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Crystals of Cs6(SO4)3(H3PO4)4 belong to the family of alkali metal acid salts that show a high protonic conductivity at relatively low temperatures. Such properties make superprotonic crystals an excellent choice for the study of the influence of the hydrogen subsystem on the physicochemical properties and promising materials for energy-efficient technologies. Single crystals of Cs6(SO4)3(H3PO4)4 were studied by neutron diffraction methods, optical polarization microscopy, scanning electron microscopy and energy-dispersive X-ray spectroscopy. Neutron diffraction studies made it possible to determine the positions of all the atoms with high accuracy, including the H atom on a hydrogen bond characterized by a single-minimum potential, to confirm the chemical com­position of the Cs6(SO4)3(H3PO4)4 crystals and their cubic symmetry in low- and high-temperature phases, and to draw conclusions about the three-dimensional system of hydrogen bonds, which is fundamentally different in com­parison with other superprotonic com­pounds. Based on the experimental data obtained, crystal transformations with temperature changes are reported, and the stability of the chemical com­position is shown.

Supporting information

cif

Crystallographic Information File (CIF) https://doi.org/10.1107/S2052520621001840/yh5010sup1.cif
Contains datablocks global, I

hkl

Structure factor file (CIF format) https://doi.org/10.1107/S2052520621001840/yh5010Isup2.hkl
Contains datablock I

CCDC reference: 2063134

Computing details top

(I) top
Crystal data top
Cs6H12O28P4S3Dx = 3.190 Mg m3
Mr = 1477.6Neutron radiation, λ = 1.455 Å
Cubic, I43dCell parameters from 2078 reflections
Hall symbol: I -4bd 2c 3θ = 7.0–59.6°
a = 14.5549 (6) ŵ = 0.0 mm1
V = 3083.4 (4) Å3T = 290 K
Z = 4, colourless
F(000) = 716.7882.45 × 2.43 × 2.42 × 1.22 (radius) mm
Data collection top
DiffractometerRint = 0.017
Radiation source: neutronθmax = 59.6°, θmin = 7.0°
2078 measured reflectionsh = 1311
437 independent reflectionsk = 017
434 reflections with I > 3σ(I)l = 913
