Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 63| Part 9

ISSN: 2056-9890

September 2007 issue

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Cover illustration: Several single-crystal diffraction studies have been reported for L-asparagine monohydrate, but until now no determination of the structure of anhydrous L-asparagine. The molecules exist in their zwitterionic form but have quite different C=O bond lengths due to different hydrogen-bond environments. The conformation of the side chain is trans, which distinguishes it sigificantly from that of L-asparagine monohydrate. See Yamada, Hashizume, Shimizu & Yokoyama [Acta Cryst. (2007), E63, o3802-o3803].

inorganic compounds

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Nd(CO₃)(OH) from single-crystal data

W.-J. Feng, G.-P. Zhou, Z.-B. Liu and Y. Xu

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Strontium magnesium borate, Sr₂Mg(BO₃)₂

G.-J. Chen, Y.-C. Wu and P.-Z. Fu

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Reinvestigation of trisodium dihydroxidotetraoxidoneptunate(VII)

M. S. Grigoriev and N. N. Krot

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Crystal growth and redetermination of strontium nitride iodide, Sr₂NI

A. S. Bailey, D. H. Gregory, P. Hubberstey and C. Wilson

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Sr₁₁InSb₉ grown from molten In

J. Hullmann, S. Xia and S. Bobev

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metal-organic compounds

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{[(5-Bromo-2-oxidophenyl)methyleneamino]methanesulfonato-κ³O,N,O′}(methanol-κO)(1,10-phenanthroline-κ²N,N′)cadmium(II)

J.-S. Xu, C.-H. Zhang, D.-Z. Kuang, Y.-L. Feng and Y.-L. Peng

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Heptaaqua(4-nitrobenzoato-κ²O,O′)strontium(II) 4-nitrobenzoate dihydrate

B. R. Srinivasan, P. Raghavaiah and J. V. Sawant

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(Diphenyl sulfoxide)dimethyl(η⁵-pentamethylcyclopentadienyl)rhodium(III)

A. Decken, A. Michaud, S. Mathiotte and F.-G. Fontaine

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Tris(2,2′-bipyridine-κ²N,N′)copper(II) bis(tetrafluoridoborate)

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Bis{methyl [1-(6-acetyl-2-pyridyl)ethylidene]hydrazinecarbodithioato}nickel(II)

M. Akbar Ali, A. H. Mirza and P. V. Bernhardt

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{6,6′-Dimethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}methanol-μ-nitrato-dinitratosamarium(III)nickel(II)

Y. Sui, J.-H. Zhang, R.-H. Hu and R.-Q. Jiang

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Poly[[aqua(μ₂-4,4′-bipyridine)(μ₅-4,4′-oxydibenzene-1,2-carboxylato)dizinc(II)] 4,4′-bipyridine hemisolvate]

P.-X. Yin, Z.-J. Li, X.-Y. Cao, Y.-Y. Qin and Y.-G. Yao

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Tetra-μ₃-bromido-tetrakis[trimethylplatinum(IV)]

A.-R. Song, I.-C. Hwang and K. Ha

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Hexaaquacobalt(II) 3-ammonionaphthalene-1,5-disulfonate tetrahydrate

D. J. Genther, P. J. Squattrito, K. Kirschbaum and A. A. Pinkerton

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Hexaaquazinc(II) 3-ammonionaphthalene-1,5-disulfonate tetrahydrate

D. J. Genther, P. J. Squattrito, K. Kirschbaum and A. A. Pinkerton

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catena-Poly[[[diaqua(3-nitrobenzoato-κ²O,O′)erbium(III)]-di-μ-3-nitrobenzoato-κ⁴O:O′] 2,2′-diamino-4,4′-bi-1,3-thiazole]

B.-X. Liu, G.-H. Chen and L.-J. Zhang

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Dichlorido[1-(1-naphthylmethyl)-3-(2-pyridyl)-1H-pyrazole-κ²N²,N³]zinc(II)

C.-S. Liu, L.-F. Yan and J.-J. Wang

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Diaquabis[2-(2-pyridylmethoxy)pyrazine-κN⁴]bis(thiocyanato-κN)manganese(II)

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Diaquabis(2,4-dioxo-1,2,3,4-tetrahydropyrimidine-5-carboxylato-κ²O,O′)cobalt(II)

H.-H. Xing, Z.-L. Chen and S. W. Ng

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Redetermination of catena-poly[[nitrato(1,10-phenanthroline)copper(II)]-μ-nitrato]

X.-C. Zhou and Y.-Q. Liu

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{2-[(2-Aminophenyl)iminomethyl]-4-bromophenolato-κ³N,N′,O}chloridobis(dimethyl sulfoxide-κS)ruthenium(II)

