7,8-Di­phenyl-9-di­methyl­sulfido-10,11-μ-hydro-7,8-dicarba-nido-undecaborane(9)

In the title compound, C₁₆H₂₅B₉S, there are two crystallographically independent mol­ecules, and the conformations of the phenyl and SMe₂ substituents indicate some intramolecular steric crowding. The bridging H atom is asymmetrically disposed. The title compound is a precursor to a crowded vertex-labelled nido carborane ligand important in establishing the mechanism of isomerization of icosahedral heteroboranes.

Computing details

Data collection: XSCANS (Siemens, 1994); cell refinement: XSCANS; data reduction: SHELXTL (Sheldrick, 1999); program(s) used to solve structure: SHELXS97 (Sheldrick, 1997); program(s) used to refine structure: SHELXL97 (Sheldrick, 1997); molecular graphics: SHELXTL; software used to prepare material for publication: SHELXTL.

(1)

Crystal data

C16H25B9S	F(000) = 1456
Mr = 346.71	Dx = 1.139 Mg m^−3
Monoclinic, P21/n	Mo Kα radiation, λ = 0.71073 Å
a = 13.039 (2) Å	Cell parameters from 45 reflections
b = 15.2610 (16) Å	θ = 2.7–16.2°
c = 21.319 (5) Å	µ = 0.16 mm^−1
β = 107.581 (14)°	T = 160 K
V = 4044.2 (13) Å^3	Plate, colourless
Z = 8	0.62 × 0.44 × 0.21 mm

Data collection

Bruker P4 diffractometer	5279 reflections with I > 2σ(I)
Radiation source: fine-focus sealed tube	Rint = 0.033
Graphite monochromator	θmax = 25.0°, θmin = 2.0°
ω scans	h = −15→1
Absorption correction: ψ scan (North et al., 1968)	k = −18→1
Tmin = 0.924, Tmax = 0.968	l = −24→25
8786 measured reflections	3 standard reflections every 97 reflections
7111 independent reflections	intensity decay: 1.7%

Refinement

Refinement on F^2	Primary atom site location: structure-invariant direct methods
Least-squares matrix: full	Secondary atom site location: difference Fourier map
R[F^2 > 2σ(F^2)] = 0.050	Hydrogen site location: inferred from neighbouring sites
wR(F^2) = 0.129	H atoms treated by a mixture of independent and constrained refinement
S = 1.04	w = 1/[σ^2(Fo^2) + (0.0523P)^2 + 1.8495P] where P = (Fo^2 + 2Fc^2)/3
7111 reflections	(Δ/σ)max = 0.001
523 parameters	Δρmax = 0.40 e Å^−3
0 restraints	Δρmin = −0.22 e Å^−3

Special details

Geometry. All e.s.d.'s (except the e.s.d. in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell e.s.d.'s are taken into account individually in the estimation of e.s.d.'s in distances, angles and torsion angles; correlations between e.s.d.'s in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell e.s.d.'s is used for estimating e.s.d.'s involving l.s. planes.

Refinement. Refinement of F² against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F², conventional R-factors R are based on F, with F set to zero for negative F². The threshold expression of F² > σ(F²) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F² are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Ų)

	x	y	z	Uiso*/Ueq
B1	0.1960 (2)	0.7691 (2)	0.73462 (13)	0.0318 (7)
H1	0.193 (2)	0.7664 (18)	0.6849 (13)	0.038*
B2	0.1626 (2)	0.6790 (2)	0.77531 (13)	0.0290 (6)
H2	0.140 (2)	0.6084 (17)	0.7558 (12)	0.035*
B3	0.2976 (2)	0.71160 (19)	0.79484 (13)	0.0258 (6)
H3	0.359 (2)	0.6745 (17)	0.7870 (12)	0.031*
B4	0.3002 (2)	0.82770 (19)	0.79263 (12)	0.0260 (6)
H4	0.370 (2)	0.8609 (16)	0.7837 (12)	0.031*
B5	0.1665 (2)	0.86587 (19)	0.77266 (13)	0.0288 (6)
H5	0.143 (2)	0.9278 (17)	0.7462 (12)	0.035*
B6	0.0785 (2)	0.7725 (2)	0.76299 (14)	0.0315 (6)
H6	0.002 (2)	0.7749 (17)	0.7278 (13)	0.038*
C7	0.23959 (18)	0.68742 (15)	0.85527 (11)	0.0231 (5)
C8	0.31320 (17)	0.77211 (15)	0.86639 (10)	0.0208 (5)
B9	0.2466 (2)	0.86275 (17)	0.85511 (12)	0.0221 (5)
B10	0.1069 (2)	0.83833 (19)	0.83629 (14)	0.0283 (6)
H10	0.039 (2)	0.8798 (17)	0.8432 (12)	0.034*
H10A	0.133 (2)	0.7874 (17)	0.8803 (12)	0.034*
B11	0.1122 (2)	0.71647 (18)	0.84050 (14)	0.0270 (6)
H11	0.054 (2)	0.6723 (17)	0.8531 (12)	0.032*
C71	0.27981 (18)	0.60779 (15)	0.89740 (11)	0.0255 (5)
C72	0.3449 (2)	0.54365 (17)	0.88264 (14)	0.0386 (6)
H72	0.3659	0.5487	0.8438	0.046*
C73	0.3796 (3)	0.4722 (2)	0.92428 (17)	0.0526 (8)
H73	0.4235	0.4287	0.9134	0.063*
C74	0.3507 (3)	0.46385 (19)	0.98121 (16)	0.0516 (8)
H74	0.3761	0.4158	1.0101	0.062*
C75	0.2850 (3)	0.52577 (19)	0.99558 (15)	0.0486 (8)
H75	0.2637	0.5200	1.0342	0.058*
C76	0.2494 (2)	0.59690 (17)	0.95394 (13)	0.0376 (6)
H76	0.2033	0.6389	0.9644	0.045*
C81	0.42039 (17)	0.76773 (14)	0.91903 (10)	0.0207 (5)
C82	0.51804 (18)	0.76491 (15)	0.90531 (11)	0.0244 (5)
H82	0.5187	0.7634	0.8609	0.029*
C83	0.61417 (19)	0.76434 (16)	0.95575 (12)	0.0278 (5)
H83	0.6803	0.7632	0.9457	0.033*
C84	0.61464 (19)	0.76538 (16)	1.02119 (12)	0.0285 (5)
H84	0.6808	0.7647	1.0557	0.034*
C85	0.51844 (19)	0.76740 (16)	1.03548 (11)	0.0293 (5)
H85	0.5180	0.7676	1.0800	0.035*
C86	0.42238 (18)	0.76916 (16)	0.98492 (11)	0.0256 (5)
H86	0.3565	0.7714	0.9952	0.031*
S9	0.32030 (5)	0.96186 (4)	0.89993 (3)	0.02614 (15)
C91	0.2739 (2)	0.97444 (18)	0.97062 (12)	0.0392 (7)
H91A	0.1951	0.9733	0.9568	0.059*
H91B	0.2994	1.0305	0.9921	0.059*
H91C	0.3020	0.9264	1.0016	0.059*
C92	0.2516 (2)	1.05178 (17)	0.85092 (13)	0.0398 (7)
H92A	0.2795	1.1071	0.8729	0.060*
H92B	0.1744	1.0475	0.8454	0.060*
H92C	0.2634	1.0499	0.8077	0.060*
B1'	1.0888 (2)	0.1781 (2)	0.96183 (13)	0.0293 (6)
H1'	1.167 (2)	0.1524 (17)	0.9866 (12)	0.035*
B2'	0.9717 (2)	0.13579 (18)	0.97508 (13)	0.0252 (6)
H2'	0.9621 (19)	0.0799 (17)	1.0058 (12)	0.030*
B3'	0.9934 (2)	0.11880 (18)	0.89842 (13)	0.0228 (5)
H3'	1.0054 (19)	0.0554 (16)	0.8793 (11)	0.027*
B4'	1.0545 (2)	0.21456 (18)	0.87886 (13)	0.0250 (6)
H4'	1.1045 (19)	0.2096 (16)	0.8455 (12)	0.030*
B5'	1.0682 (2)	0.29142 (19)	0.94310 (14)	0.0278 (6)
H5'	1.130 (2)	0.3424 (17)	0.9545 (12)	0.033*
B6'	1.0124 (2)	0.2436 (2)	1.00294 (13)	0.0303 (6)
H6'	1.045 (2)	0.2588 (17)	1.0562 (13)	0.036*
C7'	0.87104 (17)	0.15389 (14)	0.90319 (10)	0.0196 (5)
C8'	0.91539 (16)	0.20096 (14)	0.85037 (10)	0.0197 (5)
B9'	0.9596 (2)	0.29901 (17)	0.87127 (13)	0.0239 (6)
B10'	0.9384 (2)	0.32562 (19)	0.94759 (13)	0.0269 (6)
H10'	0.930 (2)	0.3909 (17)	0.9669 (12)	0.032*
H10B	0.854 (2)	0.2934 (17)	0.9279 (12)	0.032*
B11'	0.8736 (2)	0.22261 (18)	0.96343 (12)	0.0238 (6)
H11'	0.8173 (19)	0.2170 (16)	0.9890 (12)	0.029*
C71'	0.77791 (17)	0.09091 (15)	0.88172 (10)	0.0203 (5)
C72'	0.7913 (2)	0.00017 (16)	0.88165 (11)	0.0271 (5)
H72'	0.8616	−0.0240	0.8919	0.033*
C73'	0.7026 (2)	−0.05501 (17)	0.86666 (12)	0.0344 (6)
H73'	0.7126	−0.1167	0.8667	0.041*
C74'	0.5997 (2)	−0.02109 (18)	0.85165 (12)	0.0351 (6)
H74'	0.5393	−0.0591	0.8421	0.042*
C75'	0.58554 (19)	0.06914 (18)	0.85073 (12)	0.0328 (6)
H75'	0.5150	0.0930	0.8396	0.039*
C76'	0.67346 (18)	0.12424 (17)	0.86584 (11)	0.0269 (5)
H76'	0.6628	0.1858	0.8654	0.032*
C81'	0.86011 (18)	0.17961 (15)	0.77901 (11)	0.0238 (5)
C82'	0.9045 (2)	0.12516 (17)	0.74228 (12)	0.0327 (6)
H82'	0.9720	0.0980	0.7623	0.039*
C83'	0.8505 (2)	0.1099 (2)	0.67584 (13)	0.0436 (7)
H83'	0.8813	0.0725	0.6509	0.052*
C84'	0.7524 (2)	0.1492 (2)	0.64643 (13)	0.0438 (7)
H84'	0.7159	0.1388	0.6012	0.053*
C85'	0.7073 (2)	0.2035 (2)	0.68253 (12)	0.0411 (7)
H85'	0.6395	0.2302	0.6624	0.049*
C86'	0.7609 (2)	0.21891 (18)	0.74839 (12)	0.0317 (6)
H86'	0.7298	0.2568	0.7730	0.038*
S9'	0.95552 (5)	0.37969 (4)	0.80343 (3)	0.03070 (16)
C91'	0.8501 (3)	0.4552 (2)	0.80550 (17)	0.0644 (10)
H91D	0.8483	0.5038	0.7752	0.097*
H91E	0.8640	0.4781	0.8502	0.097*
H91F	0.7807	0.4247	0.7922	0.097*
C92'	1.0725 (3)	0.4470 (2)	0.83626 (16)	0.0622 (10)
H92D	1.0725	0.4706	0.8790	0.093*
H92E	1.0715	0.4954	0.8059	0.093*
H92F	1.1374	0.4117	0.8418	0.093*

