Figure 4
Crystal capillary mount to accommodate temperatures of >303 K. (a) P, brass pin; I, insulating glass capillary; E, epoxy glue; C, PYP crystal; S, stabilizing solution; G, temperature-controlled gas stream. (b) Laser-illuminated volume of the crystal (red dashed box). The capillary wall (thick black line) is temperature-controlled. Black arrows: heat diffuses out. |