Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

IUCr IT WDC

home archive editors for authors for readers submit open access

issue contents

CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 65| Part 4

ISSN: 2056-9890

April 2009 issue

Highlighted illustration

Cover illustration: The structure of the 19-electron organometallic reducing agent decamethylcobaltocene, [bis-(pentamethylcyclopentadienyl)cobalt(II)], [Co(C₁₀H₁₅)₂], fills a long-term gap in the literature. Recrystallization from a saturated hexamethyldisiloxane solution of the compound at 235 K finally provided crystals suitable for an X-ray structure determination and the structure is found to be isomorphous with decamethylferrocene and the low temperature polymorph of decamethylmanganocene. See Clark, Brennessel & Holland [Acta Cryst. (2009). E65, m391].

inorganic compounds

link to html

An orthorhombic polymorph of the ultraphosphate YP₅O₁₄

A. Mbarek, A. Oudahmane, M. El-Ghozzi and D. Avignant

Read article

link to html

[Cu₂(HF₂)(H₂O)₈][FeF₆]·2H₂O

A. Le Bail and A.-M. Mercier

Read article

link to html

Gadolinium scandium germanide, Gd₂Sc₃Ge₄

S. Misra and G. J. Miller

Read article

link to html

The Chevrel phase In_4.07Mo₁₅S_11.87Se_7.13 with mixed chalcogenide occupancy

Y.-S. Lee and S. K. Kang

Read article

link to html

Tetrasodium (dihydrogenheptaoxidodigermanato)bis(dihydrogentetraoxidogermanato)dicopper(II) monohydrate

Y.-F. Li, D.-P. Li, C.-L. Shi, Y.-S. Hu and L. Jin

Read article

link to html

A polymorph structure of copper(II) hydrogenphosphite dihydrate

L. Yang, S. Li and Q. Wang

Read article

link to html

[Cu₂(HF₂)(H₂O)₈][AlF₆]·2H₂O

Read article

link to html

Na₄Fe²⁺Fe³⁺(PO₄)₃, a new synthetic NASICON-type phosphate

Read article

metal-organic compounds

link to html

Poly[(μ₂-2-hydroxy-2-methylpropionato-κ³O¹,O²:O^1′)(μ₂-2-hydroxy-2-methylpropionato-κ²O¹:κO^1′)dioxidouranium(VI)]

T. Yoshimura, H. Kikunaga and A. Shinohara

Read article

link to html

trans-Di-μ-acetato-[μ-N,N-bis(diphenylphosphino)aniline]bis[chloridomolybdenum(II)](Mo—Mo)–dichloromethane–tetrahydrofuran (1/0.3/1.7)

M. Hapke, A. Wöhl, S. Peitz, A. Spannenberg and U. Rosenthal

Read article

link to html

Diaquadibromidobis[3-dimethylamino-1-(4-pyridyl-κN)prop-2-en-1-one]cadmium(II)

H.-Z. Dong, Z.-L. Chu and N.-L. Hu

Read article

link to html

Dichlorido-2κ²Cl-{μ-6,6′-dimethoxy-2,2′-[propane-1,3-diylbis(nitrilomethylidyne)]diphenolato-1κ⁴O¹,N,N′,O^1′:2κ²O¹,O^1′}copper(II)zinc(II)

Q. Liu, S. Ge and G. Cui

Read article

link to html

catena-Poly[[diaquazinc(II)]-μ-4,4′-(methylenedioxy)dibenzoato]

L. Xu, Y. Guo and X. Yuan

Read article

link to html

Poly[bis(methanol-κO)tris(μ-pyrimidine-κ²N:N′)tetrakis(thiocyanato-κN)dinickel(II)]

M. Wriedt, S. Sellmer, I. Jess and C. Näther

Read article

link to html

Poly[μ-chlorido-[μ₄-5-(4-pyridyl)tetrazolato]dicopper(I)]

C.-K. Wang and X.-Y. Li

Read article

link to html

Tetraquabis(5-fluorosaccharinato)nickel(II)

L. Peterson, J. Kelley, L. R. Peterson Jr, M. D. Smith and H.-C. zur Loye

Read article

link to html

(μ-3,4-Diacetylhexa-2,4-diene-2,5-diolato-κ⁴O²,O³:O⁴,O⁵)bis[aqua(1,10-phenanthroline-κ²N,N′)copper(II)] bis(tetrafluoridoborate) monohydrate

J. A. Tovilla, S. Hernández-Ortega and J. Valdés-Martínez

Read article

link to html

Tris(ethylenediamine)cobalt(II) bis(tetrahydroxypentaborate) dihydrate

L. Zhao, P. Li and B. Cao

Read article

link to html

Bis[4-chloro-2-(iminomethyl)phenolato]copper(II)

Read article

link to html

Poly[[[diaquacobalt(II)]-bis[μ₂-1,1′-(butane-1,4-diyl)diimidazole-κ²N³:N^3′]] dichloride tetrahydrate]

