research papers
Crystals of Cs6(SO4)3(H3PO4)4 belong to the family of alkali metal acid salts that show a high protonic conductivity at relatively low temperatures. Such properties make superprotonic crystals an excellent choice for the study of the influence of the hydrogen subsystem on the physicochemical properties and promising materials for energy-efficient technologies. Single crystals of Cs6(SO4)3(H3PO4)4 were studied by neutron diffraction methods, optical polarization microscopy, scanning electron microscopy and energy-dispersive X-ray spectroscopy. Neutron diffraction studies made it possible to determine the positions of all the atoms with high accuracy, including the H atom on a hydrogen bond characterized by a single-minimum potential, to confirm the chemical composition of the Cs6(SO4)3(H3PO4)4 crystals and their cubic symmetry in low- and high-temperature phases, and to draw conclusions about the three-dimensional system of hydrogen bonds, which is fundamentally different in comparison with other superprotonic compounds. Based on the experimental data obtained, crystal transformations with temperature changes are reported, and the stability of the chemical composition is shown.
Keywords: single crystal; structure analysis; neutron; crystal structure; hydrogen bonding; superprotonic phase transition.
Supporting information
Crystallographic Information File (CIF) https://doi.org/10.1107/S2052520621001840/yh5010sup1.cif | |
Structure factor file (CIF format) https://doi.org/10.1107/S2052520621001840/yh5010Isup2.hkl |
CCDC reference: 2063134
Computing details top
(I) top
Crystal data top
Cs6H12O28P4S3 | Dx = 3.190 Mg m−3 |
Mr = 1477.6 | Neutron radiation, λ = 1.455 Å |
Cubic, I43d | Cell parameters from 2078 reflections |
Hall symbol: I -4bd 2c 3 | θ = 7.0–59.6° |
a = 14.5549 (6) Å | µ = 0.0 mm−1 |
V = 3083.4 (4) Å3 | T = 290 K |
Z = 4 | , colourless |
F(000) = 716.788 | 2.45 × 2.43 × 2.42 × 1.22 (radius) mm |
Data collection top
Diffractometer | Rint = 0.017 |
Radiation source: neutron | θmax = 59.6°, θmin = 7.0° |
2078 measured reflections | h = −13→11 |
437 independent reflections | k = 0→17 |
434 reflections with I > 3σ(I) | l = −9→13 |
Refinement top
Refinement on F | All H-atom parameters refined |
R[F2 > 2σ(F2)] = 0.017 | Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0001F2) |
wR(F2) = 0.024 | (Δ/σ)max = 0.008 |
S = 1.92 | Δρmax = 0.12 e Å−3 |
434 reflections | Δρmin = −0.15 e Å−3 |
42 parameters | Extinction correction: B-C type 1 Lorentzian isotropic (Becker & Coppens, 1974) |
0 restraints | Extinction coefficient: 780 (60) |
0 constraints | Absolute structure: 185 of Friedel pairs used in the refinement |
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
x | y | z | Uiso*/Ueq | ||
Cs1 | 0.09951 (8) | 0 | 0.25 | 0.0277 (3) | |
S1 | 0.375 | 0 | 0.25 | 0.0232 (6) | |
P1 | 0.99766 (6) | 0.99766 (6) | 0.99766 (6) | 0.0225 (2) | |
O1 | 0.77889 (6) | 0.06665 (7) | 0.07790 (5) | 0.0323 (3) | |
O2 | 0.08810 (5) | 0.95100 (6) | 0.03212 (6) | 0.0281 (3) | |
O3 | 0.93913 (6) | 0.93913 (6) | 0.93913 (6) | 0.0307 (2) | |
H1 | 0.88285 (11) | 0.04628 (10) | 0.08356 (10) | 0.0378 (5) |
Atomic displacement parameters (Å2) top
U11 | U22 | U33 | U12 | U13 | U23 | |
Cs1 | 0.0303 (6) | 0.0297 (6) | 0.0230 (5) | 0 | 0 | 0.0006 (5) |
S1 | 0.0291 (14) | 0.0203 (9) | 0.0203 (9) | 0 | 0 | 0 |
P1 | 0.0225 (3) | 0.0225 (3) | 0.0225 (3) | −0.0009 (4) | −0.0009 (4) | −0.0009 (4) |
O1 | 0.0273 (4) | 0.0426 (5) | 0.0270 (4) | 0.0054 (4) | 0.0038 (3) | 0.0088 (4) |
O2 | 0.0219 (4) | 0.0274 (5) | 0.0351 (5) | 0.0006 (3) | −0.0010 (3) | 0.0034 (3) |
O3 | 0.0307 (3) | 0.0307 (3) | 0.0307 (3) | −0.0044 (3) | −0.0044 (3) | −0.0044 (3) |
H1 | 0.0372 (10) | 0.0412 (8) | 0.0350 (7) | −0.0008 (7) | 0.0037 (6) | −0.0001 (6) |
Geometric parameters (Å, º) top
Cs1—S1 | 4.0097 (12) | P1—O1xxxv | 3.5371 (12) |
Cs1—S1i | 4.3183 (4) | P1—O1xxxvi | 4.2919 (11) |
Cs1—S1ii | 4.3183 (4) | P1—O1xxxvii | 3.6823 (12) |
Cs1—P1iii | 3.9607 (9) | P1—O1xxxviii | 3.6823 (12) |
Cs1—P1iv | 3.9607 (9) | P1—O1xxxix | 3.6823 (12) |
Cs1—P1v | 4.2006 (10) | P1—O2xl | 1.5638 (11) |
Cs1—P1vi | 4.2006 (10) | P1—O2xli | 1.5638 (11) |
Cs1—O1vii | 4.1926 (9) | P1—O2xlii | 1.5638 (11) |
Cs1—O1viii | 4.1926 (9) | P1—O3 | 1.4757 (11) |
Cs1—O1ix | 3.3839 (15) | P1—H1xxxi | 2.2036 (18) |
Cs1—O1x | 3.3839 (15) | P1—H1xxxiii | 2.2036 (18) |
Cs1—O1xi | 3.2724 (11) | P1—H1xxxv | 2.2036 (18) |
Cs1—O1xii | 3.2724 (11) | P1—H1xxxvii | 4.2789 (17) |
Cs1—O2xiii | 3.2546 (8) | P1—H1xxxviii | 4.2789 (17) |
Cs1—O2xiv | 3.2546 (8) | P1—H1xxxix | 4.2789 (17) |
Cs1—O2xv | 3.2317 (12) | O1—O1xliii | 2.4185 (11) |
Cs1—O2xvi | 3.2317 (12) | O1—O1xliv | 2.4103 (13) |
Cs1—O2xvii | 4.1554 (11) | O1—O1xlv | 2.4103 (13) |
Cs1—O2xviii | 4.1554 (11) | O1—O2xlvi | 4.1345 (12) |
Cs1—O3v | 3.1724 (10) | O1—O2i | 2.5592 (12) |
Cs1—O3vi | 3.1724 (10) | O1—O2xlvii | 4.1576 (12) |
Cs1—H1xix | 4.0332 (18) | O1—O2xlviii | 3.2930 (11) |
Cs1—H1xx | 4.0332 (18) | O1—O2xlix | 3.9119 (12) |
Cs1—H1vii | 3.4283 (15) | O1—O2l | 3.3098 (12) |
Cs1—H1viii | 3.4283 (15) | O1—O3li | 3.6005 (12) |
Cs1—H1ix | 3.6633 (18) | O1—O3xxii | 3.6845 (12) |
Cs1—H1x | 3.6633 (18) | O1—O3lii | 3.9336 (13) |
Cs1—H1xi | 4.2143 (18) | O1—H1 | 1.5442 (18) |
Cs1—H1xii | 4.2143 (18) | O1—H1xliii | 3.3395 (17) |
S1—P1xxi | 4.0534 (8) | O1—H1liii | 4.0638 (18) |
S1—P1xxii | 4.0534 (8) | O1—H1liv | 3.7233 (17) |
S1—P1v | 4.0534 (8) | O1—H1xliv | 3.7447 (18) |
S1—P1vi | 4.0534 (8) | O1—H1xlv | 2.7017 (18) |
S1—O1xxiii | 1.4777 (9) | O2—O2lv | 2.4576 (12) |
S1—O1xxiv | 1.4777 (9) | O2—O2lvi | 2.4576 (12) |
S1—O1ix | 1.4777 (9) | O2—O2lvii | 4.0543 (12) |
S1—O1x | 1.4777 (9) | O2—O2lviii | 4.0543 (12) |
S1—O2xxv | 4.2022 (8) | O2—O3lix | 2.5619 (11) |
S1—O2xxvi | 4.2022 (8) | O2—O3lx | 4.4042 (12) |
S1—O2xxvii | 3.4684 (8) | O2—H1lxi | 3.3775 (18) |
S1—O2xxviii | 3.4684 (8) | O2—H1lxii | 1.0151 (18) |
S1—O2xxix | 4.2022 (8) | O2—H1lxiii | 2.9687 (18) |
S1—O2xxx | 4.2022 (8) | O2—H1lxiv | 3.5601 (17) |
S1—O2xvii | 3.4684 (8) | O2—H1lxv | 3.8069 (17) |
S1—O2xviii | 3.4684 (8) | O2—H1lxvi | 4.4161 (18) |
S1—O3xxi | 3.9600 (8) | O3—H1xxxi | 2.7426 (17) |
S1—O3xxii | 3.9600 (8) | O3—H1xxxiii | 2.7426 (17) |
S1—O3v | 3.9600 (8) | O3—H1xxxv | 2.7426 (17) |
S1—O3vi | 3.9600 (8) | O3—H1xxxvii | 4.2767 (17) |
S1—H1xxiii | 2.5556 (16) | O3—H1xxxviii | 4.2767 (17) |
S1—H1xxiv | 2.5556 (16) | O3—H1xxxix | 4.2767 (17) |
S1—H1ix | 2.5556 (16) | H1—H1lxvii | 3.806 (2) |
S1—H1x | 2.5556 (16) | H1—H1lxviii | 3.806 (2) |
P1—O1xxxi | 3.5371 (12) | H1—H1liii | 3.563 (2) |
P1—O1xxxii | 4.2919 (11) | H1—H1liv | 3.563 (2) |
P1—O1xxxiii | 3.5371 (12) | H1—H1xliv | 3.961 (2) |
P1—O1xxxiv | 4.2919 (11) | H1—H1xlv | 3.961 (2) |
S1—Cs1—S1i | 109.596 (15) | P1xxii—O1—P1lii | 104.19 (3) |
S1—Cs1—S1ii | 109.596 (15) | P1xxii—O1—O1xliii | 55.50 (3) |
S1—Cs1—P1iii | 111.98 (2) | P1xxii—O1—O1xliv | 106.09 (3) |
S1—Cs1—P1iv | 111.98 (2) | P1xxii—O1—O1xlv | 58.95 (3) |
S1—Cs1—P1v | 59.113 (18) | P1xxii—O1—O2xlvi | 137.67 (3) |
S1—Cs1—P1vi | 59.113 (18) | P1xxii—O1—O2i | 152.49 (4) |
S1—Cs1—O1vii | 94.30 (2) | P1xxii—O1—O2xlvii | 21.254 (16) |
S1—Cs1—O1viii | 94.30 (2) | P1xxii—O1—O2xlviii | 114.40 (3) |
S1—Cs1—O1ix | 20.938 (15) | P1xxii—O1—O2xlix | 90.27 (2) |
S1—Cs1—O1x | 20.938 (15) | P1xxii—O1—O2l | 79.15 (2) |
S1—Cs1—O1xi | 124.83 (2) | P1xxii—O1—O3li | 110.07 (3) |
S1—Cs1—O1xii | 124.83 (2) | P1xxii—O1—O3xxii | 19.472 (17) |
S1—Cs1—O2xiii | 92.93 (3) | P1xxii—O1—O3lii | 115.33 (3) |
S1—Cs1—O2xiv | 92.93 (3) | P1xxii—O1—H1 | 152.60 (7) |
S1—Cs1—O2xv | 131.98 (2) | P1xxii—O1—H1xliii | 30.43 (3) |
S1—Cs1—O2xvi | 131.98 (2) | P1xxii—O1—H1liii | 102.51 (3) |
S1—Cs1—O2xvii | 50.236 (17) | P1xxii—O1—H1liv | 129.32 (3) |
S1—Cs1—O2xviii | 50.236 (17) | P1xxii—O1—H1xliv | 96.55 (3) |
S1—Cs1—O3v | 65.72 (2) | P1xxii—O1—H1xlv | 71.37 (4) |
S1—Cs1—O3vi | 65.72 (2) | P1lii—O1—O1xliii | 126.35 (4) |
S1—Cs1—H1xix | 141.43 (2) | P1lii—O1—O1xliv | 86.93 (4) |
S1—Cs1—H1xx | 141.43 (2) | P1lii—O1—O1xlv | 67.27 (3) |
S1—Cs1—H1vii | 93.88 (3) | P1lii—O1—O2xlvi | 109.75 (3) |
S1—Cs1—H1viii | 93.88 (3) | P1lii—O1—O2i | 102.00 (3) |
S1—Cs1—H1ix | 38.58 (3) | P1lii—O1—O2xlvii | 113.22 (3) |
S1—Cs1—H1x | 38.58 (3) | P1lii—O1—O2xlviii | 25.12 (2) |
S1—Cs1—H1xi | 143.37 (2) | P1lii—O1—O2xlix | 106.41 (3) |
S1—Cs1—H1xii | 143.37 (2) | P1lii—O1—O2l | 25.13 (2) |
S1i—Cs1—S1ii | 140.81 (3) | P1lii—O1—O3li | 145.36 (3) |
S1i—Cs1—P1iii | 105.81 (2) | P1lii—O1—O3xxii | 108.93 (3) |
S1i—Cs1—P1iv | 58.437 (13) | P1lii—O1—O3lii | 22.027 (18) |
