Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 69| Part 8

ISSN: 2056-9890

August 2013 issue

Highlighted illustration

Cover illustration: The crystal structure of 2-hydroxy-N'-methyl-5-nitrobenzohydrazide, C₈H₉N₃O₄, shows the highly unusual situation of one neutral and one zwitterionic molecule in its asymmetric unit. The zwitterion contains an intramolecular N-HO hydrogen bond and the neutral molecule features both intramolecular N-HO and O-HO hydrogen bonds. In the crystal, the constituents are linked by N-HO and N-HN hydrogen bonds to generate a two-dimensional network. See: Yang, Jin, Zhou & Jin [Acta Cryst. (2013). E69, o1305].

inorganic compounds

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Calcium hexakis(dihydrogenphosphito)stannate(IV), Ca[Sn(H₂PO₂)₆], with some remarks on the so-called Ge₂(H₂PO₂)₆ structure type

T. Gieschen and H. Reuter

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Tetraammine(carbonato-κ²O,O′)cobalt(III) perchlorate

S. C. Mohan, S. J. Jenniefer, P. T. Muthiah and K. Jothivenkatachalam

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K_0.78Na_0.22MoO₂AsO₄

R. Jouini, C. Bouzidi, M. F. Zid and A. Driss

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Redetermination of MgCrO₄·5H₂O

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Distrontium trimanganese(II) bis(hydrogenphosphate) bis(orthophosphate)

J. Khmiyas, A. Assani, M. Saadi and L. El Ammari

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Pentazirconium copper tribismuth

A. Balinska, I. Tarasiuk and V. Pavlyuk

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RbCuFe(PO₄)₂

A. Badri, M. Hidouri and M. Ben Amara

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Na₇Al₃(As₂O₇)₄

N. Fakhar Bourguiba and A. Driss

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metal-organic compounds

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Poly[μ-aqua-μ-(N,4-dichloro-2-methylbenzenesulfonamidato)-potassium]

H. S. Spandana, S. Foro and B. T. Gowda

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catena-Poly[[triphenyltin(IV)]-μ-N-(4-acetylphenyl)maleamato]

M. H. Bhatti, U. Yunus, N. Mussarat, M. Helliwell and R. Prendergast

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Bis(1-ethyl-4,4′-bipyridin-1-ium) bis(1,2-dicyanoethene-1,2-dithiolato-κ²S,S′)nickelate(II)

Y. Chen, W. Ning and J.-L. Liu

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(2,2′-Bipyridyl-κ²N,N′)bis(η⁵-pentamethylcyclopentadienyl)barium

D. Kazhdan and S. S. Rozenel

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Tris(2-formylphenolato-κ²O,O′)(1,10-phenanthroline-κ²N,N′)samarium(III)

Y. Zhong, J. Yang and L. Hu

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Tetrakis(μ-3-chlorobenzoato-κ²O:O′)bis[(N,N-diethylnicotinamide-κN¹)copper(II)]

N. Bozkurt, T. Tunç, N. Çaylak Delibaş, H. Necefoğlu and T. Hökelek

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{2-[2,2-Bis(4,4-dimethyl-4,5-dihydro-1,3-oxazol-2-yl-κN)propyl]pyridine}dichloridoiron(II)

G. Roviello, A. Tuzi, C. Capacchione, S. Milione and C. Ferone

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Dichloridobis[3-(4-methoxyphenyl)-2-methyl-5-(piperidin-1-yl)-2,3-dihydro-1,2,4-oxadiazole-κN⁴]platinum(II)

A. S. Kritchenkov, L. V. Lavnevich, G. L. Starova, N. A. Bokach and V. A. Kalibabchuk

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catena-Poly[heptylenediammonium [[tetrachloridobismuthate(III)]-μ-chlorido]]

A. Ouasri, A. Rhandour, M. Saadi and L. El Ammari

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Triaqua(pyrazole-4-carboxylato-κN¹)lithium

W. Starosta and J. Leciejewicz

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Diaquabis[2-(2-hydroxyethyl)pyridine-κ²N,O]cobalt(II) dichloride

O. Zeghouan, F. Guenifa, N. Hadjadj, L. Bendjeddou and H. Merazig

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Trichlorido(1,3-dimethyl-2,3-dihydro-1H-imidazol-2-ylidene-κC²)aluminium(III)

C. Tian, X. Gao, Q. Chen, W. Nie and M. V. Borzov

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Bis[2-(1,3-benzothiazol-2-yl)phenyl-κ²C¹,N][1,3-bis(4-bromophenyl)propane-1,3-dionato-κ²O,O′]iridium(III)

Y.-I. Kim, S.-J. Yun and S. K. Kang

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(5,10,15,20-Tetraphenylporphyrinato-κ⁴N)zinc–18-crown-6 (1/1)