N. E. Eltayeb, S. G. Teoh, S. Chantrapromma, H.-K. Fun and K. Ibrahim

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Azido{2,4-dibromo-6-[2-(diethylamino)ethyliminomethyl]phenolato}copper(II)

K. Li, H. Zhang, X.-N. Wang, J.-Y. Peng and Y.-P. Diao

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μ-Carbonyl-1:2κ²C-carbonyl-1κC-(1η⁵-cyclopentadienyl)(μ-phenylvinylidene)bis(triphenylphosphine-2κP)rheniumplatinum(Re—Pt) diethyl ether hemisolvate

A. D. Vasiliev, O. S. Chudin and A. B. Antonova

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Poly[(μ₃-N,N-dibenzyldithiocarbamato-κ⁴S,S′:S:S′)silver(I)]

X. Yin, M.-B. Xie, W.-G. Zhang and J. Fan

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Bis{2,4-dibromo-6-[3-(cyclohexylamino)propyliminomethyl]phenolato}cobalt(III) perchlorate

K. Li, S.-S. Huang, Q. Zhou, H. Li and Y.-P. Diao

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{6,6′-Dimethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}methanol-μ-nitrato-dinitratopraseodymium(III)zinc(II)

Y. Sui, X.-N. Fang and M.-W. Yuan

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{6,6′-Dimethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato}methanol-μ-nitrato-dinitratolutetium(III)zinc(II)

Y. Sui, Y.-H. Sui, Q.-Y. Luo and Y.-D. Wang

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Bis(8-methylquinolinium) tetrachloridoferrate(III) chloride

R. Kruszynski, D. Wyrzykowski, E. Styczeń and L. Chmurzyński

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{3,3′-[Ethane-1,2-diylbis(methylimino)]bis(propane-1-thiolato)}nickel(II)

C. A. Grapperhaus, M. G. O'Toole and M. S. Mashuta

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μ-4,4′-Bipyridine-κ²N:N′-bis[aqua(nitrato-κO)(1,10-phenanthroline-κ²N,N′)copper(II)] dinitrate

Z.-X. Du and J.-X. Li

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Tetraaquabis(4,4′-bipyridine)manganese(II) pyridine-2,6-dicarboxylate tetrahydrate

Y.-X. Gao, L.-B. Wang and Y.-L. Niu

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Bis[μ-2,4-dibromo-6-(2-pyridylmethylaminomethyl)phenolato]bis[nitratocopper(II)]

J.-C. Ma, J. Yang and J.-F. Ma

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Tetrakis(1H-imidazole-κN³)(perchlorato-κO)copper(II) perchlorate dimethylamine disolvate

Y.-X. Zhou, G.-X. Cheng, B.-L. Wu and H.-Y. Zhang

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Poly[[μ-dioxane-κ²O:O′-dioxane-κO-μ-diphenylamido-κ²N:N-potassium] dioxane solvate]

M. Gärtner, H. Görls and M. Westerhausen

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Bis(μ-diphenylamido-κ²N:N)bis[tris(tetrahydrofuran-κO)potassium(I)]

M. Gärtner, H. Görls and M. Westerhausen

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Dichlorido{2-[3-(2-pyridyl)pyrazol-1-ylmethyl]pyridine}zinc(II)

C.-S. Liu and J.-N. Zhou

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Azido{2,4-dibromo-6-[(2-diethylaminoethylimino)methyl]phenolato}nickel(II)

K. Li, S.-S. Huang, B.-J. Zhang, D.-L. Meng and Y.-P. Diao

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trans-Bis[(S)-2-(4-ethyl-4,5-dihydro-1,3-oxazol-2-yl)phenolato-κ²N,O]copper(II)

Y. Zhang, T.-F. Liu, W.-G. Xu, B.-T. Zhao and J.-G. Wang

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Aqua{6,6-dimethyl-2,2′-[o-phenylenebis(nitrilomethylidyne)]diphenolato-κ⁴O,N,N′,O′}zinc(II) chloroform solvate

N. E. Eltayeb, S. G. Teoh, S. Chantrapromma, H.-K. Fun and K. Ibrahim

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Poly[[tetra-μ₂-aqua-diaqua-μ₆-oxalato-barium(II)] 2,4,6-trinitrophenolate monohydrate]

P.-Z. Hong, W.-D. Song and Z.-H. Wu

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Dichloridobis(methanol-κO)bis(6-methyl-3-phenyl-1,2,4-triazolo[3,4-b][1,3,4]thiadiazole-κN¹)cadmium(II)

P.-Z. Hong, W.-D. Song and Z.-H. Wu

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Bis[2-(1H-benzimidazol-2-yl-κN³)-4,6-dibromophenolato-κO]nickel(II)