Atomic displacement parameters (Ų)

	U^11	U^22	U^33	U^12	U^13	U^23
B1	0.0327 (16)	0.0402 (17)	0.0204 (14)	−0.0065 (13)	0.0051 (12)	−0.0045 (12)
B2	0.0270 (15)	0.0325 (16)	0.0250 (14)	−0.0038 (12)	0.0042 (12)	−0.0064 (12)
B3	0.0224 (14)	0.0314 (15)	0.0236 (13)	−0.0040 (12)	0.0069 (11)	−0.0068 (11)
B4	0.0267 (14)	0.0314 (15)	0.0192 (13)	−0.0025 (12)	0.0059 (11)	0.0014 (11)
B5	0.0288 (15)	0.0322 (15)	0.0201 (13)	−0.0009 (12)	−0.0005 (11)	0.0048 (11)
B6	0.0243 (15)	0.0330 (16)	0.0305 (15)	−0.0033 (12)	−0.0016 (12)	−0.0032 (12)
C7	0.0208 (12)	0.0235 (12)	0.0235 (12)	−0.0016 (10)	0.0045 (9)	−0.0057 (9)
C8	0.0213 (11)	0.0232 (12)	0.0176 (11)	−0.0024 (9)	0.0056 (9)	−0.0013 (9)
B9	0.0214 (13)	0.0236 (13)	0.0193 (12)	−0.0026 (11)	0.0032 (10)	0.0002 (10)
B10	0.0226 (14)	0.0296 (15)	0.0306 (15)	0.0015 (12)	0.0048 (11)	0.0003 (12)
B11	0.0225 (14)	0.0269 (14)	0.0312 (14)	−0.0035 (12)	0.0073 (12)	−0.0035 (12)
C71	0.0244 (12)	0.0182 (11)	0.0309 (13)	−0.0046 (10)	0.0036 (10)	−0.0037 (10)
C72	0.0377 (15)	0.0305 (14)	0.0481 (16)	0.0024 (12)	0.0137 (13)	−0.0028 (12)
C73	0.0494 (18)	0.0307 (16)	0.077 (2)	0.0129 (14)	0.0175 (17)	0.0025 (15)
C74	0.064 (2)	0.0286 (15)	0.0538 (19)	0.0015 (15)	0.0046 (16)	0.0090 (14)
C75	0.073 (2)	0.0321 (15)	0.0427 (16)	−0.0029 (15)	0.0202 (15)	0.0056 (13)
C76	0.0520 (17)	0.0254 (13)	0.0386 (15)	0.0015 (12)	0.0185 (13)	−0.0001 (11)
C81	0.0211 (12)	0.0157 (11)	0.0239 (11)	0.0002 (9)	0.0045 (9)	−0.0010 (9)
C82	0.0258 (12)	0.0239 (12)	0.0243 (12)	−0.0018 (10)	0.0086 (10)	−0.0024 (10)
C83	0.0199 (12)	0.0287 (13)	0.0349 (13)	−0.0010 (10)	0.0085 (10)	−0.0007 (10)
C84	0.0234 (12)	0.0272 (13)	0.0287 (13)	0.0002 (10)	−0.0013 (10)	−0.0048 (10)
C85	0.0313 (13)	0.0329 (14)	0.0209 (12)	0.0022 (11)	0.0037 (10)	−0.0018 (10)
C86	0.0221 (12)	0.0290 (13)	0.0262 (12)	0.0025 (10)	0.0080 (10)	−0.0004 (10)
S9	0.0280 (3)	0.0217 (3)	0.0284 (3)	−0.0025 (3)	0.0080 (2)	−0.0019 (2)
C91	0.0597 (18)	0.0339 (15)	0.0262 (13)	−0.0009 (13)	0.0161 (13)	−0.0023 (11)
C92	0.0571 (18)	0.0230 (13)	0.0409 (15)	0.0045 (12)	0.0171 (13)	0.0067 (11)
B1'	0.0196 (14)	0.0361 (16)	0.0276 (14)	−0.0019 (12)	0.0003 (11)	0.0026 (12)
B2'	0.0207 (13)	0.0287 (15)	0.0227 (13)	−0.0019 (11)	0.0013 (11)	0.0034 (11)
B3'	0.0168 (12)	0.0232 (14)	0.0269 (13)	−0.0006 (11)	0.0044 (10)	0.0023 (11)
B4'	0.0165 (13)	0.0279 (14)	0.0288 (14)	−0.0023 (11)	0.0043 (11)	0.0002 (11)
B5'	0.0218 (14)	0.0304 (15)	0.0292 (14)	−0.0086 (12)	0.0049 (11)	−0.0025 (12)
B6'	0.0306 (15)	0.0377 (16)	0.0202 (13)	−0.0125 (13)	0.0040 (12)	−0.0023 (12)
C7'	0.0168 (11)	0.0225 (11)	0.0176 (11)	0.0003 (9)	0.0020 (9)	0.0028 (9)
C8'	0.0148 (11)	0.0208 (11)	0.0228 (11)	0.0014 (9)	0.0049 (9)	0.0020 (9)
B9'	0.0252 (14)	0.0215 (13)	0.0249 (13)	−0.0027 (11)	0.0074 (11)	−0.0001 (11)
B10'	0.0289 (15)	0.0260 (15)	0.0275 (14)	−0.0052 (12)	0.0112 (12)	−0.0044 (12)
B11'	0.0242 (14)	0.0275 (14)	0.0207 (13)	−0.0035 (11)	0.0083 (11)	−0.0009 (11)
C71'	0.0206 (11)	0.0258 (12)	0.0139 (10)	−0.0024 (10)	0.0047 (9)	0.0024 (9)
C72'	0.0270 (13)	0.0281 (13)	0.0261 (12)	−0.0004 (10)	0.0078 (10)	−0.0004 (10)
C73'	0.0402 (15)	0.0284 (14)	0.0355 (14)	−0.0095 (12)	0.0128 (12)	−0.0048 (11)
C74'	0.0316 (14)	0.0458 (16)	0.0273 (13)	−0.0186 (12)	0.0079 (11)	−0.0087 (12)
C75'	0.0192 (12)	0.0482 (16)	0.0275 (13)	−0.0046 (11)	0.0016 (10)	0.0012 (12)
C76'	0.0230 (12)	0.0302 (13)	0.0250 (12)	−0.0005 (10)	0.0035 (10)	0.0039 (10)
C81'	0.0236 (12)	0.0274 (12)	0.0205 (11)	−0.0074 (10)	0.0070 (9)	0.0016 (10)
C82'	0.0334 (14)	0.0375 (15)	0.0281 (13)	−0.0040 (12)	0.0106 (11)	−0.0023 (11)
C83'	0.0569 (19)	0.0501 (18)	0.0294 (14)	−0.0185 (15)	0.0213 (14)	−0.0136 (13)
C84'	0.0453 (17)	0.0602 (19)	0.0209 (13)	−0.0250 (15)	0.0027 (12)	0.0006 (13)
C85'	0.0320 (14)	0.0567 (19)	0.0277 (14)	−0.0092 (13)	−0.0012 (11)	0.0121 (13)
C86'	0.0299 (13)	0.0384 (14)	0.0244 (12)	0.0001 (11)	0.0044 (10)	0.0062 (11)
S9'	0.0403 (4)	0.0243 (3)	0.0306 (3)	−0.0015 (3)	0.0153 (3)	0.0034 (3)
C91'	0.100 (3)	0.0453 (19)	0.063 (2)	0.0408 (19)	0.046 (2)	0.0247 (16)
C92'	0.083 (3)	0.052 (2)	0.0485 (18)	−0.0427 (19)	0.0142 (17)	0.0028 (15)

Geometric parameters (Å, º)