Refinement top
Refinement on FAll H-atom parameters refined
R[F2 > 2σ(F2)] = 0.017Weighting scheme based on measured s.u.'s w = 1/(σ2(F) + 0.0001F2)
wR(F2) = 0.024(Δ/σ)max = 0.008
S = 1.92Δρmax = 0.12 e Å3
434 reflectionsΔρmin = 0.15 e Å3
42 parametersExtinction correction: B-C type 1 Lorentzian isotropic (Becker & Coppens, 1974)
0 restraintsExtinction coefficient: 780 (60)
0 constraintsAbsolute structure: 185 of Friedel pairs used in the refinement
Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) top
xyzUiso*/Ueq
Cs10.09951 (8)00.250.0277 (3)
S10.37500.250.0232 (6)
P10.99766 (6)0.99766 (6)0.99766 (6)0.0225 (2)
O10.77889 (6)0.06665 (7)0.07790 (5)0.0323 (3)
O20.08810 (5)0.95100 (6)0.03212 (6)0.0281 (3)
O30.93913 (6)0.93913 (6)0.93913 (6)0.0307 (2)
H10.88285 (11)0.04628 (10)0.08356 (10)0.0378 (5)
Atomic displacement parameters (Å2) top
U11U22U33U12U13U23
Cs10.0303 (6)0.0297 (6)0.0230 (5)000.0006 (5)
S10.0291 (14)0.0203 (9)0.0203 (9)000
P10.0225 (3)0.0225 (3)0.0225 (3)0.0009 (4)0.0009 (4)0.0009 (4)
O10.0273 (4)0.0426 (5)0.0270 (4)0.0054 (4)0.0038 (3)0.0088 (4)
O20.0219 (4)0.0274 (5)0.0351 (5)0.0006 (3)0.0010 (3)0.0034 (3)
O30.0307 (3)0.0307 (3)0.0307 (3)0.0044 (3)0.0044 (3)0.0044 (3)
H10.0372 (10)0.0412 (8)0.0350 (7)0.0008 (7)0.0037 (6)0.0001 (6)
Geometric parameters (Å, º) top
Cs1—S14.0097 (12)P1—O1xxxv3.5371 (12)
Cs1—S1i4.3183 (4)P1—O1xxxvi4.2919 (11)
Cs1—S1ii4.3183 (4)P1—O1xxxvii3.6823 (12)
Cs1—P1iii3.9607 (9)P1—O1xxxviii3.6823 (12)
Cs1—P1iv3.9607 (9)P1—O1xxxix3.6823 (12)
Cs1—P1v4.2006 (10)P1—O2xl1.5638 (11)
Cs1—P1vi4.2006 (10)P1—O2xli1.5638 (11)
Cs1—O1vii4.1926 (9)P1—O2xlii1.5638 (11)
Cs1—O1viii4.1926 (9)P1—O31.4757 (11)
Cs1—O1ix3.3839 (15)P1—H1xxxi2.2036 (18)
Cs1—O1x3.3839 (15)P1—H1xxxiii2.2036 (18)
Cs1—O1xi3.2724 (11)P1—H1xxxv2.2036 (18)
Cs1—O1xii3.2724 (11)P1—H1xxxvii4.2789 (17)
Cs1—O2xiii3.2546 (8)P1—H1xxxviii4.2789 (17)
Cs1—O2xiv3.2546 (8)P1—H1xxxix4.2789 (17)
Cs1—O2xv3.2317 (12)O1—O1xliii2.4185 (11)
Cs1—O2xvi3.2317 (12)O1—O1xliv2.4103 (13)
Cs1—O2xvii4.1554 (11)O1—O1xlv2.4103 (13)
Cs1—O2xviii4.1554 (11)O1—O2xlvi4.1345 (12)
Cs1—O3v3.1724 (10)O1—O2i2.5592 (12)
