Acta Crystallographica Section E
Acta Crystallographica
Section E CRYSTALLOGRAPHIC COMMUNICATIONS

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CRYSTALLOGRAPHIC
COMMUNICATIONS

Volume 70| Part 6

ISSN: 2056-9890

June 2014 issue

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Cover illustration: The compound C₂₀H₁₄N₄ is a new polymorph of the previously reported structures, which were orthorhombic, space group Pbca [Bei et al. (2000). Acta Cryst. C56, 718-719] and monoclinic, space group P2₁/c [Dudd et al. (2003). Green Chem. 5, 187-192]. The crystal structures of two solvated forms of the same molecule have also been reported; the dimethylformamide monosolvate, monoclinic space group P2₁/n [Wu & Hu (2009). Acta Cryst. E65, o522] and the methanol monosolvate, triclinic space group P-1 [Su et al. (2011). Acta Cryst. E67, o90]. In all four crystal structures the 1,4-bis(1H-benzimidazol-2-yl)benzene molecules possess inversion symmetry. In the present monoclinic polymorph, space group P2₁/c, this is not the case, as the title compound crystallizes with two independent molecules in the asymmetric unit. See: Fu, Liang, Liu & Zhu [Acta Cryst. (2014). E70, o699].

inorganic compounds

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α-NH₄Fe(HAsO₄)₂

N. Ouerfelli, A. Souilem, M. F. Zid and A. Driss

CCDC reference: 997763

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La₃Si₆N₁₁

H. Yamane, T. Nagura and T. Miyazaki

CCDC reference: 999175

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Cs₃ScCl₆

M. D. Ward and J. A. Ibers

CCDC reference: 1000441

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Nickel hexayttrium decaiodide, [NiY₆]I₁₀

S. Steinberg and G. Meyer

CCDC reference: 1000440

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Redetermination of [EuCl₂(H₂O)₆]Cl

F. Tambornino, P. Bielec and C. Hoch

CCDC reference: 1001456

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Ba₄GaN₃O

T. Hashimoto and H. Yamane

CCDC reference: 1001671

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Cs₅Sn₉(OH)·4NH₃

U. Friedrich and N. Korber

CCDC reference: 1004528

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Na_4.25Mo₁₅S₁₉: a novel ternary reduced molybdenum sulfide containing Mo₆ and Mo₉ clusters

D. Salloum, P. Gougeon and P. Gall

CCDC reference: 1004866

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metal-organic compounds

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catena-Poly[[bis(pyridine-κN)nickel(II)]-di-μ-thiocyanato-κ²N:S;κ²S:N]

T. Neumann, I. Jess and C. Näther

CCDC reference: 1000026

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Dichlorido(N,N-diethyl-4-{[(quinolin-2-yl)methylidene]amino-κ²N,N′}aniline)mercury(II)

M. S. H. Faizi and S. Hussain

CCDC reference: 999849

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Poly[[diaqua[μ-1,4-bis(pyridin-4-ylmethyl)piperazine-κ²N:N′]{μ-2,2′-[(1,4-phenylene)bis(oxy)]diacetato-κ²O:O′}cobalt(II)] pentahydrate]

A. D. Sample and R. L. LaDuca

CCDC reference: 997809

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Dichlorido(4,4′-di-tert-butyl-2,2′-bipyridine-κ²N,N′)palladium(II) dimethyl sulfoxide monosolvate monohydrate

R. A. Gutiérrez-Márquez, C. Crisóstomo-Lucas, R. Reyes-Martínez, S. Hernández-Ortega and D. Morales-Morales

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Bis(1-methylpiperazine-1,4-diium) di-μ-bromido-bis[tetrabromidobismuthate(III)] dihydrate

M. Essid, T. Roisnel and H. Marouani

CCDC reference: 1000442

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[μ-Butane-1,4-diylbis(diphenylphosphane)-κ²P:P′]bis{[butane-1,4-diylbis(diphenylphosphane)-κ²P,P′]copper(I)} bis(hexafluoridophosphate) diethyl ether disolvate