Y. Su, Y.-J. Hou, Z.-Z. Sun, G.-F. Hou and J.-S. Gao

Read article

link to html

(2,2′-Dimethyl-4,4′-bi-1,3-thiazole-κ²N,N′)bis(thiocyanato-κS)mercury(II)

N. Safari, V. Amani, A. Abedi, B. Notash and S. W. Ng

Read article

link to html

Bis(ferrocenecarbaldehyde thiosemicarbazonato-κ²N¹,S)zinc

M. R. Vikneswaran, S. G. Teoh, I. A. Razak and H.-K. Fun

Read article

link to html

catena-Poly[[diaquacobalt(II)]-bis(μ-3-carboxyadamantane-1-carboxylato-κ²O¹:O³)]

L.-M. Tang, J.-H. Xu, X.-Y. Han and W. Xu

Read article

link to html

Aquabis(benzoato-κO)bis(1H-imidazole-κN³)copper(II) monohydrate

B.-B. Liu, T. Weng and H.-Z. Xie

Read article

link to html

Diaquabis[5-(5-carboxy-2-pyridyl)tetrazolato-κ²N¹,N⁵]cadmium(II) dihydrate

H. Yin, L. Wang and Q. Nie

Read article

link to html

Tetra(chlorido/iodido)(1,10-phenanthroline)platinum(IV) hemi[di(chlorine/iodine)]

N.-H. Kim and K. Ha

Read article

link to html

Diaquabis(2,2′-biimidazole)cobalt(II) 4,4′-dicarboxybiphenyl-3,3′-dicarboxylate

J. Kang, C.-C. Huang, L.-S. Zhai, X.-H. Qin and Z.-Q. Liu

Read article

link to html

Diaquabis[5-(2-pyridyl)tetrazolato-κ²N¹,N⁵]iron(II)

M. Hu, S.-T. Ma, L.-Q. Guo and S.-M. Fang

Read article

link to html

Poly[aqua(μ₅-2-oxido-4-sulfonatobenzoato)lanthanum(III)]

C.-F. Zhu, X. Li and E. Sheng

Read article

link to html

Bis(3-methylpyridinium) tetrachloridocuprate(II)

N. Sengottvelan, Y.-S. Lee, H.-S. Lim, Y.-I. Kim and S. K. Kang

Read article

link to html

Phyllo-poly[[μ₂-1,4-bis(cyclohexylsulfanylmethyl)benzene-κ²S:S′](μ₂-nitrato-κ²O:O′)silver(I)]

T. H. Kim, Y. W. Shin, K.-M. Park and J. Kim

Read article

link to html

catena-Poly[[(dimethylformamide-κO)copper(II)]-bis(μ-4-nitrophenylcyanamido-κ²N¹:N³)]

H. Chiniforoshan, S. Jalilpour, B. Shirinfar and H. R. Khavasi

Read article

link to html

Poly[octa-μ-aqua-tetraaquabis(μ-5-sulfonatobenzene-1,3-dicarboxylato)cobalt(II)tetrasodium]

B.-Y. Zhang, J.-J. Nie and D.-J. Xu

Read article

link to html

Diaquabis(N,N-diethylnicotinamide-κN¹)bis(4-formylbenzoato-κO)cobalt(II)

M. Sertçelik, B. Tercan, E. Şahin, H. Necefoğlu and T. Hökelek

Read article

link to html

Bis(η⁵-pentamethylcyclopentadienyl)cobalt(II)

M. M. Clark, W. W. Brennessel and P. L. Holland

Read article

link to html

Di-μ-chromato-κ⁴O:O′-bis[bis(phenanthroline-κ²N,N′)cadmium(II)] dihydrate

H.-X. Liu, F.-F. Jian and J. Wang

Read article

link to html

Poly[hemi(ethylenediammonium) [di-μ-oxalato-indium(III)] dihydrate]

Q. Sun, Y. Liu, H. Li and Z. Luo

Read article

link to html

trans-Dichloridobis(2-methylaniline-κN)palladium(II)

V. Bon, A. Dudko, S. Orysyk and V. Pekhnyo

Read article

link to html

Bis{2-[6-(1H-benzimidazol-2-yl-κN³)-2-pyridyl-κN]benzimidazolato-κN}manganese(II)

X.-Q. Bai and S.-H. Zhang

Read article

link to html

Dicyclohexyl[N-(3-methoxy-2-oxidobenzylidene)valinato-κ³O,N,O′]tin(IV)

H.-J. Yang and Y.-Q. Dang

Read article

link to html

{μ-6,6′-Dimethoxy-2,2′-[ethane-1,2-diylbis(nitrilomethylidyne)]diphenolato-1κ⁴O⁶,O¹,O^1′,O^6′:2κ⁴O¹,N,N′,O^1′}(methanol-1κO)(perchlorato-1κO)nickel(II)sodium

Read article

link to html

Isopropyl N-[1′-(methoxycarbonyl)ferrocenyl]carbamate–ethyl N-[1′-(methoxycarbonyl)ferrocenyl]carbamate (0.6/0.4)

