Figure 6
Illustration of the different peaks obtained from a typical orientation (φ) image. A threshold of sinδ ≥ 0.1 was set for all the peak analyses. It can be seen that the ordered region of the crystal results in a sharp peak as in (a) and (b). After a threshold of 0.1 was set no data remained in region (c), so it is not plotted. The loops in which the crystals are mounted are birefringent, so selection of region (d) also results in a sharp peak. The area used for analysis was chosen such that the loop did not contribute to the peak fitted to the crystal data. Disordered regions such as the solvent produce broader peaks (e). |