Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 69| Part 9

ISSN: 2056-9890

September 2013 issue

Highlighted illustration

Cover illustration: In the compound [Co(C₁₀H₁₅)₂]₂[CoCl₄]·2CH₂Cl₂, the cobalt atoms exhibit two different oxidation states. The cobaltocenium cation contains cobalt in oxidation state +III. It is located on a twofold rotation axis and has a staggered conformation. The tetrahedral CoCl₄ anion has site symmetry -4 and contains cobalt in oxidation state +II. The crystal packing is dominated by C-HCl hydrogen-bonding interactions involving the disordered dichloromethane solvent molecule as donor and the anion as acceptor groups. See: Merola, Ngo & Karpin [Acta Cryst. (2013). E69, m504].

inorganic compounds

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Li_0.5Al_0.5Mg₂(MoO₄)₃

I. Ennajeh, M. F. Zid and A. Driss

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SrMn^II₂Mn^III(PO₄)₃

G. Alhakmi, A. Assani, M. Saadi, C. Follet and L. El Ammari

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Lithium vanado(V)molybdate(VI), Li[VMoO₆]

S. Ezzine Yahmed, R. Nasri, M. F. Zid and A. Driss

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Zinc mercury(II) tetrakis(selenocyanate)

H.-Q. Sun, X.-Q. Wang and W.-W. Zhang

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BaMn^II₂Mn^III(PO₄)₃

A. Assani, M. Saadi, G. Alhakmi, E. Houmadi and L. El Ammari

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Agardite-(Y), Cu²⁺₆Y(AsO₄)₃(OH)₆·3H₂O

S. M. Morrison, K. J. Domanik, M. J. Origlieri and R. T. Downs

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metal-organic compounds

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{[Ethyl(pyridin-4-ylmethyl)carbamothioyl]sulfanido-κ²S,S′}(1,4,7,10,13,16-hexaoxacyclooctadecane-κ⁶O)potassium

H. D. Arman, P. Poplaukhin and E. R. T. Tiekink

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Diaquatetrakis(1H-imidazole-κN³)magnesium dichloride

M. Kayalvizhi, G. Vasuki, K. Kaabi and C. Ben Nasr

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Poly[[bis[μ₂-1,2-bis(pyridin-4-yl)ethene-κ²N:N′]bis(thiocyanato-κN)cobalt(II)] 1,2-bis(pyridin-4-yl)ethene monosolvate dihydrate]

S. Wöhlert, I. Jess and C. Näther

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Bis(dimethylformamide)pentakis(μ-N,2-dioxidobenzene-1-carboximidato)tetrakis(1-methylimidazole)di-μ-propionato-pentamanganese(III)manganese(II)–dimethylformamide–methanol (1/0.24/1.36)

J. C. Lutter, J. W. Kampf, M. Zeller and C. M. Zaleski

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1-(2,3-Dimethylphenyl)piperazine-1,4-diium tetrachloridocuprate(II)

S. Ben Mabrouk, I. Ameur, S. Abid and M. Rzaigui

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2-(3-Chlorobenzoyl)-3-(3,4-dichlorophenyl)-1-(4-ferrocenylphenyl)guanidine

R. Gul, A. Khan, A. Badshah and M. N. Tahir

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catena-Poly[[bis(thiocyanato-κN)iron(II)]-bis(μ-dipyrazin-2-yl disulfide-κ²N⁴:N^4′)]

S. Wöhlert, I. Jess and C. Näther

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Di-μ-chlorido-bis[(2-aminobenzamide-κ²N²,O)chloridocopper(II)]

M. Damous, G. Dénès, S. Bouacida, M. Hamlaoui, H. Merazig and J.-C. Daran

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2-Amino-6-methylpyridinium trans-diaquadioxalatochromate(III) monohydrate

R. Dridi, S. Namouchi Cherni, M. F. Zid and A. Driss

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Di-μ-chlorido-dichloridobis{8-[2-(dimethylamino)ethylamino]quinoline}dicadmium monohydrate

A.-R.H. Al-Sudani and B. M. Kariuki

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Poly[di-μ-aqua-diaquabis(μ₇-oxalato-κ⁹O¹:O¹:O¹,O²:O²:O^2′:O^2′,O^1′:O^1′)calciumdicaesium]

H. Kherfi, M. Hamadène, A. Guehria-Laïdoudi, S. Dahaoui and C. Lecomte

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Bis(4-aminopyridine){2,2′-[1,2-phenylenebis(nitrilomethanylylidene)]diphenolato}cobalt(III) nitrate

S. Dharmalingam and S. Yoon

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Triphenyl(pyrrolidine-1-carbodithioato-κS)tin(IV)

M. Sirajuddin, N. Uddin and S. Ali

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cis-Diaquatetrakis(1-butyl-1H-imidazole-κN³)nickel(II) dichloride