Cs1—O3vi3.1724 (10)O1—O2xlvii4.1576 (12)
Cs1—H1xix4.0332 (18)O1—O2xlviii3.2930 (11)
Cs1—H1xx4.0332 (18)O1—O2xlix3.9119 (12)
Cs1—H1vii3.4283 (15)O1—O2l3.3098 (12)
Cs1—H1viii3.4283 (15)O1—O3li3.6005 (12)
Cs1—H1ix3.6633 (18)O1—O3xxii3.6845 (12)
Cs1—H1x3.6633 (18)O1—O3lii3.9336 (13)
Cs1—H1xi4.2143 (18)O1—H11.5442 (18)
Cs1—H1xii4.2143 (18)O1—H1xliii3.3395 (17)
S1—P1xxi4.0534 (8)O1—H1liii4.0638 (18)
S1—P1xxii4.0534 (8)O1—H1liv3.7233 (17)
S1—P1v4.0534 (8)O1—H1xliv3.7447 (18)
S1—P1vi4.0534 (8)O1—H1xlv2.7017 (18)
S1—O1xxiii1.4777 (9)O2—O2lv2.4576 (12)
S1—O1xxiv1.4777 (9)O2—O2lvi2.4576 (12)
S1—O1ix1.4777 (9)O2—O2lvii4.0543 (12)
S1—O1x1.4777 (9)O2—O2lviii4.0543 (12)
S1—O2xxv4.2022 (8)O2—O3lix2.5619 (11)
S1—O2xxvi4.2022 (8)O2—O3lx4.4042 (12)
S1—O2xxvii3.4684 (8)O2—H1lxi3.3775 (18)
S1—O2xxviii3.4684 (8)O2—H1lxii1.0151 (18)
S1—O2xxix4.2022 (8)O2—H1lxiii2.9687 (18)
S1—O2xxx4.2022 (8)O2—H1lxiv3.5601 (17)
S1—O2xvii3.4684 (8)O2—H1lxv3.8069 (17)
S1—O2xviii3.4684 (8)O2—H1lxvi4.4161 (18)
S1—O3xxi3.9600 (8)O3—H1xxxi2.7426 (17)
S1—O3xxii3.9600 (8)O3—H1xxxiii2.7426 (17)
S1—O3v3.9600 (8)O3—H1xxxv2.7426 (17)
S1—O3vi3.9600 (8)O3—H1xxxvii4.2767 (17)
S1—H1xxiii2.5556 (16)O3—H1xxxviii4.2767 (17)
S1—H1xxiv2.5556 (16)O3—H1xxxix4.2767 (17)
S1—H1ix2.5556 (16)H1—H1lxvii3.806 (2)
S1—H1x2.5556 (16)H1—H1lxviii3.806 (2)
P1—O1xxxi3.5371 (12)H1—H1liii3.563 (2)
P1—O1xxxii4.2919 (11)H1—H1liv3.563 (2)
P1—O1xxxiii3.5371 (12)H1—H1xliv3.961 (2)
P1—O1xxxiv4.2919 (11)H1—H1xlv3.961 (2)
S1—Cs1—S1i109.596 (15)P1xxii—O1—P1lii104.19 (3)
S1—Cs1—S1ii109.596 (15)P1xxii—O1—O1xliii55.50 (3)
S1—Cs1—P1iii111.98 (2)P1xxii—O1—O1xliv106.09 (3)
S1—Cs1—P1iv111.98 (2)P1xxii—O1—O1xlv58.95 (3)
S1—Cs1—P1v59.113 (18)P1xxii—O1—O2xlvi137.67 (3)
S1—Cs1—P1vi59.113 (18)P1xxii—O1—O2i152.49 (4)
S1—Cs1—O1vii94.30 (2)P1xxii—O1—O2xlvii21.254 (16)
S1—Cs1—O1viii94.30 (2)P1xxii—O1—O2xlviii114.40 (3)
S1—Cs1—O1ix20.938 (15)P1xxii—O1—O2xlix90.27 (2)
S1—Cs1—O1x20.938 (15)P1xxii—O1—O2l79.15 (2)
S1—Cs1—O1xi124.83 (2)P1xxii—O1—O3li110.07 (3)
S1—Cs1—O1xii124.83 (2)P1xxii—O1—O3xxii19.472 (17)
S1—Cs1—O2xiii92.93 (3)P1xxii—O1—O3lii115.33 (3)