S1i—Cs1—P1v | 56.804 (11) | P1lii—O1—H1 | 102.00 (7) |
S1i—Cs1—P1vi | 153.107 (16) | P1lii—O1—H1xliii | 117.60 (4) |
S1i—Cs1—O1vii | 152.85 (3) | P1lii—O1—H1liii | 110.09 (3) |
S1i—Cs1—O1viii | 19.926 (12) | P1lii—O1—H1liv | 34.62 (3) |
S1i—Cs1—O1ix | 93.864 (17) | P1lii—O1—H1xliv | 100.42 (4) |
S1i—Cs1—O1x | 123.99 (2) | P1lii—O1—H1xlv | 36.46 (4) |
S1i—Cs1—O1xi | 125.34 (4) | O1xliii—O1—O1xliv | 59.89 (4) |
S1i—Cs1—O1xii | 15.961 (15) | O1xliii—O1—O1xlv | 59.89 (4) |
S1i—Cs1—O2xiii | 125.31 (2) | O1xliii—O1—O2xlvi | 83.75 (3) |
S1i—Cs1—O2xiv | 52.246 (16) | O1xliii—O1—O2i | 113.25 (4) |
S1i—Cs1—O2xv | 87.76 (2) | O1xliii—O1—O2xlvii | 34.44 (3) |
S1i—Cs1—O2xvi | 65.818 (18) | O1xliii—O1—O2xlviii | 151.31 (5) |
S1i—Cs1—O2xvii | 59.423 (12) | O1xliii—O1—O2xlix | 120.95 (4) |
S1i—Cs1—O2xviii | 159.68 (3) | O1xliii—O1—O2l | 109.19 (4) |
S1i—Cs1—O3v | 61.602 (15) | O1xliii—O1—O3li | 72.50 (3) |
S1i—Cs1—O3vi | 138.711 (15) | O1xliii—O1—O3xxii | 68.74 (3) |
S1i—Cs1—H1xix | 81.38 (3) | O1xliii—O1—O3lii | 115.28 (4) |
S1i—Cs1—H1xx | 68.00 (2) | O1xliii—O1—H1 | 113.00 (7) |
S1i—Cs1—H1vii | 139.53 (3) | O1xliii—O1—H1xliii | 25.19 (3) |
S1i—Cs1—H1viii | 36.28 (3) | O1xliii—O1—H1liii | 122.17 (5) |
S1i—Cs1—H1ix | 71.19 (2) | O1xliii—O1—H1liv | 156.98 (5) |
S1i—Cs1—H1x | 147.87 (4) | O1xliii—O1—H1xliv | 46.04 (4) |
S1i—Cs1—H1xi | 106.41 (3) | O1xliii—O1—H1xlv | 93.84 (5) |
S1i—Cs1—H1xii | 34.83 (2) | O1xliv—O1—O1xlv | 60.22 (4) |
S1ii—Cs1—P1iii | 58.437 (13) | O1xliv—O1—O2xlvi | 52.77 (3) |
S1ii—Cs1—P1iv | 105.81 (2) | O1xliv—O1—O2i | 83.46 (4) |
S1ii—Cs1—P1v | 153.107 (16) | O1xliv—O1—O2xlvii | 87.05 (3) |
S1ii—Cs1—P1vi | 56.804 (11) | O1xliv—O1—O2xlviii | 105.01 (4) |
S1ii—Cs1—O1vii | 19.926 (12) | O1xliv—O1—O2xlix | 155.92 (4) |
S1ii—Cs1—O1viii | 152.85 (3) | O1xliv—O1—O2l | 91.87 (4) |
S1ii—Cs1—O1ix | 123.99 (2) | O1xliv—O1—O3li | 79.04 (3) |
S1ii—Cs1—O1x | 93.864 (17) | O1xliv—O1—O3xxii | 124.51 (4) |
S1ii—Cs1—O1xi | 15.961 (15) | O1xliv—O1—O3lii | 66.02 (3) |
S1ii—Cs1—O1xii | 125.34 (4) | O1xliv—O1—H1 | 83.09 (7) |
S1ii—Cs1—O2xiii | 52.246 (16) | O1xliv—O1—H1xliii | 79.48 (4) |
S1ii—Cs1—O2xiv | 125.31 (2) | O1xliv—O1—H1liii | 141.76 (4) |
S1ii—Cs1—O2xv | 65.818 (18) | O1xliv—O1—H1liv | 99.99 (4) |
S1ii—Cs1—O2xvi | 87.76 (2) | O1xliv—O1—H1xliv | 14.86 (3) |
S1ii—Cs1—O2xvii | 159.68 (3) | O1xliv—O1—H1xlv | 81.36 (5) |
S1ii—Cs1—O2xviii | 59.423 (12) | O1xlv—O1—O2xlvi | 112.92 (4) |
S1ii—Cs1—O3v | 138.711 (15) | O1xlv—O1—O2i | 141.88 (5) |
S1ii—Cs1—O3vi | 61.602 (15) | O1xlv—O1—O2xlvii | 52.72 (3) |
S1ii—Cs1—H1xix | 68.00 (2) | O1xlv—O1—O2xlviii | 91.59 (4) |
S1ii—Cs1—H1xx | 81.38 (3) | O1xlv—O1—O2xlix | 143.29 (4) |
S1ii—Cs1—H1vii | 36.28 (3) | O1xlv—O1—O2l | 50.19 (3) |
S1ii—Cs1—H1viii | 139.53 (3) | O1xlv—O1—O3li | 127.95 (4) |
S1ii—Cs1—H1ix | 147.87 (4) | O1xlv—O1—O3xxii | 77.28 (3) |
S1ii—Cs1—H1x | 71.19 (2) | O1xlv—O1—O3lii | 63.98 (3) |
S1ii—Cs1—H1xi | 34.83 (2) | O1xlv—O1—H1 | 141.54 (8) |
S1ii—Cs1—H1xii | 106.41 (3) | O1xlv—O1—H1xliii | 53.11 (4) |
P1iii—Cs1—P1iv | 136.04 (4) | O1xlv—O1—H1liii | 157.75 (4) |
P1iii—Cs1—P1v | 101.069 (16) | O1xlv—O1—H1liv | 101.55 (4) |
P1iii—Cs1—P1vi | 101.085 (16) | O1xlv—O1—H1xliv | 61.26 (4) |
P1iii—Cs1—O1vii | 51.325 (17) | O1xlv—O1—H1xlv | 34.57 (4) |
P1iii—Cs1—O1viii | 124.66 (2) | O2xlvi—O1—O2i | 33.71 (2) |
P1iii—Cs1—O1ix | 131.40 (3) | O2xlvi—O1—O2xlvii | 117.84 (2) |
P1iii—Cs1—O1x | 92.17 (2) | O2xlvi—O1—O2xlviii | 106.99 (3) |
P1iii—Cs1—O1xi | 60.32 (2) | O2xlvi—O1—O2xlix | 103.31 (3) |
P1iii—Cs1—O1xii | 93.88 (3) | O2xlvi—O1—O2l | 130.56 (3) |
P1iii—Cs1—O2xiii | 22.409 (19) | O2xlvi—O1—O3li | 37.896 (19) |
P1iii—Cs1—O2xiv | 152.41 (4) | O2xlvi—O1—O3xxii | 140.87 (3) |
P1iii—Cs1—O2xv | 22.296 (19) | O2xlvi—O1—O3lii | 90.58 (2) |
P1iii—Cs1—O2xvi | 115.12 (4) | O2xlvi—O1—H1 | 33.36 (6) |
P1iii—Cs1—O2xvii | 122.111 (18) | O2xlvi—O1—H1xliii | 108.71 (3) |
P1iii—Cs1—O2xviii | 86.974 (17) | O2xlvi—O1—H1liii | 89.00 (3) |
P1iii—Cs1—O3v | 84.396 (19) | O2xlvi—O1—H1liv | 92.54 (3) |
P1iii—Cs1—O3vi | 113.917 (19) | O2xlvi—O1—H1xliv | 53.45 (3) |
P1iii—Cs1—H1xix | 31.99 (3) | O2xlvi—O1—H1xlv | 128.06 (5) |
P1iii—Cs1—H1xx | 105.24 (4) | O2i—O1—O2xlvii | 142.91 (4) |
P1iii—Cs1—H1vii | 33.73 (3) | O2i—O1—O2xlviii | 86.75 (3) |
P1iii—Cs1—H1viii | 141.35 (4) | O2i—O1—O2xlix | 74.31 (3) |
P1iii—Cs1—H1ix | 127.23 (3) | O2i—O1—O2l | 127.07 (4) |
P1iii—Cs1—H1x | 88.87 (3) | O2i—O1—O3li | 45.36 (3) |
P1iii—Cs1—H1xi | 63.03 (3) | O2i—O1—O3xxii | 138.42 (4) |
P1iii—Cs1—H1xii | 81.53 (3) | O2i—O1—O3lii | 92.16 (3) |
P1iv—Cs1—P1v | 101.085 (16) | O2i—O1—H1 | 0.37 (6) |
P1iv—Cs1—P1vi | 101.069 (16) | O2i—O1—H1xliii | 135.51 (4) |
P1iv—Cs1—O1vii | 124.66 (2) | O2i—O1—H1liii | 60.03 (3) |
P1iv—Cs1—O1viii | 51.325 (17) | O2i—O1—H1liv | 71.90 (4) |
P1iv—Cs1—O1ix | 92.17 (2) | O2i—O1—H1xliv | 86.80 (4) |
P1iv—Cs1—O1x | 131.40 (3) | O2i—O1—H1xlv | 136.12 (5) |
P1iv—Cs1—O1xi | 93.88 (3) | O2xlvii—O1—O2xlviii | 130.32 (3) |
P1iv—Cs1—O1xii | 60.32 (2) | O2xlvii—O1—O2xlix | 105.08 (3) |
P1iv—Cs1—O2xiii | 152.41 (4) | O2xlvii—O1—O2l | 88.91 (3) |
P1iv—Cs1—O2xiv | 22.409 (19) | O2xlvii—O1—O3li | 97.64 (3) |
P1iv—Cs1—O2xv | 115.12 (4) | O2xlvii—O1—O3xxii | 37.526 (19) |
P1iv—Cs1—O2xvi | 22.296 (19) | O2xlvii—O1—O3lii | 116.34 (3) |
P1iv—Cs1—O2xvii | 86.974 (17) | O2xlvii—O1—H1 | 142.79 (7) |
P1iv—Cs1—O2xviii | 122.111 (18) | O2xlvii—O1—H1xliii | 9.25 (3) |
P1iv—Cs1—O3v | 113.917 (19) | O2xlvii—O1—H1liii | 114.54 (3) |
P1iv—Cs1—O3vi | 84.396 (19) | O2xlvii—O1—H1liv | 145.18 (4) |
P1iv—Cs1—H1xix | 105.24 (4) | O2xlvii—O1—H1xliv | 76.08 (3) |
P1iv—Cs1—H1xx | 31.99 (3) | O2xlvii—O1—H1xlv | 76.93 (4) |
P1iv—Cs1—H1vii | 141.35 (4) | O2xlviii—O1—O2xlix | 83.18 (2) |
P1iv—Cs1—H1viii | 33.73 (3) | O2xlviii—O1—O2l | 43.70 (2) |
P1iv—Cs1—H1ix | 88.87 (3) | O2xlviii—O1—O3li | 131.75 (3) |
P1iv—Cs1—H1x | 127.23 (3) | O2xlviii—O1—O3xxii | 110.45 (3) |
P1iv—Cs1—H1xi | 81.53 (3) | O2xlviii—O1—O3lii | 40.32 (2) |
P1iv—Cs1—H1xii | 63.03 (3) | O2xlviii—O1—H1 | 86.88 (7) |
P1v—Cs1—P1vi | 118.23 (3) | O2xlviii—O1—H1xliii | 137.33 (4) |
P1v—Cs1—O1vii | 133.79 (2) | O2xlviii—O1—H1liii | 85.21 (3) |
P1v—Cs1—O1viii | 52.045 (16) | O2xlviii—O1—H1liv | 15.09 (3) |
P1v—Cs1—O1ix | 54.31 (2) | O2xlviii—O1—H1xliv | 119.75 (4) |
P1v—Cs1—O1x | 67.94 (2) | O2xlviii—O1—H1xlv | 58.38 (4) |
P1v—Cs1—O1xi | 161.38 (2) | O2xlix—O1—O2l | 108.79 (3) |
P1v—Cs1—O1xii | 68.818 (18) | O2xlix—O1—O3li | 78.77 (3) |
P1v—Cs1—O2xiii | 101.91 (2) | O2xlix—O1—O3xxii | 70.80 (2) |
P1v—Cs1—O2xiv | 81.14 (2) | O2xlix—O1—O3lii | 123.04 (3) |
P1v—Cs1—O2xv | 102.316 (18) | O2xlix—O1—H1 | 74.67 (7) |
P1v—Cs1—O2xvi | 118.256 (18) | O2xlix—O1—H1xliii | 110.10 (4) |
P1v—Cs1—O2xvii | 21.563 (16) | O2xlix—O1—H1liii | 14.46 (3) |
P1v—Cs1—O2xviii | 105.86 (3) | O2xlix—O1—H1liv | 82.03 (3) |
P1v—Cs1—O3v | 16.673 (19) | O2xlix—O1—H1xliv | 149.75 (4) |
P1v—Cs1—O3vi | 122.40 (4) | O2xlix—O1—H1xlv | 121.27 (4) |
P1v—Cs1—H1xix | 104.67 (2) | O2l—O1—O3li | 168.45 (4) |
P1v—Cs1—H1xx | 123.34 (3) | O2l—O1—O3xxii | 85.89 (3) |
P1v—Cs1—H1vii | 117.04 (3) | O2l—O1—O3lii | 40.28 (2) |
P1v—Cs1—H1viii | 67.36 (3) | O2l—O1—H1 | 127.08 (7) |
P1v—Cs1—H1ix | 31.61 (3) | O2l—O1—H1xliii | 94.43 (4) |
P1v—Cs1—H1x | 92.81 (4) | O2l—O1—H1liii | 118.28 (3) |
P1v—Cs1—H1xi | 154.68 (3) | O2l—O1—H1liv | 57.04 (3) |
P1v—Cs1—H1xii | 85.41 (2) | O2l—O1—H1xliv | 101.44 (4) |
P1vi—Cs1—O1vii | 52.045 (16) | O2l—O1—H1xlv | 15.62 (4) |
P1vi—Cs1—O1viii | 133.79 (2) | O3li—O1—O3xxii | 105.10 (3) |
P1vi—Cs1—O1ix | 67.94 (2) | O3li—O1—O3lii | 128.32 (3) |
P1vi—Cs1—O1x | 54.31 (2) | O3li—O1—H1 | 45.27 (6) |
P1vi—Cs1—O1xi | 68.818 (18) | O3li—O1—H1xliii | 90.92 (4) |
P1vi—Cs1—O1xii | 161.38 (2) | O3li—O1—H1liii | 67.52 (3) |
P1vi—Cs1—O2xiii | 81.14 (2) | O3li—O1—H1liv | 117.16 (4) |
P1vi—Cs1—O2xiv | 101.91 (2) | O3li—O1—H1xliv | 71.19 (3) |
P1vi—Cs1—O2xv | 118.256 (18) | O3li—O1—H1xlv | 159.91 (5) |
P1vi—Cs1—O2xvi | 102.316 (18) | O3xxii—O1—O3lii | 125.79 (3) |
P1vi—Cs1—O2xvii | 105.86 (3) | O3xxii—O1—H1 | 138.66 (8) |
P1vi—Cs1—O2xviii | 21.563 (16) | O3xxii—O1—H1xliii | 45.64 (3) |
P1vi—Cs1—O3v | 122.40 (4) | O3xxii—O1—H1liii | 83.22 (3) |
P1vi—Cs1—O3vi | 16.673 (19) | O3xxii—O1—H1liv | 123.44 (3) |
P1vi—Cs1—H1xix | 123.34 (3) | O3xxii—O1—H1xliv | 113.35 (3) |
P1vi—Cs1—H1xx | 104.67 (2) | O3xxii—O1—H1xlv | 82.54 (4) |
P1vi—Cs1—H1vii | 67.36 (3) | O3lii—O1—H1 | 92.04 (7) |
P1vi—Cs1—H1viii | 117.04 (3) | O3lii—O1—H1xliii | 116.95 (4) |
P1vi—Cs1—H1ix | 92.81 (4) | O3lii—O1—H1liii | 122.11 (3) |
