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Figure 1
Experimental sequence in ZOO. (a) The basic sequence for data collection in ZOO. The final crystal alignment is based on X-ray diffraction scanning. (b) Illustration of the `normal rotation scheme'. (1) Sample mounting, (2) loop centering, (3) defining the raster-scan area, (4) low-dose raster scanning, (5) crystal detection, (6) crystal alignment, (7) vertical diffraction scanning at side orientation (90° from the face angle) and (8) crystal alignment. Finally, rotation data is collected from the defined 3D coordinates. |
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