Tri­phenyl­methyl­ium tetrakis­[4-(p-tert-butyl­di­methyl­silyl)-2,3,5,6-tetra­fluoro­phenyl]­borate

The title compound, C₁₉H₁₅⁺·C₄₈H₆₀BF₁₆Si₄^-, consists of discrete cations and anions. There are two ions of each kind in the asymmetric unit.

Key indicators

• Single-crystal X-ray study
• T = 173 K
• Mean [sigma](C-C) = 0.017 Å
• R factor = 0.079
• wR factor = 0.273
• Data-to-parameter ratio = 19.5

checkCIF results

No syntax errors found

ADDSYM reports no extra symmetry


 Alert Level B:



RINTA_01  Alert B The value of Rint is greater than 0.15
          Rint given   0.182

Author response: The crystal was very weakly diffracting (see Experimental).

PLAT_213  Alert B Atom C792    has ADP max/min Ratio ...........       4.10 prolate

Author response: This atom is part of a t-butyl group.

 Alert Level C:



RFACR_01  Alert C The value of the weighted R factor is > 0.25
          Weighted R factor given   0.273

PLAT_360  Alert C Short  C(sp3)-C(sp3) Bond  C(79)  -   C(793) =       1.36 Ang.

PLAT_602  Alert C VERY LARGE Solvent Accessible VOID(S) in Structure      !


 0 Alert Level A = Potentially serious problem

 2 Alert Level B = Potential problem

 3 Alert Level C = Please check

---

S1. Comment

The title compound, (I), consists of discrete cations and anions. There are two molecules of each kind in the asymmetric unit. The central atoms of the trityl cations show a trigonal planar geometry. The dihedral angles between the plane formed by the central C atom and its three adjacent atoms and the phenyl rings are 29.7 (6), 31.2 (5) and 37.2 (3)° for C1, and 28.5 (6), 30.6 (5) and 38.4 (3)° for C2.

S2. Experimental

The title compound was synthesized according to a literature procedure (Jia et al., 1997). Comparison of ¹H, ¹³C and ¹⁹F NMR data with literature specifications (Jia et al., 1997) confirmed the identity of the synthesized material. Yellow crystals suitable for X-ray analysis were grown during four weeks from a pentane solution under solvothermal conditions. Analytical data: ²⁹Si NMR, 49.6 MHz, CD₂Cl₂, 330 K, (δ(H₃C)₂SiHCl): 11.1) δ 5.6.

S3. Refinement

H atoms were refined with fixed individual displacement parameters [U_iso(H) = 1.2U_eq(C) or 1.5U_eq(C_methyl)] using a riding model with C—H = 0.95 Å or methyl C—H = 0.98 Å. The percentage of observed data, collected by our diffractometer, was only 13% of the unique data available to a θ_max of 25.1°. Inclusion of such a high percentage of essentially unobserved data into the structure refinement restricts the precision of the results. The intensities of the data in general being weak, lead to the higher value for R_int of 0.18.

Computing details

Data collection: X-AREA (Stoe & Cie, 2001); cell refinement: X-AREA; data reduction: X-AREA; program(s) used to solve structure: SHELXS97 (Sheldrick, 1990); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: XP in SHELXTL-Plus (Sheldrick, 1991).

Figures

	Fig. 1. Perspective view of the cation of molecule 1 of the title compound with the atom numbering; displacement ellipsoids are drawn at the 50% probability level.
	Fig. 2. Perspective view of the anion of molecule 1 of the title compound with the atom numbering; displacement ellipsoids are drawn at the 30% probability level.

(I)

Crystal data

C19H15^+·C48H60BF16Si4^−	F(000) = 5456
Mr = 1307.44	Dx = 1.037 Mg m^−3
Monoclinic, P21/c	Mo Kα radiation, λ = 0.71073 Å
Hall symbol: -P 2ybc	Cell parameters from 23765 reflections
a = 22.064 (2) Å	θ = 1.4–22.4°
b = 33.477 (3) Å	µ = 0.14 mm^−1
c = 22.730 (2) Å	T = 173 K
β = 93.689 (8)°	Plate, orange
V = 16754 (3) Å^3	0.28 × 0.22 × 0.03 mm
Z = 8

Data collection

STOE IPDS-II two-circle diffractometer	30915 independent reflections
Radiation source: fine-focus sealed tube	3913 reflections with I > 2σ(I)
Graphite monochromator	Rint = 0.182
ω scans	θmax = 25.5°, θmin = 1.5°
Absorption correction: empirical (MULABS; Spek, 1990; Blessing, 1995)	h = −26→26
Tmin = 0.952, Tmax = 0.990	k = −40→40
142757 measured reflections	l = −27→27

Refinement

Refinement on F^2	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F^2 > 2σ(F^2)] = 0.079	Hydrogen site location: inferred from neighbouring sites
wR(F^2) = 0.273	H-atom parameters constrained
S = 0.84	w = 1/[σ^2(Fo^2) + (0.1144P)^2] where P = (Fo^2 + 2Fc^2)/3
30915 reflections	(Δ/σ)max < 0.001
1585 parameters	Δρmax = 0.78 e Å^−3
0 restraints	Δρmin = −0.36 e Å^−3

Special details

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F² against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F², conventional R-factors R are based on F, with F set to zero for negative F². The threshold expression of F² > σ(F²) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F² are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Ų)

