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In the crystal, mol­ecules are connected by pairs of inter­molecular C—H...O hydrogen bonds, forming dimers with R_{2}^{2}(8) motifs. These dimers form a three-dimensional network through O—H...O, O—H...S and C—H...O hydrogen bonds with each other directly and through solvent mol­ecules.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S2056989023009635/tx2077sup1.cif
Contains datablock I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S2056989023009635/tx2077Isup2.hkl
Contains datablock I

CCDC reference: 2305649

Computing details top

10-Hydroxy-2-(4-methoxyphenyl)-3-oxo-2,3,3a,4,10,10a-hexahydro-1H-9-thia-2-azacyclopenta[b]fluorene-4-carboxylic acid dimethyl sulfoxide-d6 monosolvate top
Crystal data top
C22H19NO5S·C2D6OSF(000) = 1024
Mr = 493.61Dx = 1.460 Mg m3
Monoclinic, P21/cMo Kα radiation, λ = 0.71073 Å
a = 16.3178 (4) ÅCell parameters from 9765 reflections
b = 9.2747 (2) Åθ = 2.6–30.1°
c = 14.8720 (4) ŵ = 0.28 mm1
β = 93.771 (1)°T = 100 K
V = 2245.89 (10) Å3Fragment, colourless
Z = 40.40 × 0.28 × 0.22 mm
Data collection top
Bruker Kappa APEXII area-detector
diffractometer
5693 reflections with I > 2σ(I)
φ and ω scansRint = 0.032
Absorption correction: multi-scan
(SADABS; Krause et al., 2015)
θmax = 30.0°, θmin = 4.2°
Tmin = 0.847, Tmax = 0.941h = 2222
69078 measured reflectionsk = 1313
6531 independent reflectionsl = 2020
Refinement top
Refinement on F215 restraints
Least-squares matrix: fullHydrogen site location: inferred from neighbouring sites
R[F2 > 2σ(F2)] = 0.049H-atom parameters constrained
wR(F2) = 0.129 w = 1/[σ2(Fo2) + (0.0518P)2 + 1.8241P]
where P = (Fo2 + 2Fc2)/3
S = 1.12(Δ/σ)max = 0.001
6531 reflectionsΔρmax = 0.54 e Å3
324 parametersΔρmin = 0.47 e Å3
Special details top

Geometry. All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes.

Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/UeqOcc. (<1)
S1A0.06873 (3)0.67027 (5)0.20351 (4)0.03201 (16)0.8903 (18)
S1B0.0094 (3)0.7350 (5)0.2022 (3)0.0386 (13)*0.1097 (18)
S50.21789 (3)1.16195 (5)0.65744 (3)0.03355 (13)
O10.36715 (8)0.72156 (13)0.33936 (8)0.0253 (3)
O20.14801 (9)0.83115 (17)0.39946 (10)0.0367 (3)
O30.20598 (9)0.93552 (15)0.28380 (8)0.0338 (3)
H30.1657070.8991400.2538550.041*
O40.47133 (8)0.05607 (13)0.38739 (8)0.0275 (3)
O5A0.25163 (15)0.8579 (2)0.70428 (13)0.0338 (6)0.637 (4)