P1vi—Cs1—H1x | 31.61 (3) | O3lii—O1—H1liv | 41.87 (3) |
P1vi—Cs1—H1xi | 85.41 (2) | O3lii—O1—H1xliv | 80.24 (3) |
P1vi—Cs1—H1xii | 154.68 (3) | O3lii—O1—H1xlv | 44.15 (4) |
O1vii—Cs1—O1viii | 171.39 (4) | H1—O1—H1xliii | 135.34 (7) |
O1vii—Cs1—O1ix | 112.25 (3) | H1—O1—H1liii | 60.39 (7) |
O1vii—Cs1—O1x | 76.20 (2) | H1—O1—H1liv | 72.02 (7) |
O1vii—Cs1—O1xi | 35.002 (19) | H1—O1—H1xliv | 86.43 (7) |
O1vii—Cs1—O1xii | 137.17 (4) | H1—O1—H1xlv | 136.03 (8) |
O1vii—Cs1—O2xiii | 37.60 (2) | H1xliii—O1—H1liii | 117.76 (4) |
O1vii—Cs1—O2xiv | 141.68 (2) | H1xliii—O1—H1liv | 151.47 (5) |
O1vii—Cs1—O2xv | 66.22 (2) | H1xliii—O1—H1xliv | 67.71 (4) |
O1vii—Cs1—O2xvi | 107.63 (3) | H1xliii—O1—H1xlv | 81.19 (5) |
O1vii—Cs1—O2xvii | 141.70 (3) | H1liii—O1—H1liv | 80.32 (3) |
O1vii—Cs1—O2xviii | 46.462 (16) | H1liii—O1—H1xliv | 138.31 (4) |
O1vii—Cs1—O3v | 121.27 (2) | H1liii—O1—H1xlv | 132.42 (5) |
O1vii—Cs1—O3vi | 62.778 (19) | H1liv—O1—H1xliv | 114.72 (4) |
O1vii—Cs1—H1xix | 71.77 (3) | H1liv—O1—H1xlv | 70.62 (5) |
O1vii—Cs1—H1xx | 101.27 (3) | H1xliv—O1—H1xlv | 88.73 (5) |
O1vii—Cs1—H1vii | 20.39 (3) | S1lxxiii—O2—S1lxxiv | 124.84 (2) |
O1vii—Cs1—H1viii | 158.00 (3) | S1lxxiii—O2—P1lix | 73.77 (4) |
O1vii—Cs1—H1ix | 132.47 (4) | S1lxxiii—O2—O1lxii | 111.43 (3) |
O1vii—Cs1—H1x | 56.09 (3) | S1lxxiii—O2—O1lxxv | 109.21 (2) |
O1vii—Cs1—H1xi | 52.90 (2) | S1lxxiii—O2—O1lxiii | 20.398 (13) |
O1vii—Cs1—H1xii | 118.87 (3) | S1lxxiii—O2—O1lxiv | 18.015 (18) |
O1viii—Cs1—O1ix | 76.20 (2) | S1lxxiii—O2—O1lxv | 112.80 (2) |
O1viii—Cs1—O1x | 112.25 (3) | S1lxxiii—O2—O1lxvi | 143.85 (3) |
O1viii—Cs1—O1xi | 137.17 (4) | S1lxxiii—O2—O2lv | 55.60 (3) |
O1viii—Cs1—O1xii | 35.002 (19) | S1lxxiii—O2—O2lvi | 110.25 (3) |
O1viii—Cs1—O2xiii | 141.68 (2) | S1lxxiii—O2—O2lvii | 117.31 (2) |
O1viii—Cs1—O2xiv | 37.60 (2) | S1lxxiii—O2—O2lviii | 49.640 (15) |
O1viii—Cs1—O2xv | 107.63 (3) | S1lxxiii—O2—O3lix | 66.63 (3) |
O1viii—Cs1—O2xvi | 66.22 (2) | S1lxxiii—O2—O3lx | 109.32 (2) |
O1viii—Cs1—O2xvii | 46.462 (16) | S1lxxiii—O2—H1lxi | 105.07 (3) |
O1viii—Cs1—O2xviii | 141.70 (3) | S1lxxiii—O2—H1lxii | 111.87 (10) |
O1viii—Cs1—O3v | 62.778 (19) | S1lxxiii—O2—H1lxiii | 36.94 (3) |
O1viii—Cs1—O3vi | 121.27 (2) | S1lxxiii—O2—H1lxiv | 37.30 (3) |
O1viii—Cs1—H1xix | 101.27 (3) | S1lxxiii—O2—H1lxv | 117.03 (3) |
O1viii—Cs1—H1xx | 71.77 (3) | S1lxxiii—O2—H1lxvi | 135.35 (3) |
O1viii—Cs1—H1vii | 158.00 (3) | S1lxxiv—O2—P1lix | 100.38 (5) |
O1viii—Cs1—H1viii | 20.39 (3) | S1lxxiv—O2—O1lxii | 22.55 (2) |
O1viii—Cs1—H1ix | 56.09 (3) | S1lxxiv—O2—O1lxxv | 19.821 (14) |
O1viii—Cs1—H1x | 132.47 (4) | S1lxxiv—O2—O1lxiii | 134.13 (3) |
O1viii—Cs1—H1xi | 118.87 (3) | S1lxxiv—O2—O1lxiv | 125.62 (3) |
O1viii—Cs1—H1xii | 52.90 (2) | S1lxxiv—O2—O1lxv | 100.05 (2) |
O1ix—Cs1—O1x | 41.88 (2) | S1lxxiv—O2—O1lxvi | 25.043 (16) |
O1ix—Cs1—O1xi | 136.70 (3) | S1lxxiv—O2—O2lv | 138.55 (3) |
O1ix—Cs1—O1xii | 109.81 (2) | S1lxxiv—O2—O2lvi | 88.62 (3) |
O1ix—Cs1—O2xiii | 113.66 (3) | S1lxxiv—O2—O2lvii | 67.398 (19) |
O1ix—Cs1—O2xiv | 72.18 (2) | S1lxxiv—O2—O2lviii | 89.05 (2) |
O1ix—Cs1—O2xv | 148.32 (3) | S1lxxiv—O2—O3lix | 80.57 (3) |
O1ix—Cs1—O2xvi | 113.48 (2) | S1lxxiv—O2—O3lx | 125.80 (2) |
O1ix—Cs1—O2xvii | 37.98 (2) | S1lxxiv—O2—H1lxi | 86.16 (3) |
O1ix—Cs1—O2xviii | 66.01 (3) | S1lxxiv—O2—H1lxii | 21.99 (9) |
O1ix—Cs1—O3v | 66.53 (3) | S1lxxiv—O2—H1lxiii | 139.25 (4) |
O1ix—Cs1—O3vi | 68.30 (3) | S1lxxiv—O2—H1lxiv | 101.65 (3) |
O1ix—Cs1—H1xix | 155.61 (3) | S1lxxiv—O2—H1lxv | 79.84 (3) |
O1ix—Cs1—H1xx | 123.35 (3) | S1lxxiv—O2—H1lxvi | 35.30 (2) |
O1ix—Cs1—H1vii | 114.51 (4) | P1lix—O2—O1lxii | 116.06 (5) |
O1ix—Cs1—H1viii | 73.24 (3) | P1lix—O2—O1lxxv | 84.21 (4) |
O1ix—Cs1—H1ix | 24.91 (3) | P1lix—O2—O1lxiii | 57.08 (4) |
O1ix—Cs1—H1x | 56.40 (3) | P1lix—O2—O1lxiv | 91.50 (5) |
O1ix—Cs1—H1xi | 150.99 (3) | P1lix—O2—O1lxv | 148.25 (5) |
O1ix—Cs1—H1xii | 128.65 (3) | P1lix—O2—O1lxvi | 90.88 (5) |
O1x—Cs1—O1xi | 109.81 (2) | P1lix—O2—O2lv | 38.21 (4) |
O1x—Cs1—O1xii | 136.70 (3) | P1lix—O2—O2lvi | 38.21 (4) |
O1x—Cs1—O2xiii | 72.18 (2) | P1lix—O2—O2lvii | 166.59 (5) |
O1x—Cs1—O2xiv | 113.66 (3) | P1lix—O2—O2lviii | 113.94 (5) |
O1x—Cs1—O2xv | 113.48 (2) | P1lix—O2—O3lix | 31.51 (4) |
O1x—Cs1—O2xvi | 148.32 (3) | P1lix—O2—O3lx | 96.06 (5) |
O1x—Cs1—O2xvii | 66.01 (3) | P1lix—O2—H1lxi | 31.60 (4) |
O1x—Cs1—O2xviii | 37.98 (2) | P1lix—O2—H1lxii | 115.76 (11) |
O1x—Cs1—O3v | 68.30 (3) | P1lix—O2—H1lxiii | 46.40 (5) |
O1x—Cs1—O3vi | 66.53 (3) | P1lix—O2—H1lxiv | 106.64 (5) |
O1x—Cs1—H1xix | 123.35 (3) | P1lix—O2—H1lxv | 166.88 (6) |
O1x—Cs1—H1xx | 155.61 (3) | P1lix—O2—H1lxvi | 74.73 (5) |
O1x—Cs1—H1vii | 73.24 (3) | O1lxii—O2—O1lxxv | 32.31 (2) |
O1x—Cs1—H1viii | 114.51 (4) | O1lxii—O2—O1lxiii | 127.44 (4) |
O1x—Cs1—H1ix | 56.40 (3) | O1lxii—O2—O1lxiv | 106.78 (4) |
O1x—Cs1—H1x | 24.91 (3) | O1lxii—O2—O1lxv | 91.16 (3) |
O1x—Cs1—H1xi | 128.65 (3) | O1lxii—O2—O1lxvi | 46.35 (3) |
O1x—Cs1—H1xii | 150.99 (3) | O1lxii—O2—O2lv | 150.44 (4) |
O1xi—Cs1—O1xii | 110.35 (4) | O1lxii—O2—O2lvi | 110.98 (4) |
O1xi—Cs1—O2xiii | 60.94 (2) | O1lxii—O2—O2lvii | 54.18 (3) |
O1xi—Cs1—O2xiv | 115.31 (3) | O1lxii—O2—O2lviii | 68.27 (3) |
O1xi—Cs1—O2xv | 60.83 (3) | O1lxii—O2—O3lix | 89.35 (4) |
O1xi—Cs1—O2xvi | 73.94 (3) | O1lxii—O2—O3lx | 133.45 (4) |
O1xi—Cs1—O2xvii | 174.68 (3) | O1lxii—O2—H1lxi | 107.88 (4) |
O1xi—Cs1—O2xviii | 74.627 (19) | O1lxii—O2—H1lxii | 0.56 (9) |
O1xi—Cs1—O3v | 144.71 (3) | O1lxii—O2—H1lxiii | 140.17 (5) |
O1xi—Cs1—O3vi | 69.72 (2) | O1lxii—O2—H1lxiv | 81.45 (4) |
O1xi—Cs1—H1xix | 60.22 (3) | O1lxii—O2—H1lxv | 68.38 (4) |
O1xi—Cs1—H1xx | 66.65 (3) | O1lxii—O2—H1lxvi | 57.85 (3) |
O1xi—Cs1—H1vii | 47.49 (3) | O1lxxv—O2—O1lxiii | 115.05 (3) |
O1xi—Cs1—H1viii | 126.76 (4) | O1lxxv—O2—O1lxiv | 115.17 (3) |
O1xi—Cs1—H1ix | 161.61 (4) | O1lxxv—O2—O1lxv | 119.44 (3) |
O1xi—Cs1—H1x | 86.79 (3) | O1lxxv—O2—O1lxvi | 35.41 (2) |
O1xi—Cs1—H1xi | 18.96 (3) | O1lxxv—O2—O2lv | 121.26 (3) |
O1xi—Cs1—H1xii | 91.67 (4) | O1lxxv—O2—O2lvi | 82.81 (3) |
O1xii—Cs1—O2xiii | 115.31 (3) | O1lxxv—O2—O2lvii | 84.80 (2) |
O1xii—Cs1—O2xiv | 60.94 (2) | O1lxxv—O2—O2lviii | 85.17 (2) |
O1xii—Cs1—O2xv | 73.94 (3) | O1lxxv—O2—O3lix | 61.17 (3) |
O1xii—Cs1—O2xvi | 60.83 (3) | O1lxxv—O2—O3lx | 139.88 (3) |
O1xii—Cs1—O2xvii | 74.627 (19) | O1lxxv—O2—H1lxi | 77.86 (3) |
O1xii—Cs1—O2xviii | 174.68 (3) | O1lxxv—O2—H1lxii | 31.93 (9) |
O1xii—Cs1—O3v | 69.72 (2) | O1lxxv—O2—H1lxiii | 119.49 (4) |
O1xii—Cs1—O3vi | 144.71 (3) | O1lxxv—O2—H1lxiv | 95.56 (3) |
O1xii—Cs1—H1xix | 66.65 (3) | O1lxxv—O2—H1lxv | 98.19 (3) |
O1xii—Cs1—H1xx | 60.22 (3) | O1lxxv—O2—H1lxvi | 36.58 (2) |
O1xii—Cs1—H1vii | 126.76 (4) | O1lxiii—O2—O1lxiv | 35.65 (2) |
O1xii—Cs1—H1viii | 47.49 (3) | O1lxiii—O2—O1lxv | 119.68 (3) |
O1xii—Cs1—H1ix | 86.79 (3) | O1lxiii—O2—O1lxvi | 142.74 (3) |
O1xii—Cs1—H1x | 161.61 (4) | O1lxiii—O2—O2lv | 35.31 (3) |
O1xii—Cs1—H1xi | 91.67 (4) | O1lxiii—O2—O2lvi | 91.12 (3) |
O1xii—Cs1—H1xii | 18.96 (3) | O1lxiii—O2—O2lvii | 135.37 (3) |
O2xiii—Cs1—O2xiv | 174.15 (5) | O1lxiii—O2—O2lviii | 70.00 (2) |
O2xiii—Cs1—O2xv | 44.53 (2) | O1lxiii—O2—O3lix | 59.68 (3) |
O2xiii—Cs1—O2xvi | 130.14 (4) | O1lxiii—O2—O3lx | 97.83 (2) |
O2xiii—Cs1—O2xvii | 119.18 (3) | O1lxiii—O2—H1lxi | 86.98 (3) |
O2xiii—Cs1—O2xviii | 65.02 (2) | O1lxiii—O2—H1lxii | 127.77 (10) |
O2xiii—Cs1—O3v | 86.50 (2) | O1lxiii—O2—H1lxiii | 16.62 (3) |
O2xiii—Cs1—O3vi | 95.91 (2) | O1lxiii—O2—H1lxiv | 57.67 (3) |
O2xiii—Cs1—H1xix | 53.94 (3) | O1lxiii—O2—H1lxv | 131.39 (3) |
O2xiii—Cs1—H1xx | 120.58 (4) | O1lxiii—O2—H1lxvi | 128.47 (3) |
O2xiii—Cs1—H1vii | 17.22 (3) | O1lxiv—O2—O1lxv | 96.05 (3) |
O2xiii—Cs1—H1viii | 161.49 (3) | O1lxiv—O2—O1lxvi | 149.89 (4) |
O2xiii—Cs1—H1ix | 118.62 (4) | O1lxiv—O2—O2lv | 68.51 (3) |
O2xiii—Cs1—H1x | 66.47 (3) | O1lxiv—O2—O2lvi | 126.75 (4) |
O2xiii—Cs1—H1xi | 71.18 (3) | O1lxiv—O2—O2lvii | 100.13 (3) |
O2xiii—Cs1—H1xii | 103.93 (3) | O1lxiv—O2—O2lviii | 39.07 (2) |
O2xiv—Cs1—O2xv | 130.14 (4) | O1lxiv—O2—O3lix | 83.42 (3) |
O2xiv—Cs1—O2xvi | 44.53 (2) | O1lxiv—O2—O3lx | 104.94 (3) |
O2xiv—Cs1—O2xvii | 65.02 (2) | O1lxiv—O2—H1lxi | 122.41 (4) |
O2xiv—Cs1—O2xviii | 119.18 (3) | O1lxiv—O2—H1lxii | 107.30 (10) |
O2xiv—Cs1—O3v | 95.91 (2) | O1lxiv—O2—H1lxiii | 50.80 (4) |
O2xiv—Cs1—O3vi | 86.50 (2) | O1lxiv—O2—H1lxiv | 25.66 (3) |
O2xiv—Cs1—H1xix | 120.58 (4) | O1lxiv—O2—H1lxv | 99.03 (3) |
O2xiv—Cs1—H1xx | 53.94 (3) | O1lxiv—O2—H1lxvi | 148.38 (3) |
O2xiv—Cs1—H1vii | 161.49 (3) | O1lxv—O2—O1lxvi | 97.56 (3) |
O2xiv—Cs1—H1viii | 17.22 (3) | O1lxv—O2—O2lv | 118.12 (4) |