	x	y	z	Uiso*/Ueq
B1	0.3755 (6)	0.7250 (3)	0.3090 (6)	0.065 (3)
C11	0.3528 (4)	0.7554 (3)	0.2563 (4)	0.057 (3)
C12	0.2939 (5)	0.7656 (3)	0.2387 (4)	0.058 (3)
F12	0.2471 (2)	0.74451 (18)	0.2581 (3)	0.0719 (17)
C13	0.2802 (4)	0.7969 (4)	0.2007 (5)	0.068 (3)
F13	0.2180 (2)	0.80307 (18)	0.1883 (3)	0.0765 (17)
C14	0.3195 (4)	0.8213 (3)	0.1745 (5)	0.061 (3)
C15	0.3775 (5)	0.8108 (3)	0.1919 (5)	0.063 (3)
F15	0.4255 (3)	0.83159 (19)	0.1708 (3)	0.0831 (19)
C16	0.3928 (4)	0.7802 (3)	0.2308 (5)	0.064 (3)
F16	0.4553 (2)	0.77459 (17)	0.2455 (3)	0.0691 (16)
Si1	0.29890 (15)	0.86721 (10)	0.12992 (15)	0.0740 (9)
C17	0.3536 (5)	0.8717 (4)	0.0704 (5)	0.098 (4)
H17A	0.3951	0.8737	0.0883	0.147*
H17B	0.3440	0.8956	0.0468	0.147*
H17C	0.3503	0.8480	0.0450	0.147*
C18	0.2230 (5)	0.8639 (4)	0.0939 (5)	0.082 (4)
H18A	0.2142	0.8883	0.0710	0.123*
H18B	0.1932	0.8609	0.1238	0.123*
H18C	0.2207	0.8407	0.0675	0.123*
C19	0.3013 (5)	0.9119 (4)	0.1806 (6)	0.090 (4)
C191	0.2781 (8)	0.9492 (4)	0.1432 (8)	0.149 (7)
H19A	0.3056	0.9542	0.1119	0.224*
H19B	0.2770	0.9726	0.1689	0.224*
H19C	0.2372	0.9438	0.1257	0.224*
C192	0.2589 (7)	0.9050 (4)	0.2294 (6)	0.123 (5)
H19D	0.2719	0.8812	0.2520	0.185*
H19E	0.2174	0.9010	0.2123	0.185*
H19F	0.2599	0.9282	0.2557	0.185*
C193	0.3644 (6)	0.9167 (4)	0.2092 (7)	0.123 (5)
H19G	0.3931	0.9216	0.1788	0.184*
H19H	0.3760	0.8923	0.2309	0.184*
H19I	0.3652	0.9394	0.2365	0.184*
C21	0.3987 (5)	0.7569 (3)	0.3634 (4)	0.056 (3)
C22	0.3559 (4)	0.7827 (3)	0.3885 (5)	0.062 (3)
F22	0.2956 (2)	0.77619 (18)	0.3730 (3)	0.0753 (17)
C23	0.3700 (5)	0.8138 (3)	0.4260 (5)	0.062 (3)
F23	0.3248 (3)	0.83520 (19)	0.4449 (3)	0.0755 (18)
C24	0.4317 (5)	0.8237 (3)	0.4421 (5)	0.064 (3)
C25	0.4737 (5)	0.7986 (3)	0.4193 (5)	0.061 (3)
F25	0.5343 (2)	0.80470 (18)	0.4317 (3)	0.0743 (17)
C26	0.4578 (5)	0.7674 (3)	0.3815 (4)	0.059 (3)
F26	0.5050 (3)	0.74586 (18)	0.3620 (3)	0.0721 (17)
Si2	0.45164 (15)	0.86988 (10)	0.48774 (14)	0.0717 (9)
C27	0.3956 (5)	0.8765 (4)	0.5457 (5)	0.090 (4)
H27A	0.4065	0.9002	0.5695	0.135*
H27B	0.3963	0.8529	0.5712	0.135*
H27C	0.3548	0.8799	0.5268	0.135*
C28	0.5303 (5)	0.8650 (4)	0.5240 (5)	0.080 (3)
H28A	0.5597	0.8620	0.4937	0.120*
H28B	0.5322	0.8414	0.5497	0.120*
H28C	0.5402	0.8889	0.5475	0.120*
C29	0.4515 (7)	0.9129 (4)	0.4331 (6)	0.089 (4)
C291	0.4700 (7)	0.9503 (4)	0.4696 (7)	0.117 (5)
H29A	0.5110	0.9467	0.4880	0.176*
H29B	0.4413	0.9543	0.5003	0.176*
H29C	0.4693	0.9737	0.4436	0.176*
C292	0.4973 (7)	0.9054 (5)	0.3859 (6)	0.123 (5)
H29D	0.4858	0.8812	0.3638	0.185*
H29E	0.5380	0.9021	0.4051	0.185*
H29F	0.4971	0.9283	0.3589	0.185*
C293	0.3856 (6)	0.9191 (4)	0.4026 (7)	0.120 (5)
H29G	0.3729	0.8947	0.3814	0.181*
H29H	0.3861	0.9414	0.3748	0.181*
H29I	0.3571	0.9249	0.4328	0.181*
C31	0.4294 (4)	0.6932 (3)	0.2932 (4)	0.057 (3)
C32	0.4555 (5)	0.6690 (3)	0.3371 (4)	0.062 (3)
F32	0.4433 (3)	0.67448 (18)	0.3936 (2)	0.0719 (17)
C33	0.4939 (5)	0.6368 (4)	0.3251 (5)	0.069 (3)
F33	0.5166 (3)	0.61488 (19)	0.3721 (2)	0.0804 (18)
C34	0.5085 (4)	0.6271 (3)	0.2682 (5)	0.061 (3)
C35	0.4810 (5)	0.6506 (3)	0.2256 (4)	0.058 (3)
F35	0.4911 (3)	0.64455 (18)	0.1678 (3)	0.0773 (18)
C36	0.4451 (5)	0.6826 (3)	0.2370 (4)	0.056 (3)
F36	0.4209 (3)	0.70288 (18)	0.1886 (2)	0.0684 (16)
Si3	0.54808 (16)	0.57788 (11)	0.25151 (16)	0.0810 (10)
C37	0.6100 (6)	0.5662 (4)	0.3101 (6)	0.124 (5)
H37A	0.6399	0.5878	0.3121	0.186*
H37B	0.6299	0.5411	0.3004	0.186*
H37C	0.5922	0.5635	0.3484	0.186*
C38	0.5918 (6)	0.5831 (4)	0.1820 (6)	0.126 (6)
H38A	0.6219	0.6044	0.1876	0.189*
H38B	0.5634	0.5895	0.1484	0.189*
H38C	0.6124	0.5578	0.1744	0.189*
C39	0.4881 (7)	0.5372 (4)	0.2442 (7)	0.101 (4)
C391	0.4367 (8)	0.5507 (5)	0.1952 (8)	0.176 (8)
H39A	0.4192	0.5762	0.2067	0.264*
H39B	0.4048	0.5303	0.1917	0.264*
H39C	0.4548	0.5537	0.1572	0.264*
C392	0.4595 (7)	0.5311 (5)	0.3061 (7)	0.141 (6)
H39D	0.4409	0.5561	0.3181	0.212*
H39E	0.4915	0.5232	0.3357	0.212*
H39F	0.4285	0.5101	0.3025	0.212*
C393	0.5146 (8)	0.4983 (4)	0.2254 (8)	0.156 (7)
H39G	0.5329	0.5020	0.1876	0.234*
H39H	0.4824	0.4782	0.2210	0.234*
H39I	0.5457	0.4895	0.2552	0.234*
C41	0.3222 (4)	0.6940 (3)	0.3305 (4)	0.056 (3)
C42	0.2943 (5)	0.6689 (4)	0.2889 (4)	0.065 (3)
F42	0.3085 (3)	0.67335 (18)	0.2305 (2)	0.0739 (18)
C43	0.2542 (5)	0.6385 (3)	0.3004 (5)	0.070 (3)
F43	0.2317 (3)	0.6175 (2)	0.2520 (3)	0.090 (2)
C44	0.2388 (5)	0.6303 (3)	0.3568 (5)	0.071 (3)
C45	0.2631 (5)	0.6545 (3)	0.3973 (4)	0.055 (3)
F45	0.2534 (3)	0.64976 (19)	0.4552 (3)	0.0787 (19)
C46	0.3055 (4)	0.6849 (3)	0.3863 (4)	0.060 (3)
F46	0.3294 (3)	0.70565 (18)	0.4331 (2)	0.0630 (16)
Si4	0.18981 (16)	0.58463 (11)	0.37218 (16)	0.0840 (10)
C47	0.1484 (6)	0.5924 (4)	0.4410 (6)	0.112 (5)
H47A	0.1779	0.5969	0.4745	0.167*
H47B	0.1242	0.5686	0.4486	0.167*
H47C	0.1216	0.6156	0.4360	0.167*
C48	0.1332 (6)	0.5763 (4)	0.3109 (6)	0.120 (5)
H48A	0.1056	0.5993	0.3073	0.180*
H48B	0.1099	0.5521	0.3184	0.180*
H48C	0.1537	0.5731	0.2742	0.180*
C49	0.2464 (8)	0.5428 (4)	0.3800 (8)	0.125 (5)
C491	0.2902 (7)	0.5497 (6)	0.4341 (9)	0.179 (9)
H49A	0.2670	0.5533	0.4691	0.268*
H49B	0.3146	0.5736	0.4280	0.268*
H49C	0.3172	0.5265	0.4398	0.268*
C492	0.2796 (8)	0.5349 (5)	0.3241 (9)	0.170 (9)
H49D	0.2498	0.5302	0.2909	0.254*
H49E	0.3056	0.5113	0.3300	0.254*
H49F	0.3046	0.5581	0.3155	0.254*
C493	0.2052 (10)	0.5037 (4)	0.3929 (8)	0.183 (9)
H49G	0.1775	0.4983	0.3584	0.275*
H49H	0.1817	0.5088	0.4272	0.275*
H49I	0.2318	0.4806	0.4007	0.275*
B2	0.8789 (6)	0.7739 (3)	0.3099 (6)	0.065 (3)
C51	0.9310 (4)	0.8054 (3)	0.3346 (5)	0.065 (3)
C52	0.9493 (5)	0.8150 (4)	0.3915 (5)	0.068 (3)
F52	0.9232 (3)	0.79638 (19)	0.4363 (2)	0.0677 (17)
C53	0.9919 (5)	0.8455 (4)	0.4068 (5)	0.066 (3)
F53	1.0037 (3)	0.8495 (2)	0.4650 (3)	0.085 (2)
C54	1.0222 (5)	0.8658 (4)	0.3676 (5)	0.072 (3)
C55	1.0048 (5)	0.8574 (4)	0.3079 (6)	0.076 (3)
F55	1.0323 (3)	0.8744 (2)	0.2642 (3)	0.087 (2)
C56	0.9611 (5)	0.8274 (3)	0.2931 (5)	0.068 (3)
F56	0.9475 (3)	0.82290 (19)	0.2348 (3)	0.0753 (18)
Si5	1.08113 (16)	0.90595 (11)	0.38983 (17)	0.0852 (11)
C57	1.0884 (6)	0.9420 (3)	0.3260 (6)	0.097 (4)
H57A	1.0495	0.9557	0.3174	0.146*
H57B	1.0994	0.9272	0.2911	0.146*
H57C	1.1200	0.9618	0.3367	0.146*
C58	1.0563 (7)	0.9347 (4)	0.4547 (6)	0.120 (5)
H58A	1.0179	0.9484	0.4437	0.180*
H58B	1.0874	0.9545	0.4668	0.180*
H58C	1.0505	0.9163	0.4874	0.180*
C59	1.1532 (6)	0.8803 (4)	0.4093 (7)	0.093 (4)
C591	1.2029 (7)	0.9116 (5)	0.4198 (9)	0.175 (9)
H59A	1.1929	0.9290	0.4525	0.262*
H59B	1.2059	0.9277	0.3841	0.262*
H59C	1.2418	0.8983	0.4296	0.262*
C592	1.1523 (6)	0.8553 (4)	0.4643 (6)	0.114 (5)
H59D	1.1411	0.8720	0.4972	0.170*
H59E	1.1927	0.8438	0.4734	0.170*
H59F	1.1225	0.8337	0.4580	0.170*
C593	1.1716 (6)	0.8541 (5)	0.3592 (7)	0.127 (6)
H59G	1.1722	0.8700	0.3230	0.191*
H59H	1.1424	0.8322	0.3531	0.191*
H59I	1.2122	0.8431	0.3689	0.191*
C61	0.8999 (5)	0.7412 (3)	0.2592 (4)	0.061 (3)