H5A0.2837550.8134230.7410120.041*0.637 (4)
O5B0.3604 (2)0.9025 (4)0.6728 (2)0.0282 (9)0.363 (4)
H5B0.3584020.8674060.7246660.034*0.363 (4)
O6A0.08659 (10)0.82728 (16)0.18542 (11)0.0337 (4)0.8903 (18)
O6B0.0447 (10)0.8676 (13)0.2106 (10)0.044 (3)*0.1097 (18)
N20.35684 (8)0.60178 (14)0.47516 (9)0.0193 (3)
C10.35193 (10)0.71814 (17)0.41916 (10)0.0193 (3)
C3A0.29022 (10)0.77925 (18)0.55483 (10)0.0218 (3)
H3AA0.2320170.7526570.5369850.026*
C30.34047 (11)0.64061 (18)0.56878 (10)0.0231 (3)
H3A0.3921130.6582850.6058670.028*
H3B0.3085910.5645250.5974920.028*
C4B0.29054 (12)0.8898 (2)0.63036 (11)0.0302 (4)0.637 (4)
H4A0.3491580.9107970.6498080.036*0.637 (4)
C4C0.29054 (12)0.8898 (2)0.63036 (11)0.0302 (4)0.363 (4)
H4B0.2517340.8538780.6746100.036*0.363 (4)
C4A0.25370 (11)1.02578 (19)0.58966 (11)0.0258 (3)
C5A0.19138 (11)1.26951 (19)0.56388 (11)0.0264 (3)
C60.15675 (13)1.4072 (2)0.56345 (14)0.0338 (4)
H6A0.1439221.4525190.6180550.041*
C70.14169 (12)1.4755 (2)0.48199 (14)0.0331 (4)
H7A0.1174041.5686650.4804190.040*
C80.16150 (12)1.41029 (19)0.40123 (13)0.0295 (4)
H8A0.1517071.4602840.3458100.035*
C9B0.24595 (10)1.06021 (17)0.50055 (10)0.0204 (3)
C9A0.21054 (10)1.20072 (17)0.48381 (11)0.0213 (3)
C90.19531 (10)1.27320 (18)0.40184 (11)0.0238 (3)
H9A0.2080821.2286700.3469610.029*
C10A0.32805 (9)0.84675 (16)0.47404 (10)0.0187 (3)
H10A0.3802480.8943150.4971930.022*
C100.27474 (9)0.96355 (16)0.42751 (10)0.0184 (3)
H10B0.3094921.0215070.3879810.022*
C110.20217 (10)0.90191 (17)0.36979 (11)0.0216 (3)
C120.38481 (9)0.46286 (16)0.45148 (10)0.0189 (3)
C130.42078 (10)0.37136 (18)0.51699 (11)0.0218 (3)
H13A0.4267190.4022320.5779750.026*
C140.44797 (10)0.23566 (18)0.49391 (11)0.0224 (3)
H14A0.4711770.1731020.5393200.027*
C150.44140 (10)0.19057 (16)0.40438 (11)0.0206 (3)
C160.40420 (10)0.28012 (17)0.33900 (11)0.0227 (3)
H16A0.3983530.2491900.2780210.027*
C170.37553 (10)0.41479 (17)0.36268 (10)0.0214 (3)
H17A0.3492710.4749210.3177990.026*
C180.46796 (13)0.0111 (2)0.29506 (13)0.0319 (4)
H18A0.4909090.0861810.2912090.048*
H18B0.4107330.0107250.2705320.048*
H18C0.4999470.0780070.2602860.048*
C19A0.02185 (17)0.6061 (3)0.0999 (2)0.0471 (7)0.8903 (18)
D19A0.0081390.5038110.1059230.071*0.8903 (18)
D19B0.0283870.6611650.0845720.071*0.8903 (18)
D19C0.0599290.6178920.0521920.071*0.8903 (18)
C20A0.01808 (16)0.6679 (3)0.26878 (19)0.0470 (6)0.8903 (18)
