trans-Di­chlorido­tetra­kis­(4-meth­oxy­pyridine-κN)ruthenium(II)

Reinheimer, E.W.; Tobias, R.A.; Bassel, E.R.; Cantu, N.A.; Smucker, B.W.

doi:10.1107/S2414314623001554

trans-Dichloridotetrakis(4-methoxypyridine-κN)ruthenium(II)

E. W. Reinheimer, R. A. Tobias, E. R. Bassel, N. A. Cantu and B. W. Smucker

The structure of the title complex, [RuCl₂(C₆H₆NO)₄], exhibits point group symmetry $\overline{4}$ . The structure exhibits disorder around a $\overline{4}$ axis. The 4-methoxypyridine ligands have a propeller-like arrangement around the Ru^II atom at 52.0 (3)° from the RuN₄ plane.

Keywords: crystal structure; ruthenium(II); 4-methoxypyridine.

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Supporting information

	Crystallographic Information File (CIF) https://doi.org/10.1107/S2414314623001554/bv4046sup1.cif Contains datablock I
	Structure factor file (CIF format) https://doi.org/10.1107/S2414314623001554/bv4046Isup2.hkl Contains datablock I

CCDC reference: 2243464

checkCIF report

Key indicators

Structure: I

Single-crystal X-ray study
T = 293 K
R factor = 0.030
wR factor = 0.082
Data-to-parameter ratio = 10.2

checkCIF/PLATON results

No syntax errors found



Alert level G
PLAT002_ALERT_2_G Number of Distance or Angle Restraints on AtSite          6 Note
PLAT012_ALERT_1_G No       _shelx_res_checksum Found in CIF ......     Please Check
PLAT083_ALERT_2_G SHELXL Second Parameter in WGHT  Unusually Large      15.43 Why ?
PLAT176_ALERT_4_G The CIF-Embedded .res File Contains SADI Records          2 Report
PLAT187_ALERT_4_G The CIF-Embedded .res File Contains RIGU Records          1 Report
PLAT199_ALERT_1_G Reported _cell_measurement_temperature ..... (K)        293 Check
PLAT200_ALERT_1_G Reported   _diffrn_ambient_temperature ..... (K)        293 Check
PLAT300_ALERT_4_G Atom Site Occupancy of Cl1        Constrained at        0.5 Check
PLAT300_ALERT_4_G Atom Site Occupancy of O1A        Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of N1A        Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of O1B        Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of C1A        Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of C2A        Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of C3A        Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of C4A        Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of C5A        Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of C6A        Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of N1B        Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of C1B        Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of C2B        Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of C3B        Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of C4B        Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of C5B        Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of C6B        Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H6AA       Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H1A        Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H6AB       Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H2A        Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H6AC       Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H4A        Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H5A        Constrained at       0.55 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H1B        Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H2B        Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H6BA       Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H4B        Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H6BB       Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H5B        Constrained at       0.45 Check
PLAT300_ALERT_4_G Atom Site Occupancy of H6BC       Constrained at       0.45 Check
PLAT301_ALERT_3_G Main Residue  Disorder ..............(Resd  1  )        97% Note
PLAT720_ALERT_4_G Number of Unusual/Non-Standard Labels ..........          6 Note
PLAT811_ALERT_5_G No ADDSYM Analysis: Too Many Excluded Atoms ....          ! Info
PLAT860_ALERT_3_G Number of Least-Squares Restraints .............        131 Note
PLAT870_ALERT_4_G ALERTS Related to Twinning Effects Suppressed ..          ! Info
PLAT910_ALERT_3_G Missing # of FCF Reflection(s) Below Theta(Min).          1 Note
PLAT931_ALERT_5_G CIFcalcFCF  Twin Law ( 1 1 0)         Est.d BASF       0.51 Check
PLAT933_ALERT_2_G Number of HKL-OMIT Records in Embedded .res File          1 Note

   0 ALERT level A = Most likely a serious problem - resolve or explain
   0 ALERT level B = A potentially serious problem, consider carefully
   0 ALERT level C = Check. Ensure it is not caused by an omission or oversight
  46 ALERT level G = General information/check it is not something unexpected

   3 ALERT type 1 CIF construction/syntax error, inconsistent or missing data
   3 ALERT type 2 Indicator that the structure model may be wrong or deficient
   3 ALERT type 3 Indicator that the structure quality may be low
  35 ALERT type 4 Improvement, methodology, query or suggestion
   2 ALERT type 5 Informative message, check

