Figure 5
(a) The fast-rotation function and (b) the slow-rotation function plotted against κ at (φ, ψ) = (90°, 110°). The integration radii of the calculations were five times the highest resolution limits. Each rotation function was calculated with 71 269 reflections in the resolution range 50–10 Å. The height of the crystallographic symmetry was normalized to 1000. |