Z. Denden, L. Bel Haj Hassen, M. S. Belkhiria, J.-C. Daran and H. Nasri

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Dichloridobis[3-(4-chlorophenyl)-2,N,N-trimethyl-2,3-dihydro-1,2,4-oxadiazole-5-amine-κN⁴]platinum(II)–4-chlorobenzaldehyde (1/1)

A. S. Kritchenkov, V. V. Gurzhiy, N. A. Bokach and V. A. Kalibabchuk

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(2,2′-Bipyridine-κ²N,N′)tetrakis(dimethyl sulfoxide-κO)copper(II) bis(perchlorate)

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Tetrakis(pyridine-κN)bis(tetrafluoridoborato-κF)copper(II)

N. De Silva, A. P. S. Pannu and P. G. Plieger

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catena-Poly[[[tetraaquamagnesium]-trans-μ-[(piperazine-1,4-diium-1,4-diyl)bis(methylene)]diphosphonato] hemihydrate]

L.-H. Schilling and N. Stock

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Diaquabis(pyridine-2-carboxylato-κ²N,O)zinc dimethylformamide hemisolvate

L. Croitor, D. Chisca, E. B. Coropceanu and M. S. Fonari

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Bis[μ-3,5-bis(pyridin-2-yl)pyrazolato]bis[(hexafluorophosphato)copper(II)]

A. Mishima, N. Katsuta, M. Furusyou, A. Fuyuhiro and S. Kawata

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Bis{N-benzyl-N-[2-(thiophen-2-yl)ethyl]dithiocarbamato-κ²S,S′}lead(II)

E. Sathiyaraj, S. Thirumaran, B. Sridhar and S. Selvanayagam

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Aquabis(3-chlorobenzoato-κO)bis(N,N-diethylnicotinamide-κN)copper(II)

N. Bozkurt, T. Tunç, N. Çaylak Delibaş, H. Necefoğlu and T. Hökelek

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(Methanol-κO)-cis-dioxido{(4Z,N′E)-N′-[(Z)-4-oxido-4-phenylbut-3-en-2-ylidene]isonicotinohydrazidato}molybdenum(VI)

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Tetraethylammonium dicyanido(5,10,15,20-tetraphenylporphyrinato)ferrate(III) dichloromethane monosolvate

N. Kassenova, O. Hietsoi, R. Yerkassov and M. Shatruk

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Poly[[μ-bis(4-nitrophenyl) phosphato-κ²O,O′]sodium]

A. Gerus and T. Lis

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catena-Poly[[aquabis(3-chlorobenzoato-κ²O,O′)cadmium]-μ-N,N-diethylnicotinamide-κ²N¹:O]

N. Bozkurt, T. Tunç, N. Çaylak Delibaş, H. Necefoğlu and T. Hökelek

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(Azido-κN){(E)-2-[1-(pyridin-2-yl)ethylideneamino]phenolato-κ³N,N′,O}copper(II)

A. Datta, J. K. Clegg, J.-H. Huang and S.-C. Sheu

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Diammonium tetrakis(isothiocyanato)zincate–1,4,10,13,16-hexaoxacyclooctadecane–water (1/2/1)

K. Showrilu, K. Rajarajan and M. NizamMohideen

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[5,10,15,20-Tetrakis(4-methoxyphenyl)porphyrinato]zinc dichloromethane disolvate

S. McGill, V. N. Nesterov and S. L. Gould

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trans-Bis(μ-benzenethiolato-κ²S:S)bis[chlorido(triphenylphosphane-κP)palladium(II)] chloroform disolvate

A. Avila-Sorrosa, A. Reyes-Arellano, J. M. Germán-Acacio, R. Reyes-Martínez and D. Morales-Morales

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Bis(cyclohexylammonium) tetrachlorido(oxalato)stannate(IV)

M. Sarr, A. Diasse-Sarr, W. Diallo, L. Plasseraud and H. Cattey

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trans-Acetyldicarbonyl(η⁵-cyclopentadienyl)[tris(furan-2-yl)phosphane-κP]molybdenum(II)

M. T. Whited, J. G. Bakker-Arkema, J. E. Greenwald, L. A. Morrill and D. E. Janzen

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catena-Poly[ammonium [aquabis(μ-2,3,5,6-tetraoxo-4-nitropyridin-4-ido)argentate(I)]]

N. Dinh Do, O. Kovalchukova, A. Stash and S. Strashnova

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organic compounds

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4-Chlorobutyl 7-chloro-1-cyclopropyl-4-(1,3-diethyl-4,6-dioxo-2-sulfanylidene-1,3-diazinan-5-ylidene)-6-fluoro-1,4-dihydroquinoline-3-carboxylate

K. Sweidan, S. F. Haddad, M. A. AlDamen and A. Al-Sheikhb

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2-[1′-(Benzyloxy)spiro[indane-1,2′-pyrrolidine]-5′-yl]acetonitrile