B1—B2	1.750 (4)	B1'—B2'	1.758 (4)
B1—B3	1.774 (4)	B1'—B3'	1.783 (4)
B1—B4	1.778 (4)	B1'—B4'	1.778 (4)
B1—B5	1.782 (4)	B1'—B5'	1.777 (4)
B1—B6	1.810 (4)	B1'—B6'	1.814 (4)
B1—H1	1.05 (3)	B1'—H1'	1.07 (3)
B2—B3	1.754 (4)	B2'—B3'	1.760 (4)
B2—B6	1.771 (4)	B2'—B6'	1.776 (4)
B2—C7	1.702 (3)	B2'—C7'	1.712 (3)
B2—B11	1.801 (4)	B2'—B11'	1.806 (4)
B2—H2	1.16 (3)	B2'—H2'	1.11 (3)
B3—B4	1.773 (4)	B3'—B4'	1.773 (4)
B3—C7	1.719 (3)	B3'—C7'	1.715 (3)
B3—C8	1.742 (3)	B3'—C8'	1.740 (3)
B3—H3	1.04 (3)	B3'—H3'	1.08 (2)
B4—B5	1.764 (4)	B4'—B5'	1.771 (4)
B4—C8	1.749 (3)	B4'—C8'	1.743 (3)
B4—B9	1.763 (4)	B4'—B9'	1.760 (4)
B4—H4	1.11 (3)	B4'—H4'	1.10 (2)
B5—B6	1.802 (4)	B5'—B6'	1.803 (4)
B5—B9	1.753 (3)	B5'—B9'	1.748 (4)
B5—B10	1.804 (4)	B5'—B10'	1.801 (4)
B5—H5	1.10 (3)	B5'—H5'	1.09 (3)
B6—B10	1.800 (4)	B6'—B10'	1.789 (4)
B6—B11	1.793 (4)	B6'—B11'	1.779 (4)
B6—H6	1.05 (3)	B6'—H6'	1.11 (3)
C7—C8	1.585 (3)	C7'—C8'	1.585 (3)
C7—B11	1.654 (3)	C7'—B11'	1.651 (3)
C7—C71	1.508 (3)	C7'—C71'	1.507 (3)
C8—B9	1.612 (3)	C8'—B9'	1.617 (3)
C8—C81	1.507 (3)	C8'—C81'	1.509 (3)
B9—S9	1.889 (3)	B9'—S9'	1.888 (3)
B9—B10	1.782 (4)	B9'—B10'	1.778 (4)
B10—B11	1.862 (4)	B10'—B11'	1.863 (4)
B10—H10	1.14 (3)	B10'—H10'	1.10 (3)
B10—H10A	1.19 (3)	B10'—H10B	1.17 (3)
B11—H10A	1.35 (3)	B11'—H10B	1.30 (3)
B11—H11	1.11 (3)	B11'—H11'	1.04 (2)
C71—C76	1.388 (4)	C71'—C72'	1.396 (3)
C71—C72	1.392 (3)	C71'—C76'	1.396 (3)
C72—C73	1.392 (4)	C72'—C73'	1.388 (3)
C72—H72	0.9500	C72'—H72'	0.9500
C73—C74	1.381 (5)	C73'—C74'	1.382 (4)
C73—H73	0.9500	C73'—H73'	0.9500
C74—C75	1.370 (4)	C74'—C75'	1.389 (4)
C74—H74	0.9500	C74'—H74'	0.9500
C75—C76	1.390 (4)	C75'—C76'	1.379 (3)
C75—H75	0.9500	C75'—H75'	0.9500
C76—H76	0.9500	C76'—H76'	0.9500
C81—C82	1.391 (3)	C81'—C82'	1.383 (3)
C81—C86	1.397 (3)	C81'—C86'	1.396 (3)
C82—C83	1.383 (3)	C82'—C83'	1.398 (4)
C82—H82	0.9500	C82'—H82'	0.9500
C83—C84	1.393 (3)	C83'—C84'	1.380 (4)
C83—H83	0.9500	C83'—H83'	0.9500
C84—C85	1.378 (3)	C84'—C85'	1.377 (4)
C84—H84	0.9500	C84'—H84'	0.9500
C85—C86	1.384 (3)	C85'—C86'	1.387 (3)
C85—H85	0.9500	C85'—H85'	0.9500
C86—H86	0.9500	C86'—H86'	0.9500
S9—C91	1.796 (3)	S9'—C91'	1.804 (3)
S9—C92	1.792 (3)	S9'—C92'	1.797 (3)
C91—H91A	0.9800	C91'—H91D	0.9800
C91—H91B	0.9800	C91'—H91E	0.9800
C91—H91C	0.9800	C91'—H91F	0.9800
C92—H92A	0.9800	C92'—H92D	0.9800
C92—H92B	0.9800	C92'—H92E	0.9800
C92—H92C	0.9800	C92'—H92F	0.9800
B2—B1—B3	59.69 (16)	B2'—B1'—B5'	108.3 (2)
B2—B1—B4	107.62 (19)	B2'—B1'—B4'	107.77 (18)
B3—B1—B4	59.89 (15)	B5'—B1'—B4'	59.77 (15)
B2—B1—B5	107.8 (2)	B2'—B1'—B3'	59.62 (15)
B3—B1—B5	107.30 (19)	B5'—B1'—B3'	107.49 (18)
B4—B1—B5	59.42 (16)	B4'—B1'—B3'	59.74 (15)
B2—B1—B6	59.66 (17)	B2'—B1'—B6'	59.60 (16)
B3—B1—B6	107.2 (2)	B5'—B1'—B6'	60.29 (16)
B4—B1—B6	107.43 (19)	B4'—B1'—B6'	107.4 (2)
B5—B1—B6	60.22 (16)	B3'—B1'—B6'	106.69 (19)
B2—B1—H1	122.1 (15)	B2'—B1'—H1'	122.0 (14)
B3—B1—H1	120.0 (15)	B5'—B1'—H1'	121.6 (14)
B4—B1—H1	120.4 (15)	B4'—B1'—H1'	121.4 (14)
B5—B1—H1	123.1 (15)	B3'—B1'—H1'	122.0 (14)
B6—B1—H1	124.4 (14)	B6'—B1'—H1'	123.0 (14)
C7—B2—B1	106.11 (19)	C7'—B2'—B1'	105.38 (18)
C7—B2—B3	59.66 (14)	C7'—B2'—B3'	59.18 (14)
B1—B2—B3	60.84 (16)	B1'—B2'—B3'	60.90 (15)
C7—B2—B6	103.82 (19)	C7'—B2'—B6'	102.74 (18)
B1—B2—B6	61.86 (17)	B1'—B2'—B6'	61.77 (16)
B3—B2—B6	109.8 (2)	B3'—B2'—B6'	109.37 (19)
C7—B2—B11	56.29 (14)	C7'—B2'—B11'	55.88 (13)
B1—B2—B11	109.6 (2)	B1'—B2'—B11'	108.78 (19)
B3—B2—B11	107.47 (18)	B3'—B2'—B11'	106.65 (18)
B6—B2—B11	60.26 (16)	B6'—B2'—B11'	59.57 (15)
C7—B2—H2	116.0 (13)	C7'—B2'—H2'	117.4 (13)
B1—B2—H2	128.9 (13)	B1'—B2'—H2'	129.7 (13)
B3—B2—H2	118.6 (13)	B3'—B2'—H2'	121.0 (13)
B6—B2—H2	128.0 (13)	B6'—B2'—H2'	126.4 (13)
B11—B2—H2	117.3 (13)	B11'—B2'—H2'	116.5 (13)
C7—B3—C8	54.49 (13)	C7'—B3'—C8'	54.60 (12)
C7—B3—B2	58.67 (14)	C7'—B3'—B2'	59.02 (14)
C8—B3—B2	101.66 (18)	C8'—B3'—B2'	102.18 (18)
C7—B3—B4	104.52 (19)	C7'—B3'—B4'	104.40 (18)
C8—B3—B4	59.69 (14)	C8'—B3'—B4'	59.47 (14)
B2—B3—B4	107.7 (2)	B2'—B3'—B4'	107.86 (19)
C7—B3—B1	104.30 (19)	C7'—B3'—B1'	104.17 (19)
C8—B3—B1	103.63 (19)	C8'—B3'—B1'	103.32 (18)
B2—B3—B1	59.47 (16)	B2'—B3'—B1'	59.48 (15)
B4—B3—B1	60.17 (16)	B4'—B3'—B1'	59.99 (15)
C7—B3—H3	122.8 (14)	C7'—B3'—H3'	123.0 (13)
C8—B3—H3	122.6 (14)	C8'—B3'—H3'	123.3 (13)
B2—B3—H3	125.4 (14)	B2'—B3'—H3'	124.3 (13)
B4—B3—H3	121.2 (14)	B4'—B3'—H3'	121.6 (13)
B1—B3—H3	126.8 (14)	B1'—B3'—H3'	126.5 (13)
C8—B4—B9	54.64 (13)	C8'—B4'—B9'	54.99 (13)
C8—B4—B5	101.40 (18)	C8'—B4'—B5'	101.52 (18)
B9—B4—B5	59.61 (15)	B9'—B4'—B5'	59.33 (15)
C8—B4—B3	59.26 (14)	C8'—B4'—B3'	59.32 (14)
B9—B4—B3	105.54 (19)	B9'—B4'—B3'	105.78 (18)
B5—B4—B3	108.1 (2)	B5'—B4'—B3'	108.16 (19)
C8—B4—B1	103.16 (19)	C8'—B4'—B1'	103.42 (18)
B9—B4—B1	106.50 (19)	B9'—B4'—B1'	106.21 (19)
B5—B4—B1	60.40 (16)	B5'—B4'—B1'	60.08 (16)
B3—B4—B1	59.94 (16)	B3'—B4'—B1'	60.27 (15)
C8—B4—H4	121.0 (13)	C8'—B4'—H4'	121.5 (13)
B9—B4—H4	121.7 (13)	B9'—B4'—H4'	121.8 (13)
B5—B4—H4	127.7 (13)	B5'—B4'—H4'	127.0 (13)
B3—B4—H4	119.0 (13)	B3'—B4'—H4'	119.4 (13)