D20A0.0322510.5679420.2824010.070*0.8903 (18)
D20B0.0055250.7205400.3251540.070*0.8903 (18)
D20C0.0645530.7139670.2349520.070*0.8903 (18)
C19B0.0423 (13)0.6018 (18)0.2686 (12)0.049 (4)*0.1097 (18)
D19D0.0100740.5125430.2659390.074*0.1097 (18)
D19E0.0962870.5836600.2456460.074*0.1097 (18)
D19F0.0493350.6350240.3312000.074*0.1097 (18)
C20B0.0041 (16)0.666 (2)0.0930 (9)0.049 (4)*0.1097 (18)
D20D0.0295370.5791590.0829900.074*0.1097 (18)
D20E0.0127750.7388250.0477620.074*0.1097 (18)
D20F0.0620470.6417170.0878190.074*0.1097 (18)
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
S1A0.0229 (2)0.0222 (2)0.0503 (3)0.00093 (17)0.0028 (2)0.0081 (2)
S50.0489 (3)0.0338 (2)0.01792 (19)0.0139 (2)0.00149 (17)0.00626 (16)
O10.0395 (7)0.0201 (5)0.0168 (5)0.0014 (5)0.0053 (5)0.0001 (4)
O20.0332 (7)0.0444 (8)0.0314 (7)0.0135 (6)0.0070 (6)0.0084 (6)
O30.0458 (8)0.0352 (7)0.0188 (6)0.0119 (6)0.0097 (5)0.0031 (5)
O40.0368 (7)0.0202 (6)0.0260 (6)0.0073 (5)0.0066 (5)0.0023 (4)
O5A0.0472 (13)0.0372 (12)0.0179 (9)0.0081 (9)0.0094 (8)0.0081 (8)
O5B0.0288 (18)0.036 (2)0.0193 (16)0.0038 (14)0.0041 (12)0.0009 (13)
O6A0.0408 (9)0.0232 (7)0.0346 (8)0.0094 (6)0.0158 (7)0.0074 (6)
N20.0236 (6)0.0192 (6)0.0149 (5)0.0026 (5)0.0004 (5)0.0004 (5)
C10.0218 (7)0.0183 (7)0.0174 (6)0.0003 (5)0.0009 (5)0.0003 (5)
C3A0.0264 (7)0.0258 (7)0.0131 (6)0.0056 (6)0.0004 (5)0.0014 (5)
C30.0288 (8)0.0258 (8)0.0146 (6)0.0067 (6)0.0007 (6)0.0018 (6)
C4B0.0406 (10)0.0370 (9)0.0127 (7)0.0155 (8)0.0008 (6)0.0016 (6)
C4C0.0406 (10)0.0370 (9)0.0127 (7)0.0155 (8)0.0008 (6)0.0016 (6)
C4A0.0320 (8)0.0278 (8)0.0172 (7)0.0080 (7)0.0010 (6)0.0045 (6)
C5A0.0312 (8)0.0256 (8)0.0222 (7)0.0038 (7)0.0006 (6)0.0037 (6)
C60.0391 (10)0.0281 (9)0.0345 (10)0.0060 (8)0.0054 (8)0.0086 (7)
C70.0355 (9)0.0217 (8)0.0424 (11)0.0042 (7)0.0044 (8)0.0021 (7)
C80.0324 (9)0.0221 (8)0.0337 (9)0.0021 (7)0.0005 (7)0.0032 (7)
C9B0.0212 (7)0.0220 (7)0.0179 (7)0.0023 (6)0.0005 (5)0.0041 (5)
C9A0.0196 (7)0.0221 (7)0.0218 (7)0.0002 (5)0.0009 (5)0.0037 (6)
C90.0249 (7)0.0215 (7)0.0249 (8)0.0006 (6)0.0014 (6)0.0008 (6)
C10A0.0212 (7)0.0193 (7)0.0153 (6)0.0022 (5)0.0004 (5)0.0011 (5)
C100.0213 (7)0.0192 (7)0.0144 (6)0.0011 (5)0.0015 (5)0.0012 (5)
C110.0248 (7)0.0186 (7)0.0205 (7)0.0014 (6)0.0047 (6)0.0001 (5)
C120.0187 (6)0.0182 (7)0.0196 (7)0.0002 (5)0.0009 (5)0.0014 (5)
C130.0233 (7)0.0239 (7)0.0177 (7)0.0020 (6)0.0023 (5)0.0015 (6)
