Figure 2
Rsinglets (triangles) and Rall (circles) values for deconvolution of the twinned O1M data set (a) and the artificially twinned O1BFS data set (b). Rall values diverge while Rsinglets values converge; singlet reflections are not affected by twinning operators. If NCS operators are rotated by 90° in the x axis and deconvolution is attempted (c), the R factors do not show signs of success, as expected. |