B1—B4—H4	127.3 (13)	B1'—B4'—H4'	126.9 (13)
B9—B5—B4	60.17 (15)	B9'—B5'—B4'	60.02 (15)
B9—B5—B1	106.77 (19)	B9'—B5'—B1'	106.79 (19)
B4—B5—B1	60.18 (16)	B4'—B5'—B1'	60.15 (16)
B9—B5—B6	105.04 (19)	B9'—B5'—B10'	60.11 (15)
B4—B5—B6	108.4 (2)	B4'—B5'—B10'	110.86 (18)
B1—B5—B6	60.67 (17)	B1'—B5'—B10'	110.5 (2)
B9—B5—B10	60.11 (15)	B9'—B5'—B6'	104.67 (19)
B4—B5—B10	111.10 (18)	B4'—B5'—B6'	108.14 (19)
B1—B5—B10	110.5 (2)	B1'—B5'—B6'	60.88 (16)
B6—B5—B10	59.87 (16)	B10'—B5'—B6'	59.51 (16)
B9—B5—H5	121.9 (13)	B9'—B5'—H5'	119.8 (13)
B4—B5—H5	120.8 (14)	B4'—B5'—H5'	122.6 (13)
B1—B5—H5	123.1 (13)	B1'—B5'—H5'	126.2 (13)
B6—B5—H5	123.6 (14)	B10'—B5'—H5'	115.1 (14)
B10—B5—H5	118.0 (14)	B6'—B5'—H5'	123.9 (13)
B2—B6—B11	60.68 (16)	B2'—B6'—B11'	61.07 (15)
B2—B6—B10	111.42 (19)	B2'—B6'—B10'	112.37 (19)
B11—B6—B10	62.44 (16)	B11'—B6'—B10'	62.96 (16)
B2—B6—B5	106.0 (2)	B2'—B6'—B5'	106.36 (19)
B11—B6—B5	107.51 (18)	B11'—B6'—B5'	107.96 (19)
B10—B6—B5	60.13 (16)	B10'—B6'—B5'	60.19 (15)
B2—B6—B1	58.48 (17)	B2'—B6'—B1'	58.63 (16)
B11—B6—B1	107.3 (2)	B11'—B6'—B1'	107.49 (19)
B10—B6—B1	109.44 (19)	B10'—B6'—B1'	109.40 (19)
B5—B6—B1	59.12 (16)	B5'—B6'—B1'	58.84 (16)
B2—B6—H6	123.1 (15)	B2'—B6'—H6'	121.3 (14)
B11—B6—H6	126.0 (15)	B11'—B6'—H6'	122.9 (14)
B10—B6—H6	120.0 (14)	B10'—B6'—H6'	119.5 (14)
B5—B6—H6	119.3 (15)	B5'—B6'—H6'	121.8 (14)
B1—B6—H6	118.8 (14)	B1'—B6'—H6'	120.8 (14)
C71—C7—C8	118.83 (18)	C71'—C7'—C8'	120.43 (17)
C71—C7—B11	118.5 (2)	C71'—C7'—B11'	117.81 (18)
C8—C7—B11	109.74 (18)	C8'—C7'—B11'	109.81 (18)
C71—C7—B2	121.96 (19)	C71'—C7'—B2'	119.89 (18)
C8—C7—B2	111.04 (18)	C8'—C7'—B2'	111.31 (17)
B11—C7—B2	64.88 (16)	B11'—C7'—B2'	64.93 (15)
C71—C7—B3	117.82 (19)	C71'—C7'—B3'	117.48 (19)
C8—C7—B3	63.47 (14)	C8'—C7'—B3'	63.49 (14)
B11—C7—B3	116.30 (19)	B11'—C7'—B3'	116.37 (18)
B2—C7—B3	61.67 (15)	B2'—C7'—B3'	61.79 (14)
C81—C8—C7	117.32 (18)	C81'—C8'—C7'	116.92 (18)
C81—C8—B9	119.07 (18)	C81'—C8'—B9'	119.97 (18)
C7—C8—B9	113.77 (18)	C7'—C8'—B9'	113.57 (18)
C81—C8—B3	117.75 (18)	C81'—C8'—B3'	117.02 (18)
C7—C8—B3	62.04 (14)	C7'—C8'—B3'	61.91 (14)
B9—C8—B3	114.14 (18)	B9'—C8'—B3'	114.08 (17)
C81—C8—B4	120.49 (18)	C81'—C8'—B4'	120.47 (18)
C7—C8—B4	111.79 (17)	C7'—C8'—B4'	111.78 (17)
B9—C8—B4	63.13 (15)	B9'—C8'—B4'	63.04 (15)
B3—C8—B4	61.05 (15)	B3'—C8'—B4'	61.22 (14)
C8—B9—B5	107.70 (19)	C8'—B9'—B5'	107.90 (19)
C8—B9—B4	62.24 (15)	C8'—B9'—B4'	61.97 (14)
B5—B9—B4	60.22 (15)	B5'—B9'—B4'	60.65 (15)
C8—B9—B10	108.78 (19)	C8'—B9'—B10'	108.81 (19)
B5—B9—B10	61.36 (16)	B5'—B9'—B10'	61.44 (16)
B4—B9—B10	112.19 (19)	B4'—B9'—B10'	112.49 (19)
C8—B9—S9	116.29 (16)	C8'—B9'—S9'	117.86 (17)
B5—B9—S9	122.92 (17)	B5'—B9'—S9'	122.85 (17)
B4—B9—S9	111.59 (16)	B4'—B9'—S9'	113.86 (17)
B10—B9—S9	127.61 (18)	B10'—B9'—S9'	125.16 (17)
B9—B10—B6	103.93 (19)	B9'—B10'—B6'	104.01 (19)
B9—B10—B5	58.53 (15)	B9'—B10'—B5'	58.45 (15)
B6—B10—B5	59.99 (16)	B6'—B10'—B5'	60.30 (16)
B9—B10—B11	100.20 (18)	B9'—B10'—B11'	100.23 (18)
B6—B10—B11	58.61 (16)	B6'—B10'—B11'	58.27 (15)
B5—B10—B11	104.5 (2)	B5'—B10'—B11'	104.49 (19)
B9—B10—H10	129.9 (13)	B9'—B10'—H10'	127.7 (13)
B6—B10—H10	117.3 (13)	B6'—B10'—H10'	118.9 (13)
B5—B10—H10	119.9 (13)	B5'—B10'—H10'	119.1 (13)
B11—B10—H10	124.7 (13)	B11'—B10'—H10'	126.6 (13)
B9—B10—H10A	85.9 (12)	B9'—B10'—H10B	88.1 (12)
B6—B10—H10A	104.8 (12)	B6'—B10'—H10B	101.9 (13)
B5—B10—H10A	131.4 (13)	B5'—B10'—H10B	131.5 (12)
B11—B10—H10A	46.4 (12)	B11'—B10'—H10B	43.7 (12)
H10—B10—H10A	108.1 (18)	H10'—B10'—H10B	109.1 (18)
C7—B11—B6	104.9 (2)	C7'—B11'—B6'	105.16 (19)
C7—B11—B2	58.84 (15)	C7'—B11'—B2'	59.19 (14)
B6—B11—B2	59.06 (16)	B6'—B11'—B2'	59.36 (15)
C7—B11—B10	107.31 (19)	C7'—B11'—B10'	107.38 (18)
B6—B11—B10	58.95 (16)	B6'—B11'—B10'	58.77 (15)
B2—B11—B10	107.3 (2)	B2'—B11'—B10'	107.61 (18)
C7—B11—H10A	95.5 (11)	C7'—B11'—H10B	97.0 (11)
B6—B11—H10A	98.3 (11)	B6'—B11'—H10B	97.0 (11)
B2—B11—H10A	133.5 (11)	B2'—B11'—H10B	134.3 (11)
B10—B11—H10A	39.5 (11)	B10'—B11'—H10B	38.3 (11)
C7—B11—H11	120.8 (13)	C7'—B11'—H11'	120.2 (14)
B6—B11—H11	121.3 (13)	B6'—B11'—H11'	122.9 (13)
B2—B11—H11	115.5 (13)	B2'—B11'—H11'	116.7 (14)
B10—B11—H11	127.0 (13)	B10'—B11'—H11'	126.5 (14)
H10A—B11—H11	110.9 (17)	H10B—B11'—H11'	108.9 (17)
C76—C71—C72	117.8 (2)	C72'—C71'—C76'	118.3 (2)
C76—C71—C7	118.3 (2)	C72'—C71'—C7'	122.9 (2)
C72—C71—C7	123.9 (2)	C76'—C71'—C7'	118.6 (2)
C73—C72—C71	120.6 (3)	C73'—C72'—C71'	120.4 (2)
C73—C72—H72	119.7	C73'—C72'—H72'	119.8
C71—C72—H72	119.7	C71'—C72'—H72'	119.8
C74—C73—C72	120.7 (3)	C74'—C73'—C72'	120.6 (2)
C74—C73—H73	119.6	C74'—C73'—H73'	119.7
C72—C73—H73	119.6	C72'—C73'—H73'	119.7
C75—C74—C73	119.2 (3)	C73'—C74'—C75'	119.4 (2)
C75—C74—H74	120.4	C73'—C74'—H74'	120.3
C73—C74—H74	120.4	C75'—C74'—H74'	120.3
C74—C75—C76	120.4 (3)	C76'—C75'—C74'	120.2 (2)
C74—C75—H75	119.8	C76'—C75'—H75'	119.9
C76—C75—H75	119.8	C74'—C75'—H75'	119.9
C71—C76—C75	121.3 (3)	C75'—C76'—C71'	121.0 (2)
C71—C76—H76	119.3	C75'—C76'—H76'	119.5
C75—C76—H76	119.3	C71'—C76'—H76'	119.5
C82—C81—C86	118.2 (2)	C82'—C81'—C86'	118.7 (2)