S1—Cs1—O2xiv92.93 (3)P1xxii—O1—H1152.60 (7)
S1—Cs1—O2xv131.98 (2)P1xxii—O1—H1xliii30.43 (3)
S1—Cs1—O2xvi131.98 (2)P1xxii—O1—H1liii102.51 (3)
S1—Cs1—O2xvii50.236 (17)P1xxii—O1—H1liv129.32 (3)
S1—Cs1—O2xviii50.236 (17)P1xxii—O1—H1xliv96.55 (3)
S1—Cs1—O3v65.72 (2)P1xxii—O1—H1xlv71.37 (4)
S1—Cs1—O3vi65.72 (2)P1lii—O1—O1xliii126.35 (4)
S1—Cs1—H1xix141.43 (2)P1lii—O1—O1xliv86.93 (4)
S1—Cs1—H1xx141.43 (2)P1lii—O1—O1xlv67.27 (3)
S1—Cs1—H1vii93.88 (3)P1lii—O1—O2xlvi109.75 (3)
S1—Cs1—H1viii93.88 (3)P1lii—O1—O2i102.00 (3)
S1—Cs1—H1ix38.58 (3)P1lii—O1—O2xlvii113.22 (3)
S1—Cs1—H1x38.58 (3)P1lii—O1—O2xlviii25.12 (2)
S1—Cs1—H1xi143.37 (2)P1lii—O1—O2xlix106.41 (3)
S1—Cs1—H1xii143.37 (2)P1lii—O1—O2l25.13 (2)
S1i—Cs1—S1ii140.81 (3)P1lii—O1—O3li145.36 (3)
S1i—Cs1—P1iii105.81 (2)P1lii—O1—O3xxii108.93 (3)
S1i—Cs1—P1iv58.437 (13)P1lii—O1—O3lii22.027 (18)
S1i—Cs1—P1v56.804 (11)P1lii—O1—H1102.00 (7)
S1i—Cs1—P1vi153.107 (16)P1lii—O1—H1xliii117.60 (4)
S1i—Cs1—O1vii152.85 (3)P1lii—O1—H1liii110.09 (3)
S1i—Cs1—O1viii19.926 (12)P1lii—O1—H1liv34.62 (3)
S1i—Cs1—O1ix93.864 (17)P1lii—O1—H1xliv100.42 (4)
S1i—Cs1—O1x123.99 (2)P1lii—O1—H1xlv36.46 (4)
S1i—Cs1—O1xi125.34 (4)O1xliii—O1—O1xliv59.89 (4)
S1i—Cs1—O1xii15.961 (15)O1xliii—O1—O1xlv59.89 (4)
S1i—Cs1—O2xiii125.31 (2)O1xliii—O1—O2xlvi83.75 (3)
S1i—Cs1—O2xiv52.246 (16)O1xliii—O1—O2i113.25 (4)
S1i—Cs1—O2xv87.76 (2)O1xliii—O1—O2xlvii34.44 (3)
S1i—Cs1—O2xvi65.818 (18)O1xliii—O1—O2xlviii151.31 (5)
S1i—Cs1—O2xvii59.423 (12)O1xliii—O1—O2xlix120.95 (4)
S1i—Cs1—O2xviii159.68 (3)O1xliii—O1—O2l109.19 (4)
S1i—Cs1—O3v61.602 (15)O1xliii—O1—O3li72.50 (3)
S1i—Cs1—O3vi138.711 (15)O1xliii—O1—O3xxii68.74 (3)
S1i—Cs1—H1xix81.38 (3)O1xliii—O1—O3lii115.28 (4)
S1i—Cs1—H1xx68.00 (2)O1xliii—O1—H1113.00 (7)
S1i—Cs1—H1vii139.53 (3)O1xliii—O1—H1xliii25.19 (3)
S1i—Cs1—H1viii36.28 (3)O1xliii—O1—H1liii122.17 (5)
S1i—Cs1—H1ix71.19 (2)O1xliii—O1—H1liv156.98 (5)
S1i—Cs1—H1x147.87 (4)O1xliii—O1—H1xliv46.04 (4)
S1i—Cs1—H1xi106.41 (3)O1xliii—O1—H1xlv93.84 (5)
S1i—Cs1—H1xii34.83 (2)O1xliv—O1—O1xlv60.22 (4)
S1ii—Cs1—P1iii58.437 (13)O1xliv—O1—O2xlvi52.77 (3)
S1ii—Cs1—P1iv105.81 (2)O1xliv—O1—O2i83.46 (4)