C140.0217 (7)0.0228 (7)0.0224 (7)0.0036 (6)0.0015 (6)0.0049 (6)
C150.0197 (7)0.0176 (7)0.0248 (7)0.0006 (5)0.0033 (6)0.0018 (6)
C160.0289 (8)0.0196 (7)0.0195 (7)0.0010 (6)0.0013 (6)0.0004 (6)
C170.0261 (7)0.0186 (7)0.0188 (7)0.0000 (6)0.0026 (6)0.0018 (5)
C180.0453 (11)0.0226 (8)0.0289 (9)0.0050 (7)0.0111 (8)0.0007 (7)
C19A0.0414 (14)0.0399 (14)0.0605 (17)0.0108 (11)0.0066 (12)0.0198 (12)
C20A0.0358 (12)0.0560 (16)0.0497 (15)0.0034 (11)0.0075 (11)0.0072 (12)
Geometric parameters (Å, º) top
S1A—O6A1.5127 (15)C7—C81.401 (3)
S1A—C20A1.769 (3)C7—H7A0.9500
S1A—C19A1.777 (3)C8—C91.386 (2)
S1B—O6B1.515 (12)C8—H8A0.9500
S1B—C19B1.762 (12)C9B—C9A1.441 (2)
S1B—C20B1.774 (13)C9B—C101.507 (2)
S5—C4A1.7407 (17)C9A—C91.400 (2)
S5—C5A1.7434 (18)C9—H9A0.9500
O1—C11.2288 (19)C10A—C101.526 (2)
O2—C111.207 (2)C10A—H10A1.0000
O3—C111.322 (2)C10—C111.527 (2)
O3—H30.8400C10—H10B1.0000
O4—C151.3692 (19)C12—C131.392 (2)
O4—C181.433 (2)C12—C171.393 (2)
O5A—C4B1.338 (3)C13—C141.385 (2)
O5A—H5A0.8400C13—H13A0.9500
O5B—C4C1.271 (4)C14—C151.393 (2)
O5B—H5B0.8400C14—H14A0.9500
N2—C11.362 (2)C15—C161.388 (2)
N2—C121.419 (2)C16—C171.387 (2)
N2—C31.479 (2)C16—H16A0.9500
C1—C10A1.511 (2)C17—H17A0.9500
C3A—C4C1.521 (2)C18—H18A0.9800
C3A—C4B1.521 (2)C18—H18B0.9800
C3A—C10A1.521 (2)C18—H18C0.9800
C3A—C31.532 (2)C19A—D19A0.9800
C3A—H3AA1.0000C19A—D19B0.9800
C3—H3A0.9900C19A—D19C0.9800
C3—H3B0.9900C20A—D20A0.9800
C4B—C4A1.507 (2)C20A—D20B0.9800
C4B—H4A1.0000C20A—D20C0.9800
C4C—C4A1.507 (2)C19B—D19D0.9800
C4C—H4B1.0000C19B—D19E0.9800
C4A—C9B1.361 (2)C19B—D19F0.9800
C5A—C61.396 (3)C20B—D20D0.9800
C5A—C9A1.404 (2)C20B—D20E0.9800
C6—C71.375 (3)C20B—D20F0.9800
C6—H6A0.9500
O6A—S1A—C20A106.26 (13)C8—C9—C9A119.61 (16)
O6A—S1A—C19A104.20 (12)C8—C9—H9A120.2
C20A—S1A—C19A99.03 (13)C9A—C9—H9A120.2
O6B—S1B—C19B105.6 (8)C1—C10A—C3A103.55 (12)
O6B—S1B—C20B105.2 (8)C1—C10A—C10118.36 (12)
C19B—S1B—C20B100.2 (9)C3A—C10A—C10113.66 (13)
C4A—S5—C5A91.61 (8)C1—C10A—H10A106.9
C11—O3—H3109.5C3A—C10A—H10A106.9
C15—O4—C18116.77 (13)C10—C10A—H10A106.9
C4B—O5A—H5A109.5C9B—C10—C10A106.90 (12)
C4C—O5B—H5B109.5C9B—C10—C11111.15 (13)
C1—N2—C12125.06 (13)C10A—C10—C11112.76 (13)
C1—N2—C3112.06 (13)C9B—C10—H10B108.6
C12—N2—C3122.38 (13)C10A—C10—H10B108.6
O1—C1—N2127.11 (15)C11—C10—H10B108.6
O1—C1—C10A125.25 (14)O2—C11—O3124.33 (15)
N2—C1—C10A107.58 (13)O2—C11—C10123.87 (15)
