7A	133.64 (12)	Sb6A—S9B—Pb6A^v	98.3
S5B—Pb7B—Sb9A^vii	81.68 (11)	Sb6A—S9B—Pb6B	99.3 (2)
S5B—Pb7B—Sb9B^viii	126.52 (12)	Pb6A^v—S9B—Pb5A^v	56.98 (9)
S5B—Pb7B—Ag12B^x	99.87 (12)	Pb6A^v—S9B—Sb6A^v	0.0
S5B—Pb7B—S6A^vii	91.62 (16)	Pb6B—S9B—Pb2B	91.45 (17)
S5B—Pb7B—S6B^viii	162.35 (15)	Pb6B—S9B—Pb5A^v	62.27 (11)
S5B—Pb7B—S11B	71.94 (16)	Pb6B—S9B—Sb5B	86.39 (18)
S5B—Pb7B—S13A^vii	125.34 (17)	Pb6B—S9B—Sb6A^v	96.07 (17)
S6A^vii—Pb7B—Pb7A^ii	47.49 (12)	Pb6B—S9B—Pb6A^v	96.07 (17)
S6A^vii—Pb7B—Pb7A	131.57 (12)	Ag4B^v—S10A—Ag4B'^v	9.0 (6)
S6A^vii—Pb7B—Sb9A^vii	37.51 (11)	Ag4B^v—S10A—Pb7B^i	128.74 (16)
S6A^vii—Pb7B—Sb9B^viii	80.50 (12)	Sb5B^v—S10A—Ag4B^v	65.59 (11)
S6A^vii—Pb7B—Ag12B^x	99.94 (11)	Sb5B^v—S10A—Ag4B'^v	69.5 (5)
S6A^vii—Pb7B—S11B	128.37 (17)	Sb5B^v—S10A—Pb7B^i	125.39 (16)
S6A^vii—Pb7B—S13A^vii	69.44 (15)	Pb5B^v—S10A—Ag4B^v	65.59 (11)
S6B^viii—Pb7B—Pb7A^ii	133.22 (12)	Pb5B^v—S10A—Ag4B'^v	69.5 (5)
S6B^viii—Pb7B—Pb7A	45.84 (12)	Pb5B^v—S10A—Sb5B^v	0.0
S6B^viii—Pb7B—Sb9A^vii	85.69 (11)	Pb5B^v—S10A—Pb7B^i	125.39 (16)
S6B^viii—Pb7B—Sb9B^viii	35.84 (11)	Sb6A—S10A—Ag4B^v	106.50 (17)
S6B^viii—Pb7B—Ag12B^x	97.78 (11)	Sb6A—S10A—Ag4B'^v	115.5 (7)
S6B^viii—Pb7B—S6A^vii	85.75 (17)	Sb6A—S10A—Sb5B^v	75.02 (13)
S6B^viii—Pb7B—S11B	122.84 (17)	Sb6A—S10A—Pb5B^v	75.02 (13)
S6B^viii—Pb7B—S13A^vii	69.87 (15)	Sb6A—S10A—Pb7B^i	124.75 (16)
S10B—Pb7B—Pb7A^ii	86.08 (14)	Pb6B^i—S10A—Ag4B^v	134.51 (18)
S10B—Pb7B—Pb7A	94.09 (14)	Pb6B^i—S10A—Ag4B'^v	132.6 (6)
S10B—Pb7B—Sb9A^vii	38.61 (13)	Pb6B^i—S10A—Sb5B^v	74.75 (13)
S10B—Pb7B—Sb9B^viii	47.39 (14)	Pb6B^i—S10A—Pb5B^v	74.75 (13)
S10B—Pb7B—Ag12B^x	175.75 (14)	Pb6B^i—S10A—Sb6A	82.79 (15)
S10B—Pb7B—S5A	81.91 (17)	Pb6B^i—S10A—Pb7B^i	60.95 (11)
S10B—Pb7B—S5B	79.28 (17)	Pb6B^i—S10A—Sb9B^viii	170.0 (2)
S10B—Pb7B—S6A^vii	75.96 (17)	Sb6B^i—S10A—Ag4B^v	134.51 (18)
S10B—Pb7B—S6B^viii	83.15 (17)	Sb6B^i—S10A—Ag4B'^v	132.6 (6)
S10B—Pb7B—S11B	141.78 (17)	Sb6B^i—S10A—Sb5B^v	74.75 (13)
S10B—Pb7B—S13A^vii	137.03 (16)	Sb6B^i—S10A—Pb5B^v	74.75 (13)
S11B—Pb7B—Pb7A	88.22 (13)	Sb6B^i—S10A—Sb6A	82.79 (15)
S11B—Pb7B—Pb7A^ii	92.27 (13)	Sb6B^i—S10A—Pb6B^i	0.0
S11B—Pb7B—Sb9A^vii	150.38 (14)	Sb6B^i—S10A—Pb7B^i	60.95 (11)
S11B—Pb7B—Sb9B^viii	148.19 (13)	Sb6B^i—S10A—Sb9B^viii	170.0 (2)
S11B—Pb7B—Ag12B^x	40.50 (11)	Pb7A—S10A—Ag4B^v	127.52 (18)
S11B—Pb7B—S13A^vii	80.99 (15)	Pb7A—S10A—Ag4B'^v	125.0 (5)
S13A^vii—Pb7B—Pb7A	90.40 (12)	Pb7A—S10A—Sb5B^v	163.8 (2)
S13A^vii—Pb7B—Pb7A^ii	88.79 (12)	Pb7A—S10A—Pb5B^v	163.8 (2)
S13A^vii—Pb7B—Sb9A^vii	104.60 (11)	Pb7A—S10A—Sb6A	90.91 (18)
S13A^vii—Pb7B—Sb9B^viii	101.17 (11)	Pb7A—S10A—Pb6B^i	95.90 (18)
S13A^vii—Pb7B—Ag12B^x	40.49 (11)	Pb7A—S10A—Sb6B^i	95.90 (18)
Pb4A^ix—Sb8A—Sb4A^ix	24.70 (16)	Pb7A—S10A—Pb7B^i	56.73 (10)
Pb4A^ix—Sb8A—Cu4B^x	36.6 (6)	Pb7A—S10A—Sb9B^viii	90.71 (17)
Pb4A^ix—Sb8A—Sb8B^i	83.62 (5)	Pb7B^i—S10A—Ag4B'^v	119.7 (6)
Pb4A^ix—Sb8A—Ag12A^ix	70.35 (6)	Sb9A^viii—S10A—Ag4B^v	73.36 (16)
Pb4A^ix—Sb8A—Ag12B^x	72.30 (5)	Sb9A^viii—S10A—Ag4B'^v	64.4 (7)
Pb4A^ix—Sb8A—S7A^ix	42.57 (13)	Sb9A^viii—S10A—Sb5B^v	97.39 (19)
Sb4A^ix—Sb8A—Cu4B^x	60.9 (6)	Sb9A^viii—S10A—Pb5B^v	97.39 (19)
Sb4A^ix—Sb8A—Sb8B^i	59.08 (16)	Sb9A^viii—S10A—Sb6A	171.3 (2)
Sb4A^ix—Sb8A—Ag12A^ix	60.51 (16)	Sb9A^viii—S10A—Pb6B^i	91.2 (2)
Sb4A^ix—Sb8A—Ag12B^x	90.24 (16)	Sb9A^viii—S10A—Sb6B^i	91.2 (2)
Cu4B^x—Sb8A—Sb8B^i	120.0 (6)	Sb9A^viii—S10A—Pb7A	95.96 (19)
Cu4B^x—Sb8A—Ag12A^ix	95.8 (5)	Sb9A^viii—S10A—Pb7B^i	56.23 (12)
Ag12A^ix—Sb8A—Sb8B^i	55.42 (6)	Sb9A^viii—S10A—Sb9B^viii	95.59 (19)
Ag12B^x—Sb8A—Cu4B^x	57.1 (5)	Sb9B^viii—S10A—Ag4B^v	42.08 (10)
Ag12B^x—Sb8A—Sb8B^i	123.82 (7)	Sb9B^viii—S10A—Ag4B'^v	46.0 (6)
Ag12B^x—Sb8A—Ag12A^ix	68.70 (7)	Sb9B^viii—S10A—Sb5B^v	97.03 (16)
S2A—Sb8A—Pb4A^ix	140.18 (15)	Sb9B^viii—S10A—Pb5B^v	97.03 (16)
S2A—Sb8A—Sb4A^ix	129.3 (2)	Sb9B^viii—S10A—Sb6A	89.59 (17)
S2A—Sb8A—Cu4B^x	128.5 (5)	Sb9B^viii—S10A—Pb7B^i	129.07 (16)
S2A—Sb8A—Sb8B^i	90.01 (16)	Sb4A^v—S10B—Pb4A^v	17.37 (13)
S2A—Sb8A—Ag12A^ix	134.84 (17)	Sb4A^v—S10B—Pb7A^ii	108.93 (18)
S2A—Sb8A—Ag12B^x	139.21 (16)	Sb5A^v—S10B—Pb4A^v	69.90 (10)
S2A—Sb8A—S7A^ix	175.0 (2)	Sb5A^v—S10B—Sb4A^v	70.88 (15)
S2A—Sb8A—S11A	95.0 (2)	Sb5A^v—S10B—Pb7A^ii	130.57 (17)
S2A—Sb8A—S11B	95.7 (2)	Pb5A^v—S10B—Pb4A^v	69.90 (10)
S2A—Sb8A—S12A	88.12 (19)	Pb5A^v—S10B—Sb4A^v	70.88 (15)
S2A—Sb8A—S12B	91.11 (19)	Pb5A^v—S10B—Sb5A^v	0.0
S7A^ix—Sb8A—Sb4A^ix	50.8 (2)	Pb5A^v—S10B—Pb7A^ii	130.57 (17)
S7A^ix—Sb8A—Cu4B^x	56.5 (5)	Sb6A—S10B—Pb4A^v	134.74 (16)
S7A^ix—Sb8A—Sb8B^i	86.17 (15)	Sb6A—S10B—Sb4A^v	124.4 (2)
S7A^ix—Sb8A—Ag12A^ix	40.13 (14)	Sb6A—S10B—Sb5A^v	70.56 (12)
S7A^ix—Sb8A—Ag12B^x	42.56 (15)	Sb6A—S10B—Pb5A^v	70.56 (12)
S11A—Sb8A—Pb4A^ix	105.82 (16)	Sb6A—S10B—Pb7A^ii	126.57 (17)
S11A—Sb8A—Sb4A^ix	87.3 (2)	Pb6B—S10B—Pb4A^v	107.33 (16)
S11A—Sb8A—Cu4B^x	135.9 (5)	Pb6B—S10B—Sb4A^v	123.3 (2)
S11A—Sb8A—Sb8B^i	42.42 (16)	Pb6B—S10B—Sb5A^v	76.74 (14)
S11A—Sb8A—Ag12A^ix	40.08 (16)	Pb6B—S10B—Pb5A^v	76.74 (14)
S11A—Sb8A—Ag12B^x	96.66 (17)	Pb6B—S10B—Sb6A	83.91 (16)
S11A—Sb8A—S7A^ix	79.9 (2)	Pb6B—S10B—Pb7A^ii	62.29 (12)
S11A—Sb8A—S12A	83.7 (2)	Pb6B—S10B—Sb9B^viii	169.5 (2)
S11A—Sb8A—S12B	171.8 (2)	Pb7A^ii—S10B—Pb4A^v	96.08 (11)
S11B—Sb8A—Pb4A^ix	112.72 (15)	Pb7B—S10B—Pb4A^v	129.36 (18)
S11B—Sb8A—Sb4A^ix	133.7 (2)	Pb7B—S10B—Sb4A^v	126.2 (2)
S11B—Sb8A—Cu4B^x	84.1 (6)	Pb7B—S10B—Sb5A^v	160.5 (2)
S11B—Sb8A—Sb8B^i	143.06 (17)	Pb7B—S10B—Pb5A^v	160.5 (2)
S11B—Sb8A—Ag12A^ix	97.55 (16)	Pb7B—S10B—Sb6A	90.44 (17)
S11B—Sb8A—Ag12B^x	43.71 (14)	Pb7B—S10B—Pb6B	97.35 (19)
S11B—Sb8A—S7A^ix	85.4 (2)	Pb7B—S10B—Pb7A^ii	57.71 (11)
S11B—Sb8A—S11A	100.7 (2)	Pb7B—S10B—Sb9B^viii	89.94 (17)
S11B—Sb8A—S12A	173.88 (19)	Sb9A^vii—S10B—Pb4A^v	40.00 (10)
S11B—Sb8A—S12B	84.2 (2)	Sb9A^vii—S10B—Sb4A^v	52.49 (17)
S12A—Sb8A—Pb4A^ix	61.67 (11)	Sb9A^vii—S10B—Sb5A^v	101.63 (18)
S12A—Sb8A—Sb4A^ix	41.70 (18)	Sb9A^vii—S10B—Pb5A^v	101.63 (18)
S12A—Sb8A—Cu4B^x	89.8 (6)	Sb9A^vii—S10B—Sb6A	171.9 (2)
S12A—Sb8A—Sb8B^i	41.38 (12)	Sb9A^vii—S10B—Pb6B	92.3 (2)
S12A—Sb8A—Ag12A^ix	83.00 (13)	Sb9A^vii—S10B—Pb7A^ii	56.65 (12)
S12A—Sb8A—Ag12B^x	131.94 (12)	Sb9A^vii—S10B—Pb7B	97.15 (19)
S12A—Sb8A—S7A^ix	91.17 (18)	Sb9A^vii—S10B—Sb9B^viii	94.3 (2)
S12A—Sb8A—S12B	91.00 (16)	Sb9B^viii—S10B—Pb4A^v	73.12 (12)
S12B—Sb8A—Pb4A^ix	66.01 (12)	Sb9B^viii—S10B—Sb4A^v	56.10 (16)
S12B—Sb8A—Sb4A^ix	84.6 (2)	Sb9B^viii—S10B—Sb5A^v	93.92 (16)
S12B—Sb8A—Cu4B^x	37.4 (5)	Sb9B^viii—S10B—Pb5A^v	93.92 (16)
S12B—Sb8A—Sb8B^i	132.30 (13)	Sb9B^viii—S10B—Sb6A	88.57 (17)