C82—C81—C8	123.2 (2)	C82'—C81'—C8'	123.1 (2)
C86—C81—C8	118.65 (19)	C86'—C81'—C8'	118.1 (2)
C83—C82—C81	120.6 (2)	C81'—C82'—C83'	120.3 (3)
C83—C82—H82	119.7	C81'—C82'—H82'	119.8
C81—C82—H82	119.7	C83'—C82'—H82'	119.8
C82—C83—C84	120.5 (2)	C84'—C83'—C82'	120.2 (3)
C82—C83—H83	119.8	C84'—C83'—H83'	119.9
C84—C83—H83	119.8	C82'—C83'—H83'	119.9
C85—C84—C83	119.5 (2)	C85'—C84'—C83'	120.0 (2)
C85—C84—H84	120.2	C85'—C84'—H84'	120.0
C83—C84—H84	120.2	C83'—C84'—H84'	120.0
C84—C85—C86	119.9 (2)	C84'—C85'—C86'	119.9 (3)
C84—C85—H85	120.0	C84'—C85'—H85'	120.1
C86—C85—H85	120.0	C86'—C85'—H85'	120.1
C85—C86—C81	121.3 (2)	C85'—C86'—C81'	120.9 (3)
C85—C86—H86	119.3	C85'—C86'—H86'	119.6
C81—C86—H86	119.3	C81'—C86'—H86'	119.6
C92—S9—C91	99.89 (13)	C92'—S9'—C91'	100.89 (19)
C92—S9—B9	103.29 (12)	C92'—S9'—B9'	104.49 (13)
C91—S9—B9	105.16 (12)	C91'—S9'—B9'	104.08 (13)
S9—C91—H91A	109.5	S9'—C91'—H91D	109.5
S9—C91—H91B	109.5	S9'—C91'—H91E	109.5
H91A—C91—H91B	109.5	H91D—C91'—H91E	109.5
S9—C91—H91C	109.5	S9'—C91'—H91F	109.5
H91A—C91—H91C	109.5	H91D—C91'—H91F	109.5
H91B—C91—H91C	109.5	H91E—C91'—H91F	109.5
S9—C92—H92A	109.5	S9'—C92'—H92D	109.5
S9—C92—H92B	109.5	S9'—C92'—H92E	109.5
H92A—C92—H92B	109.5	H92D—C92'—H92E	109.5
S9—C92—H92C	109.5	S9'—C92'—H92F	109.5
H92A—C92—H92C	109.5	H92D—C92'—H92F	109.5
H92B—C92—H92C	109.5	H92E—C92'—H92F	109.5
B3—B1—B2—C7	40.26 (18)	B5'—B1'—B2'—C7'	59.5 (2)
B4—B1—B2—C7	2.9 (3)	B4'—B1'—B2'—C7'	−3.7 (3)
B5—B1—B2—C7	−59.8 (2)	B3'—B1'—B2'—C7'	−40.44 (17)
B6—B1—B2—C7	−97.3 (2)	B6'—B1'—B2'—C7'	96.43 (19)
B4—B1—B2—B3	−37.31 (19)	B5'—B1'—B2'—B3'	100.0 (2)
B5—B1—B2—B3	−100.0 (2)	B4'—B1'—B2'—B3'	36.75 (18)
B6—B1—B2—B3	−137.58 (19)	B6'—B1'—B2'—B3'	136.87 (19)
B3—B1—B2—B6	137.58 (19)	B5'—B1'—B2'—B6'	−36.91 (18)
B4—B1—B2—B6	100.3 (2)	B4'—B1'—B2'—B6'	−100.1 (2)
B5—B1—B2—B6	37.56 (18)	B3'—B1'—B2'—B6'	−136.87 (19)
B3—B1—B2—B11	99.6 (2)	B5'—B1'—B2'—B11'	0.9 (2)
B4—B1—B2—B11	62.3 (3)	B4'—B1'—B2'—B11'	−62.3 (2)
B5—B1—B2—B11	−0.5 (3)	B3'—B1'—B2'—B11'	−99.03 (19)
B6—B1—B2—B11	−38.02 (18)	B6'—B1'—B2'—B11'	37.83 (18)
B1—B2—B3—C7	134.0 (2)	B1'—B2'—B3'—C7'	−133.27 (19)
B6—B2—B3—C7	94.8 (2)	B6'—B2'—B3'—C7'	−93.6 (2)
B11—B2—B3—C7	30.85 (18)	B11'—B2'—B3'—C7'	−30.67 (16)
C7—B2—B3—C8	−34.92 (16)	C7'—B2'—B3'—C8'	34.84 (15)
B1—B2—B3—C8	99.1 (2)	B1'—B2'—B3'—C8'	−98.42 (19)
B6—B2—B3—C8	59.9 (2)	B6'—B2'—B3'—C8'	−58.7 (2)
B11—B2—B3—C8	−4.1 (2)	B11'—B2'—B3'—C8'	4.2 (2)
C7—B2—B3—B4	−96.6 (2)	C7'—B2'—B3'—B4'	96.39 (19)
B1—B2—B3—B4	37.44 (19)	B1'—B2'—B3'—B4'	−36.88 (18)
B6—B2—B3—B4	−1.8 (3)	B6'—B2'—B3'—B4'	2.8 (2)
B11—B2—B3—B4	−65.7 (2)	B11'—B2'—B3'—B4'	65.7 (2)
C7—B2—B3—B1	−134.0 (2)	C7'—B2'—B3'—B1'	133.27 (19)
B6—B2—B3—B1	−39.21 (19)	B6'—B2'—B3'—B1'	39.68 (19)
B11—B2—B3—B1	−103.1 (2)	B11'—B2'—B3'—B1'	102.6 (2)
B2—B1—B3—C7	−39.35 (17)	B2'—B1'—B3'—C7'	40.08 (17)
B4—B1—B3—C7	98.75 (19)	B5'—B1'—B3'—C7'	−61.3 (2)
B5—B1—B3—C7	61.6 (2)	B4'—B1'—B3'—C7'	−98.64 (19)
B6—B1—B3—C7	−1.8 (2)	B6'—B1'—B3'—C7'	2.1 (2)
B2—B1—B3—C8	−95.64 (19)	B2'—B1'—B3'—C8'	96.43 (18)
B4—B1—B3—C8	42.46 (17)	B5'—B1'—B3'—C8'	−4.9 (2)
B5—B1—B3—C8	5.3 (2)	B4'—B1'—B3'—C8'	−42.30 (16)
B6—B1—B3—C8	−58.1 (2)	B6'—B1'—B3'—C8'	58.4 (2)
B4—B1—B3—B2	138.1 (2)	B5'—B1'—B3'—B2'	−101.4 (2)
B5—B1—B3—B2	100.9 (2)	B4'—B1'—B3'—B2'	−138.7 (2)
B6—B1—B3—B2	37.54 (18)	B6'—B1'—B3'—B2'	−38.00 (18)
B2—B1—B3—B4	−138.1 (2)	B2'—B1'—B3'—B4'	138.7 (2)
B5—B1—B3—B4	−37.20 (19)	B5'—B1'—B3'—B4'	37.35 (18)
B6—B1—B3—B4	−100.6 (2)	B6'—B1'—B3'—B4'	100.7 (2)
C7—B3—B4—C8	32.18 (16)	C7'—B3'—B4'—C8'	−32.25 (15)
B2—B3—B4—C8	93.41 (19)	B2'—B3'—B4'—C8'	−93.86 (19)
B1—B3—B4—C8	130.54 (19)	B1'—B3'—B4'—C8'	−130.51 (19)
C7—B3—B4—B9	2.0 (2)	C7'—B3'—B4'—B9'	−1.7 (2)
C8—B3—B4—B9	−30.19 (16)	C8'—B3'—B4'—B9'	30.57 (16)
B2—B3—B4—B9	63.2 (2)	B2'—B3'—B4'—B9'	−63.3 (2)
B1—B3—B4—B9	100.4 (2)	B1'—B3'—B4'—B9'	−99.9 (2)
C7—B3—B4—B5	−60.5 (2)	C7'—B3'—B4'—B5'	60.6 (2)
C8—B3—B4—B5	−92.71 (19)	C8'—B3'—B4'—B5'	92.86 (19)
B2—B3—B4—B5	0.7 (2)	B2'—B3'—B4'—B5'	−1.0 (2)
B1—B3—B4—B5	37.83 (18)	B1'—B3'—B4'—B5'	−37.66 (18)
C7—B3—B4—B1	−98.4 (2)	C7'—B3'—B4'—B1'	98.26 (19)
C8—B3—B4—B1	−130.54 (19)	C8'—B3'—B4'—B1'	130.51 (19)
B2—B3—B4—B1	−37.13 (18)	B2'—B3'—B4'—B1'	36.66 (18)
B2—B1—B4—C8	−4.9 (3)	B2'—B1'—B4'—C8'	5.5 (2)
B3—B1—B4—C8	−42.13 (17)	B5'—B1'—B4'—C8'	−95.72 (19)
B5—B1—B4—C8	95.77 (19)	B3'—B1'—B4'—C8'	42.23 (16)
B6—B1—B4—C8	58.0 (2)	B6'—B1'—B4'—C8'	−57.3 (2)
B2—B1—B4—B9	−61.5 (2)	B2'—B1'—B4'—B9'	62.5 (2)
B3—B1—B4—B9	−98.7 (2)	B5'—B1'—B4'—B9'	−38.74 (17)
B5—B1—B4—B9	39.19 (18)	B3'—B1'—B4'—B9'	99.21 (19)
B6—B1—B4—B9	1.4 (3)	B6'—B1'—B4'—B9'	−0.3 (2)
B2—B1—B4—B5	−100.7 (2)	B2'—B1'—B4'—B5'	101.3 (2)
B3—B1—B4—B5	−137.9 (2)	B3'—B1'—B4'—B5'	138.0 (2)
B6—B1—B4—B5	−37.79 (19)	B6'—B1'—B4'—B5'	38.41 (18)
B2—B1—B4—B3	37.22 (19)	B2'—B1'—B4'—B3'	−36.70 (18)
B5—B1—B4—B3	137.9 (2)	B5'—B1'—B4'—B3'	−138.0 (2)
B6—B1—B4—B3	100.1 (2)	B6'—B1'—B4'—B3'	−99.5 (2)
C8—B4—B5—B9	36.62 (16)	C8'—B4'—B5'—B9'	−36.71 (16)
B3—B4—B5—B9	97.8 (2)	B3'—B4'—B5'—B9'	−97.95 (19)
B1—B4—B5—B9	135.4 (2)	B1'—B4'—B5'—B9'	−135.7 (2)