M. Nishikawa, A. Akiyama and T. Tsubomura

CCDC reference: 1000315

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[Bis(quinolin-2-ylcarbonyl)amido-κ³N,N′,N′′]bromido(N,N-dimethylformamide-κO)copper(II)

M. S. H. Faizi and P. Sen

CCDC reference: 1000734

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catena-Poly[[dichloridomercury(II)]-μ-1,4-bis[2-(pyridin-4-yl)ethynyl]benzene-κ²N:N′]

B. Wang, M. Li and Y. Xie

CCDC reference: 1001220

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{Dimethyl [(phenylsulfonyl)amido]phosphato-κ²O,O′}bis(triphenylphosphane-κP)copper(I)

O. V. Moroz, V. A. Trush, T. Y. Sliva, K. O. Znovjyak and V. M. Amirkhanov

CCDC reference: 1000731

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Bis{μ-N-[(E)-4-benzyloxy-2-oxidobenzylidene]-4-nitrobenzenecarbohydrazidato}bis[diaquanickel(II)] dimethylformamide tetrasolvate

B. Joseph, M. Sithambaresan, M. R. P. Kurup and S. W. Ng

CCDC reference: 1001219

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Di-μ-chlorido-bis(chlorido{N′-[phenyl(pyridin-2-yl-κN)methylidene]pyridine-2-carbohydrazide-κ²N′,O}cadmium)

M. Akkurt, A. A. Khandar, M. N. Tahir, F. A. Afkhami and S. A. H. Yazdi

CCDC reference: 1001915

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Chlorido{2-[(dimethylamino)methyl]benzeneselenolato-κ²N,Se}(triphenylphosphane-κP)palladium(II)

E. M. Takaluoma, R. Oilunkaniemi and R. S. Laitinen

CCDC reference: 1002116

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(N,N′-Diethylthiourea-κS)tris(triphenylphosphane-κP)silver(I) acetate methanol monosolvate

Y. Wattanakanjana, A. Nimthong and C. Kamrod

CCDC reference: 1002206

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(2,2′-Bipyridine-κ²N,N′)dichloridopalladium(II) 1,4-dioxane hemisolvate

R. A. Gutiérrez Márquez, C. Crisóstomo-Lucas, D. Morales-Morales and S. Hernández-Ortega

CCDC reference: 999627

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(Acetonitrile-κN)iodidobis(triphenylphosphane-κP)copper(I)

Y. Wattanakanjana, A. Nimthong, J. Mokakul and P. Sukpornsawan

CCDC reference: 1002549

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Bis(cyclohexylammonium) tetrachloridodiphenylstannate(IV)

M. Sarr, C. Merkens, A. Diassé-Sarr, L. Diop and U. Englert

CCDC reference: 1002989

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Diaquabis(ethylenediamine-κ²N,N′)copper(II) bis(sulfamerazinate)

A. Direm, W. Falek, G. Pilet and N. Benali-Cherif

CCDC reference: 1002145

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Bis(μ₂-diphenylphosphinamide-κ²O:O)bis[bis(diphenylphosphinamide-κO)lithium] dichloride acetonitrile disolvate

A.-H. Li, J.-P. Han and J. Li

CCDC reference: 1002945

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Tetrakis(2,6-dimethylpyridinium) dihydrogen decavanadate dihydrate

E. Rakovský and L. Krivosudský

CCDC reference: 1003037

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Bis[tris(propane-1,3-diamine-κ²N,N′)nickel(II)] diaquabis(propane-1,3-diamine-κ²N,N′)nickel(II) hexabromide dihydrate

A. Yangui, W. Rekik, S. Elleuch and Y. Abid

CCDC reference: 1002808

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Bis(tetraphenylphosphonium) tetrachloridocobaltate(II)