S12B—Sb8A—Ag12A^ix	133.05 (13)	Sb9B^viii—S10B—Pb7A^ii	128.16 (17)
S12B—Sb8A—Ag12B^x	82.15 (14)	Pb2A—S11A—Pb2B	55.13 (10)
S12B—Sb8A—S7A^ix	93.89 (18)	Pb2A—S11A—Pb3A	61.81 (11)
Sb4A^x—Sb8B—Sb9B	60.75 (14)	Pb2A—S11A—Pb4A^ix	136.60 (19)
Ag4B^x—Sb8B—Sb4A^x	50.26 (19)	Pb2A—S11A—Sb4A^ix	134.7 (2)
Ag4B^x—Sb8B—Cu4B^x	23.7 (6)	Pb2A—S11A—Pb7B	88.64 (14)
Ag4B^x—Sb8B—Sb9B	53.02 (8)	Pb2A—S11A—Ag12B^x	126.16 (19)
Ag4B^x—Sb8B—Ag12A^x	82.17 (10)	Pb2A—S11A—Ag12B^ix	116.33 (18)
Cu4B^x—Sb8B—Sb4A^x	74.0 (6)	Pb3A—S11A—Pb2B	74.20 (9)
Cu4B^x—Sb8B—Sb9B	59.9 (5)	Pb3A—S11A—Pb7B	122.42 (14)
Ag4B'^x—Sb8B—Sb4A^x	62.5 (10)	Pb3A—S11A—Ag12B^ix	107.26 (13)
Ag4B'^x—Sb8B—Ag4B^x	13.1 (9)	Pb4A^ix—S11A—Pb2B	99.74 (13)
Ag4B'^x—Sb8B—Cu4B^x	12.9 (9)	Pb4A^ix—S11A—Pb3A	78.32 (10)
Ag4B'^x—Sb8B—Sb9B	60.8 (8)	Pb4A^ix—S11A—Pb7B	99.68 (13)
Ag4B'^x—Sb8B—Ag12A^x	84.7 (9)	Pb4A^ix—S11A—Ag12B^ix	90.26 (11)
Ag4B'^x—Sb8B—S7B^x	43.8 (9)	Sb4A^ix—S11A—Pb2B	113.8 (2)
Ag12A^x—Sb8B—Sb4A^x	59.60 (15)	Sb4A^ix—S11A—Pb3A	72.91 (15)
Ag12A^x—Sb8B—Cu4B^x	95.7 (5)	Sb4A^ix—S11A—Pb4A^ix	18.22 (14)
Ag12A^x—Sb8B—Sb9B	119.72 (7)	Sb4A^ix—S11A—Pb7B	117.5 (2)
S2B—Sb8B—Sb4A^x	132.0 (2)	Sb4A^ix—S11A—Ag12B^ix	75.79 (17)
S2B—Sb8B—Ag4B^x	143.68 (17)	Sb4A^ix—S11A—Ag12B^x	70.31 (17)
S2B—Sb8B—Cu4B^x	130.8 (6)	Pb7A—S11A—Pb2A	83.60 (15)
S2B—Sb8B—Ag4B'^x	142.5 (9)	Pb7A—S11A—Pb2B	89.66 (14)
S2B—Sb8B—Sb9B	94.17 (15)	Pb7A—S11A—Pb3A	145.20 (18)
S2B—Sb8B—Ag12A^x	132.83 (16)	Pb7A—S11A—Pb4A^ix	135.64 (19)
S2B—Sb8B—S7B^x	170.3 (2)	Pb7A—S11A—Sb4A^ix	141.5 (2)
S2B—Sb8B—S11A^ii	91.5 (2)	Pb7A—S11A—Pb7B	55.57 (10)
S2B—Sb8B—S11B	89.52 (19)	Pb7A—S11A—Ag12B^ix	83.76 (15)
S2B—Sb8B—S12A^ii	93.3 (2)	Pb7A—S11A—Ag12B^x	90.88 (15)
S2B—Sb8B—S12B	94.6 (2)	Pb7B—S11A—Pb2B	49.10 (7)
S7B^x—Sb8B—Sb4A^x	55.26 (19)	Sb8A—S11A—Pb2A	97.6 (2)
S7B^x—Sb8B—Ag4B^x	44.72 (14)	Sb8A—S11A—Pb2B	56.42 (14)
S7B^x—Sb8B—Cu4B^x	54.2 (6)	Sb8A—S11A—Pb3A	60.49 (14)
S7B^x—Sb8B—Sb9B	95.35 (13)	Sb8A—S11A—Pb4A^ix	44.37 (11)
S7B^x—Sb8B—Ag12A^x	41.63 (13)	Sb8A—S11A—Sb4A^ix	57.44 (18)
S11A^ii—Sb8B—Sb4A^x	79.4 (2)	Sb8A—S11A—Pb7A	133.7 (3)
S11A^ii—Sb8B—Ag4B^x	120.69 (18)	Sb8A—S11A—Pb7B	78.19 (17)
S11A^ii—Sb8B—Cu4B^x	137.6 (6)	Sb8A—S11A—Sb8B^i	100.7 (2)
S11A^ii—Sb8B—Ag4B'^x	125.9 (10)	Sb8A—S11A—Ag12B^x	51.37 (14)
S11A^ii—Sb8B—Sb9B	130.36 (15)	Sb8A—S11A—Ag12B^ix	133.2 (2)
S11A^ii—Sb8B—Ag12A^x	41.89 (14)	Sb8B^i—S11A—Pb2A	92.9 (2)
S11A^ii—Sb8B—S7B^x	83.53 (19)	Sb8B^i—S11A—Pb2B	131.4 (2)
S11A^ii—Sb8B—S11B	101.71 (19)	Sb8B^i—S11A—Pb3A	57.77 (12)
S11B—Sb8B—Sb4A^x	138.51 (19)	Sb8B^i—S11A—Pb4A^ix	78.62 (14)
S11B—Sb8B—Ag4B^x	98.90 (17)	Sb8B^i—S11A—Sb4A^ix	60.81 (18)
S11B—Sb8B—Cu4B^x	78.8 (6)	Sb8B^i—S11A—Pb7A	125.5 (2)
S11B—Sb8B—Ag4B'^x	85.9 (10)	Sb8B^i—S11A—Pb7B	178.3 (2)
S11B—Sb8B—Sb9B	127.58 (13)	Sb8B^i—S11A—Ag12B^x	131.00 (19)
S11B—Sb8B—Ag12A^x	93.37 (13)	Sb8B^i—S11A—Ag12B^ix	49.56 (12)
S11B—Sb8B—S7B^x	83.43 (17)	Ag12A^ix—S11A—Pb2A	163.0 (3)
S12A^ii—Sb8B—Sb4A^x	40.03 (19)	Ag12A^ix—S11A—Pb2B	133.6 (2)
S12A^ii—Sb8B—Ag4B^x	72.75 (17)	Ag12A^ix—S11A—Pb3A	131.2 (2)
S12A^ii—Sb8B—Cu4B^x	91.5 (5)	Ag12A^ix—S11A—Pb4A^ix	60.13 (15)
S12A^ii—Sb8B—Ag4B'^x	85.4 (9)	Ag12A^ix—S11A—Sb4A^ix	59.51 (19)
S12A^ii—Sb8B—Sb9B	41.75 (14)	Ag12A^ix—S11A—Pb7A	82.11 (19)
S12A^ii—Sb8B—Ag12A^x	92.38 (15)	Ag12A^ix—S11A—Pb7B	90.78 (19)
S12A^ii—Sb8B—S7B^x	94.81 (18)	Ag12A^ix—S11A—Sb8A	98.8 (2)
S12A^ii—Sb8B—S11A^ii	88.7 (2)	Ag12A^ix—S11A—Sb8B^i	88.0 (2)
S12A^ii—Sb8B—S11B	169.11 (19)	Ag12A^ix—S11A—Ag12B^x	63.27 (17)
S12A^ii—Sb8B—S12B	82.66 (19)	Ag12A^ix—S11A—Ag12B^ix	52.96 (16)
S12B—Sb8B—Sb4A^x	90.4 (2)	Ag12B^x—S11A—Pb2B	71.39 (10)
S12B—Sb8B—Ag4B^x	51.17 (17)	Ag12B^ix—S11A—Pb2B	169.95 (15)
S12B—Sb8B—Cu4B^x	37.7 (6)	Ag12B^x—S11A—Pb3A	111.82 (14)
S12B—Sb8B—Ag4B'^x	47.9 (9)	Ag12B^x—S11A—Pb4A^ix	52.99 (8)
S12B—Sb8B—Sb9B	40.93 (14)	Ag12B^x—S11A—Pb7B	47.26 (7)
S12B—Sb8B—Ag12A^x	132.53 (15)	Ag12B^ix—S11A—Pb7B	130.31 (14)
S12B—Sb8B—S7B^x	91.54 (19)	Ag12B^x—S11A—Ag12B^ix	116.16 (14)
S12B—Sb8B—S11A^ii	169.7 (2)	Pb2A—S11B—Pb7A	48.72 (6)
S12B—Sb8B—S11B	86.65 (19)	Pb2B—S11B—Pb2A	54.12 (10)
Pb4A^ix—Sb9A—Sb4A^ix	24.34 (16)	Pb2B—S11B—Pb4A^ix	133.73 (16)
Pb4A^ix—Sb9A—Cu4B^x	35.6 (5)	Pb2B—S11B—Ag4B^x	132.34 (18)
Pb4A^ix—Sb9A—Pb6B^xi	122.84 (5)	Pb2B—S11B—Ag4B'^x	136.0 (7)
Pb4A^ix—Sb9A—Sb6B^xi	122.84 (5)	Pb2B—S11B—Pb7A	88.26 (13)
Pb4A^ix—Sb9A—Pb7A^xii	153.86 (6)	Pb2B—S11B—Ag12A^x	116.74 (18)
Sb4A^ix—Sb9A—Cu4B^x	59.1 (6)	Pb2B—S11B—Ag12A^ix	122.07 (18)
Sb4A^ix—Sb9A—Pb6B^xi	122.45 (14)	Pb4A^ix—S11B—Pb2A	94.64 (11)
Sb4A^ix—Sb9A—Sb6B^xi	122.45 (14)	Pb4A^ix—S11B—Pb7A	94.08 (12)
Sb4A^ix—Sb9A—Pb7A^xii	171.79 (14)	Ag4B^x—S11B—Pb2A	132.09 (14)
Cu4B^x—Sb9A—Pb6B^xi	122.5 (5)	Ag4B^x—S11B—Pb4A^ix	43.57 (9)
Cu4B^x—Sb9A—Sb6B^xi	122.5 (5)	Ag4B^x—S11B—Pb7A	133.63 (15)
Cu4B^x—Sb9A—Pb7A^xii	118.3 (5)	Ag4B'^x—S11B—Pb2A	128.4 (8)
Pb6B^xi—Sb9A—Pb7A^xii	65.74 (3)	Ag4B'^x—S11B—Pb4A^ix	37.9 (8)
Sb6B^xi—Sb9A—Pb6B^xi	0.0	Ag4B'^x—S11B—Ag4B^x	6.0 (8)
Sb6B^xi—Sb9A—Pb7A^xii	65.74 (3)	Ag4B'^x—S11B—Pb7A	127.8 (8)
S6A—Sb9A—Pb4A^ix	135.51 (15)	Ag4B'^x—S11B—Ag12A^ix	84.2 (8)
S6A—Sb9A—Sb4A^ix	125.1 (2)	Ag4B'^x—S11B—Ag12A^x	62.2 (8)
S6A—Sb9A—Cu4B^x	123.8 (5)	Pb7B—S11B—Pb2A	87.30 (13)
S6A—Sb9A—Pb6B^xi	101.32 (14)	Pb7B—S11B—Pb2B	83.20 (14)
S6A—Sb9A—Sb6B^xi	101.32 (14)	Pb7B—S11B—Pb4A^ix	133.65 (18)
S6A—Sb9A—Pb7A^xii	48.57 (15)	Pb7B—S11B—Ag4B^x	136.21 (17)
S6A—Sb9A—S8A^ix	170.65 (18)	Pb7B—S11B—Ag4B'^x	136.3 (7)
S6A—Sb9A—S10A^xii	93.5 (2)	Pb7B—S11B—Pb7A	54.07 (10)
S6A—Sb9A—S10B^xi	92.73 (19)	Pb7B—S11B—Ag12A^x	85.00 (13)
S6A—Sb9A—S12A	85.19 (19)	Pb7B—S11B—Ag12A^ix	88.47 (15)
S6A—Sb9A—S12B	88.63 (19)	Sb8A—S11B—Pb2A	56.40 (13)
S8A^ix—Sb9A—Pb4A^ix	53.48 (11)	Sb8A—S11B—Pb2B	96.23 (19)
S8A^ix—Sb9A—Sb4A^ix	61.57 (17)	Sb8A—S11B—Pb4A^ix	40.16 (10)
S8A^ix—Sb9A—Cu4B^x	64.6 (5)	Sb8A—S11B—Ag4B^x	76.50 (16)
S8A^ix—Sb9A—Pb6B^xi	69.49 (11)	Sb8A—S11B—Ag4B'^x	72.3 (8)
S8A^ix—Sb9A—Sb6B^xi	69.49 (11)	Sb8A—S11B—Pb7A	77.86 (17)
S8A^ix—Sb9A—Pb7A^xii	125.41 (12)	Sb8A—S11B—Pb7B	131.9 (3)
S10A^xii—Sb9A—Pb4A^ix	118.67 (15)	Sb8A—S11B—Sb8B	101.6 (2)
S10A^xii—Sb9A—Sb4A^ix	139.6 (2)	Sb8A—S11B—Ag12A^x	134.4 (2)
S10A^xii—Sb9A—Cu4B^x	91.5 (6)	Sb8A—S11B—Ag12A^ix	51.35 (13)
S10A^xii—Sb9A—Pb6B^xi	48.45 (14)	Sb8A—S11B—Ag12B^x	94.1 (2)
S10A^xii—Sb9A—Sb6B^xi	48.45 (14)	Sb8B—S11B—Pb2A	131.94 (17)
S10A^xii—Sb9A—Pb7A^xii	45.24 (13)	Sb8B—S11B—Pb2B	92.98 (18)
S10A^xii—Sb9A—S8A^ix	81.65 (18)	Sb8B—S11B—Pb4A^ix	84.80 (13)
S10A^xii—Sb9A—S10B^xi	94.9 (2)	Sb8B—S11B—Ag4B^x	45.09 (11)