C8—B4—B5—B1	−98.77 (19)	C8'—B4'—B5'—B1'	98.97 (19)
B9—B4—B5—B1	−135.4 (2)	B9'—B4'—B5'—B1'	135.7 (2)
B3—B4—B5—B1	−37.63 (18)	B3'—B4'—B5'—B1'	37.74 (18)
C8—B4—B5—B6	−60.5 (2)	C8'—B4'—B5'—B10'	−3.4 (2)
B9—B4—B5—B6	−97.2 (2)	B9'—B4'—B5'—B10'	33.33 (18)
B3—B4—B5—B6	0.6 (2)	B3'—B4'—B5'—B10'	−64.6 (2)
B1—B4—B5—B6	38.23 (18)	B1'—B4'—B5'—B10'	−102.4 (2)
C8—B4—B5—B10	3.4 (2)	C8'—B4'—B5'—B6'	60.1 (2)
B9—B4—B5—B10	−33.18 (19)	B9'—B4'—B5'—B6'	96.8 (2)
B3—B4—B5—B10	64.6 (2)	B3'—B4'—B5'—B6'	−1.1 (2)
B1—B4—B5—B10	102.2 (2)	B1'—B4'—B5'—B6'	−38.88 (18)
B2—B1—B5—B9	60.8 (2)	B2'—B1'—B5'—B9'	−61.1 (2)
B3—B1—B5—B9	−2.1 (3)	B4'—B1'—B5'—B9'	39.20 (18)
B4—B1—B5—B9	−39.52 (18)	B3'—B1'—B5'—B9'	1.9 (3)
B6—B1—B5—B9	98.1 (2)	B6'—B1'—B5'—B9'	−97.7 (2)
B2—B1—B5—B4	100.3 (2)	B2'—B1'—B5'—B4'	−100.3 (2)
B3—B1—B5—B4	37.41 (19)	B3'—B1'—B5'—B4'	−37.34 (18)
B6—B1—B5—B4	137.7 (2)	B6'—B1'—B5'—B4'	−136.94 (19)
B2—B1—B5—B6	−37.32 (18)	B2'—B1'—B5'—B10'	2.6 (3)
B3—B1—B5—B6	−100.2 (2)	B4'—B1'—B5'—B10'	102.9 (2)
B4—B1—B5—B6	−137.7 (2)	B3'—B1'—B5'—B10'	65.6 (2)
B2—B1—B5—B10	−2.9 (3)	B6'—B1'—B5'—B10'	−34.03 (18)
B3—B1—B5—B10	−65.8 (2)	B2'—B1'—B5'—B6'	36.62 (18)
B4—B1—B5—B10	−103.2 (2)	B4'—B1'—B5'—B6'	136.94 (19)
B6—B1—B5—B10	34.43 (18)	B3'—B1'—B5'—B6'	99.6 (2)
C7—B2—B6—B11	−36.98 (17)	C7'—B2'—B6'—B11'	36.88 (16)
B1—B2—B6—B11	−138.1 (2)	B1'—B2'—B6'—B11'	137.66 (19)
B3—B2—B6—B11	−99.3 (2)	B3'—B2'—B6'—B11'	98.37 (19)
C7—B2—B6—B10	0.8 (3)	C7'—B2'—B6'—B10'	−1.0 (2)
B1—B2—B6—B10	−100.3 (2)	B1'—B2'—B6'—B10'	99.8 (2)
B3—B2—B6—B10	−61.5 (3)	B3'—B2'—B6'—B10'	60.5 (2)
B11—B2—B6—B10	37.8 (2)	B11'—B2'—B6'—B10'	−37.89 (19)
C7—B2—B6—B5	64.4 (2)	C7'—B2'—B6'—B5'	−64.9 (2)
B1—B2—B6—B5	−36.66 (18)	B1'—B2'—B6'—B5'	35.84 (18)
B3—B2—B6—B5	2.1 (2)	B3'—B2'—B6'—B5'	−3.5 (2)
B11—B2—B6—B5	101.4 (2)	B11'—B2'—B6'—B5'	−101.8 (2)
C7—B2—B6—B1	101.1 (2)	C7'—B2'—B6'—B1'	−100.79 (19)
B3—B2—B6—B1	38.76 (18)	B3'—B2'—B6'—B1'	−39.29 (18)
B11—B2—B6—B1	138.1 (2)	B11'—B2'—B6'—B1'	−137.66 (19)
B9—B5—B6—B2	−64.7 (2)	B9'—B5'—B6'—B2'	65.6 (2)
B4—B5—B6—B2	−1.6 (2)	B4'—B5'—B6'—B2'	2.8 (2)
B1—B5—B6—B2	36.37 (18)	B1'—B5'—B6'—B2'	−35.75 (18)
B10—B5—B6—B2	−105.9 (2)	B10'—B5'—B6'—B2'	106.8 (2)
B9—B5—B6—B11	−1.0 (3)	B9'—B5'—B6'—B11'	1.3 (3)
B4—B5—B6—B11	62.0 (2)	B4'—B5'—B6'—B11'	−61.4 (2)
B1—B5—B6—B11	100.0 (2)	B1'—B5'—B6'—B11'	−100.0 (2)
B10—B5—B6—B11	−42.21 (19)	B10'—B5'—B6'—B11'	42.57 (19)
B9—B5—B6—B10	41.19 (18)	B9'—B5'—B6'—B10'	−41.24 (18)
B4—B5—B6—B10	104.2 (2)	B4'—B5'—B6'—B10'	−104.0 (2)
B1—B5—B6—B10	142.2 (2)	B1'—B5'—B6'—B10'	−142.54 (19)
B9—B5—B6—B1	−101.1 (2)	B9'—B5'—B6'—B1'	101.3 (2)
B4—B5—B6—B1	−38.02 (18)	B4'—B5'—B6'—B1'	38.55 (18)
B10—B5—B6—B1	−142.2 (2)	B10'—B5'—B6'—B1'	142.54 (19)
B3—B1—B6—B2	−37.55 (18)	B5'—B1'—B6'—B2'	138.97 (19)
B4—B1—B6—B2	−100.6 (2)	B4'—B1'—B6'—B2'	100.8 (2)
B5—B1—B6—B2	−138.03 (19)	B3'—B1'—B6'—B2'	38.01 (17)
B2—B1—B6—B11	37.60 (18)	B2'—B1'—B6'—B11'	−38.17 (18)
B3—B1—B6—B11	0.0 (3)	B5'—B1'—B6'—B11'	100.8 (2)
B4—B1—B6—B11	−63.0 (3)	B4'—B1'—B6'—B11'	62.6 (2)
B5—B1—B6—B11	−100.4 (2)	B3'—B1'—B6'—B11'	−0.2 (3)
B2—B1—B6—B10	103.8 (2)	B2'—B1'—B6'—B10'	−104.9 (2)
B3—B1—B6—B10	66.2 (3)	B5'—B1'—B6'—B10'	34.02 (18)
B4—B1—B6—B10	3.2 (3)	B4'—B1'—B6'—B10'	−4.2 (3)
B5—B1—B6—B10	−34.27 (19)	B3'—B1'—B6'—B10'	−66.9 (2)
B2—B1—B6—B5	138.03 (19)	B2'—B1'—B6'—B5'	−138.97 (19)
B3—B1—B6—B5	100.5 (2)	B4'—B1'—B6'—B5'	−38.18 (18)
B4—B1—B6—B5	37.43 (18)	B3'—B1'—B6'—B5'	−101.0 (2)
B1—B2—C7—C71	−147.6 (2)	B1'—B2'—C7'—C71'	148.5 (2)
B3—B2—C7—C71	−106.8 (2)	B3'—B2'—C7'—C71'	107.2 (2)
B6—B2—C7—C71	148.1 (2)	B6'—B2'—C7'—C71'	−147.7 (2)
B11—B2—C7—C71	109.2 (2)	B11'—B2'—C7'—C71'	−109.0 (2)
B1—B2—C7—C8	0.5 (3)	B1'—B2'—C7'—C8'	0.1 (2)
B3—B2—C7—C8	41.32 (18)	B3'—B2'—C7'—C8'	−41.16 (18)
B6—B2—C7—C8	−63.8 (2)	B6'—B2'—C7'—C8'	64.0 (2)
B11—B2—C7—C8	−102.7 (2)	B11'—B2'—C7'—C8'	102.7 (2)
B1—B2—C7—B11	103.1 (2)	B1'—B2'—C7'—B11'	−102.5 (2)
B3—B2—C7—B11	144.0 (2)	B3'—B2'—C7'—B11'	−143.82 (19)
B6—B2—C7—B11	38.90 (18)	B6'—B2'—C7'—B11'	−38.69 (17)
B1—B2—C7—B3	−40.83 (19)	B1'—B2'—C7'—B3'	41.29 (18)
B6—B2—C7—B3	−105.1 (2)	B6'—B2'—C7'—B3'	105.1 (2)
B11—B2—C7—B3	−144.0 (2)	B11'—B2'—C7'—B3'	143.82 (19)
C8—B3—C7—C71	−110.2 (2)	C8'—B3'—C7'—C71'	112.2 (2)
B2—B3—C7—C71	113.3 (2)	B2'—B3'—C7'—C71'	−111.0 (2)
B4—B3—C7—C71	−144.6 (2)	B4'—B3'—C7'—C71'	146.57 (18)
B1—B3—C7—C71	153.0 (2)	B1'—B3'—C7'—C71'	−151.32 (19)
B2—B3—C7—C8	−136.5 (2)	B2'—B3'—C7'—C8'	136.75 (19)
B4—B3—C7—C8	−34.39 (17)	B4'—B3'—C7'—C8'	34.33 (16)
B1—B3—C7—C8	−96.72 (19)	B1'—B3'—C7'—C8'	96.44 (19)
C8—B3—C7—B11	100.0 (2)	C8'—B3'—C7'—B11'	−100.1 (2)
B2—B3—C7—B11	−36.4 (2)	B2'—B3'—C7'—B11'	36.64 (19)
B4—B3—C7—B11	65.6 (2)	B4'—B3'—C7'—B11'	−65.8 (2)
B1—B3—C7—B11	3.3 (3)	B1'—B3'—C7'—B11'	−3.7 (2)
C8—B3—C7—B2	136.5 (2)	C8'—B3'—C7'—B2'	−136.75 (19)
B4—B3—C7—B2	102.1 (2)	B4'—B3'—C7'—B2'	−102.4 (2)
B1—B3—C7—B2	39.75 (18)	B1'—B3'—C7'—B2'	−40.31 (17)
C71—C7—C8—C81	0.1 (3)	C71'—C7'—C8'—C81'	0.1 (3)
B11—C7—C8—C81	141.1 (2)	B11'—C7'—C8'—C81'	−141.80 (19)
B2—C7—C8—C81	−149.11 (19)	B2'—C7'—C8'—C81'	148.25 (19)
B3—C7—C8—C81	−108.6 (2)	B3'—C7'—C8'—C81'	107.8 (2)