Z. Ouahida, N. Hadjadj, F. Guenifa, L. Bendjeddou and H. Merazig

CCDC reference: 1003287

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1,8-Diazabicyclo[5.4.0]undec-7-en-8-ium bromido(phthalocyaninato)zincate

B. Przybył and J. Janczak

CCDC reference: 1003951

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catena-Poly[[silver(I)-μ-N-[(pyridin-2-yl)methyl]pyridine-3-amine-κ²N:N′] hexafluoridophosphate]

S.-H. Moon and K.-M. Park

CCDC reference: 1003661

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catena-Poly[[lithium-μ₂-(dihydrogen pyrazine-2,3,5,6-tetracarboxylato)-κ⁶O²,N¹,O⁶;O³,N⁴,O⁵-lithium-di-μ-aqua-κ⁴O:O] 2.5-hydrate]

W. Starosta and J. Leciejewicz

CCDC reference: 1004410

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Diaquabis(nicotinamide-κN¹)bis(thiocyanato-κS)cobalt(II)

D. Pandey, S. S. Narvi and S. Chaudhuri

CCDC reference: 850080

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Bis{μ-[(diphenylphosphoryl)methyl](phenyl)bis(1H-pyrazol-1-yl)boranuido}dilithium

M. Müller, H.-W. Lerner and M. Bolte

CCDC reference: 883935

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(1,6,7,12-Tetraazaperylene-κ²N,N′)bis(4,4′,5,5′-tetramethyl-2,2′-bipyridyl-κ²N,N′)ruthenium(II) bis(hexafluoridophosphate) acetonitrile trisolvate

T. Brietzke, D. Kässler, A. Kelling, U. Schilde and H.-J. Holdt

CCDC reference: 1004679

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organic compounds

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2-[(Z)-1,1-Dioxo-2-(2,4,5-trifluorobenzyl)-3,4-dihydro-2H-1,2-benzothiazin-4-ylidene]acetic acid

S. Parveen, S. Hussain, S. Zhu, X. Hao and C. Zhu

CCDC reference: 998389

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2-Hydroxyethylammonium iodide

C. Kohrt, A. Spannenberg and T. Werner

CCDC reference: 999797

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(5E)-1-Benzyl-5-(3,3,3-trichloro-2-oxopropylidene)pyrrolidin-2-one

A. Fabiani Claro Flores, D. Correia Flores, J. Rosa de Menezes Vicenti, L. Pizzuti and P. Teixeira Campos

CCDC reference: 740177

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N′-[(E)-2-Chlorobenzylidene]-2-(6-methoxynaphthalen-2-yl)propanohydrazide

J. T. Mague, S. K. Mohamed, M. Akkurt, H. Potgieter and M. R. Albayati

CCDC reference: 997601

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Octyl (2E)-2-[2-(diphenylphosphanyl)benzylidene]hydrazinecarbodithioate

I. Asri, M. H. S. A. Hamid, A. H. Mirza, M. A. Ali and M. R. Karim

CCDC reference: 997277

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Buprenorphine

J. Mazurek, M. Hoffmann, A. Fernandez Casares, P. D. Cox and M. D. Minardi

CCDC reference: 1000182

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N-(1,5-Dimethyl-3-oxo-2-phenyl-2,3-dihydro-1H-pyrazol-4-yl)-2-(4-nitrophenyl)acetamide

M. Kaur, J. P. Jasinski, H. S. Yathirajan, B. Narayana and K. Byrappa

CCDC reference: 1000268

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2,3-Diphenyl-2,3-dihydro-4H-pyrido[3,2-e][1,3]thiazin-4-one

H. P. Yennawar, H. Singh and L. J. Silverberg

CCDC reference: 1000248

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N,N′-(Propane-1,3-diyl)dibenzothioamide

M. Nagasawa, Y. Sasanuma and H. Masu

CCDC reference: 1000286

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4-Phenyl-1,2,4-triazaspiro[4.6]undec-1-ene-3-thione