O2xiv—Cs1—H1ix | 66.47 (3) | O1lxv—O2—O2lvi | 118.81 (4) |
O2xiv—Cs1—H1x | 118.62 (4) | O1lxv—O2—O2lvii | 37.425 (18) |
O2xiv—Cs1—H1xi | 103.93 (3) | O1lxv—O2—O2lviii | 90.43 (2) |
O2xiv—Cs1—H1xii | 71.18 (3) | O1lxv—O2—O3lix | 179.35 (4) |
O2xv—Cs1—O2xvi | 96.04 (4) | O1lxv—O2—O3lx | 52.190 (19) |
O2xv—Cs1—O2xvii | 123.434 (18) | O1lxv—O2—H1lxi | 127.30 (4) |
O2xv—Cs1—O2xviii | 107.739 (18) | O1lxv—O2—H1lxii | 91.31 (10) |
O2xv—Cs1—O3v | 86.89 (2) | O1lxv—O2—H1lxiii | 120.46 (4) |
O2xv—Cs1—O3vi | 127.17 (2) | O1lxv—O2—H1lxiv | 92.66 (3) |
O2xv—Cs1—H1xix | 9.90 (3) | O1lxv—O2—H1lxv | 23.03 (3) |
O2xv—Cs1—H1xx | 86.51 (4) | O1lxv—O2—H1lxvi | 110.71 (3) |
O2xv—Cs1—H1vii | 52.84 (3) | O1lxvi—O2—O2lv | 126.05 (4) |
O2xv—Cs1—H1viii | 120.89 (4) | O1lxvi—O2—O2lvi | 67.79 (3) |
O2xv—Cs1—H1ix | 133.52 (3) | O1lxvi—O2—O2lvii | 75.71 (2) |
O2xv—Cs1—H1x | 110.93 (3) | O1lxvi—O2—O2lviii | 114.05 (3) |
O2xv—Cs1—H1xi | 55.24 (3) | O1lxvi—O2—O3lix | 83.08 (3) |
O2xv—Cs1—H1xii | 59.78 (3) | O1lxvi—O2—O3lx | 104.64 (3) |
O2xvi—Cs1—O2xvii | 107.739 (18) | O1lxvi—O2—H1lxi | 67.66 (3) |
O2xvi—Cs1—O2xviii | 123.434 (18) | O1lxvi—O2—H1lxii | 45.79 (9) |
O2xvi—Cs1—O3v | 127.17 (2) | O1lxvi—O2—H1lxiii | 137.14 (4) |
O2xvi—Cs1—O3vi | 86.89 (2) | O1lxvi—O2—H1lxiv | 126.69 (4) |
O2xvi—Cs1—H1xix | 86.51 (4) | O1lxvi—O2—H1lxv | 83.94 (3) |
O2xvi—Cs1—H1xx | 9.90 (3) | O1lxvi—O2—H1lxvi | 16.20 (2) |
O2xvi—Cs1—H1vii | 120.89 (4) | O2lv—O2—O2lvi | 60.00 (3) |
O2xvi—Cs1—H1viii | 52.84 (3) | O2lv—O2—O2lvii | 153.87 (4) |
O2xvi—Cs1—H1ix | 110.93 (3) | O2lv—O2—O2lviii | 105.24 (3) |
O2xvi—Cs1—H1x | 133.52 (3) | O2lv—O2—O3lix | 61.34 (3) |
O2xvi—Cs1—H1xi | 59.78 (3) | O2lv—O2—O3lx | 73.80 (3) |
O2xvi—Cs1—H1xii | 55.24 (3) | O2lv—O2—H1lxi | 58.66 (4) |
O2xvii—Cs1—O2xviii | 100.47 (3) | O2lv—O2—H1lxii | 150.37 (11) |
O2xvii—Cs1—O3v | 38.03 (2) | O2lv—O2—H1lxiii | 18.69 (4) |
O2xvii—Cs1—O3vi | 105.17 (3) | O2lv—O2—H1lxiv | 92.58 (4) |
O2xvii—Cs1—H1xix | 124.60 (2) | O2lv—O2—H1lxv | 140.43 (4) |
O2xvii—Cs1—H1xx | 115.62 (2) | O2lv—O2—H1lxvi | 110.16 (4) |
O2xvii—Cs1—H1vii | 131.33 (4) | O2lvi—O2—O2lvii | 132.32 (4) |
O2xvii—Cs1—H1viii | 54.99 (3) | O2lvi—O2—O2lviii | 150.62 (4) |
O2xvii—Cs1—H1ix | 13.07 (3) | O2lvi—O2—O3lix | 61.34 (3) |
O2xvii—Cs1—H1x | 88.51 (4) | O2lvi—O2—O3lx | 73.80 (3) |
O2xvii—Cs1—H1xi | 165.31 (3) | O2lvi—O2—H1lxi | 8.55 (3) |
O2xvii—Cs1—H1xii | 93.40 (2) | O2lvi—O2—H1lxii | 110.44 (10) |
O2xviii—Cs1—O3v | 105.17 (3) | O2lvi—O2—H1lxiii | 76.34 (4) |
O2xviii—Cs1—O3vi | 38.03 (2) | O2lvi—O2—H1lxiv | 144.85 (4) |
O2xviii—Cs1—H1xix | 115.62 (2) | O2lvi—O2—H1lxv | 129.05 (4) |
O2xviii—Cs1—H1xx | 124.60 (2) | O2lvi—O2—H1lxvi | 53.64 (3) |
O2xviii—Cs1—H1vii | 54.99 (3) | O2lvii—O2—O2lviii | 72.68 (2) |
O2xviii—Cs1—H1viii | 131.33 (4) | O2lvii—O2—O3lix | 143.02 (4) |
O2xviii—Cs1—H1ix | 88.51 (4) | O2lvii—O2—O3lx | 87.43 (2) |
O2xviii—Cs1—H1x | 13.07 (3) | O2lvii—O2—H1lxi | 137.46 (4) |
O2xviii—Cs1—H1xi | 93.40 (2) | O2lvii—O2—H1lxii | 54.39 (9) |
O2xviii—Cs1—H1xii | 165.31 (3) | O2lvii—O2—H1lxiii | 146.97 (4) |
O3v—Cs1—O3vi | 131.44 (5) | O2lvii—O2—H1lxiv | 82.06 (3) |
O3v—Cs1—H1xix | 90.50 (3) | O2lvii—O2—H1lxv | 14.40 (3) |
O3v—Cs1—H1xx | 129.36 (3) | O2lvii—O2—H1lxvi | 91.86 (3) |
O3v—Cs1—H1vii | 102.58 (3) | O2lviii—O2—O3lix | 89.40 (3) |
O3v—Cs1—H1viii | 80.67 (3) | O2lviii—O2—O3lx | 129.44 (3) |
O3v—Cs1—H1ix | 46.63 (3) | O2lviii—O2—H1lxi | 142.23 (4) |
O3v—Cs1—H1x | 92.51 (4) | O2lviii—O2—H1lxii | 68.81 (10) |
O3v—Cs1—H1xi | 141.64 (3) | O2lviii—O2—H1lxiii | 86.58 (4) |
O3v—Cs1—H1xii | 82.87 (3) | O2lviii—O2—H1lxiv | 13.40 (3) |
O3vi—Cs1—H1xix | 129.36 (3) | O2lviii—O2—H1lxv | 79.16 (3) |
O3vi—Cs1—H1xx | 90.50 (3) | O2lviii—O2—H1lxvi | 121.47 (3) |
O3vi—Cs1—H1vii | 80.67 (3) | O3lix—O2—O3lx | 127.57 (3) |
O3vi—Cs1—H1viii | 102.58 (3) | O3lix—O2—H1lxi | 52.86 (3) |
O3vi—Cs1—H1ix | 92.51 (4) | O3lix—O2—H1lxii | 89.21 (10) |
O3vi—Cs1—H1x | 46.63 (3) | O3lix—O2—H1lxiii | 58.91 (4) |
O3vi—Cs1—H1xi | 82.87 (3) | O3lix—O2—H1lxiv | 87.02 (4) |
O3vi—Cs1—H1xii | 141.64 (3) | O3lix—O2—H1lxv | 157.42 (4) |
H1xix—Cs1—H1xx | 77.14 (4) | O3lix—O2—H1lxvi | 69.90 (3) |
H1xix—Cs1—H1vii | 60.70 (4) | O3lx—O2—H1lxi | 81.79 (3) |
H1xix—Cs1—H1viii | 112.55 (4) | O3lx—O2—H1lxii | 133.26 (10) |
H1xix—Cs1—H1ix | 136.26 (3) | O3lx—O2—H1lxiii | 86.37 (4) |
H1xix—Cs1—H1x | 120.00 (3) | O3lx—O2—H1lxiv | 122.22 (3) |
H1xix—Cs1—H1xi | 51.14 (3) | O3lx—O2—H1lxv | 73.75 (3) |
H1xix—Cs1—H1xii | 51.14 (3) | O3lx—O2—H1lxvi | 104.73 (3) |
H1xx—Cs1—H1vii | 112.55 (4) | H1lxi—O2—H1lxii | 107.37 (10) |
H1xx—Cs1—H1viii | 60.70 (4) | H1lxi—O2—H1lxiii | 73.38 (4) |
H1xx—Cs1—H1ix | 120.00 (3) | H1lxi—O2—H1lxiv | 137.63 (4) |
H1xx—Cs1—H1x | 136.26 (3) | H1lxi—O2—H1lxv | 136.20 (4) |
H1xx—Cs1—H1xi | 51.14 (3) | H1lxi—O2—H1lxvi | 52.37 (3) |
H1xx—Cs1—H1xii | 51.14 (3) | H1lxii—O2—H1lxiii | 140.36 (11) |
H1vii—Cs1—H1viii | 172.23 (5) | H1lxii—O2—H1lxiv | 81.98 (10) |
H1vii—Cs1—H1ix | 127.06 (4) | H1lxii—O2—H1lxv | 68.56 (10) |
H1vii—Cs1—H1x | 60.22 (4) | H1lxii—O2—H1lxvi | 57.29 (10) |
H1vii—Cs1—H1xi | 61.41 (3) | H1lxiii—O2—H1lxiv | 74.07 (4) |
H1vii—Cs1—H1xii | 111.70 (4) | H1lxiii—O2—H1lxv | 138.36 (5) |
H1viii—Cs1—H1ix | 60.22 (4) | H1lxiii—O2—H1lxvi | 121.07 (4) |
H1viii—Cs1—H1x | 127.06 (4) | H1lxiv—O2—H1lxv | 86.03 (4) |
H1viii—Cs1—H1xi | 111.70 (4) | H1lxiv—O2—H1lxvi | 132.12 (4) |
H1viii—Cs1—H1xii | 61.41 (3) | H1lxv—O2—H1lxvi | 99.50 (4) |
H1ix—Cs1—H1x | 77.15 (4) | S1lxix—O3—S1lxx | 118.53 (2) |
H1ix—Cs1—H1xi | 169.69 (3) | S1lxix—O3—S1lxxi | 118.53 (2) |
H1ix—Cs1—H1xii | 105.72 (3) | S1lxix—O3—P1 | 82.98 (4) |
H1x—Cs1—H1xi | 105.72 (3) | S1lxix—O3—O1xxxi | 135.82 (3) |
H1x—Cs1—H1xii | 169.69 (3) | S1lxix—O3—O1xxxii | 115.40 (2) |
H1xi—Cs1—H1xii | 73.26 (4) | S1lxix—O3—O1xxxiii | 96.89 (2) |
P1xxi—S1—P1xxii | 125.582 (16) | S1lxix—O3—O1xxxiv | 126.07 (3) |
P1xxi—S1—P1v | 102.068 (16) | S1lxix—O3—O1xxxv | 21.881 (14) |
P1xxi—S1—P1vi | 102.068 (16) | S1lxix—O3—O1xxxvi | 21.910 (14) |
P1xxi—S1—O1xxiii | 89.07 (4) | S1lxix—O3—O1xxxvii | 21.576 (13) |
P1xxi—S1—O1xxiv | 59.37 (3) | S1lxix—O3—O1xxxviii | 129.75 (2) |
P1xxi—S1—O1ix | 65.04 (4) | S1lxix—O3—O1xxxix | 99.28 (2) |
P1xxi—S1—O1x | 161.35 (3) | S1lxix—O3—O2xl | 76.94 (3) |
P1xxi—S1—O2xxv | 21.741 (16) | S1lxix—O3—O2xli | 59.77 (2) |
P1xxi—S1—O2xxvi | 144.290 (16) | S1lxix—O3—O2xlii | 115.09 (3) |
P1xxi—S1—O2xxvii | 22.301 (17) | S1lxix—O3—O2lxxvi | 104.58 (2) |
P1xxi—S1—O2xxviii | 124.666 (18) | S1lxix—O3—O2lxxvii | 78.296 (18) |
P1xxi—S1—O2xxix | 101.606 (16) | S1lxix—O3—O2lxxviii | 107.37 (2) |
P1xxi—S1—O2xxx | 85.164 (16) | S1lxix—O3—H1xxxi | 127.56 (4) |
P1xxi—S1—O2xvii | 80.930 (17) | S1lxix—O3—H1xxxiii | 86.47 (4) |
P1xxi—S1—O2xviii | 120.934 (17) | S1lxix—O3—H1xxxv | 39.87 (3) |
P1xxi—S1—O3xxi | 21.182 (16) | S1lxix—O3—H1xxxvii | 35.89 (2) |
P1xxi—S1—O3xxii | 107.920 (16) | S1lxix—O3—H1xxxviii | 150.89 (3) |
P1xxi—S1—O3v | 120.366 (16) | S1lxix—O3—H1xxxix | 82.74 (3) |
P1xxi—S1—O3vi | 96.848 (16) | S1lxx—O3—S1lxxi | 118.53 (2) |
P1xxi—S1—H1xxiii | 117.64 (4) | S1lxx—O3—P1 | 82.98 (4) |
P1xxi—S1—H1xxiv | 29.08 (4) | S1lxx—O3—O1xxxi | 21.881 (14) |
P1xxi—S1—H1ix | 77.02 (4) | S1lxx—O3—O1xxxii | 21.910 (14) |
P1xxi—S1—H1x | 129.39 (4) | S1lxx—O3—O1xxxiii | 135.82 (3) |
P1xxii—S1—P1v | 102.068 (16) | S1lxx—O3—O1xxxiv | 115.40 (2) |
P1xxii—S1—P1vi | 102.068 (16) | S1lxx—O3—O1xxxv | 96.89 (2) |
P1xxii—S1—O1xxiii | 59.37 (3) | S1lxx—O3—O1xxxvi | 126.07 (3) |
P1xxii—S1—O1xxiv | 89.07 (4) | S1lxx—O3—O1xxxvii | 129.75 (2) |
P1xxii—S1—O1ix | 161.35 (3) | S1lxx—O3—O1xxxviii | 99.28 (2) |
P1xxii—S1—O1x | 65.04 (4) | S1lxx—O3—O1xxxix | 21.576 (13) |
P1xxii—S1—O2xxv | 144.290 (16) | S1lxx—O3—O2xl | 115.09 (3) |
P1xxii—S1—O2xxvi | 21.741 (16) | S1lxx—O3—O2xli | 76.94 (3) |
P1xxii—S1—O2xxvii | 124.666 (18) | S1lxx—O3—O2xlii | 59.77 (2) |
P1xxii—S1—O2xxviii | 22.301 (17) | S1lxx—O3—O2lxxvi | 78.296 (18) |
P1xxii—S1—O2xxix | 85.164 (16) | S1lxx—O3—O2lxxvii | 107.37 (2) |
P1xxii—S1—O2xxx | 101.606 (16) | S1lxx—O3—O2lxxviii | 104.58 (2) |
P1xxii—S1—O2xvii | 120.934 (17) | S1lxx—O3—H1xxxi | 39.87 (3) |
P1xxii—S1—O2xviii | 80.930 (17) | S1lxx—O3—H1xxxiii | 127.56 (4) |
P1xxii—S1—O3xxi | 107.920 (16) | S1lxx—O3—H1xxxv | 86.47 (4) |
P1xxii—S1—O3xxii | 21.182 (16) | S1lxx—O3—H1xxxvii | 150.89 (3) |
P1xxii—S1—O3v | 96.848 (16) | S1lxx—O3—H1xxxviii | 82.74 (3) |
P1xxii—S1—O3vi | 120.366 (16) | S1lxx—O3—H1xxxix | 35.89 (2) |
P1xxii—S1—H1xxiii | 29.08 (4) | S1lxxi—O3—P1 | 82.98 (4) |
P1xxii—S1—H1xxiv | 117.64 (4) | S1lxxi—O3—O1xxxi | 96.89 (2) |
