Figure 5
GNNQQNY needle crystals preferentially orient in the sample-delivery stream. (a) Optical microscope image of GNNQQNY needle crystals. (b) The basis vectors of GNNQQNY crystals indexed by cctbx.small_cell in this work are displayed in reciprocal space. a*, b* and c* are displayed in red, green and blue, respectively. Axes are in units of reciprocal ångströms. Two views of the same set of vectors are displayed from different angles. Needle crystals in the injection stream tend to align along the x* axis, which is orthogonal to the beam. The real-space b axis corresponds to the length of the needle crystals and is coaxial with the direction of the hydrogen bonds formed between strands of the β-sheet. |