S1ii—Cs1—P1v153.107 (16)O1xliv—O1—O2xlvii87.05 (3)
S1ii—Cs1—P1vi56.804 (11)O1xliv—O1—O2xlviii105.01 (4)
S1ii—Cs1—O1vii19.926 (12)O1xliv—O1—O2xlix155.92 (4)
S1ii—Cs1—O1viii152.85 (3)O1xliv—O1—O2l91.87 (4)
S1ii—Cs1—O1ix123.99 (2)O1xliv—O1—O3li79.04 (3)
S1ii—Cs1—O1x93.864 (17)O1xliv—O1—O3xxii124.51 (4)
S1ii—Cs1—O1xi15.961 (15)O1xliv—O1—O3lii66.02 (3)
S1ii—Cs1—O1xii125.34 (4)O1xliv—O1—H183.09 (7)
S1ii—Cs1—O2xiii52.246 (16)O1xliv—O1—H1xliii79.48 (4)
S1ii—Cs1—O2xiv125.31 (2)O1xliv—O1—H1liii141.76 (4)
S1ii—Cs1—O2xv65.818 (18)O1xliv—O1—H1liv99.99 (4)
S1ii—Cs1—O2xvi87.76 (2)O1xliv—O1—H1xliv14.86 (3)
S1ii—Cs1—O2xvii159.68 (3)O1xliv—O1—H1xlv81.36 (5)
S1ii—Cs1—O2xviii59.423 (12)O1xlv—O1—O2xlvi112.92 (4)
S1ii—Cs1—O3v138.711 (15)O1xlv—O1—O2i141.88 (5)
S1ii—Cs1—O3vi61.602 (15)O1xlv—O1—O2xlvii52.72 (3)
S1ii—Cs1—H1xix68.00 (2)O1xlv—O1—O2xlviii91.59 (4)
S1ii—Cs1—H1xx81.38 (3)O1xlv—O1—O2xlix143.29 (4)
S1ii—Cs1—H1vii36.28 (3)O1xlv—O1—O2l50.19 (3)
S1ii—Cs1—H1viii139.53 (3)O1xlv—O1—O3li127.95 (4)
S1ii—Cs1—H1ix147.87 (4)O1xlv—O1—O3xxii77.28 (3)
S1ii—Cs1—H1x71.19 (2)O1xlv—O1—O3lii63.98 (3)
S1ii—Cs1—H1xi34.83 (2)O1xlv—O1—H1141.54 (8)
S1ii—Cs1—H1xii106.41 (3)O1xlv—O1—H1xliii53.11 (4)
P1iii—Cs1—P1iv136.04 (4)O1xlv—O1—H1liii157.75 (4)
P1iii—Cs1—P1v101.069 (16)O1xlv—O1—H1liv101.55 (4)
P1iii—Cs1—P1vi101.085 (16)O1xlv—O1—H1xliv61.26 (4)
P1iii—Cs1—O1vii51.325 (17)O1xlv—O1—H1xlv34.57 (4)
P1iii—Cs1—O1viii124.66 (2)O2xlvi—O1—O2i33.71 (2)
P1iii—Cs1—O1ix131.40 (3)O2xlvi—O1—O2xlvii117.84 (2)
P1iii—Cs1—O1x92.17 (2)O2xlvi—O1—O2xlviii106.99 (3)
P1iii—Cs1—O1xi60.32 (2)O2xlvi—O1—O2xlix103.31 (3)
P1iii—Cs1—O1xii93.88 (3)O2xlvi—O1—O2l130.56 (3)
P1iii—Cs1—O2xiii22.409 (19)O2xlvi—O1—O3li37.896 (19)
P1iii—Cs1—O2xiv152.41 (4)O2xlvi—O1—O3xxii140.87 (3)
P1iii—Cs1—O2xv22.296 (19)O2xlvi—O1—O3lii90.58 (2)
P1iii—Cs1—O2xvi115.12 (4)O2xlvi—O1—H133.36 (6)
P1iii—Cs1—O2xvii122.111 (18)O2xlvi—O1—H1xliii108.71 (3)
P1iii—Cs1—O2xviii86.974 (17)O2xlvi—O1—H1liii89.00 (3)
P1iii—Cs1—O3v84.396 (19)O2xlvi—O1—H1liv92.54 (3)
P1iii—Cs1—O3vi113.917 (19)O2xlvi—O1—H1xliv53.45 (3)
P1iii—Cs1—H1xix31.99 (3)O2xlvi—O1—H1xlv128.06 (5)