P1xxii—S1—H1ix | 129.39 (4) | S1lxxi—O3—O1xxxii | 126.07 (3) |
P1xxii—S1—H1x | 77.02 (4) | S1lxxi—O3—O1xxxiii | 21.881 (14) |
P1v—S1—P1vi | 125.582 (16) | S1lxxi—O3—O1xxxiv | 21.910 (14) |
P1v—S1—O1xxiii | 65.04 (4) | S1lxxi—O3—O1xxxv | 135.82 (3) |
P1v—S1—O1xxiv | 161.35 (3) | S1lxxi—O3—O1xxxvi | 115.40 (2) |
P1v—S1—O1ix | 59.37 (3) | S1lxxi—O3—O1xxxvii | 99.28 (2) |
P1v—S1—O1x | 89.07 (4) | S1lxxi—O3—O1xxxviii | 21.576 (13) |
P1v—S1—O2xxv | 85.164 (16) | S1lxxi—O3—O1xxxix | 129.75 (2) |
P1v—S1—O2xxvi | 101.606 (16) | S1lxxi—O3—O2xl | 59.77 (2) |
P1v—S1—O2xxvii | 120.934 (17) | S1lxxi—O3—O2xli | 115.09 (3) |
P1v—S1—O2xxviii | 80.930 (17) | S1lxxi—O3—O2xlii | 76.94 (3) |
P1v—S1—O2xxix | 21.741 (16) | S1lxxi—O3—O2lxxvi | 107.37 (2) |
P1v—S1—O2xxx | 144.290 (16) | S1lxxi—O3—O2lxxvii | 104.58 (2) |
P1v—S1—O2xvii | 22.301 (17) | S1lxxi—O3—O2lxxviii | 78.296 (18) |
P1v—S1—O2xviii | 124.666 (18) | S1lxxi—O3—H1xxxi | 86.47 (4) |
P1v—S1—O3xxi | 96.848 (16) | S1lxxi—O3—H1xxxiii | 39.87 (3) |
P1v—S1—O3xxii | 120.366 (16) | S1lxxi—O3—H1xxxv | 127.56 (4) |
P1v—S1—O3v | 21.182 (16) | S1lxxi—O3—H1xxxvii | 82.74 (3) |
P1v—S1—O3vi | 107.920 (16) | S1lxxi—O3—H1xxxviii | 35.89 (2) |
P1v—S1—H1xxiii | 77.02 (4) | S1lxxi—O3—H1xxxix | 150.89 (3) |
P1v—S1—H1xxiv | 129.39 (4) | P1—O3—O1xxxi | 75.67 (5) |
P1v—S1—H1ix | 29.08 (4) | P1—O3—O1xxxii | 104.19 (5) |
P1v—S1—H1x | 117.64 (4) | P1—O3—O1xxxiii | 75.67 (5) |
P1vi—S1—O1xxiii | 161.35 (3) | P1—O3—O1xxxiv | 104.19 (5) |
P1vi—S1—O1xxiv | 65.04 (4) | P1—O3—O1xxxv | 75.67 (5) |
P1vi—S1—O1ix | 89.07 (4) | P1—O3—O1xxxvi | 104.19 (5) |
P1vi—S1—O1x | 59.37 (3) | P1—O3—O1xxxvii | 69.36 (4) |
P1vi—S1—O2xxv | 101.606 (16) | P1—O3—O1xxxviii | 69.36 (4) |
P1vi—S1—O2xxvi | 85.164 (16) | P1—O3—O1xxxix | 69.36 (4) |
P1vi—S1—O2xxvii | 80.930 (17) | P1—O3—O2xl | 33.63 (4) |
P1vi—S1—O2xxviii | 120.934 (17) | P1—O3—O2xli | 33.63 (4) |
P1vi—S1—O2xxix | 144.290 (16) | P1—O3—O2xlii | 33.63 (4) |
P1vi—S1—O2xxx | 21.741 (16) | P1—O3—O2lxxvi | 161.21 (5) |
P1vi—S1—O2xvii | 124.666 (18) | P1—O3—O2lxxvii | 161.21 (5) |
P1vi—S1—O2xviii | 22.301 (17) | P1—O3—O2lxxviii | 161.21 (5) |
P1vi—S1—O3xxi | 120.366 (16) | P1—O3—H1xxxi | 53.24 (5) |
P1vi—S1—O3xxii | 96.848 (16) | P1—O3—H1xxxiii | 53.24 (5) |
P1vi—S1—O3v | 107.920 (16) | P1—O3—H1xxxv | 53.24 (5) |
P1vi—S1—O3vi | 21.182 (16) | P1—O3—H1xxxvii | 80.15 (5) |
P1vi—S1—H1xxiii | 129.39 (4) | P1—O3—H1xxxviii | 80.15 (5) |
P1vi—S1—H1xxiv | 77.02 (4) | P1—O3—H1xxxix | 80.15 (5) |
P1vi—S1—H1ix | 117.64 (4) | O1xxxi—O3—O1xxxii | 38.756 (19) |
P1vi—S1—H1x | 29.08 (4) | O1xxxi—O3—O1xxxiii | 114.09 (3) |
O1xxiii—S1—O1xxiv | 109.84 (5) | O1xxxi—O3—O1xxxiv | 96.77 (3) |
O1xxiii—S1—O1ix | 109.29 (5) | O1xxxi—O3—O1xxxv | 114.09 (3) |
O1xxiii—S1—O1x | 109.29 (5) | O1xxxi—O3—O1xxxvi | 147.57 (3) |
O1xxiii—S1—O2xxv | 94.27 (3) | O1xxxi—O3—O1xxxvii | 139.04 (3) |
O1xxiii—S1—O2xxvi | 77.21 (3) | O1xxxi—O3—O1xxxviii | 77.40 (2) |
O1xxiii—S1—O2xxvii | 107.44 (4) | O1xxxi—O3—O1xxxix | 36.98 (2) |
O1xxiii—S1—O2xxviii | 41.61 (3) | O1xxxi—O3—O2xl | 102.54 (3) |
O1xxiii—S1—O2xxix | 43.57 (4) | O1xxxi—O3—O2xli | 82.42 (3) |
O1xxiii—S1—O2xxx | 150.63 (4) | O1xxxi—O3—O2xlii | 45.30 (3) |
O1xxiii—S1—O2xvii | 71.46 (4) | O1xxxi—O3—O2lxxvi | 87.33 (2) |
O1xxiii—S1—O2xviii | 139.99 (3) | O1xxxi—O3—O2lxxvii | 119.52 (3) |
O1xxiii—S1—O3xxi | 68.50 (4) | O1xxxi—O3—O2lxxviii | 104.89 (3) |
O1xxiii—S1—O3xxii | 65.24 (3) | O1xxxi—O3—H1xxxi | 23.58 (4) |
O1xxiii—S1—O3v | 78.21 (4) | O1xxxi—O3—H1xxxiii | 109.36 (4) |
O1xxiii—S1—O3vi | 171.76 (4) | O1xxxi—O3—H1xxxv | 98.09 (4) |
O1xxiii—S1—H1xxiii | 33.06 (5) | O1xxxi—O3—H1xxxvii | 155.66 (3) |
O1xxiii—S1—H1xxiv | 108.83 (5) | O1xxxi—O3—H1xxxviii | 61.40 (3) |
O1xxiii—S1—H1ix | 79.20 (5) | O1xxxi—O3—H1xxxix | 55.98 (3) |
O1xxiii—S1—H1x | 134.65 (5) | O1xxxii—O3—O1xxxiii | 147.57 (3) |
O1xxiv—S1—O1ix | 109.29 (5) | O1xxxii—O3—O1xxxiv | 114.19 (3) |
O1xxiv—S1—O1x | 109.29 (5) | O1xxxii—O3—O1xxxv | 96.77 (3) |
O1xxiv—S1—O2xxv | 77.21 (3) | O1xxxii—O3—O1xxxvi | 114.19 (3) |
O1xxiv—S1—O2xxvi | 94.27 (3) | O1xxxii—O3—O1xxxvii | 133.71 (3) |
O1xxiv—S1—O2xxvii | 41.61 (3) | O1xxxii—O3—O1xxxviii | 111.72 (3) |
O1xxiv—S1—O2xxviii | 107.44 (4) | O1xxxii—O3—O1xxxix | 36.71 (2) |
O1xxiv—S1—O2xxix | 150.63 (4) | O1xxxii—O3—O2xl | 136.92 (4) |
O1xxiv—S1—O2xxx | 43.57 (4) | O1xxxii—O3—O2xli | 91.90 (3) |
O1xxiv—S1—O2xvii | 139.99 (3) | O1xxxii—O3—O2xlii | 81.31 (3) |
O1xxiv—S1—O2xviii | 71.46 (4) | O1xxxii—O3—O2lxxvi | 57.01 (2) |
O1xxiv—S1—O3xxi | 65.24 (3) | O1xxxii—O3—O2lxxvii | 85.46 (2) |
O1xxiv—S1—O3xxii | 68.50 (4) | O1xxxii—O3—O2lxxviii | 85.82 (2) |
O1xxiv—S1—O3v | 171.76 (4) | O1xxxii—O3—H1xxxi | 60.52 (4) |
O1xxiv—S1—O3vi | 78.21 (4) | O1xxxii—O3—H1xxxiii | 148.08 (4) |
O1xxiv—S1—H1xxiii | 108.83 (5) | O1xxxii—O3—H1xxxv | 94.79 (4) |
O1xxiv—S1—H1xxiv | 33.06 (5) | O1xxxii—O3—H1xxxvii | 151.02 (3) |
O1xxiv—S1—H1ix | 134.65 (5) | O1xxxii—O3—H1xxxviii | 91.75 (3) |
O1xxiv—S1—H1x | 79.20 (5) | O1xxxii—O3—H1xxxix | 38.78 (3) |
O1ix—S1—O1x | 109.84 (5) | O1xxxiii—O3—O1xxxiv | 38.756 (19) |
O1ix—S1—O2xxv | 43.57 (4) | O1xxxiii—O3—O1xxxv | 114.09 (3) |
O1ix—S1—O2xxvi | 150.63 (4) | O1xxxiii—O3—O1xxxvi | 96.77 (3) |
O1ix—S1—O2xxvii | 71.46 (4) | O1xxxiii—O3—O1xxxvii | 77.40 (2) |
O1ix—S1—O2xxviii | 139.99 (3) | O1xxxiii—O3—O1xxxviii | 36.98 (2) |
O1ix—S1—O2xxix | 77.21 (3) | O1xxxiii—O3—O1xxxix | 139.04 (3) |
O1ix—S1—O2xxx | 94.27 (3) | O1xxxiii—O3—O2xl | 45.30 (3) |
O1ix—S1—O2xvii | 41.61 (3) | O1xxxiii—O3—O2xli | 102.54 (3) |
O1ix—S1—O2xviii | 107.44 (4) | O1xxxiii—O3—O2xlii | 82.42 (3) |
O1ix—S1—O3xxi | 78.21 (4) | O1xxxiii—O3—O2lxxvi | 119.52 (3) |
O1ix—S1—O3xxii | 171.76 (4) | O1xxxiii—O3—O2lxxvii | 104.89 (3) |
O1ix—S1—O3v | 65.24 (3) | O1xxxiii—O3—O2lxxviii | 87.33 (2) |
O1ix—S1—O3vi | 68.50 (4) | O1xxxiii—O3—H1xxxi | 98.09 (4) |
O1ix—S1—H1xxiii | 134.65 (5) | O1xxxiii—O3—H1xxxiii | 23.58 (4) |
O1ix—S1—H1xxiv | 79.20 (5) | O1xxxiii—O3—H1xxxv | 109.36 (4) |
O1ix—S1—H1ix | 33.06 (5) | O1xxxiii—O3—H1xxxvii | 61.40 (3) |
O1ix—S1—H1x | 108.83 (5) | O1xxxiii—O3—H1xxxviii | 55.98 (3) |
O1x—S1—O2xxv | 150.63 (4) | O1xxxiii—O3—H1xxxix | 155.66 (3) |
O1x—S1—O2xxvi | 43.57 (4) | O1xxxiv—O3—O1xxxv | 147.57 (3) |
O1x—S1—O2xxvii | 139.99 (3) | O1xxxiv—O3—O1xxxvi | 114.19 (3) |
O1x—S1—O2xxviii | 71.46 (4) | O1xxxiv—O3—O1xxxvii | 111.72 (3) |
O1x—S1—O2xxix | 94.27 (3) | O1xxxiv—O3—O1xxxviii | 36.71 (2) |
O1x—S1—O2xxx | 77.21 (3) | O1xxxiv—O3—O1xxxix | 133.71 (3) |
O1x—S1—O2xvii | 107.44 (4) | O1xxxiv—O3—O2xl | 81.31 (3) |
O1x—S1—O2xviii | 41.61 (3) | O1xxxiv—O3—O2xli | 136.92 (4) |
O1x—S1—O3xxi | 171.76 (4) | O1xxxiv—O3—O2xlii | 91.90 (3) |
O1x—S1—O3xxii | 78.21 (4) | O1xxxiv—O3—O2lxxvi | 85.46 (2) |
O1x—S1—O3v | 68.50 (4) | O1xxxiv—O3—O2lxxvii | 85.82 (2) |
O1x—S1—O3vi | 65.24 (3) | O1xxxiv—O3—O2lxxviii | 57.01 (2) |
O1x—S1—H1xxiii | 79.20 (5) | O1xxxiv—O3—H1xxxi | 94.79 (4) |
O1x—S1—H1xxiv | 134.65 (5) | O1xxxiv—O3—H1xxxiii | 60.52 (4) |
O1x—S1—H1ix | 108.83 (5) | O1xxxiv—O3—H1xxxv | 148.08 (4) |
O1x—S1—H1x | 33.06 (5) | O1xxxiv—O3—H1xxxvii | 91.75 (3) |
O2xxv—S1—O2xxvi | 165.313 (15) | O1xxxiv—O3—H1xxxviii | 38.78 (3) |
O2xxv—S1—O2xxvii | 35.779 (18) | O1xxxiv—O3—H1xxxix | 151.02 (3) |
O2xxv—S1—O2xxviii | 135.369 (18) | O1xxxv—O3—O1xxxvi | 38.756 (19) |
O2xxv—S1—O2xxix | 90.936 (17) | O1xxxv—O3—O1xxxvii | 36.98 (2) |
O2xxv—S1—O2xxx | 90.936 (17) | O1xxxv—O3—O1xxxviii | 139.04 (3) |
O2xxv—S1—O2xvii | 62.962 (17) | O1xxxv—O3—O1xxxix | 77.40 (2) |
O2xxv—S1—O2xviii | 123.657 (17) | O1xxxv—O3—O2xl | 82.42 (3) |
O2xxv—S1—O3xxi | 36.433 (16) | O1xxxv—O3—O2xli | 45.30 (3) |
O2xxv—S1—O3xxii | 129.044 (16) | O1xxxv—O3—O2xlii | 102.54 (3) |
O2xxv—S1—O3v | 100.835 (16) | O1xxxv—O3—O2lxxvi | 104.89 (3) |
O2xxv—S1—O3vi | 89.236 (16) | O1xxxv—O3—O2lxxvii | 87.33 (2) |
O2xxv—S1—H1xxiii | 126.96 (4) | O1xxxv—O3—O2lxxviii | 119.52 (3) |
O2xxv—S1—H1xxiv | 44.28 (4) | O1xxxv—O3—H1xxxi | 109.36 (4) |
O2xxv—S1—H1ix | 57.58 (4) | O1xxxv—O3—H1xxxiii | 98.09 (4) |
O2xxv—S1—H1x | 130.60 (4) | O1xxxv—O3—H1xxxv | 23.58 (4) |
O2xxvi—S1—O2xxvii | 135.369 (18) | O1xxxv—O3—H1xxxvii | 55.98 (3) |
O2xxvi—S1—O2xxviii | 35.779 (18) | O1xxxv—O3—H1xxxviii | 155.66 (3) |
O2xxvi—S1—O2xxix | 90.936 (17) | O1xxxv—O3—H1xxxix | 61.40 (3) |
O2xxvi—S1—O2xxx | 90.936 (17) | O1xxxvi—O3—O1xxxvii | 36.71 (2) |
O2xxvi—S1—O2xvii | 123.657 (17) | O1xxxvi—O3—O1xxxviii | 133.71 (3) |
O2xxvi—S1—O2xviii | 62.962 (17) | O1xxxvi—O3—O1xxxix | 111.72 (3) |
O2xxvi—S1—O3xxi | 129.044 (16) | O1xxxvi—O3—O2xl | 91.90 (3) |