S10A^xii—Sb9A—S12A	178.23 (18)	Sb8B—S11B—Ag4B'^x	50.9 (8)
S10A^xii—Sb9A—S12B	84.57 (19)	Sb8B—S11B—Pb7A	178.71 (18)
S10B^xi—Sb9A—Pb4A^ix	112.47 (15)	Sb8B—S11B—Pb7B	126.5 (2)
S10B^xi—Sb9A—Sb4A^ix	94.4 (2)	Sb8B—S11B—Ag12A^ix	134.70 (18)
S10B^xi—Sb9A—Cu4B^x	142.5 (5)	Sb8B—S11B—Ag12A^x	49.56 (11)
S10B^xi—Sb9A—Pb6B^xi	47.14 (15)	Ag12A^ix—S11B—Pb2A	68.33 (10)
S10B^xi—Sb9A—Sb6B^xi	47.14 (15)	Ag12A^x—S11B—Pb2A	168.84 (14)
S10B^xi—Sb9A—Pb7A^xii	91.37 (15)	Ag12A^x—S11B—Pb4A^ix	96.52 (11)
S10B^xi—Sb9A—S8A^ix	79.77 (17)	Ag12A^ix—S11B—Pb4A^ix	50.61 (7)
S10B^xi—Sb9A—S12A	86.40 (19)	Ag12A^ix—S11B—Ag4B^x	90.14 (12)
S10B^xi—Sb9A—S12B	178.56 (19)	Ag12A^x—S11B—Ag4B^x	58.17 (11)
S12A—Sb9A—Pb4A^ix	61.80 (12)	Ag12A^ix—S11B—Pb7A	44.09 (7)
S12A—Sb9A—Sb4A^ix	41.32 (18)	Ag12A^x—S11B—Pb7A	130.07 (13)
S12A—Sb9A—Cu4B^x	88.2 (5)	Ag12A^ix—S11B—Ag12A^x	119.43 (13)
S12A—Sb9A—Pb6B^xi	132.99 (12)	Ag12B^x—S11B—Pb2A	129.5 (2)
S12A—Sb9A—Sb6B^xi	132.99 (12)	Ag12B^x—S11B—Pb2B	168.4 (2)
S12A—Sb9A—Pb7A^xii	133.58 (12)	Ag12B^x—S11B—Pb4A^ix	57.68 (13)
S12A—Sb9A—S8A^ix	99.79 (16)	Ag12B^x—S11B—Ag4B^x	55.69 (13)
S12B—Sb9A—Pb4A^ix	66.75 (13)	Ag12B^x—S11B—Ag4B'^x	52.9 (7)
S12B—Sb9A—Sb4A^ix	85.2 (2)	Ag12B^x—S11B—Pb7A	88.69 (18)
S12B—Sb9A—Cu4B^x	36.3 (5)	Ag12B^x—S11B—Pb7B	85.95 (17)
S12B—Sb9A—Pb6B^xi	132.09 (14)	Ag12B^x—S11B—Sb8B	90.2 (2)
S12B—Sb9A—Sb6B^xi	132.09 (14)	Ag12B^x—S11B—Ag12A^ix	61.51 (15)
S12B—Sb9A—Pb7A^xii	89.18 (13)	Ag12B^x—S11B—Ag12A^x	57.98 (15)
S12B—Sb9A—S8A^ix	98.83 (17)	Pb3A—S12A—Pb3B^i	54.20 (9)
S12B—Sb9A—S12A	94.18 (17)	Pb3A—S12A—Pb4A^ix	139.5 (2)
Sb4A^x—Sb9B—Sb9A	129.92 (16)	Pb3A—S12A—Ag4B^ix	141.1 (2)
Ag4B^x—Sb9B—Sb4A^x	50.69 (19)	Pb3A—S12A—Ag4B'^ix	132.9 (8)
Ag4B^x—Sb9B—Cu4B^x	23.1 (6)	Pb3A—S12A—Pb7B^xi	59.06 (10)
Ag4B^x—Sb9B—Ag4B'^x	11.8 (8)	Pb3A—S12A—Sb8A	86.36 (15)
Ag4B^x—Sb9B—Sb8B	57.66 (8)	Pb3A—S12A—Ag12A^ix	122.65 (16)
Ag4B^x—Sb9B—Sb9A	79.26 (13)	Pb4A^ix—S12A—Pb3B^i	165.95 (18)
Ag4B^x—Sb9B—S8B^x	50.23 (14)	Pb4A^ix—S12A—Ag4B^ix	79.23 (16)
Cu4B^x—Sb9B—Sb4A^x	72.5 (6)	Pb4A^ix—S12A—Ag4B'^ix	86.7 (7)
Cu4B^x—Sb9B—Sb8B	58.0 (5)	Pb4A^ix—S12A—Pb7B^xi	115.57 (15)
Cu4B^x—Sb9B—Sb9A	57.8 (6)	Pb4A^ix—S12A—Ag12A^ix	60.15 (10)
Ag4B'^x—Sb9B—Sb4A^x	59.0 (9)	Sb4A^ix—S12A—Pb3A	162.2 (4)
Ag4B'^x—Sb9B—Cu4B^x	13.6 (8)	Sb4A^ix—S12A—Pb3B^i	142.9 (3)
Ag4B'^x—Sb9B—Sb8B	51.8 (7)	Sb4A^ix—S12A—Pb4A^ix	23.1 (3)
Ag4B'^x—Sb9B—Sb9A	71.4 (9)	Sb4A^ix—S12A—Ag4B^ix	56.2 (3)
Sb8B—Sb9B—Sb4A^x	59.18 (13)	Sb4A^ix—S12A—Ag4B'^ix	63.6 (8)
Sb8B—Sb9B—Sb9A	95.57 (5)	Sb4A^ix—S12A—Pb7B^xi	123.8 (3)
S6B—Sb9B—Sb4A^x	131.4 (2)	Sb4A^ix—S12A—Sb8A	78.1 (3)
S6B—Sb9B—Ag4B^x	149.65 (19)	Sb4A^ix—S12A—Sb8B^i	95.2 (3)
S6B—Sb9B—Cu4B^x	132.0 (5)	Sb4A^ix—S12A—Sb9A	80.9 (3)
S6B—Sb9B—Ag4B'^x	138.6 (8)	Sb4A^ix—S12A—Sb9B^i	100.7 (3)
S6B—Sb9B—Sb8B	95.83 (14)	Sb4A^ix—S12A—Ag12A^ix	53.1 (2)
S6B—Sb9B—Sb9A	90.07 (16)	Ag4B^ix—S12A—Pb3B^i	86.94 (16)
S6B—Sb9B—S8B^x	156.97 (18)	Ag4B^ix—S12A—Ag4B'^ix	10.5 (6)
S6B—Sb9B—S10A^xii	87.79 (18)	Ag4B^ix—S12A—Pb7B^xi	114.38 (15)
S6B—Sb9B—S10B^xii	88.17 (19)	Ag4B^ix—S12A—Ag12A^ix	67.30 (13)
S6B—Sb9B—S12A^ii	93.6 (2)	Ag4B'^ix—S12A—Pb3B^i	79.3 (7)
S6B—Sb9B—S12B	96.5 (2)	Ag4B'^ix—S12A—Pb7B^xi	117.9 (7)
S8B^x—Sb9B—Sb4A^x	67.01 (17)	Ag4B'^ix—S12A—Ag12A^ix	64.6 (7)
S8B^x—Sb9B—Cu4B^x	61.2 (5)	Pb7B^xi—S12A—Pb3B^i	72.48 (8)
S8B^x—Sb9B—Ag4B'^x	59.3 (7)	Sb8A—S12A—Pb3B^i	123.26 (15)
S8B^x—Sb9B—Sb8B	106.74 (11)	Sb8A—S12A—Pb4A^ix	63.16 (12)
S8B^x—Sb9B—Sb9A	83.36 (12)	Sb8A—S12A—Ag4B^ix	119.49 (19)
S10A^xii—Sb9B—Sb4A^x	140.36 (18)	Sb8A—S12A—Ag4B'^ix	117.9 (7)
S10A^xii—Sb9B—Ag4B^x	99.90 (16)	Sb8A—S12A—Pb7B^xi	123.95 (17)
S10A^xii—Sb9B—Cu4B^x	85.4 (6)	Sb8A—S12A—Ag12A^ix	53.34 (10)
S10A^xii—Sb9B—Ag4B'^x	97.4 (9)	Sb8B^i—S12A—Pb3A	92.45 (17)
S10A^xii—Sb9B—Sb8B	133.06 (14)	Sb8B^i—S12A—Pb3B^i	60.19 (12)
S10A^xii—Sb9B—Sb9A	37.52 (13)	Sb8B^i—S12A—Pb4A^ix	110.4 (2)
S10A^xii—Sb9B—S8B^x	73.57 (16)	Sb8B^i—S12A—Ag4B^ix	63.35 (16)
S10A^xii—Sb9B—S10B^xii	94.97 (17)	Sb8B^i—S12A—Ag4B'^ix	53.3 (7)
S10B^xii—Sb9B—Sb4A^x	82.64 (19)	Sb8B^i—S12A—Pb7B^xi	132.62 (19)
S10B^xii—Sb9B—Ag4B^x	119.93 (17)	Sb8B^i—S12A—Sb8A	86.63 (17)
S10B^xii—Sb9B—Cu4B^x	139.7 (5)	Sb8B^i—S12A—Sb9A	173.6 (2)
S10B^xii—Sb9B—Ag4B'^x	131.8 (8)	Sb8B^i—S12A—Ag12A^ix	51.96 (11)
S10B^xii—Sb9B—Sb8B	131.84 (13)	Sb9A—S12A—Pb3A	89.97 (17)
S10B^xii—Sb9B—Sb9A	132.49 (13)	Sb9A—S12A—Pb3B^i	125.68 (16)
S10B^xii—Sb9B—S8B^x	80.28 (16)	Sb9A—S12A—Pb4A^ix	64.35 (12)
S12A^ii—Sb9B—Sb4A^x	38.66 (18)	Sb9A—S12A—Ag4B^ix	117.52 (19)
S12A^ii—Sb9B—Ag4B^x	77.67 (17)	Sb9A—S12A—Ag4B'^ix	127.9 (7)
S12A^ii—Sb9B—Cu4B^x	91.9 (6)	Sb9A—S12A—Pb7B^xi	53.44 (9)
S12A^ii—Sb9B—Ag4B'^x	79.9 (9)	Sb9A—S12A—Sb8A	87.64 (17)
S12A^ii—Sb9B—Sb8B	44.34 (15)	Sb9A—S12A—Ag12A^ix	121.97 (17)
S12A^ii—Sb9B—Sb9A	139.91 (16)	Sb9B^i—S12A—Pb3A	94.80 (18)
S12A^ii—Sb9B—S8B^x	105.64 (18)	Sb9B^i—S12A—Pb3B^i	58.00 (12)
S12A^ii—Sb9B—S10A^xii	177.2 (2)	Sb9B^i—S12A—Pb4A^ix	115.53 (19)
S12A^ii—Sb9B—S10B^xii	87.56 (19)	Sb9B^i—S12A—Ag4B^ix	59.82 (15)
S12B—Sb9B—Sb4A^x	92.8 (2)	Sb9B^i—S12A—Ag4B'^ix	61.7 (7)
S12B—Sb9B—Ag4B^x	55.1 (2)	Sb9B^i—S12A—Pb7B^xi	56.39 (12)
S12B—Sb9B—Cu4B^x	35.8 (5)	Sb9B^i—S12A—Sb8A	178.7 (2)
S12B—Sb9B—Ag4B'^x	43.3 (8)	Sb9B^i—S12A—Sb8B^i	93.9 (2)
S12B—Sb9B—Sb8B	45.96 (16)	Sb9B^i—S12A—Sb9A	91.76 (18)
S12B—Sb9B—Sb9A	49.67 (16)	Sb9B^i—S12A—Ag12A^ix	126.2 (2)
S12B—Sb9B—S8B^x	95.95 (19)	Ag12A^ix—S12A—Pb3B^i	112.06 (13)
S12B—Sb9B—S10A^xii	87.1 (2)	Ag12A^ix—S12A—Pb7B^xi	175.40 (16)
S12B—Sb9B—S10B^xii	175.0 (2)	Pb3B—S12B—Pb4A^ix	130.6 (2)
S12B—Sb9B—S12A^ii	90.3 (2)	Pb3B—S12B—Sb4A^ix	114.0 (2)
Pb10B^i—Sb10A—Sb10B^i	0.0	Pb3B—S12B—Sb4A^x	123.0 (2)
Sb11A^xiii—Sb10A—Sb10B^i	114.27 (6)	Pb3B—S12B—Ag12B^x	122.96 (17)
Sb11A^xiii—Sb10A—Pb10B^i	114.27 (6)	Pb4A^ix—S12B—Sb4A^ix	16.59 (12)
Pb11A^xiii—Sb10A—Sb10B^i	114.27 (6)	Pb4A^ix—S12B—Sb4A^x	106.13 (19)
Pb11A^xiii—Sb10A—Pb10B^i	114.27 (6)	Pb4A^ix—S12B—Ag12B^x	60.60 (11)
Pb11A^xiii—Sb10A—Sb11A^xiii	0.0	Sb4A^ix—S12B—Sb4A^x	122.7 (2)
Ag12A^xiii—Sb10A—Sb10B^i	123.89 (7)	Ag4B^x—S12B—Pb3B	162.0 (3)
Ag12A^xiii—Sb10A—Pb10B^i	123.89 (7)	Ag4B^x—S12B—Pb4A^ix	67.32 (19)
Ag12A^xiii—Sb10A—Sb11A^xiii	51.06 (6)	Ag4B^x—S12B—Sb4A^x	39.03 (19)
Ag12A^xiii—Sb10A—Pb11A^xiii	51.06 (6)	Ag4B^x—S12B—Sb4A^ix	83.9 (2)
Ag12A^xiii—Sb10A—Ag12B^xiii	65.56 (7)	Ag4B^x—S12B—Sb8A	108.5 (2)
Ag12B^xiii—Sb10A—Sb10B^i	58.34 (6)	Ag4B^x—S12B—Sb9A	107.2 (2)
Ag12B^xiii—Sb10A—Pb10B^i	58.34 (6)	Ag4B^x—S12B—Ag12B^x	60.66 (17)
Ag12B^xiii—Sb10A—Sb11A^xiii	78.56 (6)	Cu4B^x—S12B—Pb3B	164.4 (10)