A. Lataifeh, H.-B. Kraatz and M. C. Jennings

Read article

link to html

Low-temperature rerefinement of nonmerohedrally twinned tripyridinium bis[tetrabromidoferrate(III)] bromide

Read article

link to html

{6,6′-Diethoxy-2,2′-[2,2-dimethylpropane-1,3-diylbis(nitrilomethylidyne)]diphenolato}nickel(II) monohydrate

H. Kargar, A. Jamshidvand, H.-K. Fun and R. Kia

Read article

link to html

[μ-Bis(trimethylsilyl)amido]bis[μ-N,N-dimethyl-N′,N′′-bis(trimethylsilyl)guanidinato]-triangulo-tricopper(I)

D. Guo, X. Qiao, H.-B. Tong and M. Zhou

Read article

link to html

catena-Poly[[bis(N-ethylethylenediamine-κ²N,N′)copper(II)]-μ-cyanido-κ²N:C-[dicyanido-κ²C-palladium(II)]-μ-cyanido-κ²C:N]

T. Akitsu and Y. Endo

Read article

link to html

Poly[[tri-μ-cyanido-cyanido(1,4,10,13-tetraoxa-7,16-diazacyclooctadecane)barium(II)platinum(II)] hemihydrate]

M. M. Olmstead, C. M. Beavers and L. Paw U

Read article

link to html

catena-Poly[[[diaquaterbium(III)]-μ-6-carboxynicotinato-μ-pyridine-2,5-dicarboxylato] dihydrate]

S. Li, F.-L. Zhang, S.-B. Wang and H.-L. Bai

Read article

link to html

Retracted: catena-Poly[[[diaquathulium(III)]-μ-6-carboxynicotinato-μ-pyridine-2,5-dicarboxylato] dihydrate]

S. Li, Y. Chen, H.-M. He and Y.-F. Ma

Read article Correction

link to html

Bis(μ-biphenyl-2,2′-dicarboxylato)bis[(2,2′-bipyridine)copper(II)]

Z. An, R.-H. Cui and R.-J. Zhou

Read article

link to html

(3-Carboxy-5-sulfonatobenzoato-κ²O¹,O^1′)bis[2-(2-pyridyl)-1H-benzimidazole-κ²N²,N³]zinc(II) monohydrate

L.-J. Chen, S. Lin, M.-X. Yang and X.-Y. Wu

Read article

link to html

Poly[[bis(acetonitrile-κN)bis[μ₂-2,2′-(methylenedithio)bis(1,3,4-thiadiazole)-κ²N⁴:N^4′]copper(II)] bis(perchlorate) acetonitrile solvate]

J.-G. Wang, J.-H. Qin and P.-Z. Hu

Read article

link to html

Poly[bis(μ₃-5-nitroisophthalato)bis(1,10-phenanthroline)dimanganese(II)]

H.-D. Wang, M.-M. Li, H.-Y. He and F.-B. Jiang

Read article

link to html

Bis(2-bromoacetato-κ²O,O′)(1,10-phenanthroline-κ²N,N′)copper(II)

G. He, J. Sun, R. Zhao and J. Li

Read article

link to html

{4-Bromo-2-[(2-morpholinoethyl)iminomethyl]phenolato}iodido(methanol)zinc(II)

Read article

link to html

Redetermination of {2-[3-(dimethylammonio)propyliminomethyl]phenolato}dithiocyanatozinc(II)

Read article

link to html

Bis[bis(1-oxo-2-pyridyl)aminato]copper(II) tetrahydrate

Read article

link to html

Poly[(μ-4,4′-bipyridine)(μ-naphthalene-1,4-dicarboxylato)manganese(II)]

J. Boeckmann, I. Jess and C. Näther

Read article

link to html

(Benzohydrazidato-κ²N′,O)[2-(benzoylhydrazono-κ²N,O)propionato-κO]oxidovanadium(V)

H. W. Wong, K. M. Lo and S. W. Ng

Read article

link to html

Bis(benzoylacetonato)bis(1,3-di-4-pyridylpropane)manganese(II)

Y. Zhou, W.-N. Zhao and L. Han

Read article

link to html

Bis[μ-5-(5-carboxylato-3-pyridyl)tetrazolato-κ³N¹,N⁵:N²]bis[triaquazinc(II)]

H. Yin, L. Wang and Q. Nie

Read article

link to html

(3-Anilino-1-phenyliminothioureato)chloridodimethyltin(IV)

J. A. D. Delgado D., C. K. Y. A. Okio and R. Welter

Read article

link to html

trans,trans,trans-Diaquabis(nicotinamide-κN)bis(2-nitrobenzoato-κO)copper(II)

K.-L. Zhang, Q.-L. Xie and S. W. Ng

Read article

link to html

Poly[octa-μ-aqua-tetraaquabis(μ₄-5-sulfonatobenzene-1,3-dicarboxylato)nickel(II)tetrasodium]

B.-Y. Zhang, J.-J. Nie and D.-J. Xu

Read article

Acta Cryst. (2009). E65,