C62	0.8591 (4)	0.7171 (4)	0.2283 (5)	0.067 (3)
F62	0.7986 (2)	0.72209 (19)	0.2364 (2)	0.0748 (17)
C63	0.8748 (5)	0.6861 (4)	0.1926 (5)	0.072 (3)
F63	0.8272 (3)	0.6650 (2)	0.1666 (3)	0.0841 (19)
C64	0.9331 (5)	0.6763 (3)	0.1811 (5)	0.062 (3)
C65	0.9741 (4)	0.7008 (4)	0.2135 (5)	0.074 (3)
F65	1.0360 (3)	0.6935 (2)	0.2096 (3)	0.0834 (19)
C66	0.9604 (5)	0.7320 (3)	0.2504 (5)	0.062 (3)
F66	1.0074 (2)	0.75152 (19)	0.2780 (3)	0.0745 (17)
Si6	0.95417 (16)	0.63482 (11)	0.13028 (17)	0.0856 (11)
C67	0.9006 (5)	0.6347 (4)	0.0632 (5)	0.105 (4)
H67A	0.9020	0.6607	0.0435	0.157*
H67B	0.8592	0.6297	0.0747	0.157*
H67C	0.9124	0.6137	0.0361	0.157*
C68	1.0306 (5)	0.6419 (4)	0.1055 (5)	0.094 (4)
H68A	1.0599	0.6425	0.1398	0.141*
H68B	1.0323	0.6673	0.0840	0.141*
H68C	1.0405	0.6199	0.0795	0.141*
C69	0.9493 (9)	0.5854 (5)	0.1705 (9)	0.139 (6)
C691	0.9922 (11)	0.5860 (6)	0.2237 (10)	0.230 (12)
H69A	0.9792	0.6064	0.2513	0.345*
H69B	1.0331	0.5924	0.2121	0.345*
H69C	0.9925	0.5598	0.2428	0.345*
C692	0.9715 (11)	0.5520 (5)	0.1234 (11)	0.233 (12)
H69D	0.9429	0.5515	0.0886	0.350*
H69E	0.9728	0.5256	0.1420	0.350*
H69F	1.0121	0.5590	0.1115	0.350*
C693	0.8862 (8)	0.5760 (6)	0.1950 (9)	0.171 (8)
H69G	0.8551	0.5751	0.1623	0.256*
H69H	0.8760	0.5970	0.2228	0.256*
H69I	0.8881	0.5502	0.2152	0.256*
C71	0.8525 (5)	0.7431 (3)	0.3588 (4)	0.061 (3)
C72	0.7933 (5)	0.7319 (4)	0.3685 (5)	0.068 (3)
F72	0.7466 (2)	0.75267 (19)	0.3391 (3)	0.0748 (18)
C73	0.7764 (5)	0.7016 (4)	0.4042 (5)	0.072 (3)
F73	0.7171 (3)	0.6953 (2)	0.4084 (3)	0.084 (2)
C74	0.8176 (5)	0.6781 (4)	0.4341 (5)	0.073 (4)
C75	0.8778 (6)	0.6867 (4)	0.4271 (5)	0.071 (3)
F75	0.9248 (3)	0.6659 (2)	0.4535 (3)	0.087 (2)
C76	0.8941 (5)	0.7186 (4)	0.3907 (5)	0.069 (3)
F76	0.9553 (2)	0.72393 (19)	0.3847 (2)	0.0745 (17)
Si7	0.79672 (19)	0.63256 (14)	0.47962 (17)	0.1060 (14)
C77	0.8509 (6)	0.6281 (5)	0.5472 (6)	0.125 (5)
H77A	0.8462	0.6513	0.5728	0.187*
H77B	0.8927	0.6269	0.5352	0.187*
H77C	0.8418	0.6037	0.5688	0.187*
C78	0.7151 (6)	0.6396 (6)	0.5022 (7)	0.159 (8)
H78A	0.6875	0.6415	0.4667	0.239*
H78B	0.7126	0.6642	0.5253	0.239*
H78C	0.7036	0.6168	0.5260	0.239*
C79	0.8005 (10)	0.5888 (5)	0.4272 (10)	0.142 (7)
C791	0.7603 (11)	0.5943 (7)	0.3721 (9)	0.239 (13)
H79A	0.7184	0.5987	0.3826	0.358*
H79B	0.7619	0.5703	0.3476	0.358*
H79C	0.7742	0.6174	0.3502	0.358*
C792	0.7716 (17)	0.5527 (6)	0.4556 (14)	0.39 (3)
H79D	0.7294	0.5590	0.4633	0.578*
H79E	0.7944	0.5462	0.4927	0.578*
H79F	0.7723	0.5298	0.4288	0.578*
C793	0.8590 (12)	0.5811 (6)	0.4152 (10)	0.201 (11)
H79G	0.8844	0.5798	0.4522	0.302*
H79H	0.8738	0.6025	0.3904	0.302*
H79I	0.8610	0.5556	0.3944	0.302*
C81	0.8247 (4)	0.8043 (3)	0.2823 (5)	0.064 (3)
C82	0.7938 (5)	0.8285 (4)	0.3216 (5)	0.070 (3)
F82	0.8091 (2)	0.82421 (19)	0.3808 (2)	0.0743 (17)
C83	0.7484 (5)	0.8544 (3)	0.3037 (5)	0.069 (3)
F83	0.7214 (3)	0.8741 (2)	0.3494 (3)	0.0850 (19)
C84	0.7290 (5)	0.8617 (3)	0.2471 (5)	0.062 (3)
C85	0.7594 (5)	0.8390 (3)	0.2081 (5)	0.064 (3)
F85	0.7447 (3)	0.8430 (2)	0.1488 (3)	0.0844 (19)
C86	0.8051 (4)	0.8121 (4)	0.2249 (5)	0.064 (3)
F86	0.8329 (3)	0.79322 (19)	0.1800 (3)	0.0734 (18)
Si8	0.66575 (16)	0.89797 (10)	0.22468 (16)	0.0793 (10)
C87	0.6849 (6)	0.9222 (4)	0.1525 (6)	0.110 (5)
H87A	0.6870	0.9016	0.1220	0.165*
H87B	0.7241	0.9358	0.1579	0.165*
H87C	0.6533	0.9416	0.1403	0.165*
C88	0.6623 (6)	0.9381 (4)	0.2819 (6)	0.103 (4)
H88A	0.6297	0.9569	0.2701	0.155*
H88B	0.7011	0.9523	0.2857	0.155*
H88C	0.6541	0.9260	0.3199	0.155*
C89	0.5911 (5)	0.8702 (4)	0.2181 (6)	0.088 (4)
C891	0.5387 (5)	0.9006 (5)	0.2081 (8)	0.149 (7)
H89A	0.5449	0.9164	0.1727	0.224*
H89B	0.5380	0.9184	0.2423	0.224*
H89C	0.5000	0.8863	0.2029	0.224*
C892	0.5900 (6)	0.8428 (4)	0.1602 (6)	0.106 (4)
H89D	0.5938	0.8597	0.1255	0.159*
H89E	0.5517	0.8280	0.1562	0.159*
H89F	0.6240	0.8239	0.1637	0.159*
C893	0.5847 (6)	0.8454 (4)	0.2735 (6)	0.111 (5)
H89G	0.6192	0.8270	0.2789	0.167*
H89H	0.5468	0.8300	0.2695	0.167*
H89I	0.5840	0.8631	0.3077	0.167*
C1	0.1258 (4)	0.7389 (3)	0.5155 (4)	0.057 (3)
C101	0.1792 (4)	0.7559 (4)	0.5451 (4)	0.065 (3)
C102	0.2376 (4)	0.7444 (3)	0.5270 (5)	0.070 (3)
H102	0.2404	0.7257	0.4959	0.084*
C103	0.2899 (5)	0.7601 (4)	0.5543 (6)	0.094 (4)
H103	0.3285	0.7524	0.5420	0.113*
C104	0.2854 (6)	0.7877 (4)	0.6005 (6)	0.094 (4)
H104	0.3213	0.7988	0.6192	0.113*
C105	0.2276 (6)	0.7991 (4)	0.6196 (6)	0.091 (4)
H105	0.2245	0.8174	0.6512	0.109*
C106	0.1764 (5)	0.7829 (4)	0.5909 (5)	0.072 (3)
H106	0.1377	0.7906	0.6031	0.087*
C111	0.1234 (4)	0.7290 (4)	0.4546 (4)	0.064 (3)
C112	0.1582 (5)	0.7482 (4)	0.4148 (4)	0.069 (3)
H112	0.1841	0.7692	0.4290	0.082*
C113	0.1576 (6)	0.7387 (5)	0.3557 (6)	0.097 (5)
H113	0.1821	0.7526	0.3297	0.116*
C114	0.1205 (6)	0.7088 (5)	0.3369 (6)	0.107 (5)
H114	0.1192	0.7020	0.2962	0.128*
C115	0.0826 (5)	0.6862 (4)	0.3740 (6)	0.096 (4)
H115	0.0577	0.6649	0.3594	0.115*
C116	0.0851 (5)	0.6978 (4)	0.4320 (5)	0.086 (4)
H116	0.0601	0.6844	0.4582	0.103*
C121	0.0718 (4)	0.7343 (3)	0.5506 (5)	0.065 (3)
C122	0.0130 (5)	0.7404 (3)	0.5241 (5)	0.070 (3)
H122	0.0077	0.7485	0.4841	0.084*
C123	−0.0370 (5)	0.7346 (4)	0.5569 (5)	0.082 (4)
H123	−0.0764	0.7388	0.5385	0.098*
C124	−0.0320 (5)	0.7233 (4)	0.6140 (5)	0.086 (4)
H124	−0.0668	0.7206	0.6362	0.103*
C125	0.0281 (5)	0.7154 (4)	0.6401 (5)	0.095 (4)
H125	0.0329	0.7057	0.6794	0.114*
C126	0.0787 (5)	0.7215 (4)	0.6088 (4)	0.074 (3)
H126	0.1182	0.7170	0.6269	0.089*
C2	0.6289 (4)	0.7316 (3)	0.1038 (5)	0.062 (3)
C201	0.5729 (5)	0.7500 (3)	0.0764 (5)	0.063 (3)
C202	0.5138 (5)	0.7376 (4)	0.0959 (5)	0.073 (3)
H202	0.5103	0.7191	0.1273	0.088*
C203	0.4638 (5)	0.7541 (4)	0.0663 (5)	0.084 (4)
H203	0.4247	0.7456	0.0763	0.101*
C204	0.4673 (6)	0.7825 (4)	0.0228 (5)	0.091 (4)
H204	0.4313	0.7934	0.0043	0.109*
C205	0.5229 (5)	0.7949 (4)	0.0063 (5)	0.075 (3)
H205	0.5257	0.8150	−0.0229	0.090*
C206	0.5742 (5)	0.7781 (3)	0.0321 (5)	0.070 (3)
H206	0.6124	0.7861	0.0191	0.084*
C211	0.6318 (5)	0.7193 (3)	0.1641 (5)	0.062 (3)
C212	0.5972 (5)	0.7350 (3)	0.2062 (5)	0.070 (3)
H212	0.5688	0.7553	0.1944	0.084*
C213	0.6007 (6)	0.7234 (4)	0.2655 (5)	0.088 (4)
H213	0.5781	0.7360	0.2944	0.106*
C214	0.6408 (7)	0.6915 (5)	0.2783 (6)	0.106 (5)
H214	0.6435	0.6815	0.3175	0.127*
C215	0.6764 (6)	0.6737 (5)	0.2385 (6)	0.097 (4)
H215	0.7029	0.6522	0.2495	0.116*
C216	0.6717 (5)	0.6881 (4)	0.1825 (5)	0.075 (3)
H216	0.6966	0.6767	0.1544	0.090*
C221	0.6800 (4)	0.7285 (3)	0.0711 (4)	0.061 (3)
C222	0.6739 (5)	0.7186 (3)	0.0115 (5)	0.071 (3)
H222	0.6343	0.7151	−0.0068	0.086*
C223	0.7224 (5)	0.7138 (4)	−0.0213 (5)	0.088 (4)
H223	0.7173	0.7060	−0.0614	0.105*
C224	0.7791 (5)	0.7206 (4)	0.0049 (6)	0.096 (4)
H224	0.8135	0.7175	−0.0177	0.115*
C225	0.7879 (5)	0.7321 (4)	0.0644 (5)	0.080 (4)
H225	0.8274	0.7373	0.0818	0.096*
C226	0.7367 (5)	0.7357 (4)	0.0970 (5)	0.077 (3)
H226	0.7413	0.7431	0.1373	0.093*