Computing details top

Data collection: CrysAlis PRO 1.171.42.53a (Rigaku OD, 2022); cell refinement: CrysAlis PRO 1.171.42.53a (Rigaku OD, 2022); data reduction: CrysAlis PRO 1.171.42.53a (Rigaku OD, 2022); program(s) used to solve structure: SHELXT (Sheldrick, 2015a); program(s) used to refine structure: SHELXL2016/6 (Sheldrick, 2015b); molecular graphics: Olex2 1.3-ac4 (Dolomanov et al., 2009); software used to prepare material for publication: Olex2 1.3-ac4 (Dolomanov et al., 2009).

trans-Dichloridotetrakis(4-methoxypyridine-κN)ruthenium(II) top

Crystal data top

[RuCl₂(C₁₂H₁₄N₂O₂)₂]	D_x = 1.557 Mg m⁻³
M_r = 608.47	Mo Kα radiation, λ = 0.71073 Å
Tetragonal, I4₁/a	Cell parameters from 17604 reflections
a = 17.2417 (1) Å	θ = 2.4–30.1°
c = 8.7307 (2) Å	µ = 0.85 mm⁻¹
V = 2595.43 (7) Å³	T = 293 K
Z = 4	Block, orange
F(000) = 1240	0.25 × 0.12 × 0.1 mm

Data collection top

XtaLAB Mini II diffractometer	1494 independent reflections
Radiation source: fine-focus sealed X-ray tube, Rigaku (Mo) X-ray Source	1367 reflections with I > 2σ(I)
Graphite monochromator	R_int = 0.029
Detector resolution: 10.0000 pixels mm^-1	θ_max = 27.5°, θ_min = 2.6°
ω scans	h = −22→22
Absorption correction: multi-scan (CrysAlisPro; Rigaku OD, 2022)	k = −22→22
T_min = 0.901, T_max = 1.000	l = −11→11
102632 measured reflections

Refinement top

Refinement on F²	Primary atom site location: dual
Least-squares matrix: full	Hydrogen site location: inferred from neighbouring sites
R[F² > 2σ(F²)] = 0.030	H-atom parameters constrained
wR(F²) = 0.082	w = 1/[σ²(F_o²) + 15.430P] where P = (F_o² + 2F_c²)/3
S = 1.07	(Δ/σ)_max < 0.001
1494 reflections	Δρ_max = 0.38 e Å⁻³
147 parameters	Δρ_min = −0.38 e Å⁻³
131 restraints

Special details top

Geometry. All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes.

Refinement. Refined as a 2-component twin.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å²) top

	x	y	z	U_iso*/U_eq	Occ. (<1)
Ru1	0.500000	0.250000	0.875000	0.03156 (14)
N1B	0.4401 (5)	0.3133 (5)	0.7009 (8)	0.0333 (16)	0.45
C1B	0.3596 (5)	0.3168 (5)	0.6994 (9)	0.031 (2)	0.45
H1B	0.331203	0.293777	0.777710	0.038*	0.45
C2B	0.3214 (4)	0.3547 (7)	0.5807 (11)	0.053 (4)	0.45
H2B	0.267559	0.357028	0.579691	0.064*	0.45
C3B	0.3639 (6)	0.3891 (6)	0.4636 (9)	0.038 (2)	0.45
C4B	0.4444 (6)	0.3857 (5)	0.4652 (8)	0.033 (2)	0.45
H4B	0.472767	0.408712	0.386851	0.040*	0.45
C5B	0.4825 (4)	0.3478 (6)	0.5838 (10)	0.036 (3)	0.45
H5B	0.536412	0.345461	0.584869	0.043*	0.45
Cl1	0.3999 (6)	0.3486 (6)	0.8850 (3)	0.0360 (4)	0.5
O1B	0.3229 (10)	0.4262 (12)	0.3520 (15)	0.052 (4)	0.45
N1A	0.4418 (6)	0.3089 (5)	1.0449 (8)	0.0321 (13)	0.55
C5A	0.4350 (7)	0.3866 (6)	1.0540 (13)	0.045 (3)	0.55
H5A	0.459380	0.415337	0.977769	0.054*	0.55
C2A	0.3646 (7)	0.3066 (7)	1.2771 (14)	0.055 (4)	0.55
H2A	0.341706	0.275510	1.351489	0.066*	0.55
C1A	0.4062 (7)	0.2740 (6)	1.1595 (13)	0.044 (3)	0.55
H1A	0.409791	0.220231	1.160770	0.052*	0.55
C3A	0.3574 (7)	0.3869 (7)	1.2831 (8)	0.038 (2)	0.55
C4A	0.3959 (6)	0.4277 (5)	1.1639 (11)	0.035 (2)	0.55
H4A	0.394618	0.481609	1.160556	0.042*	0.55
C6A	0.2873 (11)	0.3862 (10)	1.5143 (15)	0.077 (5)	0.55
H6AA	0.247065	0.353501	1.474172	0.116*	0.55
H6AB	0.265534	0.421274	1.588180	0.116*	0.55
H6AC	0.326225	0.354836	1.562464	0.116*	0.55
O1A	0.3210 (10)	0.4290 (9)	1.3939 (10)	0.051 (3)	0.55
C6B	0.3627 (9)	0.4650 (8)	0.2338 (13)	0.041 (3)	0.45
H6BA	0.326401	0.493663	0.172646	0.061*	0.45
H6BB	0.389015	0.427743	0.170615	0.061*	0.45
H6BC	0.399952	0.499992	0.277467	0.061*	0.45