Y. Wu, B. Xie, L. Zou, J.-S. Feng and Z. Hu

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Diacetato(1,4,8,11-tetraazacyclotetradecane)manganese(III) perchlorate monohydrate

I.-C. Hwang and K. Ha

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Tetrakis(μ₃-2-{[1,1-bis(hydroxymethyl)-2-oxidoethyl]iminomethyl}phenolato)tetracopper(II)

J.-F. Dong, L.-Z. Li, H.-Y. Xu and D.-Q. Wang

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[8,17-Bis(5-nitro-2-oxidobenzyl-κO)-5,6:19,20-dibenzo-1,4,11,14-tetraoxa-8,17-diazacycloeicosane-κ⁴N,N′]copper(II) chloroform solvate

T.-T. Han, J.-F. Ma, G.-J. Ping and Z.-F. Jia

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catena-Poly[[manganese(II)-μ-[N,N,N′,N′-tetrakis(2-pyridylmethyl)hexane-1,6-diamine]] bis(perchlorate) acetone disolvate dihydrate]

I.-C. Hwang and K. Ha

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catena-Poly[[[diaqualithium(I)]-μ-bis(1H-imidazol-1-yl)methane-κ²N³:N^3′] chloride]

I.-C. Hwang and J. A. Chang

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[N,N′-Bis(6-methoxysalicylidene)-1,3-diaminopropane]nickel(II)

M. H. Habibi, R. Mokhtari, R. W. Harrington and W. Clegg

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Bis[chloridobis(triphenylphosphine)copper(I)-μ-chlorido]bis(1,2-diaminopropane)copper(II) acetonitrile disolvate

M. H. Habibi, M. Mikhak, R. W. Harrington and W. Clegg

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cis-Bis(acetylacetonato)diaquachromium(III) perchlorate monohydrate

N. Arulsamy and J. L. Crawford

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trans-Bis(acetonitrile-κN)bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato-κ²O,O′)nickel(II)

H. Southerland, J. Donovan, B. Twamley and J. Manson

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Bis(1,10-phenanthroline-5,6-dione-κ²N,N′)silver(I) perchlorate

J. Onuegbu, R. J. Butcher, C. Hosten, U. C. Udeochu and O. Bakare

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catena-Poly[[diaquabis(methanol)cobalt(II)]-μ-phthalato]

C.-Q. Liu, X.-T. Yang, L.-L. An, R. Li and J.-M. Shi

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Poly[[[μ₄-4,4′-carbonylbis(benzene-3,4-dicarboxylato)]tetrakis(1,10-phenanthroline)dipalladium(II)] dihydrate]

Z.-F. Li, S.-W. Wang, Q. Zhang and X.-J. Yu

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Dichlorido(dimethyl sulfoxide-κO)(1,10-phenanthroline-5,6-dione-κ²N,N′)copper(II) dimethyl sulfoxide monohydrate

G.-J. Xu, M.-J. Xie, L. Feng, S.-P. Yan and D.-Z. Liao

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catena-Poly[copper(I)-di-μ-chlorido-copper(I)-bis[μ-bis(pyrimidin-2-ylsulfanyl)methane-κ²N:N′]]

W.-J. Shi and Z.-Q. Gong

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Poly[diaqua-μ₃-malonato-μ-pyrazine-diiron(II)]

Z.-F. Li, Y. Liu, Q. Zhang and X.-J. Yu

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Diaqua[2,6-bis(2,6-diethyl-4-sulfonatophenyl)-3,5-dimethyl-2,6-diazoniaheptan-4-ido]sodium(I)

X. Guo, Q. Wang, K. Harms and H. Sun

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catena-Poly[[(benzoato-κ²O,O′)chloridocadmium(II)]-μ-2,2′-diphenyl-1,1′-(butane-1,4-diyl)diimidazole-κ²N³:N^3′]

Y.-Y. Liu, J.-F. Ma and L.-P. Zhang

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Dichloridodiglycinezinc dihydrate

S. Mary Navis Priya, B. Varghese, J. Mary Linet and S. Jerome Das

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Bis(μ-3,5-di-2-pyridyl-1,2,4-triazolato-κ⁴N¹,N⁵:N²,N³)bis[(methanol-κO)(thiocyanato-κN)iron(II)]

G.-B. Jiang, X.-N. Zeng, Y.-S. Fang, M.-H. Zeng and S. W. Ng

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Tetraimidazolium bis(imidazole-κN)di-μ₄-oxido-tetra-μ₃-oxido-hexa-μ₂-oxido-tetradecaoxidooctamolybdate(VI) monohydrate

C.-B. Li, Z.-G. Zong, J. Gong and S. W. Ng

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Poly[[pentaaqua[_