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Figure 5
Twinning in Evl. TEM images of crystals and sections through diffraction data are shown: (a) untwinned crystal, (b) h0l section of an untwinned crystal. (c) Schematic projection of the crystal structure of an untwinned crystal of Evl. (d) Twinned crystal, (e) h0l section of a twinned crystal. (f) The scheme of twinning of Evl with two twin components related by a twofold rotation around the a axis. The red and black arrows show the orientations of the Fe–H2O and Nb–O bonds, respectively; the black ellipse indicates a twofold axis acting as a twin operator; the blue dashed line shows the border between different twin domains related by the twofold axis parallel to the a axis. |
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menu![[Figure 5]](je5066fig5.jpg)