Ag12B^xiii—Sb10A—Pb11A^xiii	78.56 (6)	Cu4B^x—S12B—Pb4A^ix	35.6 (10)
S3B—Sb10A—Sb10B^i	88.94 (15)	Cu4B^x—S12B—Sb4A^ix	52.1 (10)
S3B—Sb10A—Pb10B^i	88.94 (15)	Cu4B^x—S12B—Sb4A^x	70.7 (10)
S3B—Sb10A—Sb11A^xiii	146.17 (15)	Cu4B^x—S12B—Ag4B^x	32.4 (10)
S3B—Sb10A—Pb11A^xiii	146.17 (15)	Cu4B^x—S12B—Ag4B'^x	20.6 (12)
S3B—Sb10A—Ag12A^xiii	135.12 (16)	Cu4B^x—S12B—Sb8A	81.7 (9)
S3B—Sb10A—Ag12B^xiii	135.20 (16)	Cu4B^x—S12B—Sb8B	93.8 (10)
S3B—Sb10A—S7B^xiii	172.99 (17)	Cu4B^x—S12B—Sb9A	88.4 (10)
S3B—Sb10A—S13A	92.5 (2)	Cu4B^x—S12B—Sb9B	103.5 (9)
S3B—Sb10A—S13B	94.5 (2)	Cu4B^x—S12B—Ag12B^x	49.0 (8)
S3B—Sb10A—S14A	85.53 (19)	Ag4B'^x—S12B—Pb3B	166.2 (11)
S3B—Sb10A—S14B	86.91 (19)	Ag4B'^x—S12B—Pb4A^ix	55.9 (13)
S7B^xiii—Sb10A—Sb10B^i	92.41 (12)	Ag4B'^x—S12B—Sb4A^x	51.0 (13)
S7B^xiii—Sb10A—Pb10B^i	92.41 (12)	Ag4B'^x—S12B—Sb4A^ix	72.2 (13)
S7B^xiii—Sb10A—Sb11A^xiii	38.09 (11)	Ag4B'^x—S12B—Ag4B^x	16.3 (12)
S7B^xiii—Sb10A—Pb11A^xiii	38.09 (11)	Ag4B'^x—S12B—Sb8A	92.2 (12)
S7B^xiii—Sb10A—Ag12A^xiii	39.65 (12)	Ag4B'^x—S12B—Sb8B	76.6 (12)
S7B^xiii—Sb10A—Ag12B^xiii	41.76 (12)	Ag4B'^x—S12B—Sb9A	106.7 (12)
S13A—Sb10A—Sb10B^i	40.37 (15)	Ag4B'^x—S12B—Sb9B	92.9 (12)
S13A—Sb10A—Pb10B^i	40.37 (15)	Ag4B'^x—S12B—Ag12B^x	46.2 (11)
S13A—Sb10A—Sb11A^xiii	121.20 (15)	Sb8A—S12B—Pb3B	83.47 (16)
S13A—Sb10A—Pb11A^xiii	121.20 (15)	Sb8A—S12B—Pb4A^ix	60.10 (12)
S13A—Sb10A—Ag12A^xiii	95.45 (16)	Sb8A—S12B—Sb4A^x	128.3 (2)
S13A—Sb10A—Ag12B^xiii	42.68 (14)	Sb8A—S12B—Sb4A^ix	51.06 (14)
S13A—Sb10A—S7B^xiii	84.10 (18)	Sb8A—S12B—Ag12B^x	52.81 (11)
S13A—Sb10A—S14A	169.7 (2)	Sb8B—S12B—Pb3B	89.96 (18)
S13A—Sb10A—S14B	81.24 (19)	Sb8B—S12B—Pb4A^ix	117.6 (2)
S13B—Sb10A—Sb10B^i	141.15 (17)	Sb8B—S12B—Sb4A^ix	124.9 (2)
S13B—Sb10A—Pb10B^i	141.15 (17)	Sb8B—S12B—Sb4A^x	53.76 (16)
S13B—Sb10A—Sb11A^xiii	82.58 (16)	Sb8B—S12B—Ag4B^x	77.7 (2)
S13B—Sb10A—Pb11A^xiii	82.58 (16)	Sb8B—S12B—Sb8A	86.87 (18)
S13B—Sb10A—Ag12A^xiii	40.58 (16)	Sb8B—S12B—Sb9A	173.3 (3)
S13B—Sb10A—Ag12B^xiii	94.49 (17)	Sb8B—S12B—Ag12B^x	57.33 (13)
S13B—Sb10A—S7B^xiii	80.11 (19)	Sb9A—S12B—Pb3B	86.28 (17)
S13B—Sb10A—S13A	100.8 (2)	Sb9A—S12B—Pb4A^ix	61.61 (12)
S13B—Sb10A—S14A	89.5 (2)	Sb9A—S12B—Sb4A^x	132.9 (2)
S13B—Sb10A—S14B	177.4 (2)	Sb9A—S12B—Sb4A^ix	52.33 (15)
S14A—Sb10A—Sb10B^i	129.39 (14)	Sb9A—S12B—Sb8A	87.17 (17)
S14A—Sb10A—Pb10B^i	129.39 (14)	Sb9A—S12B—Ag12B^x	120.63 (18)
S14A—Sb10A—Sb11A^xiii	60.82 (13)	Sb9B—S12B—Pb3B	91.34 (19)
S14A—Sb10A—Pb11A^xiii	60.82 (13)	Sb9B—S12B—Pb4A^ix	124.1 (2)
S14A—Sb10A—Ag12A^xiii	93.04 (15)	Sb9B—S12B—Sb4A^ix	132.1 (2)
S14A—Sb10A—Ag12B^xiii	138.32 (13)	Sb9B—S12B—Sb4A^x	54.94 (18)
S14A—Sb10A—S7B^xiii	98.87 (17)	Sb9B—S12B—Ag4B^x	76.5 (2)
S14A—Sb10A—S14B	88.55 (17)	Sb9B—S12B—Sb8A	174.8 (3)
S14B—Sb10A—Sb10B^i	40.88 (12)	Sb9B—S12B—Sb8B	93.1 (2)
S14B—Sb10A—Pb10B^i	40.88 (12)	Sb9B—S12B—Sb9A	92.5 (2)
S14B—Sb10A—Sb11A^xiii	95.05 (13)	Sb9B—S12B—Ag12B^x	131.1 (2)
S14B—Sb10A—Pb11A^xiii	95.05 (13)	Ag12B^x—S12B—Sb4A^ix	68.33 (15)
S14B—Sb10A—Ag12A^xiii	137.96 (13)	Ag12B^x—S12B—Sb4A^x	76.49 (16)
S14B—Sb10A—Ag12B^xiii	85.94 (12)	Pb3A—S13A—Pb1A	59.60 (9)
S14B—Sb10A—S7B^xiii	98.61 (16)	Pb3A—S13A—Pb7B^xi	82.88 (13)
Sb10A^ii—Sb10B—Sb11B^xiv	64.66 (6)	Pb3A—S13A—Sb11B^xiii	145.86 (17)
Pb10A^ii—Sb10B—Sb10A^ii	0.0	Pb3A—S13A—Pb11B^xiii	148.8 (8)
Pb10A^ii—Sb10B—Sb11B^xiv	64.66 (6)	Pb3A—S13A—Ag12A^xiii	121.53 (17)
Sb11B—Sb10B—Sb10A^ii	93.65 (7)	Pb3A—S13A—Ag12A^xv	117.69 (17)
Sb11B—Sb10B—Pb10A^ii	93.65 (7)	Pb7B^xi—S13A—Pb1A	142.48 (16)
Sb11B—Sb10B—Sb11B^xiv	67.80 (8)	Pb7B^xi—S13A—Sb11B^xiii	130.86 (17)
Sb11B—Sb10B—Ag12A^xiii	120.07 (7)	Pb7B^xi—S13A—Pb11B^xiii	128.2 (8)
Sb11B—Sb10B—Ag12B^xiv	119.71 (8)	Pb7B^xi—S13A—Ag12A^xv	83.35 (13)
Ag12A^xiii—Sb10B—Sb10A^ii	121.35 (7)	Pb7B^xi—S13A—Ag12A^xiii	84.43 (13)
Ag12A^xiii—Sb10B—Pb10A^ii	121.35 (7)	Sb10A—S13A—Pb1A	62.47 (12)
Ag12A^xiii—Sb10B—Sb11B^xiv	84.40 (6)	Sb10A—S13A—Pb3A	96.30 (19)
Ag12B^xiv—Sb10B—Sb10A^ii	56.96 (5)	Sb10A—S13A—Pb7B^xi	128.2 (2)
Ag12B^xiv—Sb10B—Pb10A^ii	56.96 (5)	Sb10A—S13A—Sb10B^i	101.8 (2)
Ag12B^xiv—Sb10B—Sb11B^xiv	52.35 (6)	Sb10A—S13A—Pb10B^i	101.8 (2)
Ag12B^xiv—Sb10B—Ag12A^xiii	64.59 (7)	Sb10A—S13A—Sb11B^xiii	68.31 (13)
S3A—Sb10B—Sb10A^ii	92.66 (16)	Sb10A—S13A—Pb11B^xiii	64.1 (9)
S3A—Sb10B—Pb10A^ii	92.66 (16)	Sb10A—S13A—Ag12A^xiii	52.06 (13)
S3A—Sb10B—Sb11B	94.74 (14)	Sb10A—S13A—Ag12A^xv	137.48 (19)
S3A—Sb10B—Sb11B^xiv	149.13 (16)	Sb10A—S13A—Ag12B^xiii	95.1 (2)
S3A—Sb10B—Ag12A^xiii	126.32 (16)	Sb10B^i—S13A—Pb1A	58.64 (11)
S3A—Sb10B—Ag12B^xiv	132.99 (15)	Sb10B^i—S13A—Pb3A	94.22 (19)
S3A—Sb10B—S7A^xiii	163.34 (19)	Sb10B^i—S13A—Pb7B^xi	129.9 (2)
S3A—Sb10B—S13A^ii	91.5 (2)	Sb10B^i—S13A—Sb11B^xiii	61.70 (13)
S3A—Sb10B—S13B	89.0 (2)	Sb10B^i—S13A—Pb11B^xiii	68.7 (11)
S3A—Sb10B—S14A	88.6 (2)	Sb10B^i—S13A—Ag12A^xiii	135.00 (19)
S3A—Sb10B—S14B^ii	93.6 (2)	Sb10B^i—S13A—Ag12A^xv	53.95 (12)
S7A^xiii—Sb10B—Sb10A^ii	93.15 (15)	Pb10B^i—S13A—Pb1A	58.64 (11)
S7A^xiii—Sb10B—Pb10A^ii	93.15 (15)	Pb10B^i—S13A—Pb3A	94.22 (19)
S7A^xiii—Sb10B—Sb11B	100.46 (13)	Pb10B^i—S13A—Pb7B^xi	129.9 (2)
S7A^xiii—Sb10B—Sb11B^xiv	46.09 (14)	Pb10B^i—S13A—Sb10B^i	0.0
S7A^xiii—Sb10B—Ag12A^xiii	38.67 (14)	Pb10B^i—S13A—Sb11B^xiii	61.70 (13)
S7A^xiii—Sb10B—Ag12B^xiv	42.10 (14)	Pb10B^i—S13A—Pb11B^xiii	68.7 (11)
S13A^ii—Sb10B—Sb10A^ii	37.79 (13)	Pb10B^i—S13A—Ag12A^xv	53.95 (12)
S13A^ii—Sb10B—Pb10A^ii	37.79 (13)	Pb10B^i—S13A—Ag12A^xiii	135.00 (19)
S13A^ii—Sb10B—Sb11B	131.32 (15)	Sb11B^xiii—S13A—Pb1A	86.48 (10)
S13A^ii—Sb10B—Sb11B^xiv	82.84 (14)	Sb11B^xiii—S13A—Ag12A^xiii	73.86 (11)
S13A^ii—Sb10B—Ag12A^xiii	93.18 (14)	Sb11B^xiii—S13A—Ag12A^xv	69.27 (10)
S13A^ii—Sb10B—Ag12B^xiv	42.00 (13)	Pb11B^xiii—S13A—Pb1A	89.3 (8)
S13A^ii—Sb10B—S7A^xiii	83.58 (19)	Pb11B^xiii—S13A—Sb11B^xiii	7.1 (11)
S13A^ii—Sb10B—S13B	100.52 (18)	Pb11B^xiii—S13A—Ag12A^xv	74.0 (10)
S13A^ii—Sb10B—S14A	173.96 (19)	Pb11B^xiii—S13A—Ag12A^xiii	66.8 (11)
S13B—Sb10B—Sb10A^ii	138.28 (13)	Ag12A^xiii—S13A—Pb1A	114.44 (13)
S13B—Sb10B—Pb10A^ii	138.28 (13)	Ag12A^xv—S13A—Pb1A	112.15 (13)
S13B—Sb10B—Sb11B	127.77 (15)	Ag12A^xiii—S13A—Ag12A^xv	117.05 (13)
S13B—Sb10B—Sb11B^xiv	121.87 (14)	Ag12B^xiii—S13A—Pb1A	135.37 (18)
S13B—Sb10B—Ag12A^xiii	37.66 (13)	Ag12B^xiii—S13A—Pb3A	164.7 (2)
S13B—Sb10B—Ag12B^xiv	92.85 (13)	Ag12B^xiii—S13A—Pb7B^xi	82.05 (16)
S13B—Sb10B—S7A^xiii	76.33 (19)	Ag12B^xiii—S13A—Sb10B^i	93.4 (2)
S14A—Sb10B—Sb10A^ii	136.17 (14)	Ag12B^xiii—S13A—Pb10B^i	93.4 (2)
S14A—Sb10B—Pb10A^ii	136.17 (14)	Ag12B^xiii—S13A—Sb11B^xiii	48.90 (11)