Atomic displacement parameters (Ų)

	U^11	U^22	U^33	U^12	U^13	U^23
B1	0.061 (6)	0.074 (8)	0.060 (7)	0.005 (8)	0.008 (5)	−0.021 (8)
C11	0.052 (6)	0.059 (7)	0.060 (7)	−0.005 (5)	−0.002 (5)	0.006 (5)
C12	0.048 (6)	0.075 (8)	0.049 (6)	0.000 (6)	−0.001 (5)	0.010 (6)
F12	0.044 (3)	0.092 (5)	0.079 (4)	−0.001 (3)	0.000 (3)	0.012 (3)
C13	0.035 (6)	0.092 (9)	0.075 (8)	0.005 (6)	0.000 (5)	−0.012 (7)
F13	0.058 (4)	0.091 (5)	0.079 (4)	0.002 (3)	−0.007 (3)	0.009 (4)
C14	0.028 (5)	0.065 (7)	0.088 (8)	0.004 (5)	−0.004 (5)	0.006 (6)
C15	0.054 (7)	0.064 (7)	0.072 (7)	−0.015 (6)	0.015 (6)	0.003 (6)
F15	0.071 (4)	0.081 (5)	0.098 (5)	0.001 (4)	0.006 (4)	0.015 (4)
C16	0.038 (6)	0.080 (8)	0.073 (8)	0.014 (6)	−0.013 (5)	0.001 (6)
F16	0.056 (4)	0.073 (4)	0.078 (4)	−0.003 (3)	0.002 (3)	0.006 (3)
Si1	0.074 (2)	0.072 (2)	0.075 (2)	0.0054 (18)	0.0019 (17)	0.0123 (18)
C17	0.094 (9)	0.115 (11)	0.086 (9)	0.019 (8)	0.007 (7)	0.033 (8)
C18	0.087 (9)	0.100 (10)	0.058 (7)	0.015 (8)	−0.004 (6)	0.005 (7)
C19	0.063 (8)	0.099 (11)	0.108 (10)	−0.002 (7)	0.020 (7)	0.006 (8)
C191	0.177 (16)	0.067 (10)	0.207 (19)	0.030 (10)	0.027 (14)	0.044 (11)
C192	0.124 (12)	0.119 (13)	0.125 (13)	0.022 (10)	−0.007 (10)	−0.040 (10)
C193	0.109 (11)	0.084 (10)	0.171 (15)	−0.005 (9)	−0.022 (10)	−0.042 (10)
C21	0.059 (7)	0.057 (7)	0.051 (6)	−0.001 (5)	0.007 (5)	0.000 (5)
C22	0.048 (6)	0.073 (8)	0.065 (7)	0.005 (6)	−0.004 (5)	0.003 (6)
F22	0.053 (4)	0.087 (5)	0.085 (4)	0.000 (3)	0.001 (3)	−0.016 (4)
C23	0.063 (7)	0.063 (8)	0.060 (7)	−0.005 (6)	0.001 (6)	−0.019 (6)
F23	0.056 (4)	0.076 (4)	0.094 (5)	0.013 (3)	0.003 (3)	−0.023 (4)
C24	0.078 (9)	0.058 (8)	0.055 (7)	0.004 (7)	0.004 (6)	−0.001 (6)
C25	0.057 (7)	0.053 (7)	0.071 (7)	−0.010 (6)	−0.006 (5)	−0.005 (6)
F25	0.045 (3)	0.082 (4)	0.095 (5)	−0.008 (3)	−0.001 (3)	−0.015 (4)
C26	0.053 (7)	0.062 (7)	0.064 (7)	0.009 (6)	0.014 (5)	0.004 (6)
F26	0.053 (4)	0.088 (5)	0.074 (4)	0.004 (3)	0.002 (3)	−0.012 (3)
Si2	0.079 (2)	0.072 (2)	0.064 (2)	−0.0086 (18)	0.0039 (16)	−0.0109 (17)
C27	0.090 (9)	0.110 (10)	0.072 (8)	−0.010 (8)	0.014 (6)	−0.023 (7)
C28	0.075 (8)	0.093 (9)	0.071 (8)	−0.023 (7)	−0.007 (6)	−0.016 (7)
C29	0.122 (12)	0.048 (8)	0.096 (10)	−0.011 (7)	−0.004 (9)	−0.006 (7)
C291	0.129 (12)	0.077 (10)	0.148 (14)	−0.009 (9)	0.029 (10)	−0.009 (9)
C292	0.146 (13)	0.124 (13)	0.105 (11)	0.007 (11)	0.056 (10)	0.028 (9)
C293	0.117 (12)	0.122 (13)	0.121 (12)	−0.001 (10)	−0.006 (10)	0.023 (10)
C31	0.066 (7)	0.056 (7)	0.051 (6)	−0.019 (5)	0.004 (5)	−0.012 (5)
C32	0.071 (7)	0.078 (8)	0.035 (6)	0.006 (6)	−0.003 (5)	−0.007 (6)
F32	0.072 (4)	0.086 (5)	0.056 (4)	0.006 (3)	−0.003 (3)	−0.002 (3)
C33	0.077 (8)	0.075 (8)	0.053 (7)	−0.008 (7)	−0.006 (6)	0.004 (6)
F33	0.094 (5)	0.088 (5)	0.058 (4)	0.013 (4)	−0.008 (3)	0.008 (3)
C34	0.061 (6)	0.059 (7)	0.062 (7)	−0.001 (5)	0.006 (5)	−0.011 (6)
C35	0.068 (7)	0.064 (7)	0.042 (6)	0.001 (6)	0.004 (5)	−0.010 (5)
F35	0.096 (5)	0.077 (4)	0.061 (4)	0.014 (3)	0.026 (3)	0.004 (3)
C36	0.062 (7)	0.053 (7)	0.053 (7)	0.003 (6)	−0.003 (5)	0.010 (5)
F36	0.073 (4)	0.075 (4)	0.058 (4)	0.011 (3)	0.008 (3)	0.003 (3)
Si3	0.085 (2)	0.076 (2)	0.083 (2)	0.0181 (19)	0.0143 (18)	0.0026 (19)
C37	0.115 (11)	0.117 (12)	0.134 (13)	0.048 (9)	−0.038 (9)	0.009 (10)
C38	0.163 (14)	0.114 (12)	0.109 (11)	0.021 (10)	0.069 (11)	0.010 (9)
C39	0.129 (12)	0.056 (8)	0.118 (11)	−0.017 (8)	0.008 (10)	−0.004 (8)
C391	0.188 (18)	0.143 (15)	0.184 (18)	−0.052 (13)	−0.090 (15)	0.017 (13)
C392	0.122 (12)	0.157 (16)	0.148 (15)	−0.048 (11)	0.033 (11)	−0.006 (12)
C393	0.219 (19)	0.081 (11)	0.178 (17)	−0.007 (12)	0.091 (15)	−0.019 (11)
C41	0.040 (5)	0.076 (8)	0.051 (6)	−0.005 (5)	−0.006 (5)	−0.010 (6)
C42	0.067 (7)	0.085 (9)	0.043 (6)	0.009 (6)	0.004 (5)	0.000 (6)
F42	0.085 (4)	0.087 (5)	0.049 (4)	−0.012 (4)	−0.003 (3)	−0.008 (3)
C43	0.057 (7)	0.072 (8)	0.078 (8)	−0.020 (6)	−0.008 (6)	−0.015 (7)
F43	0.098 (5)	0.114 (6)	0.058 (4)	−0.041 (4)	0.000 (3)	−0.021 (4)
C44	0.067 (7)	0.080 (8)	0.068 (8)	−0.014 (6)	0.010 (6)	0.001 (7)
C45	0.066 (7)	0.064 (7)	0.036 (6)	−0.013 (6)	0.007 (5)	−0.007 (5)
F45	0.090 (5)	0.094 (5)	0.052 (4)	−0.017 (4)	0.003 (3)	0.001 (3)
C46	0.055 (6)	0.073 (8)	0.050 (7)	0.007 (6)	−0.005 (5)	−0.017 (6)
F46	0.063 (4)	0.080 (4)	0.046 (3)	−0.010 (3)	0.003 (3)	−0.009 (3)
Si4	0.082 (2)	0.082 (3)	0.088 (2)	−0.0141 (19)	0.0108 (19)	−0.009 (2)
C47	0.118 (11)	0.102 (11)	0.123 (12)	−0.010 (8)	0.070 (10)	0.023 (9)
C48	0.096 (10)	0.136 (13)	0.129 (12)	−0.053 (9)	0.013 (9)	−0.011 (10)
C49	0.145 (14)	0.065 (10)	0.167 (16)	−0.006 (9)	0.020 (13)	−0.001 (10)
C491	0.108 (13)	0.171 (18)	0.25 (2)	0.031 (12)	−0.064 (14)	0.028 (16)
C492	0.173 (16)	0.103 (12)	0.25 (2)	0.036 (11)	0.146 (16)	0.026 (13)
C493	0.33 (3)	0.068 (10)	0.169 (17)	−0.004 (14)	0.116 (17)	0.017 (10)
B2	0.051 (6)	0.080 (8)	0.063 (7)	0.013 (8)	−0.009 (5)	0.005 (8)
C51	0.051 (6)	0.084 (8)	0.059 (7)	−0.007 (6)	0.002 (5)	−0.009 (6)
C52	0.065 (7)	0.087 (9)	0.053 (7)	0.003 (6)	0.013 (6)	0.007 (6)
F52	0.059 (4)	0.093 (5)	0.051 (4)	−0.010 (3)	0.004 (3)	−0.002 (3)
C53	0.065 (7)	0.085 (9)	0.048 (7)	−0.003 (6)	0.005 (6)	−0.012 (6)
F53	0.078 (4)	0.109 (5)	0.068 (4)	−0.026 (4)	−0.007 (3)	−0.005 (4)
C54	0.052 (6)	0.095 (9)	0.071 (8)	0.003 (6)	0.007 (6)	0.000 (7)
C55	0.077 (8)	0.075 (9)	0.078 (9)	−0.001 (7)	0.025 (7)	0.009 (7)
F55	0.083 (4)	0.107 (5)	0.074 (4)	−0.017 (4)	0.022 (4)	0.008 (4)
C56	0.056 (7)	0.075 (8)	0.071 (8)	−0.002 (6)	0.010 (6)	0.000 (7)
F56	0.066 (4)	0.101 (5)	0.059 (4)	0.000 (3)	0.003 (3)	0.004 (4)
Si5	0.069 (2)	0.088 (3)	0.098 (3)	−0.0068 (19)	0.0005 (19)	0.000 (2)
C57	0.097 (9)	0.069 (8)	0.125 (11)	−0.007 (7)	−0.008 (8)	0.017 (8)
C58	0.139 (13)	0.113 (12)	0.108 (11)	−0.018 (10)	0.005 (9)	−0.040 (9)
C59	0.078 (9)	0.101 (11)	0.101 (10)	−0.009 (8)	0.009 (8)	−0.003 (9)
C591	0.111 (13)	0.150 (16)	0.25 (2)	−0.055 (12)	−0.057 (13)	0.066 (15)
C592	0.076 (9)	0.141 (13)	0.122 (12)	0.000 (8)	−0.014 (8)	0.031 (10)
C593	0.076 (9)	0.169 (16)	0.137 (14)	0.006 (10)	0.006 (9)	0.051 (12)
C61	0.064 (7)	0.071 (7)	0.047 (6)	0.003 (6)	−0.002 (5)	0.001 (5)
C62	0.045 (6)	0.093 (9)	0.063 (7)	−0.013 (6)	−0.004 (5)	0.004 (7)
F62	0.054 (4)	0.104 (5)	0.066 (4)	0.002 (3)	−0.001 (3)	−0.005 (3)
C63	0.070 (8)	0.088 (9)	0.057 (7)	−0.031 (7)	0.000 (6)	−0.020 (7)
F63	0.067 (4)	0.106 (5)	0.078 (4)	−0.009 (4)	−0.002 (3)	−0.015 (4)
C64	0.050 (7)	0.065 (8)	0.069 (7)	−0.004 (6)	−0.005 (6)	0.001 (6)
C65	0.036 (6)	0.102 (10)	0.085 (8)	0.009 (6)	0.008 (6)	−0.001 (7)
F65	0.057 (4)	0.109 (5)	0.083 (4)	0.001 (4)	−0.002 (3)	−0.022 (4)
C66	0.049 (7)	0.076 (8)	0.059 (7)	0.000 (6)	−0.001 (5)	−0.011 (6)
F66	0.051 (4)	0.103 (5)	0.069 (4)	−0.001 (3)	−0.003 (3)	−0.013 (3)
Si6	0.081 (2)	0.084 (3)	0.090 (3)	−0.003 (2)	−0.0011 (19)	−0.012 (2)
C67	0.088 (9)	0.135 (12)	0.092 (9)	−0.004 (9)	0.005 (7)	−0.026 (9)
C68	0.055 (7)	0.145 (12)	0.081 (8)	0.010 (7)	0.001 (6)	−0.028 (8)
C69	0.169 (17)	0.090 (12)	0.152 (16)	0.002 (12)	−0.026 (13)	0.028 (11)
C691	0.28 (3)	0.17 (2)	0.23 (2)	−0.014 (19)	−0.08 (2)	0.124 (18)
C692	0.34 (3)	0.066 (11)	0.30 (3)	0.030 (15)	0.04 (2)	−0.059 (15)
C693	0.136 (16)	0.147 (17)	0.23 (2)	−0.019 (13)	0.013 (15)	0.045 (15)
C71	0.060 (7)	0.072 (8)	0.050 (6)	−0.004 (6)	−0.005 (5)	0.007 (5)
C72	0.053 (7)	0.093 (9)	0.055 (7)	0.003 (6)	−0.007 (5)	0.011 (6)
F72	0.049 (3)	0.105 (5)	0.070 (4)	−0.001 (3)	−0.001 (3)	0.015 (4)
C73	0.060 (7)	0.099 (10)	0.054 (7)	−0.001 (7)	−0.016 (6)	0.007 (7)
F73	0.058 (4)	0.111 (5)	0.082 (4)	−0.019 (4)	0.002 (3)	0.019 (4)
C74	0.063 (8)	0.092 (10)	0.061 (8)	−0.026 (7)	−0.013 (6)	0.013 (7)
C75	0.085 (9)	0.073 (8)	0.052 (7)	0.010 (7)	−0.023 (6)	0.002 (6)
F75	0.078 (5)	0.090 (5)	0.090 (5)	0.009 (4)	−0.014 (4)	0.016 (4)
C76	0.062 (7)	0.084 (9)	0.061 (7)	0.001 (6)	0.000 (6)	−0.004 (7)
F76	0.052 (4)	0.109 (5)	0.061 (4)	0.007 (3)	−0.001 (3)	0.001 (3)
Si7	0.105 (3)	0.126 (4)	0.084 (3)	−0.025 (3)	−0.017 (2)	0.033 (3)
C77	0.108 (11)	0.174 (15)	0.090 (10)	−0.012 (10)	−0.014 (8)	0.054 (10)
C78	0.113 (12)	0.25 (2)	0.110 (12)	−0.052 (13)	0.004 (9)	0.084 (13)
C79	0.145 (17)	0.074 (12)	0.20 (2)	0.003 (11)	−0.004 (16)	0.003 (13)
C791	0.26 (3)	0.26 (3)	0.17 (2)	0.03 (2)	−0.13 (2)	−0.028 (19)
C792	0.62 (6)	0.094 (16)	0.42 (5)	−0.15 (3)	−0.14 (4)	0.09 (2)
C793	0.30 (3)	0.087 (14)	0.21 (2)	0.050 (18)	−0.03 (2)	−0.037 (14)
C81	0.054 (6)	0.076 (8)	0.064 (7)	−0.001 (6)	0.009 (5)	−0.001 (6)
C82	0.062 (7)	0.093 (9)	0.054 (7)	−0.007 (7)	−0.002 (5)	0.012 (6)
F82	0.066 (4)	0.106 (5)	0.050 (4)	0.013 (3)	−0.002 (3)	−0.002 (3)
C83	0.052 (6)	0.082 (8)	0.073 (8)	0.009 (6)	0.007 (6)	−0.017 (7)
F83	0.078 (4)	0.100 (5)	0.078 (4)	0.016 (4)	0.004 (3)	−0.005 (4)
C84	0.062 (7)	0.067 (7)	0.056 (7)	0.003 (6)	0.000 (5)	0.011 (6)
C85	0.061 (7)	0.081 (8)	0.050 (7)	−0.011 (6)	−0.006 (5)	−0.003 (6)
F85	0.073 (4)	0.125 (6)	0.055 (4)	0.022 (4)	−0.003 (3)	0.006 (4)
C86	0.043 (6)	0.088 (9)	0.061 (7)	0.003 (6)	−0.002 (5)	0.006 (6)
F86	0.065 (4)	0.100 (5)	0.055 (4)	0.017 (4)	−0.001 (3)	0.003 (3)
Si8	0.073 (2)	0.076 (2)	0.087 (2)	0.0106 (18)	−0.0086 (18)	−0.0010 (19)
C87	0.099 (10)	0.097 (10)	0.135 (12)	0.021 (8)	0.018 (9)	0.043 (9)
C88	0.104 (10)	0.084 (9)	0.117 (11)	0.016 (8)	−0.023 (8)	−0.030 (8)
C89	0.065 (7)	0.088 (9)	0.112 (11)	0.000 (7)	−0.001 (7)	−0.021 (8)
C891	0.055 (8)	0.134 (13)	0.25 (2)	0.019 (8)	−0.038 (10)	−0.072 (13)
C892	0.090 (10)	0.093 (10)	0.133 (12)	0.007 (8)	−0.006 (8)	−0.022 (9)
C893	0.093 (10)	0.122 (12)	0.122 (12)	−0.020 (8)	0.034 (9)	−0.009 (10)
C1	0.055 (6)	0.072 (7)	0.045 (6)	0.015 (5)	−0.002 (5)	0.007 (5)
C101	0.046 (6)	0.104 (9)	0.045 (6)	0.002 (6)	−0.002 (5)	0.008 (6)
C102	0.049 (6)	0.096 (9)	0.064 (7)	0.009 (6)	0.002 (5)	0.000 (6)
C103	0.043 (7)	0.137 (13)	0.099 (10)	−0.019 (7)	−0.010 (6)	0.010 (9)
C104	0.075 (9)	0.125 (12)	0.082 (9)	−0.033 (8)	−0.006 (7)	−0.003 (9)
C105	0.078 (9)	0.108 (11)	0.086 (9)	0.007 (8)	−0.004 (7)	0.006 (8)
C106	0.057 (7)	0.102 (9)	0.057 (7)	−0.001 (6)	−0.003 (5)	−0.009 (7)
C111	0.038 (5)	0.102 (9)	0.052 (7)	−0.003 (6)	0.005 (5)	−0.009 (6)
C112	0.054 (6)	0.104 (9)	0.048 (6)	−0.005 (6)	0.004 (5)	−0.005 (6)
C113	0.058 (8)	0.154 (14)	0.078 (10)	−0.022 (8)	−0.001 (6)	−0.024 (9)
C114	0.073 (9)	0.186 (16)	0.063 (8)	0.065 (10)	0.022 (7)	0.014 (10)
C115	0.074 (8)	0.132 (12)	0.079 (9)	0.011 (8)	−0.014 (7)	−0.046 (9)
C116	0.058 (7)	0.134 (12)	0.065 (8)	0.025 (7)	−0.001 (6)	−0.009 (8)
C121	0.049 (6)	0.086 (8)	0.060 (7)	0.002 (6)	0.002 (5)	−0.007 (6)
C122	0.056 (7)	0.102 (9)	0.051 (6)	0.013 (6)	−0.003 (5)	0.000 (6)
C123	0.040 (6)	0.123 (11)	0.081 (9)	0.004 (6)	−0.006 (6)	−0.022 (8)
C124	0.056 (7)	0.154 (13)	0.048 (7)	−0.013 (8)	0.006 (6)	−0.005 (8)
C125	0.060 (8)	0.161 (14)	0.064 (8)	0.000 (8)	0.002 (6)	−0.019 (8)
C126	0.057 (7)	0.120 (10)	0.046 (6)	0.000 (7)	0.001 (5)	−0.012 (7)
C2	0.040 (6)	0.079 (8)	0.066 (7)	−0.004 (5)	−0.005 (5)	−0.001 (6)
C201	0.058 (7)	0.070 (8)	0.061 (7)	−0.007 (6)	0.003 (5)	−0.006 (6)
C202	0.066 (7)	0.094 (9)	0.060 (7)	0.000 (7)	0.001 (6)	−0.011 (6)
C203	0.038 (6)	0.134 (12)	0.079 (9)	0.004 (7)	−0.005 (6)	−0.013 (8)
C204	0.073 (9)	0.145 (13)	0.051 (7)	0.016 (8)	−0.016 (6)	0.011 (8)
C205	0.066 (8)	0.098 (9)	0.059 (7)	0.011 (7)	−0.009 (6)	0.010 (6)
C206	0.070 (7)	0.078 (8)	0.062 (7)	−0.017 (6)	0.007 (6)	0.007 (6)
C211	0.048 (6)	0.084 (8)	0.050 (6)	0.006 (6)	−0.014 (5)	−0.004 (6)
C212	0.066 (7)	0.078 (8)	0.064 (8)	−0.017 (6)	−0.018 (6)	0.013 (6)
C213	0.081 (9)	0.128 (12)	0.053 (8)	−0.004 (8)	−0.010 (6)	0.003 (8)
C214	0.096 (10)	0.165 (15)	0.055 (8)	−0.050 (10)	−0.026 (7)	0.037 (9)
C215	0.069 (8)	0.145 (13)	0.077 (9)	−0.012 (8)	0.003 (7)	0.023 (9)
C216	0.063 (7)	0.106 (10)	0.055 (7)	−0.005 (7)	0.005 (5)	0.013 (7)
C221	0.049 (6)	0.085 (8)	0.048 (6)	−0.005 (6)	−0.010 (5)	0.011 (6)
C222	0.048 (6)	0.097 (9)	0.070 (8)	−0.004 (6)	0.007 (6)	−0.006 (7)
C223	0.069 (8)	0.130 (12)	0.063 (8)	0.010 (8)	0.003 (7)	0.007 (8)
C224	0.064 (8)	0.152 (14)	0.075 (9)	−0.003 (8)	0.022 (7)	0.020 (9)
C225	0.064 (7)	0.112 (10)	0.061 (8)	−0.009 (7)	−0.008 (6)	0.013 (7)
C226	0.050 (7)	0.123 (11)	0.060 (7)	−0.006 (7)	0.012 (5)	0.012 (7)

Geometric parameters (Å, º)