C71—C7—C8—B9	−145.5 (2)	C71'—C7'—C8'—B9'	146.5 (2)
B11—C7—C8—B9	−4.5 (2)	B11'—C7'—C8'—B9'	4.6 (2)
B2—C7—C8—B9	65.3 (2)	B2'—C7'—C8'—B9'	−65.4 (2)
B3—C7—C8—B9	105.8 (2)	B3'—C7'—C8'—B9'	−105.8 (2)
C71—C7—C8—B3	108.7 (2)	C71'—C7'—C8'—B3'	−107.8 (2)
B11—C7—C8—B3	−110.3 (2)	B11'—C7'—C8'—B3'	110.35 (19)
B2—C7—C8—B3	−40.51 (18)	B2'—C7'—C8'—B3'	40.40 (18)
C71—C7—C8—B4	145.3 (2)	C71'—C7'—C8'—B4'	−144.5 (2)
B11—C7—C8—B4	−73.7 (2)	B11'—C7'—C8'—B4'	73.6 (2)
B2—C7—C8—B4	−3.9 (2)	B2'—C7'—C8'—B4'	3.6 (2)
B3—C7—C8—B4	36.64 (18)	B3'—C7'—C8'—B4'	−36.76 (17)
C7—B3—C8—C81	107.9 (2)	C7'—B3'—C8'—C81'	−107.7 (2)
B2—B3—C8—C81	144.9 (2)	B2'—B3'—C8'—C81'	−144.62 (19)
B4—B3—C8—C81	−111.4 (2)	B4'—B3'—C8'—C81'	111.7 (2)
B1—B3—C8—C81	−154.1 (2)	B1'—B3'—C8'—C81'	154.24 (19)
B2—B3—C8—C7	36.92 (17)	B2'—B3'—C8'—C7'	−36.94 (16)
B4—B3—C8—C7	140.7 (2)	B4'—B3'—C8'—C7'	−140.64 (18)
B1—B3—C8—C7	97.99 (19)	B1'—B3'—C8'—C7'	−98.07 (19)
C7—B3—C8—B9	−105.2 (2)	C7'—B3'—C8'—B9'	104.9 (2)
B2—B3—C8—B9	−68.3 (2)	B2'—B3'—C8'—B9'	68.0 (2)
B4—B3—C8—B9	35.51 (19)	B4'—B3'—C8'—B9'	−35.70 (19)
B1—B3—C8—B9	−7.2 (2)	B1'—B3'—C8'—B9'	6.9 (2)
C7—B3—C8—B4	−140.70 (19)	C7'—B3'—C8'—B4'	140.64 (18)
B2—B3—C8—B4	−103.8 (2)	B2'—B3'—C8'—B4'	103.71 (19)
B1—B3—C8—B4	−42.71 (17)	B1'—B3'—C8'—B4'	42.57 (17)
B9—B4—C8—C81	−109.5 (2)	B9'—B4'—C8'—C81'	110.5 (2)
B5—B4—C8—C81	−148.6 (2)	B5'—B4'—C8'—C81'	149.4 (2)
B3—B4—C8—C81	107.0 (2)	B3'—B4'—C8'—C81'	−106.2 (2)
B1—B4—C8—C81	149.4 (2)	B1'—B4'—C8'—C81'	−148.9 (2)
B9—B4—C8—C7	106.5 (2)	B9'—B4'—C8'—C7'	−106.3 (2)
B5—B4—C8—C7	67.4 (2)	B5'—B4'—C8'—C7'	−67.4 (2)
B3—B4—C8—C7	−37.05 (18)	B3'—B4'—C8'—C7'	37.05 (18)
B1—B4—C8—C7	5.4 (2)	B1'—B4'—C8'—C7'	−5.7 (2)
B5—B4—C8—B9	−39.12 (17)	B5'—B4'—C8'—B9'	38.89 (17)
B3—B4—C8—B9	−143.5 (2)	B3'—B4'—C8'—B9'	143.30 (19)
B1—B4—C8—B9	−101.1 (2)	B1'—B4'—C8'—B9'	100.6 (2)
B9—B4—C8—B3	143.5 (2)	B9'—B4'—C8'—B3'	−143.30 (19)
B5—B4—C8—B3	104.4 (2)	B5'—B4'—C8'—B3'	−104.4 (2)
B1—B4—C8—B3	42.49 (18)	B1'—B4'—C8'—B3'	−42.74 (17)
C81—C8—B9—B5	152.4 (2)	C81'—C8'—B9'—B5'	−152.2 (2)
C7—C8—B9—B5	−62.6 (2)	C7'—C8'—B9'—B5'	62.5 (2)
B3—C8—B9—B5	6.1 (2)	B3'—C8'—B9'—B5'	−5.9 (3)
B4—C8—B9—B5	40.78 (18)	B4'—C8'—B9'—B5'	−40.93 (18)
C81—C8—B9—B4	111.7 (2)	C81'—C8'—B9'—B4'	−111.3 (2)
C7—C8—B9—B4	−103.39 (19)	C7'—C8'—B9'—B4'	103.44 (19)
B3—C8—B9—B4	−34.73 (19)	B3'—C8'—B9'—B4'	35.01 (18)
C81—C8—B9—B10	−142.6 (2)	C81'—C8'—B9'—B10'	142.6 (2)
C7—C8—B9—B10	2.4 (2)	C7'—C8'—B9'—B10'	−2.6 (2)
B3—C8—B9—B10	71.0 (2)	B3'—C8'—B9'—B10'	−71.0 (2)
B4—C8—B9—B10	105.8 (2)	B4'—C8'—B9'—B10'	−106.1 (2)
C81—C8—B9—S9	9.9 (3)	C81'—C8'—B9'—S9'	−7.6 (3)
C7—C8—B9—S9	154.85 (16)	C7'—C8'—B9'—S9'	−152.85 (16)
B3—C8—B9—S9	−136.49 (17)	B3'—C8'—B9'—S9'	138.72 (17)
B4—C8—B9—S9	−101.76 (19)	B4'—C8'—B9'—S9'	103.7 (2)
B4—B5—B9—C8	−41.76 (18)	B4'—B5'—B9'—C8'	41.56 (18)
B1—B5—B9—C8	−2.2 (3)	B1'—B5'—B9'—C8'	2.3 (3)
B6—B5—B9—C8	61.1 (2)	B10'—B5'—B9'—C8'	−102.1 (2)
B10—B5—B9—C8	102.2 (2)	B6'—B5'—B9'—C8'	−61.2 (2)
B1—B5—B9—B4	39.52 (19)	B1'—B5'—B9'—B4'	−39.26 (18)
B6—B5—B9—B4	102.9 (2)	B10'—B5'—B9'—B4'	−143.7 (2)
B10—B5—B9—B4	143.9 (2)	B6'—B5'—B9'—B4'	−102.7 (2)
B4—B5—B9—B10	−143.9 (2)	B4'—B5'—B9'—B10'	143.7 (2)
B1—B5—B9—B10	−104.4 (2)	B1'—B5'—B9'—B10'	104.4 (2)
B6—B5—B9—B10	−41.07 (18)	B6'—B5'—B9'—B10'	40.94 (18)
B4—B5—B9—S9	97.7 (2)	B4'—B5'—B9'—S9'	−100.9 (2)
B1—B5—B9—S9	137.26 (19)	B1'—B5'—B9'—S9'	−140.18 (19)
B6—B5—B9—S9	−159.41 (18)	B10'—B5'—B9'—S9'	115.4 (2)
B10—B5—B9—S9	−118.3 (2)	B6'—B5'—B9'—S9'	156.34 (18)
B5—B4—B9—C8	134.19 (19)	B5'—B4'—B9'—C8'	−134.34 (19)
B3—B4—B9—C8	32.01 (17)	B3'—B4'—B9'—C8'	−32.28 (17)
B1—B4—B9—C8	94.6 (2)	B1'—B4'—B9'—C8'	−95.25 (19)
C8—B4—B9—B5	−134.19 (19)	C8'—B4'—B9'—B5'	134.34 (19)
B3—B4—B9—B5	−102.2 (2)	B3'—B4'—B9'—B5'	102.1 (2)
B1—B4—B9—B5	−39.56 (19)	B1'—B4'—B9'—B5'	39.09 (18)
C8—B4—B9—B10	−100.3 (2)	C8'—B4'—B9'—B10'	100.1 (2)
B5—B4—B9—B10	33.93 (19)	B5'—B4'—B9'—B10'	−34.27 (19)
B3—B4—B9—B10	−68.3 (2)	B3'—B4'—B9'—B10'	67.8 (2)
B1—B4—B9—B10	−5.6 (3)	B1'—B4'—B9'—B10'	4.8 (3)
C8—B4—B9—S9	109.26 (18)	C8'—B4'—B9'—S9'	−110.08 (18)
B5—B4—B9—S9	−116.54 (19)	B5'—B4'—B9'—S9'	115.58 (19)
B3—B4—B9—S9	141.27 (17)	B3'—B4'—B9'—S9'	−142.36 (16)
B1—B4—B9—S9	−156.10 (17)	B1'—B4'—B9'—S9'	154.67 (16)
C8—B9—B10—B6	−59.5 (2)	C8'—B9'—B10'—B6'	59.4 (2)
B5—B9—B10—B6	40.89 (18)	B5'—B9'—B10'—B6'	−41.19 (18)
B4—B9—B10—B6	7.4 (3)	B4'—B9'—B10'—B6'	−7.2 (2)
S9—B9—B10—B6	152.04 (18)	S9'—B9'—B10'—B6'	−153.04 (18)
C8—B9—B10—B5	−100.4 (2)	C8'—B9'—B10'—B5'	100.6 (2)
B4—B9—B10—B5	−33.50 (19)	B4'—B9'—B10'—B5'	33.97 (19)
S9—B9—B10—B5	111.2 (2)	S9'—B9'—B10'—B5'	−111.8 (2)
C8—B9—B10—B11	0.5 (2)	C8'—B9'—B10'—B11'	−0.2 (2)
B5—B9—B10—B11	100.8 (2)	B5'—B9'—B10'—B11'	−100.81 (19)
B4—B9—B10—B11	67.3 (2)	B4'—B9'—B10'—B11'	−66.8 (2)
S9—B9—B10—B11	−147.99 (18)	S9'—B9'—B10'—B11'	147.35 (18)
B2—B6—B10—B9	56.5 (3)	B2'—B6'—B10'—B9'	−56.4 (2)
B11—B6—B10—B9	93.6 (2)	B11'—B6'—B10'—B9'	−93.49 (19)
B5—B6—B10—B9	−40.14 (17)	B5'—B6'—B10'—B9'	40.25 (17)
B1—B6—B10—B9	−6.3 (3)	B1'—B6'—B10'—B9'	6.8 (2)
B2—B6—B10—B5	96.7 (2)	B2'—B6'—B10'—B5'	−96.6 (2)