C4C—C3A—C10A108.91 (14)O3—C11—C10111.81 (14)
C4B—C3A—C10A108.91 (14)C13—C12—C17118.87 (14)
C4C—C3A—C3119.35 (13)C13—C12—N2120.50 (14)
C4B—C3A—C3119.35 (13)C17—C12—N2120.62 (13)
C10A—C3A—C3102.18 (12)C14—C13—C12120.51 (15)
C4B—C3A—H3AA108.6C14—C13—H13A119.7
C10A—C3A—H3AA108.6C12—C13—H13A119.7
C3—C3A—H3AA108.6C13—C14—C15120.25 (14)
N2—C3—C3A101.83 (12)C13—C14—H14A119.9
N2—C3—H3A111.4C15—C14—H14A119.9
C3A—C3—H3A111.4O4—C15—C16124.11 (15)
N2—C3—H3B111.4O4—C15—C14116.36 (14)
C3A—C3—H3B111.4C16—C15—C14119.51 (14)
H3A—C3—H3B109.3C17—C16—C15120.02 (15)
O5A—C4B—C4A108.46 (16)C17—C16—H16A120.0
O5A—C4B—C3A118.61 (19)C15—C16—H16A120.0
C4A—C4B—C3A106.60 (13)C16—C17—C12120.76 (14)
O5A—C4B—H4A107.6C16—C17—H17A119.6
C4A—C4B—H4A107.6C12—C17—H17A119.6
C3A—C4B—H4A107.6O4—C18—H18A109.5
O5B—C4C—C4A116.3 (2)O4—C18—H18B109.5
O5B—C4C—C3A112.9 (2)H18A—C18—H18B109.5
C4A—C4C—C3A106.60 (13)O4—C18—H18C109.5
O5B—C4C—H4B106.9H18A—C18—H18C109.5
C4A—C4C—H4B106.9H18B—C18—H18C109.5
C3A—C4C—H4B106.9S1A—C19A—D19A109.5
C9B—C4A—C4C126.63 (15)S1A—C19A—D19B109.5
C9B—C4A—C4B126.63 (15)D19A—C19A—D19B109.5
C9B—C4A—S5112.36 (13)S1A—C19A—D19C109.5
C4C—C4A—S5120.99 (12)D19A—C19A—D19C109.5
C4B—C4A—S5120.99 (12)D19B—C19A—D19C109.5
C6—C5A—C9A121.61 (17)S1A—C20A—D20A109.5
C6—C5A—S5127.31 (14)S1A—C20A—D20B109.5
C9A—C5A—S5111.07 (13)D20A—C20A—D20B109.5
C7—C6—C5A118.33 (17)S1A—C20A—D20C109.5
C7—C6—H6A120.8D20A—C20A—D20C109.5
C5A—C6—H6A120.8D20B—C20A—D20C109.5
C6—C7—C8121.20 (17)S1B—C19B—D19D109.5
C6—C7—H7A119.4S1B—C19B—D19E109.5
C8—C7—H7A119.4D19D—C19B—D19E109.5
C9—C8—C7120.31 (17)S1B—C19B—D19F109.5
C9—C8—H8A119.8D19D—C19B—D19F109.5
C7—C8—H8A119.8D19E—C19B—D19F109.5
C4A—C9B—C9A113.02 (14)S1B—C20B—D20D109.5
C4A—C9B—C10123.29 (14)S1B—C20B—D20E109.5
C9A—C9B—C10123.65 (14)D20D—C20B—D20E109.5
C9—C9A—C5A118.92 (15)S1B—C20B—D20F109.5
C9—C9A—C9B129.13 (15)D20D—C20B—D20F109.5
C5A—C9A—C9B111.94 (15)D20E—C20B—D20F109.5
C12—N2—C1—O13.3 (3)C10—C9B—C9A—C90.6 (3)
C3—N2—C1—O1175.30 (16)C4A—C9B—C9A—C5A0.6 (2)
C12—N2—C1—C10A174.00 (13)C10—C9B—C9A—C5A178.18 (15)
C3—N2—C1—C10A1.96 (18)C7—C8—C9—C9A0.8 (3)
C1—N2—C3—C3A23.14 (17)C5A—C9A—C9—C80.3 (2)
C12—N2—C3—C3A164.58 (14)C9B—C9A—C9—C8179.02 (17)
C4C—C3A—C3—N2154.00 (15)O1—C1—C10A—C3A162.34 (16)
C4B—C3A—C3—N2154.00 (15)N2—C1—C10A—C3A20.34 (16)
C10A—C3A—C3—N233.89 (15)O1—C1—C10A—C1035.5 (2)
C10A—C3A—C4B—O5A172.66 (17)N2—C1—C10A—C10147.14 (14)