P. S. Kannan, A. S. Ganeshraja, K. Rajkumar, K. Anbalagan and A. SubbiahPandi

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6-Ferrocenoyl-7-phenylspiro[hexahydropyrrolo[1,2-c][1,3]thiazole-5,11′-indeno[1,2-b]quinoxaline]

S. Suhitha, K. Gunasekaran, A. R. Sureshbabu, R. Raghunathan and D. Velmurugan

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6-Ferrocenoyl-7-(4-fluorophenyl)spiro[hexahydropyrrolo[1,2-c][1,3]thiazole-5,11′-indeno[1,2-b]quinoxaline]

S. Suhitha, K. Gunasekaran, D. Gavaskar, R. Raghunathan and D. Velmurugan

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Dipotassium tetraaquabis(μ-citrato-κ⁴O:O′,O′′,O′′′)nickelate(II) tetrahydrate

H.-G. Yao, J.-N. Huang, R.-K. Deng and Z.-B. Yao

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Bis[bis(pentamethylcyclopentadienyl)cobalt(III)] tetrachloridocobaltate(II) dichloromethane disolvate

J. S. Merola, M. Ngo and G. W. Karpin

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Trichlorido{methyl[4-(methylimino)pent-2-en-2-yl]azanido-κ²N,N′}hafnium(IV)

K. Ikeda and H. Masuda

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Bis(1,10-phenanthroline-κ²N,N′)(sulfato-κ²O,O′)nickel(II) propane-1,2-diol monosolvate

K.-L. Zhong and C.-X. Duan

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Diaquadichloridobis(pyridine-κN)cobalt(II)

P. S. Kannan, A. S. Ganeshraja, K. Anbalagan, E. Govindan and A. SubbiahPandi

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(2,2′-Bipyridine)chlorido[diethyl (2,2′:6′,2′′-terpyridin-4-yl)phosphonate]ruthenium(II) hexafluoridophosphate acetonitrile/water solvate

W. Chen, F. N. Rein, B. L. Scott and R. C. Rocha

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2-(4-Bromobenzoyl)-1-ferrocenylspiro[11H-pyrrolidizine-3,11′-indeno[1,2-b]quinoxaline]

S. Suhitha, K. Gunasekaran, A. R. Sureshbabu, R. Raghunathan and D. Velmurugan

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trans-Difluoridotetrakis(pyridine-κN)chromium(III) perchlorate from synchrotron radiation

D. Moon and J.-H. Choi

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Di-μ-aqua-bis[aqua(5-carboxylato-1H-1,2,3-triazole-4-carboxylic acid-κ²N³,O⁴)lithium]

W. Starosta and J. Leciejewicz

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Tetrakis(μ-2-phenylacetato-κ²O:O′)bis{[4-(dimethylamino)pyridine-κN¹]cobalt(II)}

M. Benslimane, Y. K. Redjel, G. Dénès and H. Merazig

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Bis(dimethyl sulfoxide-κO)tetrakis(μ₂-3,4,5-trimethoxybenzoato-κ²O:O′)dizinc

D. Deutsch, T. Zevaco and O. Walter

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Dichlorido[6,8,22,24,34,36-hexamethyl-33,35-diaza-3,11,19,27-tetraazoniapentacyclo[27.3.1.1^5,9.1^13,17.1^21,25]hexatriaconta-1(33),5,7,9(34),13,15,17(35),21,23,25(36),29,31-dodecaene-κ⁶N³,N¹¹,N¹⁹,N²⁷,N³³,N³⁵]dipalladium(II) bis(perchlorate) N,N-dimethylformamide disolvate methanol disolvate

K. Oda, Y. Funahashi and H. Masuda

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catena-Poly[[[2-(1,3-thiazol-4-yl)-1H-benzimidazole]manganese(II)]-μ-oxalato]

P. Liang, L.-N. Huang and X.-H. Yin

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catena-Poly[{μ-N′-[2-(carboxylatomethoxy)benzylidene]-2-hydroxybenzohydrazidato}(methanol-κO)nickel(II)]

F. Luo, H. Du, L. Yang and P. Zhang

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Bis[O,O′-bis(4-tert-butylphenyl) dithiophosphato-κ²S,S′]bis(pyridine-κN)lead(II)

X. Zhang, B. Xie, L. He, L. Lu and N. Chen

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organic compounds

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2-(3-Cyano-4-methyl-5,5-diphenyl-5H-furan-2-ylidene)malononitrile

M. D. H. Bhuiyan, G. J. Gainsford, A. Kay and J. Anderson

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(E)-2-Bromomethyl-3-(o-tolyl)acrylonitrile