O2xxvi—S1—O3xxii | 36.433 (16) | O1xxxvi—O3—O2xli | 81.31 (3) |
O2xxvi—S1—O3v | 89.236 (16) | O1xxxvi—O3—O2xlii | 136.92 (4) |
O2xxvi—S1—O3vi | 100.835 (16) | O1xxxvi—O3—O2lxxvi | 85.82 (2) |
O2xxvi—S1—H1xxiii | 44.28 (4) | O1xxxvi—O3—O2lxxvii | 57.01 (2) |
O2xxvi—S1—H1xxiv | 126.96 (4) | O1xxxvi—O3—O2lxxviii | 85.46 (2) |
O2xxvi—S1—H1ix | 130.60 (4) | O1xxxvi—O3—H1xxxi | 148.08 (4) |
O2xxvi—S1—H1x | 57.58 (4) | O1xxxvi—O3—H1xxxiii | 94.79 (4) |
O2xxvii—S1—O2xxviii | 134.123 (19) | O1xxxvi—O3—H1xxxv | 60.52 (4) |
O2xxvii—S1—O2xxix | 123.657 (17) | O1xxxvi—O3—H1xxxvii | 38.78 (3) |
O2xxvii—S1—O2xxx | 62.962 (17) | O1xxxvi—O3—H1xxxviii | 151.02 (3) |
O2xxvii—S1—O2xvii | 98.737 (19) | O1xxxvi—O3—H1xxxix | 91.75 (3) |
O2xxvii—S1—O2xviii | 98.737 (19) | O1xxxvii—O3—O1xxxviii | 108.28 (3) |
O2xxvii—S1—O3xxi | 39.658 (18) | O1xxxvii—O3—O1xxxix | 108.28 (3) |
O2xxvii—S1—O3xxii | 103.729 (18) | O1xxxvii—O3—O2xl | 56.27 (3) |
O2xxvii—S1—O3v | 135.395 (18) | O1xxxvii—O3—O2xli | 56.64 (3) |
O2xxvii—S1—O3vi | 79.663 (18) | O1xxxvii—O3—O2xlii | 102.99 (3) |
O2xxvii—S1—H1xxiii | 129.75 (4) | O1xxxvii—O3—O2lxxvi | 122.49 (3) |
O2xxvii—S1—H1xxiv | 8.55 (4) | O1xxxvii—O3—O2lxxvii | 92.25 (2) |
O2xxvii—S1—H1ix | 93.04 (4) | O1xxxvii—O3—O2lxxviii | 115.13 (2) |
O2xxvii—S1—H1x | 107.24 (4) | O1xxxvii—O3—H1xxxi | 121.20 (4) |
O2xxviii—S1—O2xxix | 62.962 (17) | O1xxxvii—O3—H1xxxiii | 64.96 (4) |
O2xxviii—S1—O2xxx | 123.657 (17) | O1xxxvii—O3—H1xxxv | 43.33 (4) |
O2xxviii—S1—O2xvii | 98.737 (19) | O1xxxvii—O3—H1xxxvii | 21.15 (2) |
O2xxviii—S1—O2xviii | 98.737 (19) | O1xxxvii—O3—H1xxxviii | 129.38 (3) |
O2xxviii—S1—O3xxi | 103.729 (18) | O1xxxvii—O3—H1xxxix | 96.74 (3) |
O2xxviii—S1—O3xxii | 39.658 (18) | O1xxxviii—O3—O1xxxix | 108.28 (3) |
O2xxviii—S1—O3v | 79.663 (18) | O1xxxviii—O3—O2xl | 56.64 (3) |
O2xxviii—S1—O3vi | 135.395 (18) | O1xxxviii—O3—O2xli | 102.99 (3) |
O2xxviii—S1—H1xxiii | 8.55 (4) | O1xxxviii—O3—O2xlii | 56.27 (3) |
O2xxviii—S1—H1xxiv | 129.75 (4) | O1xxxviii—O3—O2lxxvi | 115.13 (2) |
O2xxviii—S1—H1ix | 107.24 (4) | O1xxxviii—O3—O2lxxvii | 122.49 (3) |
O2xxviii—S1—H1x | 93.04 (4) | O1xxxviii—O3—O2lxxviii | 92.25 (2) |
O2xxix—S1—O2xxx | 165.313 (15) | O1xxxviii—O3—H1xxxi | 64.96 (4) |
O2xxix—S1—O2xvii | 35.779 (18) | O1xxxviii—O3—H1xxxiii | 43.33 (4) |
O2xxix—S1—O2xviii | 135.369 (18) | O1xxxviii—O3—H1xxxv | 121.20 (4) |
O2xxix—S1—O3xxi | 89.236 (16) | O1xxxviii—O3—H1xxxvii | 96.74 (3) |
O2xxix—S1—O3xxii | 100.835 (16) | O1xxxviii—O3—H1xxxviii | 21.15 (2) |
O2xxix—S1—O3v | 36.433 (16) | O1xxxviii—O3—H1xxxix | 129.38 (3) |
O2xxix—S1—O3vi | 129.044 (16) | O1xxxix—O3—O2xl | 102.99 (3) |
O2xxix—S1—H1xxiii | 57.58 (4) | O1xxxix—O3—O2xli | 56.27 (3) |
O2xxix—S1—H1xxiv | 130.60 (4) | O1xxxix—O3—O2xlii | 56.64 (3) |
O2xxix—S1—H1ix | 44.28 (4) | O1xxxix—O3—O2lxxvi | 92.25 (2) |
O2xxix—S1—H1x | 126.96 (4) | O1xxxix—O3—O2lxxvii | 115.13 (2) |
O2xxx—S1—O2xvii | 135.369 (18) | O1xxxix—O3—O2lxxviii | 122.49 (3) |
O2xxx—S1—O2xviii | 35.779 (18) | O1xxxix—O3—H1xxxi | 43.33 (4) |
O2xxx—S1—O3xxi | 100.835 (16) | O1xxxix—O3—H1xxxiii | 121.20 (4) |
O2xxx—S1—O3xxii | 89.236 (16) | O1xxxix—O3—H1xxxv | 64.96 (4) |
O2xxx—S1—O3v | 129.044 (16) | O1xxxix—O3—H1xxxvii | 129.38 (3) |
O2xxx—S1—O3vi | 36.433 (16) | O1xxxix—O3—H1xxxviii | 96.74 (3) |
O2xxx—S1—H1xxiii | 130.60 (4) | O1xxxix—O3—H1xxxix | 21.15 (2) |
O2xxx—S1—H1xxiv | 57.58 (4) | O2xl—O3—O2xli | 57.32 (3) |
O2xxx—S1—H1ix | 126.96 (4) | O2xl—O3—O2xlii | 57.32 (3) |
O2xxx—S1—H1x | 44.28 (4) | O2xl—O3—O2lxxvi | 164.30 (4) |
O2xvii—S1—O2xviii | 134.123 (19) | O2xl—O3—O2lxxvii | 137.17 (3) |
O2xvii—S1—O3xxi | 79.663 (18) | O2xl—O3—O2lxxviii | 131.96 (3) |
O2xvii—S1—O3xxii | 135.395 (18) | O2xl—O3—H1xxxi | 79.01 (4) |
O2xvii—S1—O3v | 39.658 (18) | O2xl—O3—H1xxxiii | 21.72 (4) |
O2xvii—S1—O3vi | 103.729 (18) | O2xl—O3—H1xxxv | 67.96 (4) |
O2xvii—S1—H1xxiii | 93.04 (4) | O2xl—O3—H1xxxvii | 56.23 (3) |
O2xvii—S1—H1xxiv | 107.24 (4) | O2xl—O3—H1xxxviii | 75.86 (3) |
O2xvii—S1—H1ix | 8.55 (4) | O2xl—O3—H1xxxix | 111.89 (4) |
O2xvii—S1—H1x | 129.75 (4) | O2xli—O3—O2xlii | 57.32 (3) |
O2xviii—S1—O3xxi | 135.395 (18) | O2xli—O3—O2lxxvi | 137.17 (3) |
O2xviii—S1—O3xxii | 79.663 (18) | O2xli—O3—O2lxxvii | 131.96 (3) |
O2xviii—S1—O3v | 103.729 (18) | O2xli—O3—O2lxxviii | 164.30 (4) |
O2xviii—S1—O3vi | 39.658 (18) | O2xli—O3—H1xxxi | 67.96 (4) |
O2xviii—S1—H1xxiii | 107.24 (4) | O2xli—O3—H1xxxiii | 79.01 (4) |
O2xviii—S1—H1xxiv | 93.04 (4) | O2xli—O3—H1xxxv | 21.72 (4) |
O2xviii—S1—H1ix | 129.75 (4) | O2xli—O3—H1xxxvii | 75.86 (3) |
O2xviii—S1—H1x | 8.55 (4) | O2xli—O3—H1xxxviii | 111.89 (4) |
O3xxi—S1—O3xxii | 93.815 (17) | O2xli—O3—H1xxxix | 56.23 (3) |
O3xxi—S1—O3v | 117.822 (17) | O2xlii—O3—O2lxxvi | 131.96 (3) |
O3xxi—S1—O3vi | 117.822 (17) | O2xlii—O3—O2lxxvii | 164.30 (4) |
O3xxi—S1—H1xxiii | 96.50 (4) | O2xlii—O3—O2lxxviii | 137.17 (3) |
O3xxi—S1—H1xxiv | 43.46 (4) | O2xlii—O3—H1xxxi | 21.72 (4) |
O3xxi—S1—H1ix | 78.83 (4) | O2xlii—O3—H1xxxiii | 67.96 (4) |
O3xxi—S1—H1x | 143.75 (4) | O2xlii—O3—H1xxxv | 79.01 (4) |
O3xxii—S1—O3v | 117.822 (17) | O2xlii—O3—H1xxxvii | 111.89 (4) |
O3xxii—S1—O3vi | 117.822 (17) | O2xlii—O3—H1xxxviii | 56.23 (3) |
O3xxii—S1—H1xxiii | 43.46 (4) | O2xlii—O3—H1xxxix | 75.86 (3) |
O3xxii—S1—H1xxiv | 96.50 (4) | O2lxxvi—O3—O2lxxvii | 32.402 (16) |
O3xxii—S1—H1ix | 143.75 (4) | O2lxxvi—O3—O2lxxviii | 32.402 (16) |
O3xxii—S1—H1x | 78.83 (4) | O2lxxvi—O3—H1xxxi | 110.64 (4) |
O3v—S1—O3vi | 93.815 (17) | O2lxxvi—O3—H1xxxiii | 142.99 (4) |
O3v—S1—H1xxiii | 78.83 (4) | O2lxxvi—O3—H1xxxv | 123.26 (4) |
O3v—S1—H1xxiv | 143.75 (4) | O2lxxvi—O3—H1xxxvii | 116.13 (3) |
O3v—S1—H1ix | 43.46 (4) | O2lxxvi—O3—H1xxxviii | 98.89 (3) |
O3v—S1—H1x | 96.50 (4) | O2lxxvi—O3—H1xxxix | 83.73 (3) |
O3vi—S1—H1xxiii | 143.75 (4) | O2lxxvii—O3—O2lxxviii | 32.402 (16) |
O3vi—S1—H1xxiv | 78.83 (4) | O2lxxvii—O3—H1xxxi | 142.99 (4) |
O3vi—S1—H1ix | 96.50 (4) | O2lxxvii—O3—H1xxxiii | 123.26 (4) |
O3vi—S1—H1x | 43.46 (4) | O2lxxvii—O3—H1xxxv | 110.64 (4) |
H1xxiii—S1—H1xxiv | 126.72 (5) | O2lxxvii—O3—H1xxxvii | 83.73 (3) |
H1xxiii—S1—H1ix | 101.60 (5) | O2lxxvii—O3—H1xxxviii | 116.13 (3) |
H1xxiii—S1—H1x | 101.60 (5) | O2lxxvii—O3—H1xxxix | 98.89 (3) |
H1xxiv—S1—H1ix | 101.60 (5) | O2lxxviii—O3—H1xxxi | 123.26 (4) |
H1xxiv—S1—H1x | 101.60 (5) | O2lxxviii—O3—H1xxxiii | 110.64 (4) |
H1ix—S1—H1x | 126.72 (5) | O2lxxviii—O3—H1xxxv | 142.99 (4) |
S1lxix—P1—S1lxx | 114.220 (19) | O2lxxviii—O3—H1xxxvii | 98.89 (3) |
S1lxix—P1—S1lxxi | 114.220 (19) | O2lxxviii—O3—H1xxxviii | 83.73 (3) |
S1lxix—P1—O1xxxi | 134.66 (3) | O2lxxviii—O3—H1xxxix | 116.13 (3) |
S1lxix—P1—O1xxxii | 101.48 (2) | H1xxxi—O3—H1xxxiii | 87.87 (5) |
S1lxix—P1—O1xxxiii | 96.26 (2) | H1xxxi—O3—H1xxxv | 87.87 (5) |
S1lxix—P1—O1xxxiv | 109.46 (2) | H1xxxi—O3—H1xxxvii | 133.13 (5) |
S1lxix—P1—O1xxxv | 21.069 (14) | H1xxxi—O3—H1xxxviii | 56.01 (4) |
S1lxix—P1—O1xxxvi | 20.136 (13) | H1xxxi—O3—H1xxxix | 64.43 (4) |
S1lxix—P1—O1xxxvii | 21.335 (14) | H1xxxiii—O3—H1xxxv | 87.87 (5) |
S1lxix—P1—O1xxxviii | 134.94 (3) | H1xxxiii—O3—H1xxxvii | 56.01 (4) |
S1lxix—P1—O1xxxix | 101.97 (2) | H1xxxiii—O3—H1xxxviii | 64.43 (4) |
S1lxix—P1—O2xl | 84.49 (4) | H1xxxiii—O3—H1xxxix | 133.13 (5) |
S1lxix—P1—O2xli | 57.32 (4) | H1xxxv—O3—H1xxxvii | 64.43 (4) |
S1lxix—P1—O2xlii | 160.81 (5) | H1xxxv—O3—H1xxxviii | 133.13 (5) |
S1lxix—P1—O3 | 75.84 (4) | H1xxxv—O3—H1xxxix | 56.01 (4) |
S1lxix—P1—H1xxxi | 148.06 (5) | H1xxxvii—O3—H1xxxviii | 117.14 (3) |
S1lxix—P1—H1xxxiii | 91.86 (5) | H1xxxvii—O3—H1xxxix | 117.14 (3) |
S1lxix—P1—H1xxxv | 34.32 (4) | H1xxxviii—O3—H1xxxix | 117.14 (3) |
S1lxix—P1—H1xxxvii | 35.59 (2) | S1lxxii—H1—P1li | 116.60 (7) |
S1lxix—P1—H1xxxviii | 146.20 (3) | S1lxxii—H1—P1lii | 67.38 (3) |
S1lxix—P1—H1xxxix | 81.64 (3) | S1lxxii—H1—O1 | 31.47 (5) |
S1lxx—P1—S1lxxi | 114.220 (19) | S1lxxii—H1—O1xliii | 24.76 (2) |
S1lxx—P1—O1xxxi | 21.069 (14) | S1lxxii—H1—O1liii | 146.04 (6) |
S1lxx—P1—O1xxxii | 20.136 (13) | S1lxxii—H1—O1liv | 115.75 (5) |
S1lxx—P1—O1xxxiii | 134.66 (3) | S1lxxii—H1—O1xliv | 32.50 (3) |
S1lxx—P1—O1xxxiv | 101.48 (2) | S1lxxii—H1—O1xlv | 16.303 (19) |
S1lxx—P1—O1xxxv | 96.26 (2) | S1lxxii—H1—O2lxxix | 138.40 (6) |
S1lxx—P1—O1xxxvi | 109.46 (2) | S1lxxii—H1—O2xlvi | 98.77 (5) |
S1lxx—P1—O1xxxvii | 134.94 (3) | S1lxxii—H1—O2i | 149.45 (12) |
S1lxx—P1—O1xxxviii | 101.97 (2) | S1lxxii—H1—O2xlviii | 85.12 (4) |
S1lxx—P1—O1xxxix | 21.335 (14) | S1lxxii—H1—O2xlix | 111.02 (5) |
S1lxx—P1—O2xl | 160.81 (5) | S1lxxii—H1—O2l | 51.66 (3) |