B11—B6—B10—B5	133.7 (2)	B11'—B6'—B10'—B5'	−133.74 (19)
B1—B6—B10—B5	33.87 (19)	B1'—B6'—B10'—B5'	−33.49 (18)
B2—B6—B10—B11	−37.05 (19)	B2'—B6'—B10'—B11'	37.12 (18)
B5—B6—B10—B11	−133.7 (2)	B5'—B6'—B10'—B11'	133.74 (19)
B1—B6—B10—B11	−99.9 (2)	B1'—B6'—B10'—B11'	100.3 (2)
B4—B5—B10—B9	33.20 (19)	B4'—B5'—B10'—B9'	−33.30 (18)
B1—B5—B10—B9	98.1 (2)	B1'—B5'—B10'—B9'	−98.1 (2)
B6—B5—B10—B9	132.8 (2)	B6'—B5'—B10'—B9'	−132.6 (2)
B9—B5—B10—B6	−132.8 (2)	B9'—B5'—B10'—B6'	132.6 (2)
B4—B5—B10—B6	−99.6 (2)	B4'—B5'—B10'—B6'	99.3 (2)
B1—B5—B10—B6	−34.74 (19)	B1'—B5'—B10'—B6'	34.56 (18)
B9—B5—B10—B11	−93.22 (19)	B9'—B5'—B10'—B11'	93.24 (19)
B4—B5—B10—B11	−60.0 (2)	B4'—B5'—B10'—B11'	59.9 (2)
B1—B5—B10—B11	4.8 (2)	B1'—B5'—B10'—B11'	−4.8 (2)
B6—B5—B10—B11	39.59 (17)	B6'—B5'—B10'—B11'	−39.40 (17)
C71—C7—B11—B6	−152.8 (2)	C71'—C7'—B11'—B6'	151.12 (19)
C8—C7—B11—B6	66.1 (2)	C8'—C7'—B11'—B6'	−65.9 (2)
B2—C7—B11—B6	−38.55 (18)	B2'—C7'—B11'—B6'	39.07 (17)
B3—C7—B11—B6	−3.3 (3)	B3'—C7'—B11'—B6'	3.6 (3)
C71—C7—B11—B2	−114.2 (2)	C71'—C7'—B11'—B2'	112.0 (2)
C8—C7—B11—B2	104.7 (2)	C8'—C7'—B11'—B2'	−104.95 (19)
B3—C7—B11—B2	35.27 (19)	B3'—C7'—B11'—B2'	−35.49 (18)
C71—C7—B11—B10	145.7 (2)	C71'—C7'—B11'—B10'	−147.44 (19)
C8—C7—B11—B10	4.5 (2)	C8'—C7'—B11'—B10'	−4.4 (2)
B2—C7—B11—B10	−100.1 (2)	B2'—C7'—B11'—B10'	100.52 (19)
B3—C7—B11—B10	−64.8 (2)	B3'—C7'—B11'—B10'	65.0 (2)
B2—B6—B11—C7	38.44 (17)	B2'—B6'—B11'—C7'	−38.99 (17)
B10—B6—B11—C7	−101.5 (2)	B10'—B6'—B11'—C7'	101.40 (19)
B5—B6—B11—C7	−60.4 (2)	B5'—B6'—B11'—C7'	60.2 (2)
B1—B6—B11—C7	1.8 (2)	B1'—B6'—B11'—C7'	−1.9 (2)
B10—B6—B11—B2	−140.0 (2)	B10'—B6'—B11'—B2'	140.39 (19)
B5—B6—B11—B2	−98.9 (2)	B5'—B6'—B11'—B2'	99.2 (2)
B1—B6—B11—B2	−36.62 (18)	B1'—B6'—B11'—B2'	37.08 (18)
B2—B6—B11—B10	140.0 (2)	B2'—B6'—B11'—B10'	−140.39 (19)
B5—B6—B11—B10	41.09 (19)	B5'—B6'—B11'—B10'	−41.23 (18)
B1—B6—B11—B10	103.3 (2)	B1'—B6'—B11'—B10'	−103.3 (2)
B1—B2—B11—C7	−96.7 (2)	B1'—B2'—B11'—C7'	96.2 (2)
B3—B2—B11—C7	−32.14 (18)	B3'—B2'—B11'—C7'	31.95 (17)
B6—B2—B11—C7	−135.4 (2)	B6'—B2'—B11'—C7'	135.00 (19)
C7—B2—B11—B6	135.4 (2)	C7'—B2'—B11'—B6'	−135.00 (19)
B1—B2—B11—B6	38.72 (19)	B1'—B2'—B11'—B6'	−38.81 (18)
B3—B2—B11—B6	103.2 (2)	B3'—B2'—B11'—B6'	−103.1 (2)
C7—B2—B11—B10	100.1 (2)	C7'—B2'—B11'—B10'	−100.11 (19)
B1—B2—B11—B10	3.5 (3)	B1'—B2'—B11'—B10'	−3.9 (2)
B3—B2—B11—B10	68.0 (2)	B3'—B2'—B11'—B10'	−68.2 (2)
B6—B2—B11—B10	−35.26 (18)	B6'—B2'—B11'—B10'	34.89 (17)
B9—B10—B11—C7	−3.0 (2)	B9'—B10'—B11'—C7'	2.7 (2)
B6—B10—B11—C7	97.2 (2)	B6'—B10'—B11'—C7'	−97.5 (2)
B5—B10—B11—C7	56.9 (2)	B5'—B10'—B11'—C7'	−57.1 (2)
B9—B10—B11—B6	−100.2 (2)	B9'—B10'—B11'—B6'	100.2 (2)
B5—B10—B11—B6	−40.28 (18)	B5'—B10'—B11'—B6'	40.40 (18)
B9—B10—B11—B2	−64.9 (2)	B9'—B10'—B11'—B2'	65.1 (2)
B6—B10—B11—B2	35.30 (18)	B6'—B10'—B11'—B2'	−35.14 (17)
B5—B10—B11—B2	−5.0 (2)	B5'—B10'—B11'—B2'	5.3 (2)
C8—C7—C71—C76	94.3 (3)	C8'—C7'—C71'—C72'	98.0 (3)
B11—C7—C71—C76	−43.3 (3)	B11'—C7'—C71'—C72'	−123.0 (2)
B2—C7—C71—C76	−120.0 (3)	B2'—C7'—C71'—C72'	−47.5 (3)
B3—C7—C71—C76	167.7 (2)	B3'—C7'—C71'—C72'	24.2 (3)
C8—C7—C71—C72	−86.5 (3)	C8'—C7'—C71'—C76'	−86.9 (3)
B11—C7—C71—C72	136.0 (2)	B11'—C7'—C71'—C76'	52.1 (3)
B2—C7—C71—C72	59.3 (3)	B2'—C7'—C71'—C76'	127.7 (2)
B3—C7—C71—C72	−13.1 (3)	B3'—C7'—C71'—C76'	−160.73 (19)
C76—C71—C72—C73	−1.3 (4)	C76'—C71'—C72'—C73'	−0.5 (3)
C7—C71—C72—C73	179.5 (2)	C7'—C71'—C72'—C73'	174.6 (2)
C71—C72—C73—C74	−0.5 (5)	C71'—C72'—C73'—C74'	−0.1 (4)
C72—C73—C74—C75	1.6 (5)	C72'—C73'—C74'—C75'	0.9 (4)
C73—C74—C75—C76	−1.1 (5)	C73'—C74'—C75'—C76'	−1.2 (4)
C72—C71—C76—C75	1.8 (4)	C74'—C75'—C76'—C71'	0.6 (4)
C7—C71—C76—C75	−178.9 (2)	C72'—C71'—C76'—C75'	0.3 (3)
C74—C75—C76—C71	−0.7 (5)	C7'—C71'—C76'—C75'	−175.0 (2)
C7—C8—C81—C82	109.2 (2)	C7'—C8'—C81'—C82'	−104.6 (3)
B9—C8—C81—C82	−107.1 (2)	B9'—C8'—C81'—C82'	111.3 (3)
B3—C8—C81—C82	38.1 (3)	B3'—C8'—C81'—C82'	−34.1 (3)
B4—C8—C81—C82	−32.9 (3)	B4'—C8'—C81'—C82'	36.9 (3)
C7—C8—C81—C86	−72.8 (3)	C7'—C8'—C81'—C86'	77.4 (3)
B9—C8—C81—C86	70.9 (3)	B9'—C8'—C81'—C86'	−66.8 (3)
B3—C8—C81—C86	−143.9 (2)	B3'—C8'—C81'—C86'	147.9 (2)
B4—C8—C81—C86	145.1 (2)	B4'—C8'—C81'—C86'	−141.2 (2)
C86—C81—C82—C83	−0.6 (3)	C86'—C81'—C82'—C83'	−0.2 (4)
C8—C81—C82—C83	177.5 (2)	C8'—C81'—C82'—C83'	−178.2 (2)
C81—C82—C83—C84	0.9 (4)	C81'—C82'—C83'—C84'	0.0 (4)
C82—C83—C84—C85	−0.3 (4)	C82'—C83'—C84'—C85'	−0.1 (4)
C83—C84—C85—C86	−0.6 (4)	C83'—C84'—C85'—C86'	0.4 (4)
C84—C85—C86—C81	0.9 (4)	C84'—C85'—C86'—C81'	−0.5 (4)
C82—C81—C86—C85	−0.3 (3)	C82'—C81'—C86'—C85'	0.4 (4)
C8—C81—C86—C85	−178.5 (2)	C8'—C81'—C86'—C85'	178.6 (2)
C8—B9—S9—C92	155.50 (18)	C8'—B9'—S9'—C92'	−146.0 (2)
B5—B9—S9—C92	19.1 (2)	B5'—B9'—S9'—C92'	−7.0 (3)
B4—B9—S9—C92	86.80 (18)	B4'—B9'—S9'—C92'	−76.3 (2)
B10—B9—S9—C92	−58.0 (2)	B10'—B9'—S9'—C92'	69.1 (2)
C8—B9—S9—C91	−100.21 (19)	C8'—B9'—S9'—C91'	108.6 (2)
B5—B9—S9—C91	123.4 (2)	B5'—B9'—S9'—C91'	−112.4 (2)
B4—B9—S9—C91	−168.90 (17)	B4'—B9'—S9'—C91'	178.2 (2)
B10—B9—S9—C91	46.3 (2)	B10'—B9'—S9'—C91'	−36.4 (3)