Figure 2
ENaCt solvent/oil combinations that provided crystals suitable for SCXRD analysis [grade 4 crystals (Fig. S2, supporting information)] for dihydropyridines 1–6 y-axis: number of wells containing crystals of grade 4 and x-axis: solvent (a-l) used for the experiment [DMSO (a), DMF (b), MeOH (c), 2,2,2-TFE (d), toluene (e), DCE (f), 2-MeTHF (g), 1,4-dioxane (h), EtOAc (i), MeCN (j), MIBK (k) MeNO2 (l)]. |