S1lxx—P1—O2xli | 84.49 (4) | S1lxxii—H1—O3li | 96.67 (5) |
S1lxx—P1—O2xlii | 57.32 (4) | S1lxxii—H1—O3lii | 65.28 (3) |
S1lxx—P1—O3 | 75.84 (4) | S1lxxii—H1—H1lxvii | 142.48 (6) |
S1lxx—P1—H1xxxi | 34.32 (4) | S1lxxii—H1—H1lxviii | 92.50 (5) |
S1lxx—P1—H1xxxiii | 148.06 (5) | S1lxxii—H1—H1liii | 125.07 (6) |
S1lxx—P1—H1xxxv | 91.86 (5) | S1lxxii—H1—H1liv | 98.33 (5) |
S1lxx—P1—H1xxxvii | 146.20 (3) | S1lxxii—H1—H1xliv | 39.20 (3) |
S1lxx—P1—H1xxxviii | 81.64 (3) | S1lxxii—H1—H1xlv | 39.20 (3) |
S1lxx—P1—H1xxxix | 35.59 (2) | P1li—H1—P1lii | 151.45 (6) |
S1lxxi—P1—O1xxxi | 96.26 (2) | P1li—H1—O1 | 140.76 (10) |
S1lxxi—P1—O1xxxii | 109.46 (2) | P1li—H1—O1xliii | 99.43 (6) |
S1lxxi—P1—O1xxxiii | 21.069 (14) | P1li—H1—O1liii | 71.68 (5) |
S1lxxi—P1—O1xxxiv | 20.136 (13) | P1li—H1—O1liv | 112.25 (6) |
S1lxxi—P1—O1xxxv | 134.66 (3) | P1li—H1—O1xliv | 96.77 (6) |
S1lxxi—P1—O1xxxvi | 101.48 (2) | P1li—H1—O1xlv | 132.20 (6) |
S1lxxi—P1—O1xxxvii | 101.97 (2) | P1li—H1—O2lxxix | 21.83 (3) |
S1lxxi—P1—O1xxxviii | 21.335 (14) | P1li—H1—O2xlvi | 30.93 (3) |
S1lxxi—P1—O1xxxix | 134.94 (3) | P1li—H1—O2i | 39.73 (8) |
S1lxxi—P1—O2xl | 57.32 (4) | P1li—H1—O2xlviii | 150.73 (7) |
S1lxxi—P1—O2xli | 160.81 (5) | P1li—H1—O2xlix | 106.19 (6) |
S1lxxi—P1—O2xlii | 84.49 (4) | P1li—H1—O2l | 162.44 (6) |
S1lxxi—P1—O3 | 75.84 (4) | P1li—H1—O3li | 32.45 (3) |
S1lxxi—P1—H1xxxi | 91.86 (5) | P1li—H1—O3lii | 132.74 (6) |
S1lxxi—P1—H1xxxiii | 34.32 (4) | P1li—H1—H1lxvii | 30.28 (4) |
S1lxxi—P1—H1xxxv | 148.06 (5) | P1li—H1—H1lxviii | 30.28 (4) |
S1lxxi—P1—H1xxxvii | 81.64 (3) | P1li—H1—H1liii | 92.76 (6) |
S1lxxi—P1—H1xxxviii | 35.59 (2) | P1li—H1—H1liv | 134.36 (7) |
S1lxxi—P1—H1xxxix | 146.20 (3) | P1li—H1—H1xliv | 82.65 (5) |
O1xxxi—P1—O1xxxii | 34.298 (18) | P1li—H1—H1xlv | 153.08 (7) |
O1xxxi—P1—O1xxxiii | 117.33 (3) | P1lii—H1—O1 | 57.33 (6) |
O1xxxi—P1—O1xxxiv | 87.61 (3) | P1lii—H1—O1xliii | 91.01 (4) |
O1xxxi—P1—O1xxxv | 117.33 (3) | P1lii—H1—O1liii | 122.26 (4) |
O1xxxi—P1—O1xxxvi | 126.37 (3) | P1lii—H1—O1liv | 50.09 (2) |
O1xxxi—P1—O1xxxvii | 155.79 (3) | P1lii—H1—O1xliv | 71.89 (4) |
O1xxxi—P1—O1xxxviii | 81.59 (3) | P1lii—H1—O1xlv | 51.79 (3) |
O1xxxi—P1—O1xxxix | 38.94 (2) | P1lii—H1—O2lxxix | 143.53 (5) |
O1xxxi—P1—O2xl | 140.82 (5) | P1lii—H1—O2xlvi | 122.95 (5) |
O1xxxi—P1—O2xli | 101.14 (5) | P1lii—H1—O2i | 122.66 (11) |
O1xxxi—P1—O2xlii | 40.54 (4) | P1lii—H1—O2xlviii | 20.496 (19) |
O1xxxi—P1—O3 | 80.49 (5) | P1lii—H1—O2xlix | 97.40 (4) |
O1xxxi—P1—H1xxxi | 16.03 (4) | P1lii—H1—O2l | 20.643 (17) |
O1xxxi—P1—H1xxxiii | 128.31 (5) | P1lii—H1—O3li | 163.54 (6) |
O1xxxi—P1—H1xxxv | 112.23 (5) | P1lii—H1—O3lii | 19.865 (17) |
O1xxxi—P1—H1xxxvii | 160.27 (3) | P1lii—H1—H1lxvii | 149.14 (5) |
O1xxxi—P1—H1xxxviii | 61.80 (3) | P1lii—H1—H1lxviii | 127.30 (5) |
O1xxxi—P1—H1xxxix | 56.29 (3) | P1lii—H1—H1liii | 107.85 (5) |
O1xxxii—P1—O1xxxiii | 126.37 (3) | P1lii—H1—H1liv | 30.96 (3) |
O1xxxii—P1—O1xxxiv | 92.24 (2) | P1lii—H1—H1xliv | 87.59 (4) |
O1xxxii—P1—O1xxxv | 87.61 (3) | P1lii—H1—H1xlv | 30.71 (3) |
O1xxxii—P1—O1xxxvi | 92.24 (2) | O1—H1—O1xliii | 41.81 (5) |
O1xxxii—P1—O1xxxvii | 122.75 (3) | O1—H1—O1liii | 121.52 (8) |
O1xxxii—P1—O1xxxviii | 104.28 (3) | O1—H1—O1liv | 105.53 (7) |
O1xxxii—P1—O1xxxix | 34.11 (2) | O1—H1—O1xliv | 62.34 (6) |
O1xxxii—P1—O2xl | 166.71 (5) | O1—H1—O1xlv | 23.60 (5) |
O1xxxii—P1—O2xli | 89.58 (5) | O1—H1—O2lxxix | 159.03 (9) |
O1xxxii—P1—O2xlii | 74.53 (4) | O1—H1—O2xlvi | 130.02 (8) |
O1xxxii—P1—O3 | 56.33 (4) | O1—H1—O2i | 179.07 (15) |
O1xxxii—P1—H1xxxi | 50.14 (4) | O1—H1—O2xlviii | 67.46 (6) |
O1xxxii—P1—H1xxxiii | 142.35 (5) | O1—H1—O2xlix | 82.30 (7) |
O1xxxii—P1—H1xxxv | 88.52 (5) | O1—H1—O2l | 36.72 (5) |
O1xxxii—P1—H1xxxvii | 128.18 (3) | O1—H1—O3li | 111.16 (8) |
O1xxxii—P1—H1xxxviii | 83.90 (3) | O1—H1—O3lii | 66.81 (6) |
O1xxxii—P1—H1xxxix | 36.75 (2) | O1—H1—H1lxvii | 149.83 (9) |
O1xxxiii—P1—O1xxxiv | 34.298 (18) | O1—H1—H1lxviii | 122.96 (8) |
O1xxxiii—P1—O1xxxv | 117.33 (3) | O1—H1—H1liii | 97.48 (8) |
O1xxxiii—P1—O1xxxvi | 87.61 (3) | O1—H1—H1liv | 83.64 (7) |
O1xxxiii—P1—O1xxxvii | 81.59 (3) | O1—H1—H1xliv | 70.67 (7) |
O1xxxiii—P1—O1xxxviii | 38.94 (2) | O1—H1—H1xlv | 28.27 (6) |
O1xxxiii—P1—O1xxxix | 155.79 (3) | O1xliii—H1—O1liii | 126.41 (5) |
O1xxxiii—P1—O2xl | 40.54 (4) | O1xliii—H1—O1liv | 140.38 (5) |
O1xxxiii—P1—O2xli | 140.82 (5) | O1xliii—H1—O1xliv | 45.53 (3) |
O1xxxiii—P1—O2xlii | 101.14 (5) | O1xliii—H1—O1xlv | 39.26 (3) |
O1xxxiii—P1—O3 | 80.49 (5) | O1xliii—H1—O2lxxix | 120.27 (5) |
O1xxxiii—P1—H1xxxi | 112.23 (5) | O1xliii—H1—O2xlvi | 92.31 (4) |
O1xxxiii—P1—H1xxxiii | 16.03 (4) | O1xliii—H1—O2i | 138.82 (12) |
O1xxxiii—P1—H1xxxv | 128.31 (5) | O1xliii—H1—O2xlviii | 106.71 (5) |
O1xxxiii—P1—H1xxxvii | 61.80 (3) | O1xliii—H1—O2xlix | 101.89 (4) |
O1xxxiii—P1—H1xxxviii | 56.29 (3) | O1xliii—H1—O2l | 73.07 (3) |
O1xxxiii—P1—H1xxxix | 160.27 (3) | O1xliii—H1—O3li | 73.84 (4) |
O1xxxiv—P1—O1xxxv | 126.37 (3) | O1xliii—H1—O3lii | 90.01 (4) |
O1xxxiv—P1—O1xxxvi | 92.24 (2) | O1xliii—H1—H1lxvii | 119.75 (5) |
O1xxxiv—P1—O1xxxvii | 104.28 (3) | O1xliii—H1—H1lxviii | 83.56 (4) |
O1xxxiv—P1—O1xxxviii | 34.11 (2) | O1xliii—H1—H1liii | 112.17 (5) |
O1xxxiv—P1—O1xxxix | 122.75 (3) | O1xliii—H1—H1liv | 121.51 (5) |
O1xxxiv—P1—O2xl | 74.53 (4) | O1xliii—H1—H1xliv | 42.38 (3) |
O1xxxiv—P1—O2xli | 166.71 (5) | O1xliii—H1—H1xlv | 61.02 (4) |
O1xxxiv—P1—O2xlii | 89.58 (5) | O1liii—H1—O1liv | 87.13 (4) |
O1xxxiv—P1—O3 | 56.33 (4) | O1liii—H1—O1xliv | 165.68 (6) |
O1xxxiv—P1—H1xxxi | 88.52 (5) | O1liii—H1—O1xlv | 145.12 (5) |
O1xxxiv—P1—H1xxxiii | 50.14 (4) | O1liii—H1—O2lxxix | 55.31 (3) |
O1xxxiv—P1—H1xxxv | 142.35 (5) | O1liii—H1—O2xlvi | 100.14 (5) |
O1xxxiv—P1—H1xxxvii | 83.90 (3) | O1liii—H1—O2i | 57.61 (9) |
O1xxxiv—P1—H1xxxviii | 36.75 (2) | O1liii—H1—O2xlviii | 101.84 (4) |
O1xxxiv—P1—H1xxxix | 128.18 (3) | O1liii—H1—O2xlix | 39.72 (2) |
O1xxxv—P1—O1xxxvi | 34.298 (18) | O1liii—H1—O2l | 125.67 (4) |
O1xxxv—P1—O1xxxvii | 38.94 (2) | O1liii—H1—O3li | 73.18 (4) |
O1xxxv—P1—O1xxxviii | 155.79 (3) | O1liii—H1—O3lii | 135.49 (4) |
O1xxxv—P1—O1xxxix | 81.59 (3) | O1liii—H1—H1lxvii | 42.04 (3) |
O1xxxv—P1—O2xl | 101.14 (5) | O1liii—H1—H1lxviii | 101.86 (5) |
O1xxxv—P1—O2xli | 40.54 (4) | O1liii—H1—H1liii | 24.34 (3) |
O1xxxv—P1—O2xlii | 140.82 (5) | O1liii—H1—H1liv | 95.87 (5) |
O1xxxv—P1—O3 | 80.49 (5) | O1liii—H1—H1xliv | 150.07 (5) |
O1xxxv—P1—H1xxxi | 128.31 (5) | O1liii—H1—H1xlv | 134.24 (5) |
O1xxxv—P1—H1xxxiii | 112.23 (5) | O1liv—H1—O1xliv | 105.46 (5) |
O1xxxv—P1—H1xxxv | 16.03 (4) | O1liv—H1—O1xlv | 101.31 (4) |
O1xxxv—P1—H1xxxvii | 56.29 (3) | O1liv—H1—O2lxxix | 95.19 (4) |
O1xxxv—P1—H1xxxviii | 160.27 (3) | O1liv—H1—O2xlvi | 102.64 (5) |
O1xxxv—P1—H1xxxix | 61.80 (3) | O1liv—H1—O2i | 74.23 (9) |
O1xxxvi—P1—O1xxxvii | 34.11 (2) | O1liv—H1—O2xlviii | 38.52 (2) |
O1xxxvi—P1—O1xxxviii | 122.75 (3) | O1liv—H1—O2xlix | 91.79 (4) |
O1xxxvi—P1—O1xxxix | 104.28 (3) | O1liv—H1—O2l | 69.64 (3) |
O1xxxvi—P1—O2xl | 89.58 (5) | O1liv—H1—O3li | 143.30 (6) |
O1xxxvi—P1—O2xli | 74.53 (4) | O1liv—H1—O3lii | 51.07 (2) |
O1xxxvi—P1—O2xlii | 166.71 (5) | O1liv—H1—H1lxvii | 99.09 (4) |
O1xxxvi—P1—O3 | 56.33 (4) | O1liv—H1—H1lxviii | 112.27 (5) |
O1xxxvi—P1—H1xxxi | 142.35 (5) | O1liv—H1—H1liii | 90.12 (4) |
O1xxxvi—P1—H1xxxiii | 88.52 (5) | O1liv—H1—H1liv | 22.13 (3) |
O1xxxvi—P1—H1xxxv | 50.14 (4) | O1liv—H1—H1xliv | 117.41 (4) |
O1xxxvi—P1—H1xxxvii | 36.75 (2) | O1liv—H1—H1xlv | 80.76 (4) |
O1xxxvi—P1—H1xxxviii | 128.18 (3) | O1xliv—H1—O1xlv | 40.12 (3) |
O1xxxvi—P1—H1xxxix | 83.90 (3) | O1xliv—H1—O2lxxix | 115.52 (5) |
O1xxxvii—P1—O1xxxviii | 119.94 (3) | O1xliv—H1—O2xlvi | 70.83 (4) |
O1xxxvii—P1—O1xxxix | 119.94 (3) | O1xliv—H1—O2i | 118.59 (12) |
O1xxxvii—P1—O2xl | 63.37 (4) | O1xliv—H1—O2xlviii | 92.36 (5) |
O1xxxvii—P1—O2xli | 63.99 (4) | O1xliv—H1—O2xlix | 143.51 (6) |
O1xxxvii—P1—O2xlii | 156.53 (5) | O1xliv—H1—O2l | 66.50 (4) |
O1xxxvii—P1—O3 | 88.61 (5) | O1xliv—H1—O3li | 92.52 (5) |
O1xxxvii—P1—H1xxxi | 166.16 (5) | O1xliv—H1—O3lii | 58.68 (4) |
O1xxxvii—P1—H1xxxiii | 73.71 (5) | O1xliv—H1—H1lxvii | 127.04 (6) |
O1xxxvii—P1—H1xxxv | 46.77 (4) | O1xliv—H1—H1lxviii | 67.34 (4) |
O1xxxvii—P1—H1xxxvii | 20.67 (3) | O1xliv—H1—H1liii | 156.93 (7) |
O1xxxvii—P1—H1xxxviii | 137.53 (3) | O1xliv—H1—H1liv | 98.33 (5) |
O1xxxvii—P1—H1xxxix | 100.68 (3) | O1xliv—H1—H1xliv | 15.71 (3) |
O1xxxviii—P1—O1xxxix | 119.94 (3) | O1xliv—H1—H1xlv | 56.43 (4) |
O1xxxviii—P1—O2xl | 63.99 (4) | O1xlv—H1—O2lxxix | 153.66 (5) |