R. Moreno-Fuquen, D. M. Soto, L. M. Jaramillo-Gómez, J. Ellena and J. C. Tenorio

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1′-(1,3-Diphenyl-1H-pyrazol-4-yl)-1′′-(prop-2-en-1-yl)-2′,3′,5′,6′,7′,7a'-hexahydro-1′H-dispiro[1-benzopyran-3,2′-pyrrolizine-3′,3′′-indoline]-2′′,4-dione 0.75-hydrate

G. Jagadeesan, D. Kathirvelan, J. Haribabu, B. S. R. Reddy and K. Sethusankar

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3-{5-Bromo-2-[(triphenylphosphanylidene)amino]phenyl}-4,5-dihydro-1,2,3-oxadiazol-3-ylium-5-olate

D. Grossie, L. Harrison and K. Turnbull

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(2S,3R)-3-(2-Bromophenyl)-2-nitro-2,3,6,7-tetrahydro-1-benzofuran-4(5H)-one

Y. Wang, L. Lou, K. Dong and D. Xu

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2,2′-[(4-Methyl-2-phenylimidazolidine-1,3-diyl)bis(methylene)]diphenol

A. Rivera, L. Cárdenas, J. Ríos-Motta, V. Eigner and M. Dušek

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14-Methoxy-4,6-dimethyl-9-phenyl-8,12-dioxa-4,6-diazatetracyclo[8.8.0.0^2,7.0^13,18]octadeca-2(7),13,15,17-tetraene-3,5,11-trione

G. Jagadeesan, S. Jayashree, D. Kannan, M. Bakthadoss and S. Aravindhan

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(Naphthalen-1-yl){2-[(5,6,7,8-tetrahydronaphthalen-2-yl)carbonyl]phenyl}methanone

J. Kanchanadevi, G. Anbalagan, R. Sivasakthikumaran, A. K. Mohanakrishnan, B. Gunasekaran and V. Manivannan

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5-Fluoro-3-phenyl-N′-(4-propylcyclohexylidene)-1H-indole-2-carbohydrazide

S. T. Çelikesir, M. Akkurt, G. C. Üstündağ and O. Büyükgüngör

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1-(2,4-Dinitrophenyl)-2-[(E)-2,4,5-trimethoxybenzylidene]hydrazine

H.-K. Fun, S. Chantrapromma, B. Nilwanna, T. Kobkeatthawin and N. Boonnak

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3-(4-Bromophenylsulfinyl)-2,5,6-trimethyl-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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Bifenox: methyl 5-(2,4-dichlorophenoxy)-2-nitrobenzoate

Y. Jeon, J. Kim, S. Cho and T. H. Kim

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Napropamide

S. Cho, J. Kim, Y. Jeon and T. H. Kim

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5′′-(4-Nitrobenzylidene)-7′-(4-nitrophenyl)-1′′-methyl-1′,3′,5′,6′,7′,7a′-hexahydrodispiro[acenaphthylene-1,5′-pyrrolo[1,2-c][1,3]thiazole-6′,3′′-piperidine]-2,4′′(1H)-dione including an unknown solvate

R. Vishnupriya, J. Suresh, S. Sivakumar, R. R. Kumar and P. L. N. Lakshman

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5-Chloro-3-ethylsulfinyl-2-(3-fluorophenyl)-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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5-Fluoro-N′-(4-methylcyclohexylidene)-3-phenyl-1H-indole-2-carbohydrazide

S. T. Çelikesir, M. Akkurt, G. C. Üstündağ, G. Çapan and O. Büyükgüngör

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5-Chloro-2-(4-methylphenyl)-3-methylsulfinyl-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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Methyl 3′-benzyl-4′-(2-chlorophenyl)-1′-methyl-2-oxospiro[indoline-3,2′-pyrrolidine]-3′-carboxylate

T. Anuradha, A. Devaraj, P. R. Seshadri and M. Bakthadoss

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2-Chloro-N-(3-methoxybenzoyl)benzenesulfonamide

P. A. Suchetan, B. S. Palakshamurthy, G. R. Mamatha, V. Kumar, N. R. Mohan and S. Sreenivasa

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Bis(1,3-dimethyl-1H-imidazolium) hexafluorosilicate methanol 0.33-solvate

C. Tian, W. Nie and M. V. Borzov

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Bis(1,3-dimethyl-1H-imidazolium) hexafluorosilicate: the second monoclinic polymorph

C. Tian, W. Nie and M. V. Borzov

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1-(2-Chlorophenyl)-3-(2-ethylhexanoyl)thiourea

R. Santhakumari, S. Selvanayagam, K. Ramamurthi, N. Radha and B. M. Yamin

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Acta Cryst. (2013). E69, o1221-o1222
doi: 10.1107/S1600536813017923