B1—C11	1.626 (16)	C61—C62	1.370 (14)
B1—C31	1.653 (16)	C61—C66	1.399 (13)
B1—C41	1.665 (16)	C62—F62	1.371 (11)
B1—C21	1.687 (15)	C62—C63	1.373 (15)
C11—C16	1.368 (14)	C63—F63	1.368 (11)
C11—C12	1.377 (13)	C63—C64	1.370 (15)
C12—F12	1.348 (11)	C64—C65	1.393 (14)
C12—C13	1.379 (14)	C64—Si6	1.884 (12)
C13—C14	1.356 (14)	C65—C66	1.385 (14)
C13—F13	1.399 (10)	C65—F65	1.397 (10)
C14—C15	1.362 (13)	C66—F66	1.346 (11)
C14—Si1	1.880 (11)	Si6—C68	1.827 (11)
C15—F15	1.380 (11)	Si6—C67	1.869 (12)
C15—C16	1.381 (14)	Si6—C69	1.896 (16)
C16—F16	1.411 (10)	C67—H67A	0.9800
Si1—C18	1.819 (11)	C67—H67B	0.9800
Si1—C17	1.877 (12)	C67—H67C	0.9800
Si1—C19	1.888 (14)	C68—H68A	0.9800
C17—H17A	0.9800	C68—H68B	0.9800
C17—H17B	0.9800	C68—H68C	0.9800
C17—H17C	0.9800	C69—C691	1.49 (2)
C18—H18A	0.9800	C69—C693	1.56 (2)
C18—H18B	0.9800	C69—C692	1.65 (2)
C18—H18C	0.9800	C691—H69A	0.9800
C19—C193	1.506 (16)	C691—H69B	0.9800
C19—C192	1.516 (17)	C691—H69C	0.9800
C19—C191	1.575 (17)	C692—H69D	0.9800
C191—H19A	0.9800	C692—H69E	0.9800
C191—H19B	0.9800	C692—H69F	0.9800
C191—H19C	0.9800	C693—H69G	0.9800
C192—H19D	0.9800	C693—H69H	0.9800
C192—H19E	0.9800	C693—H69I	0.9800
C192—H19F	0.9800	C71—C72	1.390 (14)
C193—H19G	0.9800	C71—C76	1.398 (14)
C193—H19H	0.9800	C72—C73	1.367 (15)
C193—H19I	0.9800	C72—F72	1.380 (11)
C21—C26	1.388 (13)	C73—F73	1.335 (11)
C21—C22	1.424 (13)	C73—C74	1.350 (15)
C22—C23	1.369 (14)	C74—C75	1.379 (15)
C22—F22	1.372 (10)	C74—Si7	1.915 (12)
C23—F23	1.323 (11)	C75—F75	1.355 (11)
C23—C24	1.425 (14)	C75—C76	1.412 (15)
C24—C25	1.378 (14)	C76—F76	1.378 (11)
C24—Si2	1.898 (12)	Si7—C77	1.891 (12)
C25—F25	1.364 (10)	Si7—C79	1.89 (2)
C25—C26	1.382 (13)	Si7—C78	1.918 (15)
C26—F26	1.365 (11)	C77—H77A	0.9800
Si2—C27	1.877 (11)	C77—H77B	0.9800
Si2—C28	1.881 (10)	C77—H77C	0.9800
Si2—C29	1.902 (13)	C78—H78A	0.9800
C27—H27A	0.9800	C78—H78B	0.9800
C27—H27B	0.9800	C78—H78C	0.9800
C27—H27C	0.9800	C79—C793	1.36 (2)
C28—H28A	0.9800	C79—C791	1.50 (2)
C28—H28B	0.9800	C79—C792	1.53 (3)
C28—H28C	0.9800	C791—H79A	0.9800
C29—C292	1.540 (17)	C791—H79B	0.9800
C29—C291	1.541 (17)	C791—H79C	0.9800
C29—C293	1.583 (17)	C792—H79D	0.9800
C291—H29A	0.9800	C792—H79E	0.9800
C291—H29B	0.9800	C792—H79F	0.9800
C291—H29C	0.9800	C793—H79G	0.9800
C292—H29D	0.9800	C793—H79H	0.9800
C292—H29E	0.9800	C793—H79I	0.9800
C292—H29F	0.9800	C81—C86	1.374 (13)
C293—H29G	0.9800	C81—C82	1.413 (14)
C293—H29H	0.9800	C82—C83	1.368 (14)
C293—H29I	0.9800	C82—F82	1.375 (11)
C31—C32	1.381 (13)	C83—C84	1.350 (14)
C31—C36	1.391 (13)	C83—F83	1.395 (11)
C32—F32	1.342 (10)	C84—C85	1.374 (14)
C32—C33	1.408 (14)	C84—Si8	1.895 (10)
C33—F33	1.366 (11)	C85—F85	1.372 (11)
C33—C34	1.391 (14)	C85—C86	1.387 (14)
C34—C35	1.361 (13)	C86—F86	1.379 (12)
C34—Si3	1.913 (11)	Si8—C88	1.874 (12)
C35—F35	1.362 (10)	Si8—C89	1.889 (12)
C35—C36	1.368 (13)	Si8—C87	1.902 (13)
C36—F36	1.370 (10)	C87—H87A	0.9800
Si3—C37	1.887 (12)	C87—H87B	0.9800
Si3—C39	1.900 (13)	C87—H87C	0.9800
Si3—C38	1.910 (12)	C88—H88A	0.9800
C37—H37A	0.9800	C88—H88B	0.9800
C37—H37B	0.9800	C88—H88C	0.9800
C37—H37C	0.9800	C89—C893	1.523 (17)
C38—H38A	0.9800	C89—C891	1.548 (16)
C38—H38B	0.9800	C89—C892	1.602 (16)
C38—H38C	0.9800	C891—H89A	0.9800
C39—C393	1.498 (17)	C891—H89B	0.9800
C39—C392	1.591 (19)	C891—H89C	0.9800
C39—C391	1.603 (19)	C892—H89D	0.9800
C391—H39A	0.9800	C892—H89E	0.9800
C391—H39B	0.9800	C892—H89F	0.9800
C391—H39C	0.9800	C893—H89G	0.9800
C392—H39D	0.9800	C893—H89H	0.9800
C392—H39E	0.9800	C893—H89I	0.9800
C392—H39F	0.9800	C1—C111	1.421 (13)
C393—H39G	0.9800	C1—C101	1.435 (13)
C393—H39H	0.9800	C1—C121	1.485 (14)
C393—H39I	0.9800	C101—C106	1.385 (14)
C41—C46	1.379 (13)	C101—C102	1.430 (13)
C41—C42	1.381 (13)	C102—C103	1.378 (14)
C42—C43	1.384 (14)	C102—H102	0.9500
C42—F42	1.391 (11)	C103—C104	1.405 (17)
C43—F43	1.371 (11)	C103—H103	0.9500
C43—C44	1.375 (14)	C104—C105	1.425 (16)
C44—C45	1.314 (13)	C104—H104	0.9500
C44—Si4	1.918 (11)	C105—C106	1.379 (15)
C45—F45	1.356 (10)	C105—H105	0.9500
C45—C46	1.414 (14)	C106—H106	0.9500
C46—F46	1.349 (10)	C111—C112	1.382 (13)
Si4—C48	1.832 (13)	C111—C116	1.420 (15)
Si4—C47	1.881 (12)	C112—C113	1.378 (15)
Si4—C49	1.878 (16)	C112—H112	0.9500
C47—H47A	0.9800	C113—C114	1.348 (18)
C47—H47B	0.9800	C113—H113	0.9500
C47—H47C	0.9800	C114—C115	1.438 (18)
C48—H48A	0.9800	C114—H114	0.9500
C48—H48B	0.9800	C115—C116	1.372 (15)
C48—H48C	0.9800	C115—H115	0.9500
C49—C491	1.53 (2)	C116—H116	0.9500
C49—C492	1.53 (2)	C121—C126	1.388 (13)
C49—C493	1.63 (2)	C121—C122	1.411 (13)
C491—H49A	0.9800	C122—C123	1.383 (14)
C491—H49B	0.9800	C122—H122	0.9500
C491—H49C	0.9800	C123—C124	1.350 (15)
C492—H49D	0.9800	C123—H123	0.9500
C492—H49E	0.9800	C124—C125	1.442 (15)
C492—H49F	0.9800	C124—H124	0.9500
C493—H49G	0.9800	C125—C126	1.377 (14)
C493—H49H	0.9800	C125—H125	0.9500
C493—H49I	0.9800	C126—H126	0.9500
B2—C51	1.631 (16)	C2—C221	1.393 (14)
B2—C71	1.651 (16)	C2—C211	1.429 (14)
B2—C81	1.661 (15)	C2—C201	1.481 (14)
B2—C61	1.676 (16)	C201—C206	1.378 (13)
C51—C52	1.368 (14)	C201—C202	1.466 (14)
C51—C56	1.398 (14)	C202—C203	1.372 (14)
C52—F52	1.354 (11)	C202—H202	0.9500
C52—C53	1.419 (15)	C203—C204	1.375 (16)
C53—C54	1.333 (14)	C203—H203	0.9500
C53—F53	1.338 (11)	C204—C205	1.371 (15)
C54—C55	1.414 (15)	C204—H204	0.9500
C54—Si5	1.917 (12)	C205—C206	1.362 (14)
C55—F55	1.325 (12)	C205—H205	0.9500
C55—C56	1.416 (15)	C206—H206	0.9500
C56—F56	1.347 (12)	C211—C212	1.369 (14)
Si5—C59	1.836 (14)	C211—C216	1.410 (14)
Si5—C58	1.872 (13)	C212—C213	1.399 (15)
Si5—C57	1.903 (12)	C212—H212	0.9500
C57—H57A	0.9800	C213—C214	1.406 (18)
C57—H57B	0.9800	C213—H213	0.9500
C57—H57C	0.9800	C214—C215	1.372 (18)
C58—H58A	0.9800	C214—H214	0.9500
C58—H58B	0.9800	C215—C216	1.359 (15)
C58—H58C	0.9800	C215—H215	0.9500
C59—C592	1.507 (17)	C216—H216	0.9500
C59—C593	1.513 (18)	C221—C226	1.369 (13)
C59—C591	1.523 (18)	C221—C222	1.394 (13)
C591—H59A	0.9800	C222—C223	1.353 (14)
C591—H59B	0.9800	C222—H222	0.9500
C591—H59C	0.9800	C223—C224	1.369 (15)
C592—H59D	0.9800	C223—H223	0.9500
C592—H59E	0.9800	C224—C225	1.407 (15)
C592—H59F	0.9800	C224—H224	0.9500
C593—H59G	0.9800	C225—C226	1.394 (14)
C593—H59H	0.9800	C225—H225	0.9500
C593—H59I	0.9800	C226—H226	0.9500
C11—B1—C31	115.8 (10)	C59—C592—H59F	109.5
C11—B1—C41	114.6 (10)	H59D—C592—H59F	109.5
C31—B1—C41	101.1 (7)	H59E—C592—H59F	109.5
C11—B1—C21	102.1 (7)	C59—C593—H59G	109.5
C31—B1—C21	112.3 (10)	C59—C593—H59H	109.5
C41—B1—C21	111.4 (9)	H59G—C593—H59H	109.5
C16—C11—C12	110.5 (9)	C59—C593—H59I	109.5
C16—C11—B1	121.0 (9)	H59G—C593—H59I	109.5
C12—C11—B1	127.6 (10)	H59H—C593—H59I	109.5
F12—C12—C11	120.3 (9)	C62—C61—C66	113.5 (10)
F12—C12—C13	117.5 (9)	C62—C61—B2	122.5 (10)
C11—C12—C13	122.2 (10)	C66—C61—B2	123.5 (9)
C14—C13—C12	127.9 (9)	C61—C62—F62	118.1 (11)
C14—C13—F13	117.9 (10)	C61—C62—C63	124.5 (10)
C12—C13—F13	114.2 (10)	F62—C62—C63	117.2 (10)
C13—C14—C15	109.3 (10)	F63—C63—C64	119.8 (11)
C13—C14—Si1	126.2 (8)	F63—C63—C62	115.5 (10)
C15—C14—Si1	123.9 (8)	C64—C63—C62	124.6 (10)
C14—C15—F15	119.8 (10)	C63—C64—C65	110.1 (10)
C14—C15—C16	124.4 (10)	C63—C64—Si6	124.4 (8)
F15—C15—C16	115.8 (10)	C65—C64—Si6	125.5 (8)
C11—C16—C15	125.7 (9)	C66—C65—C64	127.2 (9)
C11—C16—F16	117.8 (9)	C66—C65—F65	114.9 (10)
C15—C16—F16	116.5 (10)	C64—C65—F65	117.9 (10)
C18—Si1—C17	107.3 (6)	F66—C66—C65	117.3 (9)
C18—Si1—C14	112.1 (5)	F66—C66—C61	122.7 (10)
C17—Si1—C14	108.0 (5)	C65—C66—C61	120.0 (10)
C18—Si1—C19	108.2 (6)	C68—Si6—C67	107.3 (6)
C17—Si1—C19	112.5 (6)	C68—Si6—C64	111.2 (5)
C14—Si1—C19	108.9 (6)	C67—Si6—C64	109.5 (5)
Si1—C17—H17A	109.5	C68—Si6—C69	110.2 (8)
Si1—C17—H17B	109.5	C67—Si6—C69	109.8 (7)
H17A—C17—H17B	109.5	C64—Si6—C69	108.9 (7)
Si1—C17—H17C	109.5	Si6—C67—H67A	109.5
H17A—C17—H17C	109.5	Si6—C67—H67B	109.5
H17B—C17—H17C	109.5	H67A—C67—H67B	109.5
Si1—C18—H18A	109.5	Si6—C67—H67C	109.5