O1xxxviii—P1—O2xli | 156.53 (5) | O1xlv—H1—O2xlvi | 110.62 (5) |
O1xxxviii—P1—O2xlii | 63.37 (4) | O1xlv—H1—O2i | 157.26 (12) |
O1xxxviii—P1—O3 | 88.61 (5) | O1xlv—H1—O2xlviii | 68.89 (3) |
O1xxxviii—P1—H1xxxi | 73.71 (5) | O1xlv—H1—O2xlix | 105.70 (4) |
O1xxxviii—P1—H1xxxiii | 46.77 (4) | O1xlv—H1—O2l | 35.35 (2) |
O1xxxviii—P1—H1xxxv | 166.16 (5) | O1xlv—H1—O3li | 112.63 (5) |
O1xxxviii—P1—H1xxxvii | 100.68 (3) | O1xlv—H1—O3lii | 52.84 (3) |
O1xxxviii—P1—H1xxxviii | 20.67 (3) | O1xlv—H1—H1lxvii | 158.65 (5) |
O1xxxviii—P1—H1xxxix | 137.53 (3) | O1xlv—H1—H1lxviii | 105.84 (4) |
O1xxxix—P1—O2xl | 156.53 (5) | O1xlv—H1—H1liii | 120.98 (5) |
O1xxxix—P1—O2xli | 63.37 (4) | O1xlv—H1—H1liv | 82.56 (4) |
O1xxxix—P1—O2xlii | 63.99 (4) | O1xlv—H1—H1xliv | 51.27 (3) |
O1xxxix—P1—O3 | 88.61 (5) | O1xlv—H1—H1xlv | 22.90 (3) |
O1xxxix—P1—H1xxxi | 46.77 (4) | O2lxxix—H1—O2xlvi | 45.00 (3) |
O1xxxix—P1—H1xxxiii | 166.16 (5) | O2lxxix—H1—O2i | 21.09 (8) |
O1xxxix—P1—H1xxxv | 73.71 (5) | O2lxxix—H1—O2xlviii | 132.63 (5) |
O1xxxix—P1—H1xxxvii | 137.53 (3) | O2lxxix—H1—O2xlix | 94.05 (4) |
O1xxxix—P1—H1xxxviii | 100.68 (3) | O2lxxix—H1—O2l | 164.18 (5) |
O1xxxix—P1—H1xxxix | 20.67 (3) | O2lxxix—H1—O3li | 48.13 (3) |
O2xl—P1—O2xli | 103.59 (6) | O2lxxix—H1—O3lii | 131.76 (5) |
O2xl—P1—O2xlii | 103.59 (6) | O2lxxix—H1—H1lxvii | 14.75 (3) |
O2xl—P1—O3 | 114.86 (7) | O2lxxix—H1—H1lxviii | 48.37 (3) |
O2xl—P1—H1xxxi | 126.57 (7) | O2lxxix—H1—H1liii | 78.98 (4) |
O2xl—P1—H1xxxiii | 24.51 (5) | O2lxxix—H1—H1liv | 116.80 (5) |
O2xl—P1—H1xxxv | 102.67 (6) | O2lxxix—H1—H1xliv | 102.80 (5) |
O2xl—P1—H1xxxvii | 52.86 (4) | O2lxxix—H1—H1xlv | 168.84 (5) |
O2xl—P1—H1xxxviii | 84.63 (5) | O2xlvi—H1—O2i | 50.87 (9) |
O2xl—P1—H1xxxix | 156.45 (5) | O2xlvi—H1—O2xlviii | 132.96 (5) |
O2xli—P1—O2xlii | 103.59 (6) | O2xlvi—H1—O2xlix | 137.02 (5) |
O2xli—P1—O3 | 114.86 (7) | O2xlvi—H1—O2l | 131.95 (5) |
O2xli—P1—H1xxxi | 102.67 (6) | O2xlvi—H1—O3li | 53.12 (4) |
O2xli—P1—H1xxxiii | 126.57 (7) | O2xlvi—H1—O3lii | 103.19 (4) |
O2xli—P1—H1xxxv | 24.51 (5) | O2xlvi—H1—H1lxvii | 58.25 (4) |
O2xli—P1—H1xxxvii | 84.63 (5) | O2xlvi—H1—H1lxviii | 9.80 (3) |
O2xli—P1—H1xxxviii | 156.45 (5) | O2xlvi—H1—H1liii | 122.96 (6) |
O2xli—P1—H1xxxix | 52.86 (4) | O2xlvi—H1—H1liv | 120.73 (6) |
O2xlii—P1—O3 | 114.86 (7) | O2xlvi—H1—H1xliv | 59.81 (4) |
O2xlii—P1—H1xxxi | 24.51 (5) | O2xlvi—H1—H1xlv | 125.53 (5) |
O2xlii—P1—H1xxxiii | 102.67 (6) | O2i—H1—O2xlviii | 112.21 (11) |
O2xlii—P1—H1xxxv | 126.57 (7) | O2i—H1—O2xlix | 96.79 (10) |
O2xlii—P1—H1xxxvii | 156.45 (5) | O2i—H1—O2l | 143.23 (11) |
O2xlii—P1—H1xxxviii | 52.86 (4) | O2i—H1—O3li | 69.07 (9) |
O2xlii—P1—H1xxxix | 84.63 (5) | O2i—H1—O3lii | 113.49 (11) |
O3—P1—H1xxxi | 94.31 (6) | O2i—H1—H1lxvii | 29.84 (8) |
O3—P1—H1xxxiii | 94.31 (6) | O2i—H1—H1lxviii | 57.88 (9) |
O3—P1—H1xxxv | 94.31 (6) | O2i—H1—H1liii | 81.63 (10) |
O3—P1—H1xxxvii | 79.98 (5) | O2i—H1—H1liv | 96.07 (10) |
O3—P1—H1xxxviii | 79.98 (5) | O2i—H1—H1xliv | 110.25 (11) |
O3—P1—H1xxxix | 79.98 (5) | O2i—H1—H1xlv | 151.96 (12) |
H1xxxi—P1—H1xxxiii | 119.44 (7) | O2xlviii—H1—O2xlix | 81.34 (4) |
H1xxxi—P1—H1xxxv | 119.44 (7) | O2xlviii—H1—O2l | 33.78 (2) |
H1xxxi—P1—H1xxxvii | 172.21 (5) | O2xlviii—H1—O3li | 173.41 (6) |
H1xxxi—P1—H1xxxviii | 56.28 (5) | O2xlviii—H1—O3lii | 36.74 (2) |
H1xxxi—P1—H1xxxix | 66.64 (5) | O2xlviii—H1—H1lxvii | 132.40 (5) |
H1xxxiii—P1—H1xxxv | 119.44 (7) | O2xlviii—H1—H1lxviii | 140.35 (5) |
H1xxxiii—P1—H1xxxvii | 56.28 (5) | O2xlviii—H1—H1liii | 89.44 (4) |
H1xxxiii—P1—H1xxxviii | 66.64 (5) | O2xlviii—H1—H1liv | 16.39 (3) |
H1xxxiii—P1—H1xxxix | 172.21 (5) | O2xlviii—H1—H1xliv | 108.06 (5) |
H1xxxv—P1—H1xxxvii | 66.64 (5) | O2xlviii—H1—H1xlv | 46.12 (3) |
H1xxxv—P1—H1xxxviii | 172.21 (5) | O2xlix—H1—O2l | 91.03 (4) |
H1xxxv—P1—H1xxxix | 56.28 (5) | O2xlix—H1—O3li | 92.11 (4) |
H1xxxvii—P1—H1xxxviii | 117.04 (3) | O2xlix—H1—O3lii | 116.98 (4) |
H1xxxvii—P1—H1xxxix | 117.04 (3) | O2xlix—H1—H1lxvii | 79.74 (4) |
H1xxxviii—P1—H1xxxix | 117.04 (3) | O2xlix—H1—H1lxviii | 135.07 (5) |
S1lxxii—O1—P1li | 99.56 (4) | O2xlix—H1—H1liii | 15.38 (3) |
S1lxxii—O1—P1xxii | 70.79 (3) | O2xlix—H1—H1liv | 85.64 (4) |
S1lxxii—O1—P1lii | 93.62 (4) | O2xlix—H1—H1xliv | 144.18 (5) |
S1lxxii—O1—O1xliii | 35.08 (3) | O2xlix—H1—H1xlv | 96.46 (4) |
S1lxxii—O1—O1xliv | 35.36 (3) | O2l—H1—O3li | 146.69 (5) |
S1lxxii—O1—O1xlv | 35.36 (3) | O2l—H1—O3lii | 34.233 (19) |
S1lxxii—O1—O2xlvi | 82.39 (3) | O2l—H1—H1lxvii | 165.37 (5) |
S1lxxii—O1—O2i | 115.84 (5) | O2l—H1—H1lxviii | 132.19 (5) |
S1lxxii—O1—O2xlvii | 52.74 (3) | O2l—H1—H1liii | 104.76 (4) |
S1lxxii—O1—O2xlviii | 118.42 (5) | O2l—H1—H1liv | 48.65 (3) |
S1lxxii—O1—O2xlix | 155.46 (5) | O2l—H1—H1xliv | 81.30 (4) |
S1lxxii—O1—O2l | 83.50 (4) | O2l—H1—H1xlv | 12.45 (3) |
S1lxxii—O1—O3li | 92.88 (4) | O3li—H1—O3lii | 149.38 (5) |
S1lxxii—O1—O3xxii | 89.59 (4) | O3li—H1—H1lxvii | 46.06 (4) |
S1lxxii—O1—O3lii | 80.22 (4) | O3li—H1—H1lxviii | 46.06 (4) |
S1lxxii—O1—H1 | 115.48 (8) | O3li—H1—H1liii | 84.34 (5) |
S1lxxii—O1—H1xliii | 46.41 (4) | O3li—H1—H1liv | 164.63 (7) |
S1lxxii—O1—H1liii | 156.29 (5) | O3li—H1—H1xliv | 76.91 (4) |
S1lxxii—O1—H1liv | 121.93 (5) | O3li—H1—H1xlv | 134.86 (6) |
S1lxxii—O1—H1xliv | 29.04 (3) | O3lii—H1—H1lxvii | 143.32 (5) |
S1lxxii—O1—H1xlv | 68.31 (5) | O3lii—H1—H1lxviii | 107.49 (4) |
P1li—O1—P1xxii | 133.89 (3) | O3lii—H1—H1liii | 126.18 (5) |
P1li—O1—P1lii | 121.63 (3) | O3lii—H1—H1liv | 39.65 (3) |
P1li—O1—O1xliii | 90.20 (3) | O3lii—H1—H1xliv | 73.76 (4) |
P1li—O1—O1xliv | 73.78 (3) | O3lii—H1—H1xlv | 38.66 (3) |
P1li—O1—O1xlv | 133.07 (4) | H1lxvii—H1—H1lxviii | 60.00 (4) |
P1li—O1—O2xlvi | 21.784 (18) | H1lxvii—H1—H1liii | 64.93 (4) |
P1li—O1—O2i | 23.40 (2) | H1lxvii—H1—H1liv | 118.68 (5) |
P1li—O1—O2xlvii | 119.89 (3) | H1lxvii—H1—H1xliv | 112.78 (5) |
P1li—O1—O2xlviii | 109.72 (3) | H1lxvii—H1—H1xlv | 176.20 (6) |
P1li—O1—O2xlix | 82.14 (3) | H1lxviii—H1—H1liii | 122.73 (5) |
P1li—O1—O2l | 146.16 (3) | H1lxviii—H1—H1liv | 129.57 (6) |
P1li—O1—O3li | 23.843 (19) | H1lxviii—H1—H1xliv | 54.57 (4) |
P1li—O1—O3xxii | 127.60 (3) | H1lxviii—H1—H1xlv | 123.61 (5) |
P1li—O1—O3lii | 106.61 (3) | H1liii—H1—H1liv | 89.76 (5) |
P1li—O1—H1 | 23.21 (6) | H1liii—H1—H1xliv | 151.82 (6) |
P1li—O1—H1xliii | 112.15 (4) | H1liii—H1—H1xlv | 111.27 (5) |
P1li—O1—H1liii | 68.11 (3) | H1liv—H1—H1xliv | 113.29 (5) |
P1li—O1—H1liv | 94.70 (3) | H1liv—H1—H1xlv | 60.50 (4) |
P1li—O1—H1xliv | 71.91 (3) | H1xliv—H1—H1xlv | 70.44 (4) |
P1li—O1—H1xlv | 148.51 (5) |
Symmetry codes: (i) y, z, x; (ii) −y, z−1/2, −x+1/2; (iii) x−1, y−1, z−1; (iv) x−1, −y+1, −z+3/2; (v) y−3/4, x−3/4, z−3/4; (vi) y−3/4, −x+3/4, −z+5/4; (vii) z, x−1, y; (viii) z, −x+1, −y+1/2; (ix) y+1/4, x−3/4, z+1/4; (x) y+1/4, −x+3/4, −z+1/4; (xi) −x+3/4, z−1/4, −y+1/4; (xii) −x+3/4, −z+1/4, y+1/4; (xiii) x, y−1, z; (xiv) x, −y+1, −z+1/2; (xv) y−1, z, x; (xvi) y−1, −z, −x+1/2; (xvii) z+1/4, y−3/4, x+1/4; (xviii) z+1/4, −y+3/4, −x+1/4; (xix) x−1, y, z; (xx) x−1, −y, −z+1/2; (xxi) −x+3/2, −y+1, z−1/2; (xxii) −x+3/2, y−1, −z+1; (xxiii) −y+1/2, z, −x+1; (xxiv) −y+1/2, −z, x−1/2; (xxv) −x+1/2, −y+1, z+1/2; (xxvi) −x+1/2, y−1, −z; (xxvii) −z+1/2, −x, y−1/2; (xxviii) −z+1/2, x, −y+1; (xxix) x+1/4, z+1/4, y−3/4; (xxx) x+1/4, −z−1/4, −y+5/4; (xxxi) x, y+1, z+1; (xxxii) −x+3/2, y+1, −z+1; (xxxiii) z+1, x, y+1; (xxxiv) −z+1, −x+3/2, y+1; (xxxv) y+1, z+1, x; (xxxvi) y+1, −z+1, −x+3/2; (xxxvii) −y+5/4, −x+7/4, z+3/4; (xxxviii) −x+7/4, z+3/4, −y+5/4; (xxxix) z+3/4, −y+5/4, −x+7/4; (xl) x+1, y, z+1; (xli) z+1, x+1, y; (xlii) y, z+1, x+1; (xliii) −x+3/2, y, −z; (xliv) z+3/4, −y+1/4, −x+3/4; (xlv) −z+3/4, −y+1/4, x−3/4; (xlvi) z+1, x, y−1; (xlvii) −y+3/2, z, −x; (xlviii) −y+7/4, −x+1/4, z+1/4; (xlix) −y+7/4, x−1/4, −z+1/4; (l) −x+3/4, −z+1/4, y−3/4; (li) x, y−1, z−1; (lii) −y+7/4, −x+5/4, z−3/4; (liii) −x+7/4, z−1/4, −y+1/4; (liv) −x+7/4, −z+1/4, y+1/4; (lv) z, x+1, y−1; (lvi) y−1, z+1, x; (lvii) z+1/4, −y+7/4, −x+1/4; (lviii) −z+1/4, −y+7/4, x−1/4; (lix) x−1, y, z−1; (lx) y−3/4, x+1/4, z−3/4; (lxi) x−1, y+1, z; (lxii) z, x, y; (lxiii) y, z+1, x−1; (lxiv) −y+1/4, −x+7/4, z−1/4; (lxv) y+1/4, −x+7/4, −z+1/4; (lxvi) −x+3/4, z+3/4, −y+1/4; (lxvii) z+1, x−1, y; (lxviii) y+1, z, x−1; (lxix) −x+3/2, −y+1, z+1/2; (lxx) z+1/2, −x+3/2, −y+1; (lxxi) −y+1, z+1/2, −x+3/2; (lxxii) z+1/2, −x+1/2, −y; (lxxiii) −x+1/2, −y+1, z−1/2; (lxxiv) −y, z+1/2, −x+1/2; (lxxv) −z, −x+3/2, y; (lxxvi) y−1/4, x+3/4, z+3/4; (lxxvii) x+3/4, z+3/4, y−1/4; (lxxviii) z+3/4, y−1/4, x+3/4; (lxxix) x+1, y−1, z. |