Atomic displacement parameters (Å²) top

	U¹¹	U²²	U³³	U¹²	U¹³	U²³
Ru1	0.02965 (17)	0.02965 (17)	0.0354 (3)	0.000	0.000	0.000
N1B	0.034 (3)	0.030 (5)	0.036 (3)	0.004 (3)	0.000 (3)	0.004 (3)
C1B	0.034 (3)	0.026 (6)	0.033 (4)	0.006 (3)	−0.001 (3)	−0.002 (4)
C2B	0.040 (4)	0.056 (10)	0.063 (6)	0.003 (5)	−0.008 (4)	0.027 (7)
C3B	0.038 (4)	0.030 (6)	0.047 (5)	0.003 (4)	−0.014 (3)	0.011 (5)
C4B	0.039 (4)	0.041 (6)	0.020 (4)	0.002 (4)	−0.012 (3)	−0.005 (3)
C5B	0.032 (4)	0.048 (7)	0.029 (4)	−0.004 (4)	−0.010 (3)	0.007 (4)
Cl1	0.032 (2)	0.042 (3)	0.0339 (8)	0.0063 (6)	−0.0015 (13)	0.0008 (13)
O1B	0.047 (6)	0.055 (9)	0.054 (6)	0.009 (5)	−0.018 (5)	0.022 (6)
N1A	0.039 (4)	0.023 (3)	0.034 (2)	0.001 (2)	0.001 (2)	0.007 (2)
C5A	0.058 (7)	0.023 (3)	0.053 (5)	−0.001 (3)	0.018 (5)	0.006 (3)
C2A	0.068 (8)	0.035 (3)	0.061 (6)	0.004 (4)	0.029 (6)	0.013 (3)
C1A	0.056 (7)	0.025 (3)	0.049 (4)	0.004 (4)	0.016 (4)	0.013 (3)
C3A	0.050 (6)	0.036 (3)	0.030 (3)	0.003 (3)	−0.005 (3)	0.005 (3)
C4A	0.041 (6)	0.028 (3)	0.034 (3)	0.005 (3)	−0.005 (3)	0.006 (3)
C6A	0.117 (13)	0.070 (9)	0.046 (6)	0.008 (8)	0.029 (7)	0.006 (6)
O1A	0.073 (9)	0.049 (5)	0.032 (4)	0.006 (4)	0.003 (5)	−0.001 (4)
C6B	0.056 (7)	0.029 (5)	0.037 (5)	0.005 (5)	−0.020 (5)	0.003 (4)

Geometric parameters (Å, º) top

Ru1—N1Bⁱ	2.137 (5)	C4B—C5B	1.3900
Ru1—N1Bⁱⁱ	2.137 (5)	C5B—H5B	0.9300
Ru1—N1Bⁱⁱⁱ	2.137 (5)	O1B—C6B	1.409 (11)
Ru1—N1B	2.137 (5)	N1A—C5A	1.346 (9)
Ru1—Cl1ⁱⁱⁱ	2.4235 (15)	N1A—C1A	1.319 (10)
Ru1—Cl1ⁱⁱ	2.4235 (15)	C5A—H5A	0.9300
Ru1—Cl1ⁱ	2.4235 (16)	C5A—C4A	1.370 (11)
Ru1—Cl1	2.4236 (15)	C2A—H2A	0.9300
Ru1—N1A	2.059 (7)	C2A—C1A	1.372 (12)
Ru1—N1Aⁱⁱⁱ	2.059 (7)	C2A—C3A	1.391 (11)
Ru1—N1Aⁱ	2.059 (7)	C1A—H1A	0.9300
Ru1—N1Aⁱⁱ	2.059 (7)	C3A—C4A	1.421 (11)
N1B—C1B	1.3900	C3A—O1A	1.363 (7)
N1B—C5B	1.3900	C4A—H4A	0.9300
C1B—H1B	0.9300	C6A—H6AA	0.9600
C1B—C2B	1.3900	C6A—H6AB	0.9600
C2B—H2B	0.9300	C6A—H6AC	0.9600
C2B—C3B	1.3900	C6A—O1A	1.409 (11)
C3B—C4B	1.3900	C6B—H6BA	0.9600
C3B—O1B	1.363 (7)	C6B—H6BB	0.9600
C4B—H4B	0.9300	C6B—H6BC	0.9600