Si1—C18—H18B	109.5	H67A—C67—H67C	109.5
H18A—C18—H18B	109.5	H67B—C67—H67C	109.5
Si1—C18—H18C	109.5	Si6—C68—H68A	109.5
H18A—C18—H18C	109.5	Si6—C68—H68B	109.5
H18B—C18—H18C	109.5	H68A—C68—H68B	109.5
C193—C19—C192	107.3 (12)	Si6—C68—H68C	109.5
C193—C19—C191	114.1 (12)	H68A—C68—H68C	109.5
C192—C19—C191	108.8 (12)	H68B—C68—H68C	109.5
C193—C19—Si1	109.7 (9)	C691—C69—C693	104.4 (18)
C192—C19—Si1	109.3 (9)	C691—C69—C692	109.8 (18)
C191—C19—Si1	107.7 (10)	C693—C69—C692	113.9 (16)
C19—C191—H19A	109.5	C691—C69—Si6	109.0 (13)
C19—C191—H19B	109.5	C693—C69—Si6	115.2 (13)
H19A—C191—H19B	109.5	C692—C69—Si6	104.5 (13)
C19—C191—H19C	109.5	C69—C691—H69A	109.5
H19A—C191—H19C	109.5	C69—C691—H69B	109.5
H19B—C191—H19C	109.5	H69A—C691—H69B	109.5
C19—C192—H19D	109.5	C69—C691—H69C	109.5
C19—C192—H19E	109.5	H69A—C691—H69C	109.5
H19D—C192—H19E	109.5	H69B—C691—H69C	109.5
C19—C192—H19F	109.5	C69—C692—H69D	109.5
H19D—C192—H19F	109.5	C69—C692—H69E	109.5
H19E—C192—H19F	109.5	H69D—C692—H69E	109.5
C19—C193—H19G	109.5	C69—C692—H69F	109.5
C19—C193—H19H	109.5	H69D—C692—H69F	109.5
H19G—C193—H19H	109.5	H69E—C692—H69F	109.5
C19—C193—H19I	109.5	C69—C693—H69G	109.5
H19G—C193—H19I	109.5	C69—C693—H69H	109.5
H19H—C193—H19I	109.5	H69G—C693—H69H	109.5
C26—C21—C22	111.2 (9)	C69—C693—H69I	109.5
C26—C21—B1	127.7 (10)	H69G—C693—H69I	109.5
C22—C21—B1	120.0 (9)	H69H—C693—H69I	109.5
C23—C22—F22	117.2 (9)	C72—C71—C76	110.6 (10)
C23—C22—C21	125.5 (10)	C72—C71—B2	130.6 (9)
F22—C22—C21	117.2 (9)	C76—C71—B2	117.9 (10)
F23—C23—C22	118.0 (10)	C73—C72—F72	116.0 (9)
F23—C23—C24	121.2 (10)	C73—C72—C71	126.1 (10)
C22—C23—C24	120.8 (10)	F72—C72—C71	117.9 (10)
C25—C24—C23	114.6 (10)	F73—C73—C74	120.3 (11)
C25—C24—Si2	124.4 (9)	F73—C73—C72	117.7 (9)
C23—C24—Si2	121.0 (9)	C74—C73—C72	122.0 (11)
F25—C25—C24	120.3 (10)	C73—C74—C75	116.3 (11)
F25—C25—C26	116.7 (9)	C73—C74—Si7	123.9 (9)
C24—C25—C26	122.9 (10)	C75—C74—Si7	119.6 (9)
F26—C26—C25	115.6 (9)	F75—C75—C74	124.0 (11)
F26—C26—C21	119.5 (10)	F75—C75—C76	115.5 (11)
C25—C26—C21	124.9 (10)	C74—C75—C76	120.5 (10)
C27—Si2—C28	109.5 (5)	F76—C76—C71	119.1 (10)
C27—Si2—C24	109.9 (5)	F76—C76—C75	116.4 (10)
C28—Si2—C24	110.1 (5)	C71—C76—C75	124.4 (10)
C27—Si2—C29	113.3 (6)	C77—Si7—C79	113.5 (9)
C28—Si2—C29	108.3 (6)	C77—Si7—C74	109.9 (6)
C24—Si2—C29	105.7 (5)	C79—Si7—C74	104.7 (8)
Si2—C27—H27A	109.5	C77—Si7—C78	110.3 (7)
Si2—C27—H27B	109.5	C79—Si7—C78	110.1 (9)
H27A—C27—H27B	109.5	C74—Si7—C78	108.0 (7)
Si2—C27—H27C	109.5	Si7—C77—H77A	109.5
H27A—C27—H27C	109.5	Si7—C77—H77B	109.5
H27B—C27—H27C	109.5	H77A—C77—H77B	109.5
Si2—C28—H28A	109.5	Si7—C77—H77C	109.5
Si2—C28—H28B	109.5	H77A—C77—H77C	109.5
H28A—C28—H28B	109.5	H77B—C77—H77C	109.5
Si2—C28—H28C	109.5	Si7—C78—H78A	109.5
H28A—C28—H28C	109.5	Si7—C78—H78B	109.5
H28B—C28—H28C	109.5	H78A—C78—H78B	109.5
C292—C29—C291	110.2 (12)	Si7—C78—H78C	109.5
C292—C29—C293	109.9 (12)	H78A—C78—H78C	109.5
C291—C29—C293	109.5 (12)	H78B—C78—H78C	109.5
C292—C29—Si2	111.0 (9)	C793—C79—C791	112 (2)
C291—C29—Si2	106.0 (9)	C793—C79—C792	111 (2)
C293—C29—Si2	110.3 (9)	C791—C79—C792	102.0 (19)
C29—C291—H29A	109.5	C793—C79—Si7	110.7 (16)
C29—C291—H29B	109.5	C791—C79—Si7	112.5 (14)
H29A—C291—H29B	109.5	C792—C79—Si7	108.0 (19)
C29—C291—H29C	109.5	C79—C791—H79A	109.5
H29A—C291—H29C	109.5	C79—C791—H79B	109.5
H29B—C291—H29C	109.5	H79A—C791—H79B	109.5
C29—C292—H29D	109.5	C79—C791—H79C	109.5
C29—C292—H29E	109.5	H79A—C791—H79C	109.5
H29D—C292—H29E	109.5	H79B—C791—H79C	109.5
C29—C292—H29F	109.5	C79—C792—H79D	109.5
H29D—C292—H29F	109.5	C79—C792—H79E	109.5
H29E—C292—H29F	109.5	H79D—C792—H79E	109.5
C29—C293—H29G	109.5	C79—C792—H79F	109.5
C29—C293—H29H	109.5	H79D—C792—H79F	109.5
H29G—C293—H29H	109.5	H79E—C792—H79F	109.5
C29—C293—H29I	109.5	C79—C793—H79G	109.5
H29G—C293—H29I	109.5	C79—C793—H79H	109.5
H29H—C293—H29I	109.5	H79G—C793—H79H	109.5
C32—C31—C36	113.4 (9)	C79—C793—H79I	109.5
C32—C31—B1	119.6 (10)	H79G—C793—H79I	109.5
C36—C31—B1	126.0 (10)	H79H—C793—H79I	109.5
F32—C32—C31	120.7 (10)	C86—C81—C82	110.8 (10)
F32—C32—C33	116.7 (9)	C86—C81—B2	130.6 (10)
C31—C32—C33	122.5 (9)	C82—C81—B2	118.6 (10)
F33—C33—C34	120.4 (11)	C83—C82—F82	119.2 (10)
F33—C33—C32	117.1 (9)	C83—C82—C81	123.4 (10)
C34—C33—C32	122.5 (10)	F82—C82—C81	117.4 (10)
C35—C34—C33	114.0 (10)	C84—C83—C82	125.4 (11)
C35—C34—Si3	123.1 (8)	C84—C83—F83	120.1 (10)
C33—C34—Si3	121.4 (9)	C82—C83—F83	114.6 (10)
C34—C35—F35	120.4 (9)	C83—C84—C85	112.2 (10)
C34—C35—C36	123.8 (9)	C83—C84—Si8	123.6 (9)
F35—C35—C36	115.6 (9)	C85—C84—Si8	124.2 (8)
F36—C36—C35	115.9 (9)	F85—C85—C84	119.1 (10)
F36—C36—C31	120.3 (9)	F85—C85—C86	117.1 (10)
C35—C36—C31	123.7 (9)	C84—C85—C86	123.8 (10)
C37—Si3—C39	112.4 (7)	C81—C86—F86	119.2 (9)
C37—Si3—C38	102.8 (7)	C81—C86—C85	124.4 (11)
C39—Si3—C38	112.2 (7)	F86—C86—C85	116.3 (9)
C37—Si3—C34	111.0 (6)	C88—Si8—C89	109.5 (6)
C39—Si3—C34	108.1 (6)	C88—Si8—C84	109.6 (5)
C38—Si3—C34	110.3 (6)	C89—Si8—C84	109.2 (5)
Si3—C37—H37A	109.5	C88—Si8—C87	108.3 (7)
Si3—C37—H37B	109.5	C89—Si8—C87	112.5 (6)
H37A—C37—H37B	109.5	C84—Si8—C87	107.7 (5)
Si3—C37—H37C	109.5	Si8—C87—H87A	109.5
H37A—C37—H37C	109.5	Si8—C87—H87B	109.5
H37B—C37—H37C	109.5	H87A—C87—H87B	109.5
Si3—C38—H38A	109.5	Si8—C87—H87C	109.5
Si3—C38—H38B	109.5	H87A—C87—H87C	109.5
H38A—C38—H38B	109.5	H87B—C87—H87C	109.5
Si3—C38—H38C	109.5	Si8—C88—H88A	109.5
H38A—C38—H38C	109.5	Si8—C88—H88B	109.5
H38B—C38—H38C	109.5	H88A—C88—H88B	109.5
C393—C39—C392	109.0 (12)	Si8—C88—H88C	109.5
C393—C39—C391	108.5 (14)	H88A—C88—H88C	109.5
C392—C39—C391	110.4 (14)	H88B—C88—H88C	109.5
C393—C39—Si3	111.4 (11)	C893—C89—C891	111.9 (12)
C392—C39—Si3	109.2 (10)	C893—C89—C892	111.7 (11)
C391—C39—Si3	108.4 (9)	C891—C89—C892	106.5 (11)
C39—C391—H39A	109.5	C893—C89—Si8	109.3 (9)
C39—C391—H39B	109.5	C891—C89—Si8	109.1 (9)
H39A—C391—H39B	109.5	C892—C89—Si8	108.3 (9)
C39—C391—H39C	109.5	C89—C891—H89A	109.5
H39A—C391—H39C	109.5	C89—C891—H89B	109.5
H39B—C391—H39C	109.5	H89A—C891—H89B	109.5
C39—C392—H39D	109.5	C89—C891—H89C	109.5
C39—C392—H39E	109.5	H89A—C891—H89C	109.5
H39D—C392—H39E	109.5	H89B—C891—H89C	109.5
C39—C392—H39F	109.5	C89—C892—H89D	109.5
H39D—C392—H39F	109.5	C89—C892—H89E	109.5
H39E—C392—H39F	109.5	H89D—C892—H89E	109.5
C39—C393—H39G	109.5	C89—C892—H89F	109.5
C39—C393—H39H	109.5	H89D—C892—H89F	109.5
H39G—C393—H39H	109.5	H89E—C892—H89F	109.5
C39—C393—H39I	109.5	C89—C893—H89G	109.5
H39G—C393—H39I	109.5	C89—C893—H89H	109.5
H39H—C393—H39I	109.5	H89G—C893—H89H	109.5
C46—C41—C42	111.2 (9)	C89—C893—H89I	109.5
C46—C41—B1	130.1 (9)	H89G—C893—H89I	109.5
C42—C41—B1	118.1 (9)	H89H—C893—H89I	109.5
C41—C42—C43	125.5 (10)	C111—C1—C101	121.7 (9)
C41—C42—F42	118.1 (10)	C111—C1—C121	121.2 (9)
C43—C42—F42	116.4 (10)	C101—C1—C121	117.0 (9)
F43—C43—C44	123.2 (10)	C106—C101—C102	118.5 (10)
F43—C43—C42	115.4 (10)	C106—C101—C1	122.4 (9)
C44—C43—C42	121.5 (10)	C102—C101—C1	119.1 (10)
C45—C44—C43	114.6 (10)	C103—C102—C101	120.8 (11)
C45—C44—Si4	125.0 (9)	C103—C102—H102	119.6
C43—C44—Si4	120.3 (9)	C101—C102—H102	119.6
C44—C45—F45	121.6 (10)	C102—C103—C104	119.3 (12)
C44—C45—C46	124.3 (10)	C102—C103—H103	120.3
F45—C45—C46	113.8 (9)	C104—C103—H103	120.3
F46—C46—C41	119.8 (10)	C103—C104—C105	120.7 (12)
F46—C46—C45	117.4 (9)	C103—C104—H104	119.6
C41—C46—C45	122.8 (9)	C105—C104—H104	119.6
C48—Si4—C47	108.0 (7)	C106—C105—C104	118.3 (13)
C48—Si4—C49	112.1 (8)	C106—C105—H105	120.9
C47—Si4—C49	112.3 (7)	C104—C105—H105	120.9
C48—Si4—C44	110.4 (6)	C105—C106—C101	122.4 (11)
C47—Si4—C44	110.6 (6)	C105—C106—H106	118.8
C49—Si4—C44	103.5 (6)	C101—C106—H106	118.8
Si4—C47—H47A	109.5	C112—C111—C116	116.6 (10)
Si4—C47—H47B	109.5	C112—C111—C1	122.8 (10)
H47A—C47—H47B	109.5	C116—C111—C1	120.6 (10)
Si4—C47—H47C	109.5	C113—C112—C111	124.1 (11)
H47A—C47—H47C	109.5	C113—C112—H112	118.0
H47B—C47—H47C	109.5	C111—C112—H112	118.0
Si4—C48—H48A	109.5	C114—C113—C112	116.7 (13)
