Figure 3
Diffuse scattering scaling model after refinement. The model was refined globally in mdx2 to all 17 wedges in the multi-crystal insulin data set. (a) Columns show each model parameter as a function of observation coordinates (rotation angle φ, detector position and scattering-vector magnitude s). Each row corresponds to a 50° wedge (sweep) of data (only three are shown for clarity). Panels, from left to right, show the scale correction (b parameter), the offset correction (c parameter) and the absorption correction (a parameter) at the beginning, middle and end of the rotation range. (b) The detector correction (d parameter) refined globally to all 17 wedges. |