S14A—Sb10B—Sb11B	42.68 (14)	Ag12B^xiii—S13A—Pb11B^xiii	46.4 (7)
S14A—Sb10B—Sb11B^xiv	93.95 (15)	Ag12B^xiii—S13A—Ag12A^xiii	59.41 (15)
S14A—Sb10B—Ag12A^xiii	91.59 (14)	Ag12B^xiii—S13A—Ag12A^xv	57.80 (14)
S14A—Sb10B—Ag12B^xiv	138.37 (15)	Pb3B—S13B—Pb7A^xii	84.36 (15)
S14A—Sb10B—S7A^xiii	97.91 (19)	Pb3B—S13B—Pb7B^xi	89.07 (14)
S14A—Sb10B—S13B	85.52 (18)	Pb3B—S13B—Sb11A^xiii	145.48 (18)
S14B^ii—Sb10B—Sb10A^ii	52.53 (14)	Pb3B—S13B—Pb11A^xiii	145.48 (18)
S14B^ii—Sb10B—Pb10A^ii	52.53 (14)	Pb3B—S13B—Ag12B^xiii	124.78 (19)
S14B^ii—Sb10B—Sb11B	41.17 (15)	Pb3B—S13B—Ag12B^xiv	116.80 (18)
S14B^ii—Sb10B—Sb11B^xiv	56.26 (14)	Pb7A^xii—S13B—Pb7B^xi	53.28 (10)
S14B^ii—Sb10B—Ag12A^xiii	139.72 (15)	Pb7A^xii—S13B—Sb11A^xiii	130.12 (19)
S14B^ii—Sb10B—Ag12B^xiv	93.31 (15)	Pb7A^xii—S13B—Pb11A^xiii	130.12 (19)
S14B^ii—Sb10B—S7A^xiii	102.3 (2)	Pb7A^xii—S13B—Ag12B^xiv	85.63 (14)
S14B^ii—Sb10B—S13A^ii	90.3 (2)	Pb7A^xii—S13B—Ag12B^xiii	89.95 (15)
S14B^ii—Sb10B—S13B	168.8 (2)	Sb10A—S13B—Pb3B	95.0 (2)
S14B^ii—Sb10B—S14A	83.66 (18)	Sb10A—S13B—Pb7A^xii	134.4 (3)
Pb4A—Sb11A—Pb10A^xiii	130.93 (6)	Sb10A—S13B—Pb7B^xi	81.13 (18)
Pb4A—Sb11A—Sb11B	128.27 (7)	Sb10A—S13B—Sb10B	99.4 (2)
Sb4A—Sb11A—Pb4A	23.14 (17)	Sb10A—S13B—Sb11A^xiii	63.34 (14)
Sb4A—Sb11A—Pb10A^xiii	122.04 (15)	Sb10A—S13B—Pb11A^xiii	63.34 (14)
Sb4A—Sb11A—Sb11B	105.75 (18)	Sb10A—S13B—Ag12B^xiii	53.44 (14)
Sb4A—Sb11A—S14A^xiii	150.6 (2)	Sb10A—S13B—Ag12B^xiv	132.6 (2)
Sb11B—Sb11A—Pb10A^xiii	66.70 (5)	Sb10B—S13B—Pb3B	89.84 (18)
Pb11B—Sb11A—Pb4A	125.6 (10)	Sb10B—S13B—Pb7A^xii	126.1 (2)
Pb11B—Sb11A—Sb4A	102.9 (10)	Sb10B—S13B—Pb7B^xi	178.8 (2)
Pb11B—Sb11A—Pb10A^xiii	66.7 (9)	Sb10B—S13B—Sb11A^xiii	69.40 (13)
Pb11B—Sb11A—Sb11B	3.3 (10)	Sb10B—S13B—Pb11A^xiii	69.40 (13)
Pb11B—Sb11A—S14A^xiii	97.6 (10)	Sb10B—S13B—Ag12B^xiii	134.06 (19)
Ag12A—Sb11A—Pb4A	70.19 (7)	Sb10B—S13B—Ag12B^xiv	50.27 (11)
Ag12A—Sb11A—Sb4A	64.94 (15)	Sb11A^xiii—S13B—Pb7B^xi	111.79 (15)
Ag12A—Sb11A—Pb10A^xiii	60.83 (6)	Sb11A^xiii—S13B—Ag12B^xiii	65.25 (10)
Ag12A—Sb11A—Sb11B	100.14 (8)	Sb11A^xiii—S13B—Ag12B^xiv	71.13 (10)
Ag12A—Sb11A—Pb11B	97.5 (9)	Pb11A^xiii—S13B—Pb7B^xi	111.79 (15)
Ag12A—Sb11A—S14A^xiii	91.83 (12)	Pb11A^xiii—S13B—Sb11A^xiii	0.0
Ag12A—Sb11A—S14B	124.41 (14)	Pb11A^xiii—S13B—Ag12B^xiii	65.25 (10)
S4A—Sb11A—Pb4A	45.28 (15)	Pb11A^xiii—S13B—Ag12B^xiv	71.13 (10)
S4A—Sb11A—Sb4A	42.03 (19)	Ag12A^xiii—S13B—Pb3B	165.3 (3)
S4A—Sb11A—Pb10A^xiii	154.91 (17)	Ag12A^xiii—S13B—Pb7A^xii	81.81 (18)
S4A—Sb11A—Sb11B	96.62 (17)	Ag12A^xiii—S13B—Pb7B^xi	86.59 (19)
S4A—Sb11A—Pb11B	95.6 (9)	Ag12A^xiii—S13B—Sb10A	98.1 (2)
S4A—Sb11A—Ag12A	106.90 (16)	Ag12A^xiii—S13B—Sb10B	94.4 (2)
S4A—Sb11A—S7A	86.6 (2)	Ag12A^xiii—S13B—Sb11A^xiii	48.40 (13)
S4A—Sb11A—S7B	90.0 (2)	Ag12A^xiii—S13B—Pb11A^xiii	48.40 (13)
S4A—Sb11A—S14A	88.3 (2)	Ag12A^xiii—S13B—Ag12B^xiv	57.31 (16)
S4A—Sb11A—S14A^xiii	155.42 (19)	Ag12A^xiii—S13B—Ag12B^xiii	60.27 (17)
S4A—Sb11A—S14B	81.4 (2)	Ag12B^xiv—S13B—Pb7B^xi	129.98 (13)
S7A—Sb11A—Pb4A	41.69 (18)	Ag12B^xiii—S13B—Pb7B^xi	47.09 (7)
S7A—Sb11A—Sb4A	56.1 (2)	Ag12B^xiii—S13B—Ag12B^xiv	117.41 (14)
S7A—Sb11A—Pb10A^xiii	97.22 (17)	Pb1B—S14A—Ag4B	56.94 (12)
S7A—Sb11A—Sb11B	146.05 (17)	Pb1B—S14A—Sb10A	90.81 (17)
S7A—Sb11A—Pb11B	143.0 (10)	Pb1B—S14A—Sb11A^xiii	160.1 (2)
S7A—Sb11A—Ag12A	47.35 (17)	Pb1B—S14A—Pb11A^xiii	160.1 (2)
S7A—Sb11A—S14A^xiii	95.1 (2)	Sb10A—S14A—Ag4B	133.6 (2)
S7A—Sb11A—S14B	79.7 (2)	Sb10A—S14A—Sb11A^xiii	69.93 (13)
S7B—Sb11A—Pb4A	85.35 (19)	Sb10A—S14A—Pb11A^xiii	69.93 (13)
S7B—Sb11A—Sb4A	64.5 (2)	Sb10B—S14A—Pb1B	92.77 (19)
S7B—Sb11A—Pb10A^xiii	65.31 (19)	Sb10B—S14A—Ag4B	124.3 (2)
S7B—Sb11A—Sb11B	56.49 (18)	Sb10B—S14A—Sb10A	85.57 (18)
S7B—Sb11A—Pb11B	53.3 (10)	Sb10B—S14A—Sb11A^xiii	81.26 (17)
S7B—Sb11A—Ag12A	48.80 (17)	Sb10B—S14A—Pb11A^xiii	81.26 (17)
S7B—Sb11A—S7A	89.8 (2)	Sb11A—S14A—Pb1B	93.0 (2)
S7B—Sb11A—S14A^xiii	114.5 (2)	Sb11A^xiii—S14A—Ag4B	141.06 (18)
S7B—Sb11A—S14A	96.4 (2)	Sb11A—S14A—Ag4B	60.09 (15)
S7B—Sb11A—S14B	166.8 (2)	Sb11A—S14A—Sb10A	93.5 (2)
S14A—Sb11A—Pb4A	133.57 (15)	Sb11A—S14A—Sb10B	174.2 (3)
S14A^xiii—Sb11A—Pb4A	134.19 (13)	Sb11A—S14A—Sb11A^xiii	93.00 (18)
S14A—Sb11A—Sb4A	122.4 (2)	Sb11A—S14A—Pb11A^xiii	93.0
S14A^xiii—Sb11A—Pb10A^xiii	49.24 (10)	Pb11A^xiii—S14A—Ag4B	141.06 (18)
S14A—Sb11A—Pb10A^xiii	90.05 (15)	Pb11A^xiii—S14A—Sb11A^xiii	0.0
S14A^xiii—Sb11A—Sb11B	95.53 (13)	Sb11B—S14A—Pb1B	96.7 (2)
S14A—Sb11A—Sb11B	40.96 (14)	Sb11B—S14A—Ag4B	56.93 (17)
S14A—Sb11A—Pb11B	43.9 (10)	Sb11B—S14A—Sb10A	169.4 (3)
S14A—Sb11A—Ag12A	140.51 (16)	Sb11B—S14A—Sb10B	86.7 (2)
S14A—Sb11A—S7A	171.9 (2)	Sb11B—S14A—Sb11A	93.5 (2)
S14A—Sb11A—S14A^xiii	87.00 (18)	Sb11B—S14A—Sb11A^xiii	101.8 (2)
S14A—Sb11A—S14B	93.32 (17)	Sb11B—S14A—Pb11A^xiii	101.8 (2)
S14B—Sb11A—Pb4A	81.47 (12)	Pb11B—S14A—Pb1B	95.1 (13)
S14B—Sb11A—Sb4A	102.7 (2)	Pb11B—S14A—Ag4B	47.9 (17)
S14B—Sb11A—Pb10A^xiii	123.72 (13)	Pb11B—S14A—Sb10A	172.4 (15)
S14B—Sb11A—Sb11B	134.20 (13)	Pb11B—S14A—Sb10B	99 (2)
S14B—Sb11A—Pb11B	137.2 (10)	Pb11B—S14A—Sb11A^xiii	104.5 (13)
S14B—Sb11A—S14A^xiii	74.84 (15)	Pb11B—S14A—Sb11A	81 (2)
Cu4B—Sb11B—Sb10B	132.1 (5)	Pb11B—S14A—Pb11A^xiii	104.5 (13)
Ag4B'—Sb11B—Cu4B	13.6 (8)	Pb11B—S14A—Sb11B	12.3 (19)
Ag4B'—Sb11B—Sb10B	132.6 (7)	Pb1A—S14B—Pb4A	56.90 (9)
Pb11B—Sb11B—Cu4B	66 (6)	Pb1A—S14B—Sb10A	87.86 (16)
Pb11B—Sb11B—Ag4B'	52 (6)	Pb1A—S14B—Sb11A	87.68 (15)
Pb11B—Sb11B—Sb10B	114 (6)	Pb1A—S14B—Sb11B^xiii	169.4 (2)
Pb11B—Sb11B—Ag12B	66 (6)	Pb1A—S14B—Pb11B^xiii	161.3 (13)
Pb11B—Sb11B—S4B	80 (6)	Sb10A—S14B—Pb4A	123.02 (17)
Pb11B—Sb11B—S7A^ii	109 (6)	Sb10A—S14B—Sb11A	84.26 (16)
Pb11B—Sb11B—S7B	20 (6)	Sb10A—S14B—Sb11B^xiii	81.83 (16)
Pb11B—Sb11B—S14A	64 (6)	Sb10A—S14B—Pb11B^xiii	73.5 (12)
Pb11B—Sb11B—S14B^xiii	103 (6)	Sb10B^i—S14B—Pb1A	93.53 (19)
Pb11B—Sb11B—S14B^ii	156 (6)	Sb10B^i—S14B—Pb4A	133.2 (2)
Ag12B—Sb11B—Cu4B	58.0 (5)	Sb10B^i—S14B—Sb10A	86.59 (17)
Ag12B—Sb11B—Ag4B'	56.4 (7)	Sb10B^i—S14B—Sb11A	170.7 (2)
Ag12B—Sb11B—Sb10B	169.61 (8)	Sb10B^i—S14B—Sb11B^xiii	83.31 (17)
S4B—Sb11B—Cu4B	37.8 (5)	Sb10B^i—S14B—Pb11B^xiii	86.2 (10)
S4B—Sb11B—Ag4B'	42.8 (8)	Sb10B^i—S14B—Pb11B^i	91.0 (12)
S4B—Sb11B—Sb10B	94.48 (15)	Pb10B^i—S14B—Pb1A	93.53 (19)
S4B—Sb11B—Ag12B	95.73 (16)	Pb10B^i—S14B—Pb4A	133.2 (2)
S4B—Sb11B—S7A^ii	83.6 (2)	Pb10B^i—S14B—Sb10A	86.59 (17)
S4B—Sb11B—S7B	80.6 (2)	Pb10B^i—S14B—Sb10B^i	0.0
S4B—Sb11B—S14A	89.9 (2)	Pb10B^i—S14B—Sb11A	170.7 (2)
S4B—Sb11B—S14B^ii	91.0 (2)	Pb10B^i—S14B—Sb11B^xiii	83.31 (17)
