Figure 5
Degree of twinning and orientation of the tetramer in the P21 unit cell of Mg2+-containing crystals of F. tularensis FBPase. (a) SRF of data collected from crystal A, for which the twinning law was impossible to estimate. (b) SRF from crystal B that was interpreted as two 222 tetramers (axes directions labeled as PQR and P′Q′R′ related by a crystallographic 21 screw axis; horizontal) with a twinning fraction of 0.433 as refined by REFMAC5 (Murshudov et al., 2011). The structure was solved and fully refined (PDB entry 7js3). Reproduced with permission from Selezneva et al. (2020). |