C3—C3A—C4B—O5A70.7 (2)C4C—C3A—C10A—C1160.51 (13)
C10A—C3A—C4B—C4A50.03 (19)C4B—C3A—C10A—C1160.51 (13)
C3—C3A—C4B—C4A166.67 (15)C3—C3A—C10A—C133.35 (15)
C10A—C3A—C4C—O5B78.8 (2)C4C—C3A—C10A—C1069.78 (17)
C3—C3A—C4C—O5B37.8 (3)C4B—C3A—C10A—C1069.78 (17)
C10A—C3A—C4C—C4A50.03 (19)C3—C3A—C10A—C10163.06 (13)
C3—C3A—C4C—C4A166.67 (15)C4A—C9B—C10—C10A12.4 (2)
O5B—C4C—C4A—C9B107.8 (3)C9A—C9B—C10—C10A165.01 (14)
C3A—C4C—C4A—C9B19.0 (3)C4A—C9B—C10—C11111.08 (18)
O5B—C4C—C4A—S570.3 (3)C9A—C9B—C10—C1171.54 (19)
C3A—C4C—C4A—S5162.82 (13)C1—C10A—C10—C9B168.32 (13)
O5A—C4B—C4A—C9B147.8 (2)C3A—C10A—C10—C9B46.52 (17)
C3A—C4B—C4A—C9B19.0 (3)C1—C10A—C10—C1145.88 (19)
O5A—C4B—C4A—S534.0 (2)C3A—C10A—C10—C1175.93 (17)
C3A—C4B—C4A—S5162.82 (13)C9B—C10—C11—O257.9 (2)
C5A—S5—C4A—C9B0.01 (15)C10A—C10—C11—O262.1 (2)
C5A—S5—C4A—C4C178.43 (16)C9B—C10—C11—O3122.07 (15)
C5A—S5—C4A—C4B178.43 (16)C10A—C10—C11—O3117.90 (15)
C4A—S5—C5A—C6179.43 (19)C1—N2—C12—C13152.25 (16)
C4A—S5—C5A—C9A0.33 (14)C3—N2—C12—C1319.0 (2)
C9A—C5A—C6—C70.2 (3)C1—N2—C12—C1728.8 (2)
S5—C5A—C6—C7178.84 (16)C3—N2—C12—C17159.92 (15)
C5A—C6—C7—C80.9 (3)C17—C12—C13—C141.0 (2)
C6—C7—C8—C91.4 (3)N2—C12—C13—C14179.89 (15)
C4C—C4A—C9B—C9A178.00 (17)C12—C13—C14—C151.6 (2)
C4B—C4A—C9B—C9A178.00 (17)C18—O4—C15—C164.1 (2)
S5—C4A—C9B—C9A0.3 (2)C18—O4—C15—C14177.49 (15)
C4C—C4A—C9B—C100.4 (3)C13—C14—C15—O4178.70 (15)
C4B—C4A—C9B—C100.4 (3)C13—C14—C15—C162.8 (2)
S5—C4A—C9B—C10177.93 (13)O4—C15—C16—C17179.86 (15)
C6—C5A—C9A—C90.8 (3)C14—C15—C16—C171.5 (2)
S5—C5A—C9A—C9178.38 (13)C15—C16—C17—C121.1 (2)
C6—C5A—C9A—C9B179.71 (17)C13—C12—C17—C162.3 (2)
S5—C5A—C9A—C9B0.55 (19)N2—C12—C17—C16178.78 (15)
C4A—C9B—C9A—C9178.24 (17)
Hydrogen-bond geometry (Å, º) top
D—H···AD—HH···AD···AD—H···A
O3—H3···S1A0.842.723.4846 (15)152
O3—H3···O6A0.841.722.563 (2)176
O3—H3···O6B0.842.062.852 (16)158
O5A—H5A···O1i0.841.962.763 (2)160
C3A—H3AA···O21.002.493.202 (2)127
C3—H3A···O5B0.992.542.887 (4)100
C6—H6A···O6Aii0.952.483.307 (3)145
C14—H14A···O4iii0.952.543.445 (2)159
C17—H17A···O10.952.332.868 (2)116
C17—H17A···O5Biv0.952.463.289 (4)146
C18—H18C···O5Bv0.982.432.922 (4)110
C20A—D20A···O6Avi0.982.463.434 (3)173
C20A—D20A···O6Bvi0.981.872.839 (13)168
Symmetry codes: (i) x, y+3/2, z+1/2; (ii) x, y+5/2, z+1/2; (iii) x+1, y, z+1; (iv) x, y+3/2, z1/2; (v) x+1, y+1, z+1; (vi) x, y1/2, z+1/2.
 

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