N1Bⁱ—Ru1—N1Bⁱⁱ	120.4 (3)	N1Aⁱⁱ—Ru1—N1Aⁱ	121.2 (2)
N1Bⁱ—Ru1—N1B	120.4 (3)	N1A—Ru1—N1Aⁱⁱⁱ	121.2 (2)
N1Bⁱⁱ—Ru1—N1B	89.4 (5)	N1Aⁱⁱⁱ—Ru1—N1Aⁱ	87.9 (4)
N1Bⁱⁱⁱ—Ru1—N1B	120.4 (3)	C1B—N1B—Ru1	120.8 (5)
N1Bⁱⁱⁱ—Ru1—Cl1ⁱⁱ	90.0 (4)	C1B—N1B—C5B	120.0
N1Bⁱⁱⁱ—Ru1—Cl1ⁱ	136.7 (2)	C5B—N1B—Ru1	119.1 (5)
N1Bⁱ—Ru1—Cl1ⁱⁱ	87.1 (4)	N1B—C1B—H1B	120.0
N1Bⁱⁱ—Ru1—Cl1ⁱ	90.0 (4)	N1B—C1B—C2B	120.0
N1Bⁱ—Ru1—Cl1ⁱ	47.4 (2)	C2B—C1B—H1B	120.0
N1Bⁱⁱ—Ru1—Cl1ⁱⁱ	47.4 (2)	C1B—C2B—H2B	120.0
N1Bⁱⁱⁱ—Ru1—Cl1	87.1 (4)	C1B—C2B—C3B	120.0
N1Bⁱⁱ—Ru1—Cl1	136.7 (2)	C3B—C2B—H2B	120.0
N1B—Ru1—Cl1ⁱ	87.1 (4)	C4B—C3B—C2B	120.0
N1B—Ru1—Cl1	47.4 (2)	O1B—C3B—C2B	117.0 (9)
N1B—Ru1—Cl1ⁱⁱ	136.7 (2)	O1B—C3B—C4B	123.0 (9)
N1Bⁱ—Ru1—Cl1	90.0 (4)	C3B—C4B—H4B	120.0
Cl1ⁱ—Ru1—Cl1ⁱⁱ	90.075 (5)	C3B—C4B—C5B	120.0
Cl1ⁱ—Ru1—Cl1	90.076 (5)	C5B—C4B—H4B	120.0
Cl1ⁱⁱ—Ru1—Cl1	175.86 (12)	N1B—C5B—H5B	120.0
Cl1ⁱⁱⁱ—Ru1—Cl1ⁱⁱ	90.075 (5)	C4B—C5B—N1B	120.0
Cl1ⁱⁱⁱ—Ru1—Cl1	90.074 (5)	C4B—C5B—H5B	120.0
Cl1ⁱⁱⁱ—Ru1—Cl1ⁱ	175.86 (12)	C3B—O1B—C6B	119.6 (13)
N1A—Ru1—N1Bⁱ	59.9 (2)	C5A—N1A—Ru1	125.2 (7)
N1Aⁱ—Ru1—N1Bⁱⁱⁱ	178.8 (3)	C1A—N1A—Ru1	123.2 (6)
N1Aⁱⁱ—Ru1—N1Bⁱⁱⁱ	59.9 (2)	C1A—N1A—C5A	111.6 (7)
N1Aⁱⁱⁱ—Ru1—N1Bⁱⁱ	58.5 (2)	N1A—C5A—H5A	116.6
N1Aⁱⁱ—Ru1—N1Bⁱ	58.5 (2)	N1A—C5A—C4A	126.8 (8)
N1A—Ru1—N1Bⁱⁱ	178.8 (3)	C4A—C5A—H5A	116.6
N1Aⁱⁱ—Ru1—N1Bⁱⁱ	91.40 (18)	C1A—C2A—H2A	120.6
N1Aⁱⁱⁱ—Ru1—N1Bⁱ	178.8 (3)	C1A—C2A—C3A	118.8 (8)
N1Aⁱ—Ru1—N1Bⁱ	91.40 (18)	C3A—C2A—H2A	120.6
N1Aⁱ—Ru1—N1Bⁱⁱ	59.9 (2)	N1A—C1A—C2A	128.6 (8)
N1A—Ru1—N1Bⁱⁱⁱ	58.5 (2)	N1A—C1A—H1A	115.7
N1Aⁱⁱⁱ—Ru1—N1Bⁱⁱⁱ	91.40 (18)	C2A—C1A—H1A	115.7
N1Aⁱⁱ—Ru1—Cl1ⁱⁱⁱ	90.9 (4)	C2A—C3A—C4A	115.1 (8)
N1A—Ru1—Cl1ⁱⁱ	131.8 (2)	O1A—C3A—C2A	126.7 (11)
N1Aⁱⁱⁱ—Ru1—Cl1ⁱⁱ	92.0 (4)	O1A—C3A—C4A	118.1 (10)
N1Aⁱ—Ru1—Cl1	92.0 (4)	C5A—C4A—C3A	119.1 (7)
N1A—Ru1—Cl1	44.0 (2)	C5A—C4A—H4A	120.4
N1Aⁱ—Ru1—Cl1ⁱⁱ	90.9 (4)	C3A—C4A—H4A	120.4
N1Aⁱⁱ—Ru1—Cl1	131.9 (2)	H6AA—C6A—H6AB	109.5
N1Aⁱ—Ru1—Cl1ⁱⁱⁱ	131.8 (2)	H6AA—C6A—H6AC	109.5
N1Aⁱⁱⁱ—Ru1—Cl1ⁱⁱⁱ	44.0 (2)	H6AB—C6A—H6AC	109.5
N1Aⁱⁱ—Ru1—Cl1ⁱ	92.0 (4)	O1A—C6A—H6AA	109.5
N1Aⁱⁱⁱ—Ru1—Cl1	90.9 (4)	O1A—C6A—H6AB	109.5
N1A—Ru1—Cl1ⁱ	90.9 (4)	O1A—C6A—H6AC	109.5
N1Aⁱⁱ—Ru1—Cl1ⁱⁱ	44.0 (2)	C3A—O1A—C6A	116.2 (12)
N1Aⁱⁱⁱ—Ru1—Cl1ⁱ	131.8 (2)	O1B—C6B—H6BA	109.5
N1A—Ru1—Cl1ⁱⁱⁱ	92.0 (4)	O1B—C6B—H6BB	109.5
N1Aⁱ—Ru1—Cl1ⁱ	44.0 (2)	O1B—C6B—H6BC	109.5
N1A—Ru1—N1Aⁱⁱ	87.9 (4)	H6BA—C6B—H6BB	109.5
N1Aⁱⁱⁱ—Ru1—N1Aⁱⁱ	121.2 (2)	H6BA—C6B—H6BC	109.5
N1A—Ru1—N1Aⁱ	121.2 (2)	H6BB—C6B—H6BC	109.5