Si4—C48—H48B	109.5	C114—C113—H113	121.7
H48A—C48—H48B	109.5	C112—C113—H113	121.7
Si4—C48—H48C	109.5	C113—C114—C115	124.6 (13)
H48A—C48—H48C	109.5	C113—C114—H114	117.7
H48B—C48—H48C	109.5	C115—C114—H114	117.7
C491—C49—C492	112.4 (16)	C116—C115—C114	115.3 (13)
C491—C49—C493	107.9 (15)	C116—C115—H115	122.4
C492—C49—C493	108.2 (13)	C114—C115—H115	122.4
C491—C49—Si4	110.2 (11)	C115—C116—C111	122.8 (12)
C492—C49—Si4	113.6 (12)	C115—C116—H116	118.6
C493—C49—Si4	104.0 (12)	C111—C116—H116	118.6
C49—C491—H49A	109.5	C126—C121—C122	119.6 (10)
C49—C491—H49B	109.5	C126—C121—C1	120.1 (9)
H49A—C491—H49B	109.5	C122—C121—C1	120.2 (9)
C49—C491—H49C	109.5	C123—C122—C121	119.5 (10)
H49A—C491—H49C	109.5	C123—C122—H122	120.2
H49B—C491—H49C	109.5	C121—C122—H122	120.2
C49—C492—H49D	109.5	C124—C123—C122	122.6 (10)
C49—C492—H49E	109.5	C124—C123—H123	118.7
H49D—C492—H49E	109.5	C122—C123—H123	118.7
C49—C492—H49F	109.5	C123—C124—C125	117.6 (11)
H49D—C492—H49F	109.5	C123—C124—H124	121.2
H49E—C492—H49F	109.5	C125—C124—H124	121.2
C49—C493—H49G	109.5	C126—C125—C124	121.0 (12)
C49—C493—H49H	109.5	C126—C125—H125	119.5
H49G—C493—H49H	109.5	C124—C125—H125	119.5
C49—C493—H49I	109.5	C125—C126—C121	119.6 (10)
H49G—C493—H49I	109.5	C125—C126—H126	120.2
H49H—C493—H49I	109.5	C121—C126—H126	120.2
C51—B2—C71	116.3 (10)	C221—C2—C211	120.0 (9)
C51—B2—C81	102.0 (8)	C221—C2—C201	119.3 (10)
C71—B2—C81	111.1 (10)	C211—C2—C201	120.6 (9)
C51—B2—C61	116.1 (10)	C206—C201—C202	118.4 (10)
C71—B2—C61	100.3 (7)	C206—C201—C2	122.3 (10)
C81—B2—C61	111.4 (9)	C202—C201—C2	119.3 (10)
C52—C51—C56	112.9 (10)	C203—C202—C201	116.1 (11)
C52—C51—B2	129.4 (11)	C203—C202—H202	122.0
C56—C51—B2	117.6 (10)	C201—C202—H202	122.0
F52—C52—C51	119.4 (11)	C202—C203—C204	123.4 (11)
F52—C52—C53	117.0 (10)	C202—C203—H203	118.3
C51—C52—C53	123.5 (10)	C204—C203—H203	118.3
C54—C53—F53	122.5 (11)	C205—C204—C203	120.0 (11)
C54—C53—C52	123.7 (10)	C205—C204—H204	120.0
F53—C53—C52	113.5 (10)	C203—C204—H204	120.0
C53—C54—C55	115.1 (11)	C206—C205—C204	119.3 (11)
C53—C54—Si5	122.7 (9)	C206—C205—H205	120.4
C55—C54—Si5	122.1 (9)	C204—C205—H205	120.4
F55—C55—C54	121.6 (11)	C205—C206—C201	122.8 (11)
F55—C55—C56	117.6 (11)	C205—C206—H206	118.6
C54—C55—C56	120.5 (11)	C201—C206—H206	118.6
F56—C56—C51	121.2 (10)	C212—C211—C216	116.2 (10)
F56—C56—C55	114.7 (10)	C212—C211—C2	124.6 (10)
C51—C56—C55	124.0 (11)	C216—C211—C2	119.2 (10)
C59—Si5—C58	110.1 (7)	C211—C212—C213	124.7 (12)
C59—Si5—C57	111.5 (6)	C211—C212—H212	117.7
C58—Si5—C57	108.5 (6)	C213—C212—H212	117.7
C59—Si5—C54	107.3 (6)	C212—C213—C214	113.9 (12)
C58—Si5—C54	110.0 (6)	C212—C213—H213	123.0
C57—Si5—C54	109.5 (6)	C214—C213—H213	123.0
Si5—C57—H57A	109.5	C215—C214—C213	124.9 (12)
Si5—C57—H57B	109.5	C215—C214—H214	117.5
H57A—C57—H57B	109.5	C213—C214—H214	117.5
Si5—C57—H57C	109.5	C216—C215—C214	116.8 (13)
H57A—C57—H57C	109.5	C216—C215—H215	121.6
H57B—C57—H57C	109.5	C214—C215—H215	121.6
Si5—C58—H58A	109.5	C215—C216—C211	123.4 (12)
Si5—C58—H58B	109.5	C215—C216—H216	118.3
H58A—C58—H58B	109.5	C211—C216—H216	118.3
Si5—C58—H58C	109.5	C226—C221—C222	119.2 (10)
H58A—C58—H58C	109.5	C226—C221—C2	120.5 (10)
H58B—C58—H58C	109.5	C222—C221—C2	120.3 (9)
C592—C59—C593	108.7 (12)	C223—C222—C221	122.2 (10)
C592—C59—C591	107.4 (12)	C223—C222—H222	118.9
C593—C59—C591	107.0 (13)	C221—C222—H222	118.9
C592—C59—Si5	113.7 (9)	C222—C223—C224	118.3 (12)
C593—C59—Si5	111.1 (10)	C222—C223—H223	120.8
C591—C59—Si5	108.6 (11)	C224—C223—H223	120.8
C59—C591—H59A	109.5	C223—C224—C225	121.9 (11)
C59—C591—H59B	109.5	C223—C224—H224	119.0
H59A—C591—H59B	109.5	C225—C224—H224	119.0
C59—C591—H59C	109.5	C226—C225—C224	117.8 (10)
H59A—C591—H59C	109.5	C226—C225—H225	121.1
H59B—C591—H59C	109.5	C224—C225—H225	121.1
C59—C592—H59D	109.5	C221—C226—C225	120.5 (11)
C59—C592—H59E	109.5	C221—C226—H226	119.8
H59D—C592—H59E	109.5	C225—C226—H226	119.8
C31—B1—C11—C16	−57.3 (14)	C58—Si5—C59—C592	52.3 (12)
C41—B1—C11—C16	−174.4 (9)	C57—Si5—C59—C592	172.7 (10)
C21—B1—C11—C16	65.1 (13)	C54—Si5—C59—C592	−67.4 (12)
C31—B1—C11—C12	135.4 (11)	C58—Si5—C59—C593	175.3 (10)
C41—B1—C11—C12	18.3 (15)	C57—Si5—C59—C593	−64.3 (11)
C21—B1—C11—C12	−102.3 (12)	C54—Si5—C59—C593	55.6 (11)
C16—C11—C12—F12	179.1 (9)	C58—Si5—C59—C591	−67.3 (13)
B1—C11—C12—F12	−12.5 (16)	C57—Si5—C59—C591	53.2 (13)
C16—C11—C12—C13	−0.3 (15)	C54—Si5—C59—C591	173.1 (11)
B1—C11—C12—C13	168.1 (10)	C51—B2—C61—C62	−170.1 (10)
F12—C12—C13—C14	−178.0 (10)	C71—B2—C61—C62	63.7 (12)
C11—C12—C13—C14	1.4 (19)	C81—B2—C61—C62	−53.9 (14)
F12—C12—C13—F13	1.3 (14)	C51—B2—C61—C66	19.1 (15)
C11—C12—C13—F13	−179.3 (9)	C71—B2—C61—C66	−107.1 (11)
C12—C13—C14—C15	−0.8 (17)	C81—B2—C61—C66	135.2 (11)
F13—C13—C14—C15	180.0 (9)	C66—C61—C62—F62	176.3 (9)
C12—C13—C14—Si1	−172.5 (9)	B2—C61—C62—F62	4.6 (15)
F13—C13—C14—Si1	8.2 (15)	C66—C61—C62—C63	1.2 (16)
C13—C14—C15—F15	−179.8 (9)	B2—C61—C62—C63	−170.5 (11)
Si1—C14—C15—F15	−7.9 (15)	C61—C62—C63—F63	178.5 (10)
C13—C14—C15—C16	−0.8 (16)	F62—C62—C63—F63	3.3 (15)
Si1—C14—C15—C16	171.1 (9)	C61—C62—C63—C64	−2.9 (19)
C12—C11—C16—C15	−1.2 (16)	F62—C62—C63—C64	−178.1 (10)
B1—C11—C16—C15	−170.6 (10)	F63—C63—C64—C65	−178.2 (10)
C12—C11—C16—F16	178.3 (9)	C62—C63—C64—C65	3.3 (17)
B1—C11—C16—F16	8.9 (15)	F63—C63—C64—Si6	0.5 (16)
C14—C15—C16—C11	2.0 (19)	C62—C63—C64—Si6	−178.0 (9)
F15—C15—C16—C11	−179.0 (10)	C63—C64—C65—C66	−2.6 (17)
C14—C15—C16—F16	−177.5 (10)	Si6—C64—C65—C66	178.7 (9)
F15—C15—C16—F16	1.5 (14)	C63—C64—C65—F65	176.6 (10)
C13—C14—Si1—C18	−28.7 (12)	Si6—C64—C65—F65	−2.1 (16)
C15—C14—Si1—C18	160.7 (10)	C64—C65—C66—F66	179.3 (11)
C13—C14—Si1—C17	−146.7 (10)	F65—C65—C66—F66	0.1 (15)
C15—C14—Si1—C17	42.8 (11)	C64—C65—C66—C61	1.3 (19)
C13—C14—Si1—C19	90.9 (11)	F65—C65—C66—C61	−177.9 (9)
C15—C14—Si1—C19	−79.7 (11)	C62—C61—C66—F66	−178.3 (9)
C18—Si1—C19—C193	−177.5 (10)	B2—C61—C66—F66	−6.7 (16)
C17—Si1—C19—C193	−59.2 (11)	C62—C61—C66—C65	−0.4 (15)
C14—Si1—C19—C193	60.5 (11)	B2—C61—C66—C65	171.2 (10)
C18—Si1—C19—C192	65.2 (11)	C63—C64—Si6—C68	159.4 (10)
C17—Si1—C19—C192	−176.6 (9)	C65—C64—Si6—C68	−22.1 (12)
C14—Si1—C19—C192	−56.9 (10)	C63—C64—Si6—C67	41.0 (12)
C18—Si1—C19—C191	−52.8 (10)	C65—C64—Si6—C67	−140.5 (10)
C17—Si1—C19—C191	65.5 (10)	C63—C64—Si6—C69	−79.1 (12)
C14—Si1—C19—C191	−174.8 (9)	C65—C64—Si6—C69	99.4 (12)
C11—B1—C21—C26	−102.9 (12)	C68—Si6—C69—C691	62.1 (18)
C31—B1—C21—C26	21.8 (15)	C67—Si6—C69—C691	−180.0 (15)
C41—B1—C21—C26	134.4 (11)	C64—Si6—C69—C691	−60.1 (18)
C11—B1—C21—C22	64.1 (12)	C68—Si6—C69—C693	179.0 (13)
C31—B1—C21—C22	−171.2 (9)	C67—Si6—C69—C693	−63.1 (16)
C41—B1—C21—C22	−58.6 (13)	C64—Si6—C69—C693	56.8 (15)
C26—C21—C22—C23	−0.4 (15)	C68—Si6—C69—C692	−55.2 (14)
B1—C21—C22—C23	−169.4 (11)	C67—Si6—C69—C692	62.7 (14)
C26—C21—C22—F22	178.4 (8)	C64—Si6—C69—C692	−177.4 (12)
B1—C21—C22—F22	9.4 (14)	C51—B2—C71—C72	134.8 (12)
F22—C22—C23—F23	0.5 (15)	C81—B2—C71—C72	18.7 (17)
C21—C22—C23—F23	179.3 (9)	C61—B2—C71—C72	−99.2 (13)
F22—C22—C23—C24	−177.0 (9)	C51—B2—C71—C76	−57.1 (14)
C21—C22—C23—C24	1.8 (17)	C81—B2—C71—C76	−173.2 (9)
F23—C23—C24—C25	179.7 (10)	C61—B2—C71—C76	68.9 (12)
C22—C23—C24—C25	−2.8 (16)	C76—C71—C72—C73	0.5 (17)
F23—C23—C24—Si2	−3.7 (15)	B2—C71—C72—C73	169.4 (11)
C22—C23—C24—Si2	173.8 (8)	C76—C71—C72—F72	−178.7 (9)
C23—C24—C25—F25	−179.6 (9)	B2—C71—C72—F72	−9.8 (18)
Si2—C24—C25—F25	3.9 (15)	F72—C72—C73—F73	−1.2 (15)
C23—C24—C25—C26	2.9 (16)	C71—C72—C73—F73	179.6 (10)
Si2—C24—C25—C26	−173.7 (8)	F72—C72—C73—C74	178.0 (10)
F25—C25—C26—F26	1.1 (14)	C71—C72—C73—C74	−1.2 (19)
C24—C25—C26—F26	178.7 (9)	F73—C73—C74—C75	179.9 (10)
F25—C25—C26—C21	−179.4 (9)	C72—C73—C74—C75	0.7 (18)
C24—C25—C26—C21	−1.7 (17)	F73—C73—C74—Si7	4.5 (17)
C22—C21—C26—F26	179.8 (8)	C72—C73—C74—Si7	−174.7 (9)
B1—C21—C26—F26	−12.3 (16)	C73—C74—C75—F75	−179.5 (11)
C22—C21—C26—C25	0.3 (15)	Si7—C74—C75—F75	−3.8 (16)
