Figure 1
Anomalous difference Patterson map. Harker section (v = 1/2). Self-vectors are shown as cyan circles. Heavy-atom positions found by SHELXD were 0.610, 0.797, 0.126 with occupancy 1, 0.210, 0.710, 0.485 with occupancy 0.9 and 0.033, 0.333, 0.065 with occupancy 0.9. SOLVE positions were 0.610, 0.796, 0.126 with occupancy 0.44 and B = 34 Å2, 0.210, 0.710, 0.485 with occupancy 0.40 and B = 28 Å2 and 0.033, 0.333, 0.065 with occupancy 0.40 and B = 31 Å2. |