Ru1—N1B—C1B—C2B	−176.5 (7)	C5B—N1B—C1B—C2B	0.0
Ru1—N1B—C5B—C4B	176.6 (7)	O1B—C3B—C4B—C5B	179.1 (15)
Ru1—N1A—C5A—C4A	179.0 (9)	N1A—C5A—C4A—C3A	−0.1 (16)
Ru1—N1A—C1A—C2A	−178.7 (10)	C5A—N1A—C1A—C2A	1.3 (14)
N1B—C1B—C2B—C3B	0.0	C2A—C3A—C4A—C5A	1.0 (14)
C1B—N1B—C5B—C4B	0.0	C2A—C3A—O1A—C6A	0 (2)
C1B—C2B—C3B—C4B	0.0	C1A—N1A—C5A—C4A	−1.0 (14)
C1B—C2B—C3B—O1B	−179.2 (14)	C1A—C2A—C3A—C4A	−0.8 (14)
C2B—C3B—C4B—C5B	0.0	C1A—C2A—C3A—O1A	−177.4 (14)
C2B—C3B—O1B—C6B	177.3 (13)	C3A—C2A—C1A—N1A	−0.5 (16)
C3B—C4B—C5B—N1B	0.0	C4A—C3A—O1A—C6A	−176.6 (14)
C4B—C3B—O1B—C6B	−2 (3)	O1A—C3A—C4A—C5A	178.0 (12)

Symmetry codes: (i) y+1/4, −x+3/4, −z+7/4; (ii) −x+1, −y+1/2, z; (iii) −y+3/4, x−1/4, −z+7/4.

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Format		BIBTeX
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trans-Di­chlorido­tetra­kis­(4-meth­oxy­pyridine-κN)ruthenium(II)

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trans-Dichloridotetrakis(4-methoxypyridine-κN)ruthenium(II)