S4B—Sb11B—S14B^xiii	176.1 (2)	Pb10B^i—S14B—Pb11B^i	91.0 (12)
S7A^ii—Sb11B—Cu4B	60.4 (6)	Pb10B^i—S14B—Pb11B^xiii	86.2 (10)
S7A^ii—Sb11B—Ag4B'	70.3 (9)	Sb11A—S14B—Pb4A	54.50 (9)
S7A^ii—Sb11B—Sb10B	136.2 (2)	Sb11A—S14B—Sb11B^xiii	93.83 (18)
S7A^ii—Sb11B—Ag12B	47.36 (16)	Sb11A—S14B—Pb11B^xiii	89.7 (11)
S7A^ii—Sb11B—S7B	88.4 (2)	Sb11B^i—S14B—Pb1A	95.7 (2)
S7A^ii—Sb11B—S14B^xiii	97.4 (2)	Sb11B^i—S14B—Pb4A	58.21 (13)
S7B—Sb11B—Cu4B	54.3 (6)	Sb11B^xiii—S14B—Pb4A	131.74 (17)
S7B—Sb11B—Ag4B'	42.0 (9)	Sb11B^i—S14B—Sb10A	176.1 (3)
S7B—Sb11B—Sb10B	134.57 (16)	Sb11B^i—S14B—Sb10B^i	94.8 (2)
S7B—Sb11B—Ag12B	45.99 (13)	Sb11B^i—S14B—Pb10B^i	94.8 (2)
S7B—Sb11B—S14B^xiii	103.11 (19)	Sb11B^i—S14B—Sb11A	94.20 (19)
S14A—Sb11B—Cu4B	110.6 (6)	Sb11B^i—S14B—Sb11B^xiii	94.7 (2)
S14A—Sb11B—Ag4B'	100.4 (9)	Sb11B^i—S14B—Pb11B^i	4.3 (12)
S14A—Sb11B—Sb10B	50.64 (17)	Sb11B^xiii—S14B—Pb11B^xiii	8.9 (13)
S14A—Sb11B—Ag12B	127.4 (2)	Sb11B^i—S14B—Pb11B^xiii	103.0 (13)
S14A—Sb11B—S7A^ii	170.7 (3)	Pb11B^i—S14B—Pb1A	93.9 (10)
S14A—Sb11B—S7B	84.0 (2)	Pb11B^i—S14B—Pb4A	59.9 (11)
S14A—Sb11B—S14B^xiii	89.56 (19)	Pb11B^xiii—S14B—Pb4A	133.7 (9)
S14B^ii—Sb11B—Cu4B	119.0 (6)	Pb11B^i—S14B—Sb10A	177.1 (11)
S14B^xiii—Sb11B—Cu4B	145.7 (5)	Pb11B^i—S14B—Sb11A	98.1 (12)
S14B^ii—Sb11B—Ag4B'	130.6 (9)	Pb11B^i—S14B—Sb11B^xiii	96.3 (11)
S14B^xiii—Sb11B—Ag4B'	141.0 (8)	Pb11B^i—S14B—Pb11B^xiii	104.7 (16)
Pb4A^ii—Ag4B—Cu4B—Sb4A^ii	12.6 (18)	Pb11B—Ag4B—Ag4B'—S7B	−54.3 (19)
Pb4A^ii—Ag4B—Cu4B—Ag4B'	−118 (10)	Pb11B—Ag4B—Ag4B'—S8B	99 (5)
Pb4A^ii—Ag4B—Cu4B—Sb8A^iv	−166 (7)	Pb11B—Ag4B—Ag4B'—S12B^iv	178 (4)
Pb4A^ii—Ag4B—Cu4B—Sb8B^iv	−169 (5)	Pb11B—Cu4B—Ag4B'—Pb4A^ii	6 (11)
Pb4A^ii—Ag4B—Cu4B—Sb9B^iv	122 (4)	Pb11B—Cu4B—Ag4B'—Ag4B	−113 (7)
Pb4A^ii—Ag4B—Cu4B—Sb11B	−55 (4)	Pb11B—Cu4B—Ag4B'—Sb8B^iv	130 (4)
Pb4A^ii—Ag4B—Cu4B—Pb11B	−58 (5)	Pb11B—Cu4B—Ag4B'—Sb9B^iv	−164 (2)
Pb4A^ii—Ag4B—Cu4B—Ag12B	−110 (5)	Pb11B—Cu4B—Ag4B'—Sb11B	−0.5 (11)
Pb4A^ii—Ag4B—Cu4B—S4B	−14 (4)	Pb11B—Cu4B—Ag4B'—Ag12B	59.4 (16)
Pb4A^ii—Ag4B—Cu4B—S12B^iv	147 (5)	Pb11B—Cu4B—Ag4B'—S4B	−39.6 (19)
Pb4A^ii—Ag4B—Ag4B'—Cu4B	22 (4)	Pb11B—Cu4B—Ag4B'—S7B	43 (6)
Pb4A^ii—Ag4B—Ag4B'—Sb8B^iv	146 (5)	Pb11B—Cu4B—Ag4B'—S8B	−106 (2)
Pb4A^ii—Ag4B—Ag4B'—Sb9B^iv	89 (4)	Pb11B—Cu4B—Ag4B'—S12B^iv	160.4 (15)
Pb4A^ii—Ag4B—Ag4B'—Sb11B	−82 (4)	Ag12B—Cu4B—Ag4B'—Pb4A^ii	−54 (10)
Pb4A^ii—Ag4B—Ag4B'—Pb11B	−89 (5)	Ag12B—Cu4B—Ag4B'—Ag4B	−172 (8)
Pb4A^ii—Ag4B—Ag4B'—Ag12B	−145 (9)	Ag12B—Cu4B—Ag4B'—Sb8B^iv	71 (2)
Pb4A^ii—Ag4B—Ag4B'—S4B	−43 (4)	Ag12B—Cu4B—Ag4B'—Sb9B^iv	136.9 (16)
Pb4A^ii—Ag4B—Ag4B'—S7B	−143 (5)	Ag12B—Cu4B—Ag4B'—Sb11B	−59.9 (10)
Pb4A^ii—Ag4B—Ag4B'—S8B	10 (8)	Ag12B—Cu4B—Ag4B'—Pb11B	−59.4 (16)
Pb4A^ii—Ag4B—Ag4B'—S12B^iv	90 (5)	Ag12B—Cu4B—Ag4B'—S4B	−99.1 (12)
Pb4A^ii—Cu4B—Ag4B'—Ag4B	−118 (9)	Ag12B—Cu4B—Ag4B'—S7B	−16 (6)
Pb4A^ii—Cu4B—Ag4B'—Sb8B^iv	125 (8)	Ag12B—Cu4B—Ag4B'—S8B	−166 (2)
Pb4A^ii—Cu4B—Ag4B'—Sb9B^iv	−169 (9)	Ag12B—Cu4B—Ag4B'—S12B^iv	101.0 (14)
Pb4A^ii—Cu4B—Ag4B'—Sb11B	−6 (10)	Ag12B—Sb11B—Pb11B—Ag4B	78 (5)
Pb4A^ii—Cu4B—Ag4B'—Pb11B	−6 (11)	Ag12B—Sb11B—Pb11B—Cu4B	64 (3)
Pb4A^ii—Cu4B—Ag4B'—Ag12B	54 (10)	Ag12B—Sb11B—Pb11B—Ag4B'	65 (4)
Pb4A^ii—Cu4B—Ag4B'—S4B	−45 (9)	Ag12B—Sb11B—Pb11B—Sb11A	−142 (17)
Pb4A^ii—Cu4B—Ag4B'—S7B	38 (15)	Ag12B—Sb11B—Pb11B—S4B	101 (3)
Pb4A^ii—Cu4B—Ag4B'—S8B	−112 (9)	Ag12B—Sb11B—Pb11B—S7A^ii	21 (4)
Pb4A^ii—Cu4B—Ag4B'—S12B^iv	155 (10)	Ag12B—Sb11B—Pb11B—S7B	12 (12)
Sb4A—Ag4B—Cu4B—Pb4A^ii	171.8 (17)	Ag12B—Sb11B—Pb11B—S14A	−165 (5)
Sb4A—Ag4B—Cu4B—Sb4A^ii	−176 (3)	Ag12B—Sb11B—Pb11B—S14B^ii	171 (11)
Sb4A—Ag4B—Cu4B—Ag4B'	54 (9)	S4A—Pb4A—Sb4A—Ag4B	−1.2 (12)
Sb4A—Ag4B—Cu4B—Sb8A^iv	6 (5)	S4A—Pb4A—Sb4A—Ag4B'	−27 (3)
Sb4A—Ag4B—Cu4B—Sb8B^iv	2 (3)	S4A—Pb4A—Sb4A—Sb8A^iii	−154.9 (3)
Sb4A—Ag4B—Cu4B—Sb9B^iv	−66 (3)	S4A—Pb4A—Sb4A—Sb9A^iii	126.6 (3)
Sb4A—Ag4B—Cu4B—Sb11B	117 (3)	S4A—Pb4A—Sb4A—Sb11A	−43.8 (2)
Sb4A—Ag4B—Cu4B—Pb11B	113 (3)	S4A—Pb4A—Sb4A—S7A	−84.4 (3)
Sb4A—Ag4B—Cu4B—Ag12B	61 (3)	S4A—Pb4A—Sb4A—S7B	−66.5 (4)
Sb4A—Ag4B—Cu4B—S4B	158 (3)	S4A—Pb4A—Sb4A—S8A	68.6 (3)
Sb4A—Ag4B—Cu4B—S12B^iv	−41 (4)	S4A—Pb4A—Sb4A—S12A^iii	163.4 (6)
Sb4A—Ag4B—Ag4B'—Pb4A^ii	−176.5 (10)	S4A—Ag4B—Cu4B—Pb4A^ii	34 (7)
Sb4A—Ag4B—Ag4B'—Cu4B	−154 (5)	S4A—Ag4B—Cu4B—Sb4A^ii	47 (8)
Sb4A—Ag4B—Ag4B'—Sb8B^iv	−31 (5)	S4A—Ag4B—Cu4B—Ag4B'	−84 (8)
Sb4A—Ag4B—Ag4B'—Sb9B^iv	−88 (4)	S4A—Ag4B—Cu4B—Sb8A^iv	−131 (2)
Sb4A—Ag4B—Ag4B'—Sb11B	101 (3)	S4A—Ag4B—Cu4B—Sb8B^iv	−135 (3)
Sb4A—Ag4B—Ag4B'—Pb11B	95 (4)	S4A—Ag4B—Cu4B—Sb9B^iv	156 (3)
Sb4A—Ag4B—Ag4B'—Ag12B	39 (8)	S4A—Ag4B—Cu4B—Sb11B	−20 (3)
Sb4A—Ag4B—Ag4B'—S4B	140 (3)	S4A—Ag4B—Cu4B—Pb11B	−24 (3)
Sb4A—Ag4B—Ag4B'—S7B	40 (4)	S4A—Ag4B—Cu4B—Ag12B	−76 (3)
Sb4A—Ag4B—Ag4B'—S8B	−166 (8)	S4A—Ag4B—Cu4B—S4B	20 (4)
Sb4A—Ag4B—Ag4B'—S12B^iv	−87 (4)	S4A—Ag4B—Cu4B—S12B^iv	−179 (2)
Sb4A^ii—Cu4B—Ag4B'—Pb4A^ii	−19 (5)	S4A—Ag4B—Ag4B'—Pb4A^ii	118 (5)
Sb4A^ii—Cu4B—Ag4B'—Ag4B	−138 (9)	S4A—Ag4B—Ag4B'—Cu4B	140 (5)
Sb4A^ii—Cu4B—Ag4B'—Sb8B^iv	105 (11)	S4A—Ag4B—Ag4B'—Sb8B^iv	−97 (4)
Sb4A^ii—Cu4B—Ag4B'—Sb9B^iv	171 (11)	S4A—Ag4B—Ag4B'—Sb9B^iv	−153 (6)
Sb4A^ii—Cu4B—Ag4B'—Sb11B	−25 (12)	S4A—Ag4B—Ag4B'—Sb11B	35 (6)
Sb4A^ii—Cu4B—Ag4B'—Pb11B	−25 (13)	S4A—Ag4B—Ag4B'—Pb11B	29 (6)
Sb4A^ii—Cu4B—Ag4B'—Ag12B	34 (13)	S4A—Ag4B—Ag4B'—Ag12B	−27 (10)
Sb4A^ii—Cu4B—Ag4B'—S4B	−65 (12)	S4A—Ag4B—Ag4B'—S4B	74 (5)
Sb4A^ii—Cu4B—Ag4B'—S7B	18 (18)	S4A—Ag4B—Ag4B'—S7B	−26 (6)
Sb4A^ii—Cu4B—Ag4B'—S8B	−131 (11)	S4A—Ag4B—Ag4B'—S8B	128 (8)
Sb4A^ii—Cu4B—Ag4B'—S12B^iv	135 (13)	S4A—Ag4B—Ag4B'—S12B^iv	−153 (3)
Ag4B^i—Pb4A—Sb4A—Ag4B	−160.8 (7)	S4B^i—Pb4A—Sb4A—Ag4B	−7 (2)
Ag4B^i—Pb4A—Sb4A—Ag4B'	174 (2)	S4B^i—Pb4A—Sb4A—Ag4B'	−33 (3)
Ag4B^i—Pb4A—Sb4A—Sb8A^iii	45.5 (12)	S4B^i—Pb4A—Sb4A—Sb8A^iii	−160.8 (6)
Ag4B^i—Pb4A—Sb4A—Sb9A^iii	−33.1 (12)	S4B^i—Pb4A—Sb4A—Sb9A^iii	120.6 (7)
Ag4B^i—Pb4A—Sb4A—Sb11A	156.5 (11)	S4B^i—Pb4A—Sb4A—Sb11A	−49.8 (8)
Ag4B^i—Pb4A—Sb4A—S4A	−159.6 (11)	S4B^i—Pb4A—Sb4A—S4A	−5.9 (9)
Ag4B^i—Pb4A—Sb4A—S7A	116.0 (12)	S4B^i—Pb4A—Sb4A—S7A	−90.4 (7)
Ag4B^i—Pb4A—Sb4A—S7B	133.9 (10)	S4B^i—Pb4A—Sb4A—S7B	−72.4 (9)
Ag4B^i—Pb4A—Sb4A—S8A	−91.1 (12)	S4B^i—Pb4A—Sb4A—S8A	62.6 (7)
Ag4B^i—Pb4A—Sb4A—S12A^iii	3.8 (16)	S4B^i—Pb4A—Sb4A—S12A^iii	157.5 (4)
Ag4B—Cu4B—Ag4B'—Pb4A^ii	118 (9)	S4B—Ag4B—Cu4B—Pb4A^ii	14 (4)
Ag4B—Cu4B—Ag4B'—Sb8B^iv	−117 (8)	S4B—Ag4B—Cu4B—Sb4A^ii	27 (5)
Ag4B—Cu4B—Ag4B'—Sb9B^iv	−51 (6)	S4B—Ag4B—Cu4B—Ag4B'	−104 (8)
Ag4B—Cu4B—Ag4B'—Sb11B	112 (7)	S4B—Ag4B—Cu4B—Sb8A^iv	−151 (3)
Ag4B—Cu4B—Ag4B'—Pb11B	113 (7)	S4B—Ag4B—Cu4B—Sb8B^iv	−155.3 (7)
