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Crystal structure determinations of (η5-cyclopentadienyl)(4,5-dimercapto-1,3-dithiole-2-thionato)cobalt(III), [Co(C8H5S5)], and (η5-pentamethylcyclopentadienyl)(4,5-dimercapto-1,3-dithiole-2-thionato) cobalt(II), [Co(C13H15S5)], show that Cp* substitution does not significantly modify the geometric features of these complexes, which are characterized by a perpendicular arrangement of the planar Cp or Cp* and (CoS2C2) moieties.

Supporting information

cif

Crystallographic Information File (CIF)
Contains datablocks paper, I, II

fcf

Structure factor file (CIF format)
Contains datablock I

hkl

Structure factor file (CIF format)
Contains datablock (II)

CCDC references: 129030; 129031

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