B1—C21—C26—C25	168.2 (10)	C73—C74—C75—C76	0.3 (17)
C25—C24—Si2—C27	−144.8 (10)	Si7—C74—C75—C76	175.9 (9)
C23—C24—Si2—C27	38.9 (11)	C72—C71—C76—F76	177.2 (9)
C25—C24—Si2—C28	−24.1 (11)	B2—C71—C76—F76	6.8 (15)
C23—C24—Si2—C28	159.6 (9)	C72—C71—C76—C75	0.5 (16)
C25—C24—Si2—C29	92.7 (11)	B2—C71—C76—C75	−169.9 (10)
C23—C24—Si2—C29	−83.7 (10)	F75—C75—C76—F76	2.0 (14)
C27—Si2—C29—C292	−178.8 (9)	C74—C75—C76—F76	−177.7 (10)
C28—Si2—C29—C292	59.5 (11)	F75—C75—C76—C71	178.8 (10)
C24—Si2—C29—C292	−58.4 (11)	C74—C75—C76—C71	−0.9 (18)
C27—Si2—C29—C291	61.6 (11)	C73—C74—Si7—C77	−144.3 (11)
C28—Si2—C29—C291	−60.1 (11)	C75—C74—Si7—C77	40.4 (12)
C24—Si2—C29—C291	−178.0 (9)	C73—C74—Si7—C79	93.4 (13)
C27—Si2—C29—C293	−56.8 (11)	C75—C74—Si7—C79	−81.9 (12)
C28—Si2—C29—C293	−178.5 (9)	C73—C74—Si7—C78	−23.9 (13)
C24—Si2—C29—C293	63.6 (11)	C75—C74—Si7—C78	160.8 (10)
C11—B1—C31—C32	173.7 (9)	C77—Si7—C79—C793	−50 (2)
C41—B1—C31—C32	−61.9 (12)	C74—Si7—C79—C793	69.8 (19)
C21—B1—C31—C32	57.0 (13)	C78—Si7—C79—C793	−174.3 (17)
C11—B1—C31—C36	−18.2 (15)	C77—Si7—C79—C791	−176.2 (15)
C41—B1—C31—C36	106.2 (11)	C74—Si7—C79—C791	−56.3 (18)
C21—B1—C31—C36	−135.0 (10)	C78—Si7—C79—C791	59.5 (18)
C36—C31—C32—F32	−178.0 (9)	C77—Si7—C79—C792	72.0 (19)
B1—C31—C32—F32	−8.5 (15)	C74—Si7—C79—C792	−168.1 (17)
C36—C31—C32—C33	−0.4 (15)	C78—Si7—C79—C792	−52.3 (19)
B1—C31—C32—C33	169.1 (10)	C51—B2—C81—C86	108.8 (13)
F32—C32—C33—F33	−1.9 (14)	C71—B2—C81—C86	−126.5 (12)
C31—C32—C33—F33	−179.6 (9)	C61—B2—C81—C86	−15.6 (17)
F32—C32—C33—C34	177.9 (9)	C51—B2—C81—C82	−67.4 (13)
C31—C32—C33—C34	0.3 (17)	C71—B2—C81—C82	57.3 (13)
F33—C33—C34—C35	177.9 (9)	C61—B2—C81—C82	168.2 (10)
C32—C33—C34—C35	−1.9 (16)	C86—C81—C82—C83	3.4 (16)
F33—C33—C34—Si3	11.5 (14)	B2—C81—C82—C83	−179.7 (10)
C32—C33—C34—Si3	−168.3 (8)	C86—C81—C82—F82	−179.5 (9)
C33—C34—C35—F35	179.9 (9)	B2—C81—C82—F82	−2.6 (15)
Si3—C34—C35—F35	−13.9 (14)	F82—C82—C83—C84	179.6 (10)
C33—C34—C35—C36	4.0 (16)	C81—C82—C83—C84	−3.4 (19)
Si3—C34—C35—C36	170.1 (8)	F82—C82—C83—F83	−0.3 (15)
C34—C35—C36—F36	−179.8 (9)	C81—C82—C83—F83	176.7 (10)
F35—C35—C36—F36	4.1 (13)	C82—C83—C84—C85	1.7 (17)
C34—C35—C36—C31	−4.5 (17)	F83—C83—C84—C85	−178.4 (9)
F35—C35—C36—C31	179.3 (9)	C82—C83—C84—Si8	−180.0 (9)
C32—C31—C36—F36	177.5 (9)	F83—C83—C84—Si8	−0.1 (15)
B1—C31—C36—F36	8.8 (15)	C83—C84—C85—F85	179.8 (9)
C32—C31—C36—C35	2.4 (15)	Si8—C84—C85—F85	1.5 (15)
B1—C31—C36—C35	−166.3 (10)	C83—C84—C85—C86	−0.6 (16)
C35—C34—Si3—C37	153.0 (10)	Si8—C84—C85—C86	−178.9 (8)
C33—C34—Si3—C37	−41.8 (11)	C82—C81—C86—F86	175.7 (9)
C35—C34—Si3—C39	−83.3 (10)	B2—C81—C86—F86	−0.8 (18)
C33—C34—Si3—C39	81.8 (10)	C82—C81—C86—C85	−2.4 (16)
C35—C34—Si3—C38	39.8 (11)	B2—C81—C86—C85	−178.8 (11)
C33—C34—Si3—C38	−155.1 (9)	F85—C85—C86—C81	−179.3 (10)
C37—Si3—C39—C393	−62.7 (13)	C84—C85—C86—C81	1.2 (18)
C38—Si3—C39—C393	52.6 (13)	F85—C85—C86—F86	2.6 (14)
C34—Si3—C39—C393	174.5 (11)	C84—C85—C86—F86	−176.9 (10)
C37—Si3—C39—C392	57.8 (12)	C83—C84—Si8—C88	28.2 (12)
C38—Si3—C39—C392	173.1 (10)	C85—C84—Si8—C88	−153.7 (10)
C34—Si3—C39—C392	−65.0 (11)	C83—C84—Si8—C89	−91.7 (11)
C37—Si3—C39—C391	178.0 (11)	C85—C84—Si8—C89	86.4 (11)
C38—Si3—C39—C391	−66.7 (13)	C83—C84—Si8—C87	145.8 (10)
C34—Si3—C39—C391	55.2 (13)	C85—C84—Si8—C87	−36.1 (11)
C11—B1—C41—C46	−131.5 (11)	C88—Si8—C89—C893	−70.1 (10)
C31—B1—C41—C46	103.2 (12)	C84—Si8—C89—C893	49.9 (10)
C21—B1—C41—C46	−16.3 (16)	C87—Si8—C89—C893	169.4 (9)
C11—B1—C41—C42	58.2 (13)	C88—Si8—C89—C891	52.5 (12)
C31—B1—C41—C42	−67.1 (12)	C84—Si8—C89—C891	172.5 (10)
C21—B1—C41—C42	173.5 (9)	C87—Si8—C89—C891	−68.0 (11)
C46—C41—C42—C43	0.6 (16)	C88—Si8—C89—C892	168.0 (9)
B1—C41—C42—C43	172.6 (10)	C84—Si8—C89—C892	−72.0 (10)
C46—C41—C42—F42	−177.5 (8)	C87—Si8—C89—C892	47.6 (10)
B1—C41—C42—F42	−5.5 (14)	C111—C1—C101—C106	147.2 (11)
C41—C42—C43—F43	179.6 (10)	C121—C1—C101—C106	−29.5 (15)
F42—C42—C43—F43	−2.2 (14)	C111—C1—C101—C102	−33.3 (16)
C41—C42—C43—C44	−0.7 (18)	C121—C1—C101—C102	150.0 (10)
F42—C42—C43—C44	177.4 (10)	C106—C101—C102—C103	−0.7 (17)
F43—C43—C44—C45	−177.8 (10)	C1—C101—C102—C103	179.9 (11)
C42—C43—C44—C45	2.7 (17)	C101—C102—C103—C104	0.3 (18)
F43—C43—C44—Si4	6.1 (16)	C102—C103—C104—C105	1 (2)
C42—C43—C44—Si4	−173.5 (9)	C103—C104—C105—C106	−1 (2)
C43—C44—C45—F45	−178.4 (10)	C104—C105—C106—C101	0.6 (19)
Si4—C44—C45—F45	−2.5 (17)	C102—C101—C106—C105	0.2 (17)
C43—C44—C45—C46	−4.7 (18)	C1—C101—C106—C105	179.6 (11)
Si4—C44—C45—C46	171.3 (8)	C101—C1—C111—C112	−27.1 (17)
C42—C41—C46—F46	178.4 (9)	C121—C1—C111—C112	149.5 (11)
B1—C41—C46—F46	7.6 (16)	C101—C1—C111—C116	151.8 (10)
C42—C41—C46—C45	−2.5 (14)	C121—C1—C111—C116	−31.7 (16)
B1—C41—C46—C45	−173.2 (10)	C116—C111—C112—C113	−0.1 (18)
C44—C45—C46—F46	−175.9 (10)	C1—C111—C112—C113	178.8 (11)
F45—C45—C46—F46	−1.7 (13)	C111—C112—C113—C114	0 (2)
C44—C45—C46—C41	4.9 (18)	C112—C113—C114—C115	−1 (2)
F45—C45—C46—C41	179.1 (9)	C113—C114—C115—C116	1.5 (19)
C45—C44—Si4—C48	148.5 (11)	C114—C115—C116—C111	−1.7 (17)
C43—C44—Si4—C48	−35.8 (12)	C112—C111—C116—C115	1.1 (17)
C45—C44—Si4—C47	29.0 (13)	C1—C111—C116—C115	−177.8 (11)
C43—C44—Si4—C47	−155.2 (10)	C111—C1—C121—C126	143.0 (11)
C45—C44—Si4—C49	−91.4 (12)	C101—C1—C121—C126	−40.3 (15)
C43—C44—Si4—C49	84.3 (11)	C111—C1—C121—C122	−33.3 (16)
C48—Si4—C49—C491	−176.3 (12)	C101—C1—C121—C122	143.4 (11)
C47—Si4—C49—C491	−54.5 (14)	C126—C121—C122—C123	1.6 (17)
C44—Si4—C49—C491	64.8 (14)	C1—C121—C122—C123	177.8 (11)
C48—Si4—C49—C492	56.5 (14)	C121—C122—C123—C124	0.2 (19)
C47—Si4—C49—C492	178.3 (12)	C122—C123—C124—C125	−3 (2)
C44—Si4—C49—C492	−62.4 (13)	C123—C124—C125—C126	4 (2)
C48—Si4—C49—C493	−60.9 (13)	C124—C125—C126—C121	−2 (2)
C47—Si4—C49—C493	60.9 (13)	C122—C121—C126—C125	−0.5 (18)
C44—Si4—C49—C493	−179.8 (10)	C1—C121—C126—C125	−176.8 (11)
C71—B2—C51—C52	−12.4 (17)	C221—C2—C201—C206	−27.3 (16)
C81—B2—C51—C52	108.7 (13)	C211—C2—C201—C206	149.0 (11)
C61—B2—C51—C52	−130.0 (12)	C221—C2—C201—C202	151.4 (10)
C71—B2—C51—C56	170.0 (10)	C211—C2—C201—C202	−32.3 (15)
C81—B2—C51—C56	−68.9 (13)	C206—C201—C202—C203	2.4 (15)
C61—B2—C51—C56	52.4 (13)	C2—C201—C202—C203	−176.3 (10)
C56—C51—C52—F52	179.0 (9)	C201—C202—C203—C204	−3.5 (18)
B2—C51—C52—F52	1.3 (18)	C202—C203—C204—C205	1 (2)
C56—C51—C52—C53	3.1 (16)	C203—C204—C205—C206	1.8 (19)
B2—C51—C52—C53	−174.5 (11)	C204—C205—C206—C201	−2.8 (18)
F52—C52—C53—C54	178.3 (10)	C202—C201—C206—C205	0.6 (16)
C51—C52—C53—C54	−5.7 (19)	C2—C201—C206—C205	179.3 (10)
F52—C52—C53—F53	4.7 (15)	C221—C2—C211—C212	151.2 (11)
C51—C52—C53—F53	−179.3 (10)	C201—C2—C211—C212	−25.1 (17)
F53—C53—C54—C55	178.8 (10)	C221—C2—C211—C216	−30.4 (16)
C52—C53—C54—C55	5.8 (18)	C201—C2—C211—C216	153.4 (10)
F53—C53—C54—Si5	−5.3 (17)	C216—C211—C212—C213	2.6 (17)
C52—C53—C54—Si5	−178.3 (9)	C2—C211—C212—C213	−178.9 (10)
C53—C54—C55—F55	−177.9 (10)	C211—C212—C213—C214	−4.2 (18)
Si5—C54—C55—F55	6.2 (16)	C212—C213—C214—C215	3.0 (19)
C53—C54—C55—C56	−4.1 (17)	C213—C214—C215—C216	0 (2)
Si5—C54—C55—C56	180.0 (8)	C214—C215—C216—C211	−1.5 (19)
C52—C51—C56—F56	−177.8 (9)	C212—C211—C216—C215	0.5 (17)
B2—C51—C56—F56	0.2 (15)	C2—C211—C216—C215	−178.1 (11)
C52—C51—C56—C55	−1.6 (16)	C211—C2—C221—C226	−36.5 (17)
B2—C51—C56—C55	176.3 (10)	C201—C2—C221—C226	139.7 (11)
F55—C55—C56—F56	−7.3 (15)	C211—C2—C221—C222	144.3 (11)
C54—C55—C56—F56	178.7 (10)	C201—C2—C221—C222	−39.4 (16)
F55—C55—C56—C51	176.3 (10)	C226—C221—C222—C223	3.4 (18)
C54—C55—C56—C51	2.3 (18)	C2—C221—C222—C223	−177.5 (12)
C53—C54—Si5—C59	83.2 (11)	C221—C222—C223—C224	−2.7 (19)
C55—C54—Si5—C59	−101.2 (11)	C222—C223—C224—C225	0 (2)
C53—C54—Si5—C58	−36.6 (12)	C223—C224—C225—C226	1 (2)
C55—C54—Si5—C58	139.0 (10)	C222—C221—C226—C225	−1.6 (18)
C53—C54—Si5—C57	−155.7 (10)	C2—C221—C226—C225	179.2 (11)
C55—C54—Si5—C57	19.9 (11)	C224—C225—C226—C221	−0.7 (18)