Ag4B—Cu4B—Ag4B'—Ag12B	172 (8)	S4B—Ag4B—Cu4B—Sb9B^iv	136.1 (5)
Ag4B—Cu4B—Ag4B'—S4B	73 (7)	S4B—Ag4B—Cu4B—Sb11B	−40.5 (4)
Ag4B—Cu4B—Ag4B'—S7B	156 (13)	S4B—Ag4B—Cu4B—Pb11B	−44.4 (11)
Ag4B—Cu4B—Ag4B'—S8B	6 (6)	S4B—Ag4B—Cu4B—Ag12B	−96.3 (10)
Ag4B—Cu4B—Ag4B'—S12B^iv	−87 (7)	S4B—Ag4B—Cu4B—S12B^iv	161.1 (15)
Cu4B^i—Pb4A—Sb4A—Ag4B	−175 (2)	S4B—Ag4B—Ag4B'—Pb4A^ii	43 (4)
Cu4B^i—Pb4A—Sb4A—Ag4B'	159 (3)	S4B—Ag4B—Ag4B'—Cu4B	66 (7)
Cu4B^i—Pb4A—Sb4A—Sb8A^iii	31 (2)	S4B—Ag4B—Ag4B'—Sb8B^iv	−171 (2)
Cu4B^i—Pb4A—Sb4A—Sb9A^iii	−47 (2)	S4B—Ag4B—Ag4B'—Sb9B^iv	132.2 (10)
Cu4B^i—Pb4A—Sb4A—Sb11A	142 (2)	S4B—Ag4B—Ag4B'—Sb11B	−39.0 (14)
Cu4B^i—Pb4A—Sb4A—S4A	−174 (2)	S4B—Ag4B—Ag4B'—Pb11B	−45.6 (17)
Cu4B^i—Pb4A—Sb4A—S7A	102 (2)	S4B—Ag4B—Ag4B'—Ag12B	−102 (6)
Cu4B^i—Pb4A—Sb4A—S7B	120 (2)	S4B—Ag4B—Ag4B'—S7B	−100.0 (15)
Cu4B^i—Pb4A—Sb4A—S8A	−105 (2)	S4B—Ag4B—Ag4B'—S8B	53 (5)
Cu4B^i—Pb4A—Sb4A—S12A^iii	−10 (2)	S4B—Ag4B—Ag4B'—S12B^iv	133 (3)
Cu4B—Ag4B—Ag4B'—Pb4A^ii	−22 (4)	S4B—Cu4B—Ag4B'—Pb4A^ii	45 (9)
Cu4B—Ag4B—Ag4B'—Sb8B^iv	123 (8)	S4B—Cu4B—Ag4B'—Ag4B	−73 (7)
Cu4B—Ag4B—Ag4B'—Sb9B^iv	66 (8)	S4B—Cu4B—Ag4B'—Sb8B^iv	170 (2)
Cu4B—Ag4B—Ag4B'—Sb11B	−105 (8)	S4B—Cu4B—Ag4B'—Sb9B^iv	−124.0 (10)
Cu4B—Ag4B—Ag4B'—Pb11B	−111 (8)	S4B—Cu4B—Ag4B'—Sb11B	39.1 (11)
Cu4B—Ag4B—Ag4B'—Ag12B	−167 (12)	S4B—Cu4B—Ag4B'—Pb11B	39.6 (19)
Cu4B—Ag4B—Ag4B'—S4B	−66 (7)	S4B—Cu4B—Ag4B'—Ag12B	99.1 (12)
Cu4B—Ag4B—Ag4B'—S7B	−166 (8)	S4B—Cu4B—Ag4B'—S7B	83 (7)
Cu4B—Ag4B—Ag4B'—S8B	−12 (11)	S4B—Cu4B—Ag4B'—S8B	−66.7 (13)
Cu4B—Ag4B—Ag4B'—S12B^iv	67 (7)	S4B—Cu4B—Ag4B'—S12B^iv	−159.9 (17)
Cu4B—Sb11B—Pb11B—Ag4B	14 (3)	S4B—Sb11B—Pb11B—Ag4B	−23 (4)
Cu4B—Sb11B—Pb11B—Ag4B'	1 (2)	S4B—Sb11B—Pb11B—Cu4B	−36.5 (19)
Cu4B—Sb11B—Pb11B—Sb11A	153 (17)	S4B—Sb11B—Pb11B—Ag4B'	−36 (4)
Cu4B—Sb11B—Pb11B—Ag12B	−64 (3)	S4B—Sb11B—Pb11B—Sb11A	117 (15)
Cu4B—Sb11B—Pb11B—S4B	36.5 (19)	S4B—Sb11B—Pb11B—Ag12B	−101 (3)
Cu4B—Sb11B—Pb11B—S7A^ii	−43 (4)	S4B—Sb11B—Pb11B—S7A^ii	−80 (2)
Cu4B—Sb11B—Pb11B—S7B	−52 (14)	S4B—Sb11B—Pb11B—S7B	−89 (15)
Cu4B—Sb11B—Pb11B—S14A	131 (5)	S4B—Sb11B—Pb11B—S14A	95 (3)
Cu4B—Sb11B—Pb11B—S14B^ii	107 (13)	S4B—Sb11B—Pb11B—S14B^ii	70 (13)
Ag4B'^i—Pb4A—Sb4A—Ag4B	171 (3)	S7A—Pb4A—Sb4A—Ag4B	83.2 (14)
Ag4B'^i—Pb4A—Sb4A—Ag4B'	146 (5)	S7A—Pb4A—Sb4A—Ag4B'	58 (3)
Ag4B'^i—Pb4A—Sb4A—Sb8A^iii	18 (3)	S7A—Pb4A—Sb4A—Sb8A^iii	−70.46 (18)
Ag4B'^i—Pb4A—Sb4A—Sb9A^iii	−61 (3)	S7A—Pb4A—Sb4A—Sb9A^iii	−149.02 (18)
Ag4B'^i—Pb4A—Sb4A—Sb11A	129 (3)	S7A—Pb4A—Sb4A—Sb11A	40.6 (2)
Ag4B'^i—Pb4A—Sb4A—S4A	172 (3)	S7A—Pb4A—Sb4A—S4A	84.4 (3)
Ag4B'^i—Pb4A—Sb4A—S7A	88 (3)	S7A—Pb4A—Sb4A—S7B	17.9 (5)
Ag4B'^i—Pb4A—Sb4A—S7B	106 (3)	S7A—Pb4A—Sb4A—S8A	153.0 (2)
Ag4B'^i—Pb4A—Sb4A—S8A	−119 (3)	S7A—Pb4A—Sb4A—S12A^iii	−112.2 (5)
Ag4B'^i—Pb4A—Sb4A—S12A^iii	−24 (3)	S7A^ii—Sb11B—Pb11B—Ag4B	57 (6)
Ag4B'—Ag4B—Cu4B—Pb4A^ii	118 (10)	S7A^ii—Sb11B—Pb11B—Cu4B	43 (4)
Ag4B'—Ag4B—Cu4B—Sb4A^ii	131 (11)	S7A^ii—Sb11B—Pb11B—Ag4B'	44 (6)
Ag4B'—Ag4B—Cu4B—Sb8A^iv	−48 (7)	S7A^ii—Sb11B—Pb11B—Sb11A	−163 (13)
Ag4B'—Ag4B—Cu4B—Sb8B^iv	−51 (8)	S7A^ii—Sb11B—Pb11B—Ag12B	−21 (4)
Ag4B'—Ag4B—Cu4B—Sb9B^iv	−120 (8)	S7A^ii—Sb11B—Pb11B—S4B	80 (2)
Ag4B'—Ag4B—Cu4B—Sb11B	63 (8)	S7A^ii—Sb11B—Pb11B—S7B	−9 (17)
Ag4B'—Ag4B—Cu4B—Pb11B	60 (8)	S7A^ii—Sb11B—Pb11B—S14A	174.5 (9)
Ag4B'—Ag4B—Cu4B—Ag12B	8 (7)	S7A^ii—Sb11B—Pb11B—S14B^ii	150 (15)
Ag4B'—Ag4B—Cu4B—S4B	104 (8)	S7B—Ag4B—Cu4B—Pb4A^ii	104 (5)
Ag4B'—Ag4B—Cu4B—S12B^iv	−95 (8)	S7B—Ag4B—Cu4B—Sb4A^ii	117 (6)
Ag4B'—Sb11B—Pb11B—Ag4B	12.9 (17)	S7B—Ag4B—Cu4B—Ag4B'	−14 (8)
Ag4B'—Sb11B—Pb11B—Cu4B	−1 (2)	S7B—Ag4B—Cu4B—Sb8A^iv	−61 (2)
Ag4B'—Sb11B—Pb11B—Sb11A	153 (19)	S7B—Ag4B—Cu4B—Sb8B^iv	−65.2 (3)
Ag4B'—Sb11B—Pb11B—Ag12B	−65 (4)	S7B—Ag4B—Cu4B—Sb9B^iv	−133.8 (4)
Ag4B'—Sb11B—Pb11B—S4B	36 (4)	S7B—Ag4B—Cu4B—Sb11B	49.6 (6)
Ag4B'—Sb11B—Pb11B—S7A^ii	−44 (6)	S7B—Ag4B—Cu4B—Pb11B	45.7 (11)
Ag4B'—Sb11B—Pb11B—S7B	−53 (13)	S7B—Ag4B—Cu4B—Ag12B	−6.2 (9)
Ag4B'—Sb11B—Pb11B—S14A	130 (6)	S7B—Ag4B—Cu4B—S4B	90.1 (7)
Ag4B'—Sb11B—Pb11B—S14B^ii	106 (13)	S7B—Ag4B—Cu4B—S12B^iv	−108.7 (9)
Sb8A^iii—Pb4A—Sb4A—Ag4B	153.7 (14)	S7B—Ag4B—Ag4B'—Pb4A^ii	143 (5)
Sb8A^iii—Pb4A—Sb4A—Ag4B'	128 (3)	S7B—Ag4B—Ag4B'—Cu4B	166 (8)
Sb8A^iii—Pb4A—Sb4A—Sb9A^iii	−78.57 (7)	S7B—Ag4B—Ag4B'—Sb8B^iv	−71.0 (16)
Sb8A^iii—Pb4A—Sb4A—Sb11A	111.04 (16)	S7B—Ag4B—Ag4B'—Sb9B^iv	−127.8 (12)
Sb8A^iii—Pb4A—Sb4A—S4A	154.9 (3)	S7B—Ag4B—Ag4B'—Sb11B	61.0 (18)
Sb8A^iii—Pb4A—Sb4A—S7A	70.46 (18)	S7B—Ag4B—Ag4B'—Pb11B	54.3 (19)
Sb8A^iii—Pb4A—Sb4A—S7B	88.4 (4)	S7B—Ag4B—Ag4B'—Ag12B	−2 (5)
Sb8A^iii—Pb4A—Sb4A—S8A	−136.56 (13)	S7B—Ag4B—Ag4B'—S4B	100.0 (15)
Sb8A^iii—Pb4A—Sb4A—S12A^iii	−41.7 (4)	S7B—Ag4B—Ag4B'—S8B	153 (3)
Sb8A^iv—Cu4B—Ag4B'—Pb4A^ii	−95 (10)	S7B—Ag4B—Ag4B'—S12B^iv	−127 (3)
Sb8A^iv—Cu4B—Ag4B'—Ag4B	146 (5)	S7B—Sb11B—Pb11B—Ag4B	66 (14)
Sb8A^iv—Cu4B—Ag4B'—Sb8B^iv	29 (5)	S7B—Sb11B—Pb11B—Cu4B	52 (14)
Sb8A^iv—Cu4B—Ag4B'—Sb9B^iv	95 (3)	S7B—Sb11B—Pb11B—Ag4B'	53 (13)
Sb8A^iv—Cu4B—Ag4B'—Sb11B	−102 (3)	S7B—Sb11B—Pb11B—Sb11A	−154 (29)
Sb8A^iv—Cu4B—Ag4B'—Pb11B	−101 (3)	S7B—Sb11B—Pb11B—Ag12B	−12 (12)
Sb8A^iv—Cu4B—Ag4B'—Ag12B	−42 (3)	S7B—Sb11B—Pb11B—S4B	89 (15)
Sb8A^iv—Cu4B—Ag4B'—S4B	−141 (3)	S7B—Sb11B—Pb11B—S7A^ii	9 (17)
Sb8A^iv—Cu4B—Ag4B'—S7B	−58 (8)	S7B—Sb11B—Pb11B—S14A	−177 (18)
Sb8A^iv—Cu4B—Ag4B'—S8B	153 (2)	S7B—Sb11B—Pb11B—S14B^ii	159 (6)
Sb8A^iv—Cu4B—Ag4B'—S12B^iv	59 (2)	S8A—Pb4A—Sb4A—Ag4B	−69.7 (14)
Sb8B^iv—Ag4B—Cu4B—Pb4A^ii	169 (5)	S8A—Pb4A—Sb4A—Ag4B'	−95 (3)
Sb8B^iv—Ag4B—Cu4B—Sb4A^ii	−178 (6)	S8A—Pb4A—Sb4A—Sb8A^iii	136.56 (13)
Sb8B^iv—Ag4B—Cu4B—Ag4B'	51 (8)	S8A—Pb4A—Sb4A—Sb9A^iii	57.99 (13)
Sb8B^iv—Ag4B—Cu4B—Sb8A^iv	4 (2)	S8A—Pb4A—Sb4A—Sb11A	−112.40 (17)
Sb8B^iv—Ag4B—Cu4B—Sb9B^iv	−68.6 (2)	S8A—Pb4A—Sb4A—S4A	−68.6 (3)
Sb8B^iv—Ag4B—Cu4B—Sb11B	114.8 (4)	S8A—Pb4A—Sb4A—S7A	−153.0 (2)
Sb8B^iv—Ag4B—Cu4B—Pb11B	110.9 (10)	S8A—Pb4A—Sb4A—S7B	−135.1 (4)
Sb8B^iv—Ag4B—Cu4B—Ag12B	59.0 (7)	S8A—Pb4A—Sb4A—S12A^iii	94.8 (4)
Sb8B^iv—Ag4B—Cu4B—S4B	155.3 (7)	S8B—Ag4B—Cu4B—Pb4A^ii	−54 (5)
Sb8B^iv—Ag4B—Cu4B—S12B^iv	−43.5 (9)	S8B—Ag4B—Cu4B—Sb4A^ii	−41 (6)
Sb8B^iv—Ag4B—Ag4B'—Pb4A^ii	−146 (5)	S8B—Ag4B—Cu4B—Ag4B'	−172 (8)
Sb8B^iv—Ag4B—Ag4B'—Cu4B	−123 (8)	S8B—Ag4B—Cu4B—Sb8A^iv	140.9 (19)
Sb8B^iv—Ag4B—Ag4B'—Sb9B^iv	−57 (3)	S8B—Ag4B—Cu4B—Sb8B^iv	137.0 (5)
Sb8B^iv—Ag4B—Ag4B'—Sb11B	132 (3)	S8B—Ag4B—Cu4B—Sb9B^iv	68.4 (5)
Sb8B^iv—Ag4B—Ag4B'—Pb11B	125 (3)	S8B—Ag4B—Cu4B—Sb11B	−108.1 (6)
Sb8B^iv—Ag4B—Ag4B'—Ag12B	69 (5)	S8B—Ag4B—Cu4B—Pb11B	−112.0 (11)
Sb8B^iv—Ag4B—Ag4B'—S4B	171 (2)	S8B—Ag4B—Cu4B—Ag12B	−164.0 (3)
Sb8B^iv—Ag4B—Ag4B'—S7B	71.0 (16)	S8B—Ag4B—Cu4B—S4B	−67.7 (9)