S. K. Mohamed, J. T. Mague, M. Akkurt, A. A. Hassan and M. R. Albayati

CCDC reference: 1000439

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4-(Prop-2-ynyl)-2H-1,4-benzothiazin-3(4H)-one

N. K. Sebbar, A. Zerzouf, E. M. Essassi, M. Saadi and L. El Ammari

CCDC reference: 999603

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4-Azaniumyl-2,2,6,6-tetramethylpiperidin-1-ium dinitrate

H. Chebbi, R. Ben Smail and M. F. Zid

CCDC reference: 1000438

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3-Chloro-2-methylanilinium chloride monohydrate

A. Maroua, K. Lamia, H. Ahmed and R. Mohamed

CCDC reference: 1000637

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2-[(1-Oxidopyridin-4-yl)sulfanyl]benzoic acid

R. Moreno-Fuquen, L. Valencia and J. Ellena

CCDC reference: 1000546

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A new polymorph of N-(2-{N′-[(1E)-2-hydroxybenzylidene]hydrazinecarbonyl}phenyl)benzamide

S. K. Mohamed, J. T. Mague, M. Akkurt, H. Potgieter and M. R. Albayati

CCDC reference: 1000727

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(Z)-1-[(2E)-3,4-Diphenyl-2,3-dihydro-1,3-thiazol-2-ylidene]-2-[1-(4-hydroxyphenyl)ethylidene]hydrazinium bromide including an unknown solvate

J. T. Mague, S. K. Mohamed, M. Akkurt, A. A. Hassan and M. R. Albayati

CCDC reference: 1000895

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5-(4-Hydroxyphenyl)imidazolidine-2,4-dione

J. Xue, Y. Qin, Z. Zhang and Y. Qiao

CCDC reference: 1000728

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3-Iodo-1H-pyrazolo[3,4-b]pyridine

P.-H. Huang, Y.-S. Wen and J.-Y. Shen

CCDC reference: 1000735

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Deacetylcinobufalactam monohydrate

H.-J. Tang, X.-F. Yuan, H.-Y. Tian, L.-J. Ruan and R.-W. Jiang

CCDC reference: 1000729

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N-(1-Allyl-3-chloro-4-ethoxy-1H-indazol-5-yl)-4-methylbenzenesulfonamide

H. Chicha, E. M. Rakib, L. Bouissane, M. Saadi and L. El Ammari

CCDC reference: 1001396

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1-[4-Bromo-2-(trifluoromethoxy)phenyl]-3-methyl-1H-1,2,4-triazole

C. Sandeep, B. Padmashali, P. A. Suchetan and R. S. Kulkarni

CCDC reference: 1000730

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Diethyl 7,7′-dichloro-4-oxo-4H-[1,4′-biquinoline]-3,3′-dicarboxylate

Y. Ishikawa and Y. Sugisawa

CCDC reference: 1001457

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2-Methoxy-4-(2-methoxyphenyl)-5,6,7,8,9,10-hexahydrocycloocta[b]pyridine-3-carbonitrile

R. Vishnupriya, J. Suresh, S. Maharani, R. R. Kumar and P. L. N. Lakshman

CCDC reference: 1001458

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9-Aminoacridin-10-ium 4-aminobenzoate dihydrate

N. Dhanabalan, K. Thanigaimani, S. Arshad, I. A. Razak and K. J. Santhanaraj

CCDC reference: 1001221

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2-(2-Fluorophenyl)-5-iodo-7-methyl-3-methylsulfinyl-1-benzofuran

H. D. Choi and U. Lee

CCDC reference: 1001669

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N-(2-Formylphenyl)-4-methyl-N-[(4-methylphenyl)sulfonyl]benzenesulfonamide

CCDC reference: 1002056

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Ethyl 5-oxo-4-phenyl-5,6-dihydro-4H-1,3,4-oxadiazine-2-carboxylate

K. Shubakara, Chandra, N. Srikantamurthy, M. Mahendra and K. B. Umesha

CCDC reference: 1003020

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