J. Kanchanadevi, G. Anbalagan, R. Selvakumar, M. Bakthadoss, B. Gunasekaran and V. Manivannan

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1-[3-({[Bis(2-methylpropyl)carbamothioyl]amino}carbonyl)benzoyl]-3,3-bis(2-methylpropyl)thiourea

N. Selvakumaran, R. Karvembu, S. W. Ng and E. R. T. Tiekink

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Epibisdehydroneotuberostemonine J

L. Jin, R.-R. Zhang, H.-Y. Tian, P.P.-H. But and R.-W. Jiang

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r-2,c-6-Diphenylpiperidine

V. Maheshwaran, S. Abdul Basheer, A. Akila, S. Ponnuswamy and M. N. Ponnuswamy

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Methyl 2-[(tert-butoxycarbonyl)amino]-3-(4-hydroxyphenyl)propanoate

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Biphenyl-2,4,4′,6-tetracarboxylic acid monohydrate

Y.-N. Wang and J. Zhao

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N,N′-Bis(phenylcarbamothioyl)benzene-1,3-dicarboxamide

Z. Ngaini, M. A. Mohd Ariff, W. S. H. Wan Zullkiplee, H. Hussain and M. M. Rosli

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Ethyl 5-amino-1-[(4-methylphenyl)sulfonyl]-1H-pyrazole-4-carboxylate

A.-S.S.H. Elgazwy, I. F. Nassar and P. G. Jones

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1,1′-Methylenebis[3-(2,6-diisopropylphenyl)-3,4,5,6-tetrahydropyrimidin-1-ium] dibromide ethanol monosolvate monohydrate

H. Bian, L. Yang, J. Yuan, P. Mao and Y. Xiao

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2-[2-(5-Bromothiophen-2-yl)-4,5-diphenyl-1H-imidazol-1-yl]-3-phenylpropan-1-ol

J. Gao, L. Yang, W. Mai, J. Yuan and P. Mao

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(4S*)-2-Methylamino-3-nitro-4-(4-nitrophenyl)-5,6,7,8-tetrahydro-4H-chromen-5-one

P. Narayanan, J. Kamalraja, P. T. Perumal and K. Sethusankar

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2-Oxo-2-(2-oxo-2H-chromen-3-yl)ethyl pyrrolidine-1-carbodithioate

K. M. Kumar, N. M. Mahabhaleshwaraiah, O. Kotresh, K. R. Roopashree and H. C. Devarajegowda

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3-(4-Chlorophenylsulfinyl)-2,4,7-trimethyl-1-benzofuran

H. D. Choi, P. J. Seo and U. Lee

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(Z)-N-(2,6-Diisopropylphenyl)-4-nitrobenzimidoyl chloride

G. A. El-Hiti, K. Smith, D. H. Jones, A. Masmali and B. M. Kariuki

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(E)-3-(4-Bromo-5-methylthiophen-2-yl)acrylonitrile

G. A. El-Hiti, K. Smith, A. A. Balakit, A. Masmali and B. M. Kariuki

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4-Cyclopropyl-1-(6′-deoxy-1′,2′-O-isopropylidene-α-D-glucofuranosyl)-1H-1,2,3-triazole

Q. Zhang, P. He, G. Zhou, K. Yu and H. Liu

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(2E,4E)-Ethyl 5-(2,4-dichlorophenylsulfonyl)penta-2,4-dienoate

U. Sankar, V. Sabari, S. Mahalakshmi, K. K. Balasubramanian and S. Aravindhan

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1,2-Ethylenediaminium bis(2-benzamidobenzoate)

M. Ziyaev, J. Ashurov, S. Talipov and B. Ibragimov

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Tetrahydroalstonine

X. Cachet, F.-H. Porée, S. Michel and P. Lemoine

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2-Isopropyl-2-(6-methoxy-1,3-benzothiazol-2-yl)-5,5-dimethyl-1,3-thiazolidin-4-one

H. Würfel, H. Görls, D. Weiss and R. Beckert

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Lacinilene C 7-methyl ether

V. V. Uzbekov, S. A. Talipov, B. T. Ibragimov, R. D. Stipanovic and A. A. Bell

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(2E)-3-(2-Chlorobenzo[h]quinolin-3-yl)-1-(2-methyl-4-phenylquinolin-3-yl)prop-2-en-1-one

R. Prasath, S. Sarveswari, S. W. Ng and E. R. T. Tiekink

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1,2-Bis(2-hydroxy-5-methylbenzylidene)hydrazine

B. Saravanan, A. Jayamani, N. Sengottuvelan, G. Chakkaravarthi and V. Manivannan

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(3R,3aR,6R,6aR)-Hexahydrofuro[3,2-b]furan-3,6-diyl dibenzoate

V. Piccialli, S. Zaccaria, N. Borbone, R. Centore and A. Tuzi

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