Sb8B^iv—Ag4B—Ag4B'—S8B	−136 (3)	S8B—Ag4B—Cu4B—S12B^iv	93.5 (10)
Sb8B^iv—Ag4B—Ag4B'—S12B^iv	−56.2 (16)	S8B—Ag4B—Ag4B'—Pb4A^ii	−10 (8)
Sb8B^iv—Cu4B—Ag4B'—Pb4A^ii	−125 (8)	S8B—Ag4B—Ag4B'—Cu4B	12 (11)
Sb8B^iv—Cu4B—Ag4B'—Ag4B	117 (8)	S8B—Ag4B—Ag4B'—Sb8B^iv	136 (3)
Sb8B^iv—Cu4B—Ag4B'—Sb9B^iv	66 (2)	S8B—Ag4B—Ag4B'—Sb9B^iv	79 (4)
Sb8B^iv—Cu4B—Ag4B'—Sb11B	−131 (3)	S8B—Ag4B—Ag4B'—Sb11B	−92 (5)
Sb8B^iv—Cu4B—Ag4B'—Pb11B	−130 (4)	S8B—Ag4B—Ag4B'—Pb11B	−99 (5)
Sb8B^iv—Cu4B—Ag4B'—Ag12B	−71 (2)	S8B—Ag4B—Ag4B'—Ag12B	−155 (3)
Sb8B^iv—Cu4B—Ag4B'—S4B	−170 (2)	S8B—Ag4B—Ag4B'—S4B	−53 (5)
Sb8B^iv—Cu4B—Ag4B'—S7B	−87 (7)	S8B—Ag4B—Ag4B'—S7B	−153 (3)
Sb8B^iv—Cu4B—Ag4B'—S8B	123 (3)	S8B—Ag4B—Ag4B'—S12B^iv	79 (5)
Sb8B^iv—Cu4B—Ag4B'—S12B^iv	30 (3)	S12A^iii—Pb4A—Sb4A—Ag4B	−164.6 (18)
Sb9A^iii—Pb4A—Sb4A—Ag4B	−127.7 (14)	S12A^iii—Pb4A—Sb4A—Ag4B'	170 (3)
Sb9A^iii—Pb4A—Sb4A—Ag4B'	−153 (3)	S12A^iii—Pb4A—Sb4A—Sb8A^iii	41.7 (4)
Sb9A^iii—Pb4A—Sb4A—Sb8A^iii	78.57 (7)	S12A^iii—Pb4A—Sb4A—Sb9A^iii	−36.8 (4)
Sb9A^iii—Pb4A—Sb4A—Sb11A	−170.39 (17)	S12A^iii—Pb4A—Sb4A—Sb11A	152.8 (5)
Sb9A^iii—Pb4A—Sb4A—S4A	−126.6 (3)	S12A^iii—Pb4A—Sb4A—S4A	−163.4 (6)
Sb9A^iii—Pb4A—Sb4A—S7A	149.02 (18)	S12A^iii—Pb4A—Sb4A—S7A	112.2 (5)
Sb9A^iii—Pb4A—Sb4A—S7B	166.9 (5)	S12A^iii—Pb4A—Sb4A—S7B	130.1 (7)
Sb9A^iii—Pb4A—Sb4A—S8A	−57.99 (13)	S12A^iii—Pb4A—Sb4A—S8A	−94.8 (4)
Sb9A^iii—Pb4A—Sb4A—S12A^iii	36.8 (4)	S12B^iii—Pb4A—Sb4A—Ag4B	−166.0 (12)
Sb9B^iv—Ag4B—Cu4B—Pb4A^ii	−122 (5)	S12B^iii—Pb4A—Sb4A—Ag4B'	168 (3)
Sb9B^iv—Ag4B—Cu4B—Sb4A^ii	−109 (6)	S12B^iii—Pb4A—Sb4A—Sb8A^iii	40.3 (3)
Sb9B^iv—Ag4B—Cu4B—Ag4B'	120 (8)	S12B^iii—Pb4A—Sb4A—Sb9A^iii	−38.3 (3)
Sb9B^iv—Ag4B—Cu4B—Sb8A^iv	73 (2)	S12B^iii—Pb4A—Sb4A—Sb11A	151.30 (17)
Sb9B^iv—Ag4B—Cu4B—Sb8B^iv	68.6 (2)	S12B^iii—Pb4A—Sb4A—S4A	−164.9 (2)
Sb9B^iv—Ag4B—Cu4B—Sb11B	−176.5 (3)	S12B^iii—Pb4A—Sb4A—S7A	110.7 (3)
Sb9B^iv—Ag4B—Cu4B—Pb11B	179.6 (10)	S12B^iii—Pb4A—Sb4A—S7B	128.6 (4)
Sb9B^iv—Ag4B—Cu4B—Ag12B	127.6 (6)	S12B^iii—Pb4A—Sb4A—S8A	−96.3 (3)
Sb9B^iv—Ag4B—Cu4B—S4B	−136.1 (5)	S12B^iii—Pb4A—Sb4A—S12A^iii	−1.5 (6)
Sb9B^iv—Ag4B—Cu4B—S12B^iv	25.1 (11)	S12B^iv—Ag4B—Cu4B—Pb4A^ii	−147 (5)
Sb9B^iv—Ag4B—Ag4B'—Pb4A^ii	−89 (4)	S12B^iv—Ag4B—Cu4B—Sb4A^ii	−134 (7)
Sb9B^iv—Ag4B—Ag4B'—Cu4B	−66 (8)	S12B^iv—Ag4B—Cu4B—Ag4B'	95 (8)
Sb9B^iv—Ag4B—Ag4B'—Sb8B^iv	57 (3)	S12B^iv—Ag4B—Cu4B—Sb8A^iv	47.4 (17)
Sb9B^iv—Ag4B—Ag4B'—Sb11B	−171.2 (6)	S12B^iv—Ag4B—Cu4B—Sb8B^iv	43.5 (9)
Sb9B^iv—Ag4B—Ag4B'—Pb11B	−177.8 (13)	S12B^iv—Ag4B—Cu4B—Sb9B^iv	−25.1 (11)
Sb9B^iv—Ag4B—Ag4B'—Ag12B	126 (5)	S12B^iv—Ag4B—Cu4B—Sb11B	158.4 (13)
Sb9B^iv—Ag4B—Ag4B'—S4B	−132.2 (10)	S12B^iv—Ag4B—Cu4B—Pb11B	154.5 (15)
Sb9B^iv—Ag4B—Ag4B'—S7B	127.8 (12)	S12B^iv—Ag4B—Cu4B—Ag12B	102.5 (12)
Sb9B^iv—Ag4B—Ag4B'—S8B	−79 (4)	S12B^iv—Ag4B—Cu4B—S4B	−161.1 (15)
Sb9B^iv—Ag4B—Ag4B'—S12B^iv	1 (3)	S12B^iv—Ag4B—Ag4B'—Pb4A^ii	−90 (5)
Sb9B^iv—Cu4B—Ag4B'—Pb4A^ii	169 (9)	S12B^iv—Ag4B—Ag4B'—Cu4B	−67 (7)
Sb9B^iv—Cu4B—Ag4B'—Ag4B	51 (6)	S12B^iv—Ag4B—Ag4B'—Sb8B^iv	56.2 (16)
Sb9B^iv—Cu4B—Ag4B'—Sb8B^iv	−66 (2)	S12B^iv—Ag4B—Ag4B'—Sb9B^iv	−1 (4)
Sb9B^iv—Cu4B—Ag4B'—Sb11B	163.1 (16)	S12B^iv—Ag4B—Ag4B'—Sb11B	−172 (4)
Sb9B^iv—Cu4B—Ag4B'—Pb11B	164 (2)	S12B^iv—Ag4B—Ag4B'—Pb11B	−178 (4)
Sb9B^iv—Cu4B—Ag4B'—Ag12B	−136.9 (16)	S12B^iv—Ag4B—Ag4B'—Ag12B	126 (7)
Sb9B^iv—Cu4B—Ag4B'—S4B	124.0 (10)	S12B^iv—Ag4B—Ag4B'—S4B	−133 (3)
Sb9B^iv—Cu4B—Ag4B'—S7B	−153 (7)	S12B^iv—Ag4B—Ag4B'—S7B	127 (3)
Sb9B^iv—Cu4B—Ag4B'—S8B	57.3 (10)	S12B^iv—Ag4B—Ag4B'—S8B	−79 (5)
Sb9B^iv—Cu4B—Ag4B'—S12B^iv	−35.9 (16)	S12B^iv—Cu4B—Ag4B'—Pb4A^ii	−155 (10)
Sb10B—Sb11B—Pb11B—Ag4B	−113 (5)	S12B^iv—Cu4B—Ag4B'—Ag4B	87 (7)
Sb10B—Sb11B—Pb11B—Cu4B	−127 (2)	S12B^iv—Cu4B—Ag4B'—Sb8B^iv	−30 (3)
Sb10B—Sb11B—Pb11B—Ag4B'	−126 (4)	S12B^iv—Cu4B—Ag4B'—Sb9B^iv	35.9 (16)
Sb10B—Sb11B—Pb11B—Sb11A	26 (17)	S12B^iv—Cu4B—Ag4B'—Sb11B	−160.9 (10)
Sb10B—Sb11B—Pb11B—Ag12B	168.6 (5)	S12B^iv—Cu4B—Ag4B'—Pb11B	−160.4 (15)
Sb10B—Sb11B—Pb11B—S4B	−91 (3)	S12B^iv—Cu4B—Ag4B'—Ag12B	−101.0 (14)
Sb10B—Sb11B—Pb11B—S7A^ii	−171 (4)	S12B^iv—Cu4B—Ag4B'—S4B	159.9 (17)
Sb10B—Sb11B—Pb11B—S7B	−179 (100)	S12B^iv—Cu4B—Ag4B'—S7B	−117 (6)
Sb10B—Sb11B—Pb11B—S14A	4 (5)	S12B^iv—Cu4B—Ag4B'—S8B	93.2 (14)
Sb10B—Sb11B—Pb11B—S14B^ii	−20 (11)	S14A—Sb11B—Pb11B—Ag4B	−117 (7)
Sb11B—Cu4B—Ag4B'—Pb4A^ii	6 (10)	S14A—Sb11B—Pb11B—Cu4B	−131 (5)
Sb11B—Cu4B—Ag4B'—Ag4B	−112 (7)	S14A—Sb11B—Pb11B—Ag4B'	−130 (6)
Sb11B—Cu4B—Ag4B'—Sb8B^iv	131 (3)	S14A—Sb11B—Pb11B—Sb11A	22 (13)
Sb11B—Cu4B—Ag4B'—Sb9B^iv	−163.1 (16)	S14A—Sb11B—Pb11B—Ag12B	165 (5)
Sb11B—Cu4B—Ag4B'—Pb11B	0.5 (11)	S14A—Sb11B—Pb11B—S4B	−95 (3)
Sb11B—Cu4B—Ag4B'—Ag12B	59.9 (10)	S14A—Sb11B—Pb11B—S7A^ii	−174.5 (9)
Sb11B—Cu4B—Ag4B'—S4B	−39.1 (11)	S14A—Sb11B—Pb11B—S7B	177 (18)
Sb11B—Cu4B—Ag4B'—S7B	44 (6)	S14A—Sb11B—Pb11B—S14B^ii	−24 (16)
Sb11B—Cu4B—Ag4B'—S8B	−105.8 (15)	S14B^xiii—Sb11B—Pb11B—Ag4B	160 (4)
Sb11B—Cu4B—Ag4B'—S12B^iv	160.9 (10)	S14B^ii—Sb11B—Pb11B—Ag4B	−93 (14)
Pb11B—Ag4B—Cu4B—Pb4A^ii	58 (5)	S14B^xiii—Sb11B—Pb11B—Cu4B	145.8 (17)
Pb11B—Ag4B—Cu4B—Sb4A^ii	71 (6)	S14B^ii—Sb11B—Pb11B—Cu4B	−107 (13)
Pb11B—Ag4B—Cu4B—Ag4B'	−60 (8)	S14B^xiii—Sb11B—Pb11B—Ag4B'	147 (3)
Pb11B—Ag4B—Cu4B—Sb8A^iv	−107 (3)	S14B^ii—Sb11B—Pb11B—Ag4B'	−106 (13)
Pb11B—Ag4B—Cu4B—Sb8B^iv	−110.9 (10)	S14B^xiii—Sb11B—Pb11B—Sb11A	−61 (16)
Pb11B—Ag4B—Cu4B—Sb9B^iv	−179.6 (10)	S14B^ii—Sb11B—Pb11B—Sb11A	47 (26)
Pb11B—Ag4B—Cu4B—Sb11B	3.9 (10)	S14B^xiii—Sb11B—Pb11B—Ag12B	82 (3)
Pb11B—Ag4B—Cu4B—Ag12B	−52.0 (11)	S14B^ii—Sb11B—Pb11B—Ag12B	−171 (11)
Pb11B—Ag4B—Cu4B—S4B	44.4 (11)	S14B^ii—Sb11B—Pb11B—S4B	−70 (13)
Pb11B—Ag4B—Cu4B—S12B^iv	−154.5 (15)	S14B^xiii—Sb11B—Pb11B—S4B	−177.7 (4)
Pb11B—Ag4B—Ag4B'—Pb4A^ii	89 (5)	S14B^ii—Sb11B—Pb11B—S7A^ii	−150 (15)
Pb11B—Ag4B—Ag4B'—Cu4B	111 (8)	S14B^xiii—Sb11B—Pb11B—S7A^ii	102 (2)
Pb11B—Ag4B—Ag4B'—Sb8B^iv	−125 (3)	S14B^ii—Sb11B—Pb11B—S7B	−159 (6)
Pb11B—Ag4B—Ag4B'—Sb9B^iv	177.8 (13)	S14B^xiii—Sb11B—Pb11B—S7B	94 (15)
Pb11B—Ag4B—Ag4B'—Sb11B	6.7 (13)	S14B^xiii—Sb11B—Pb11B—S14A	−83 (3)
Pb11B—Ag4B—Ag4B'—Ag12B	−56 (5)	S14B^ii—Sb11B—Pb11B—S14A	24 (16)
Pb11B—Ag4B—Ag4B'—S4B	45.6 (17)	S14B^xiii—Sb11B—Pb11B—S14B^ii	−107 (14)

Symmetry codes: (i) x−1, y, z; (ii) x+1, y, z; (iii) −x+1/2, y−1/2, −z+3/2; (iv) −x+3/2, y−1/2, −z+3/2; (v) −x+1, −y+1, −z+2; (vi) −x+2, −y+1, −z+2; (vii) x+1/2, −y+3/2, z+1/2; (viii) x−1/2, −y+3/2, z+1/2; (ix) −x+1/2, y+1/2, −z+3/2; (x) −x+3/2, y+1/2, −z+3/2; (xi) x−1/2, −y+3/2, z−1/2; (xii) x+1/2, −y+3/2, z−1/2; (xiii) −x+1, −y+1, −z+1; (xiv) −x+2, −y+1, −z+1; (xv) −x, −y+1, −z+1.