P1iii—Cs1—H1xx105.24 (4)O2i—O1—O2xlvii142.91 (4)
P1iii—Cs1—H1vii33.73 (3)O2i—O1—O2xlviii86.75 (3)
P1iii—Cs1—H1viii141.35 (4)O2i—O1—O2xlix74.31 (3)
P1iii—Cs1—H1ix127.23 (3)O2i—O1—O2l127.07 (4)
P1iii—Cs1—H1x88.87 (3)O2i—O1—O3li45.36 (3)
P1iii—Cs1—H1xi63.03 (3)O2i—O1—O3xxii138.42 (4)
P1iii—Cs1—H1xii81.53 (3)O2i—O1—O3lii92.16 (3)
P1iv—Cs1—P1v101.085 (16)O2i—O1—H10.37 (6)
P1iv—Cs1—P1vi101.069 (16)O2i—O1—H1xliii135.51 (4)
P1iv—Cs1—O1vii124.66 (2)O2i—O1—H1liii60.03 (3)
P1iv—Cs1—O1viii51.325 (17)O2i—O1—H1liv71.90 (4)
P1iv—Cs1—O1ix92.17 (2)O2i—O1—H1xliv86.80 (4)
P1iv—Cs1—O1x131.40 (3)O2i—O1—H1xlv136.12 (5)
P1iv—Cs1—O1xi93.88 (3)O2xlvii—O1—O2xlviii130.32 (3)
P1iv—Cs1—O1xii60.32 (2)O2xlvii—O1—O2xlix105.08 (3)
P1iv—Cs1—O2xiii152.41 (4)O2xlvii—O1—O2l88.91 (3)
P1iv—Cs1—O2xiv22.409 (19)O2xlvii—O1—O3li97.64 (3)
P1iv—Cs1—O2xv115.12 (4)O2xlvii—O1—O3xxii37.526 (19)
P1iv—Cs1—O2xvi22.296 (19)O2xlvii—O1—O3lii116.34 (3)
P1iv—Cs1—O2xvii86.974 (17)O2xlvii—O1—H1142.79 (7)
P1iv—Cs1—O2xviii122.111 (18)O2xlvii—O1—H1xliii9.25 (3)
P1iv—Cs1—O3v113.917 (19)O2xlvii—O1—H1liii114.54 (3)
P1iv—Cs1—O3vi84.396 (19)O2xlvii—O1—H1liv145.18 (4)
P1iv—Cs1—H1xix105.24 (4)O2xlvii—O1—H1xliv76.08 (3)
P1iv—Cs1—H1xx31.99 (3)O2xlvii—O1—H1xlv76.93 (4)
P1iv—Cs1—H1vii141.35 (4)O2xlviii—O1—O2xlix83.18 (2)
P1iv—Cs1—H1viii33.73 (3)O2xlviii—O1—O2l43.70 (2)
P1iv—Cs1—H1ix88.87 (3)O2xlviii—O1—O3li131.75 (3)
P1iv—Cs1—H1x127.23 (3)O2xlviii—O1—O3xxii110.45 (3)
P1iv—Cs1—H1xi81.53 (3)O2xlviii—O1—O3lii40.32 (2)
P1iv—Cs1—H1xii63.03 (3)O2xlviii—O1—H186.88 (7)
P1v—Cs1—P1vi118.23 (3)O2xlviii—O1—H1xliii137.33 (4)
P1v—Cs1—O1vii133.79 (2)O2xlviii—O1—H1liii85.21 (3)
P1v—Cs1—O1viii52.045 (16)O2xlviii—O1—H1liv15.09 (3)
P1v—Cs1—O1ix54.31 (2)O2xlviii—O1—H1xliv119.75 (4)
P1v—Cs1—O1x67.94 (2)O2xlviii—O1—H1xlv58.38 (4)
P1v—Cs1—O1xi161.38 (2)O2xlix—O1—O2l108.79 (3)
P1v—Cs1—O1xii68.818 (18)O2xlix—O1—O3li78.77 (3)
P1v—Cs1—O2xiii101.91 (2)O2xlix—O1—O3xxii70.80 (2)
P1v—Cs1—O2xiv81.14 (2)O2xlix—O1—O3lii123.04 (3)
P1v—Cs1—O2xv102.316 (18)O2xlix—O1—H174.67 (7)
P1v—Cs1—O2xvi118.256 (18)O2xlix—O1—H1xliii110.10 (4)
P1v—Cs1—O2xvii21.563 (16)O2xlix—O1—H1liii14.46 (3)
P1v—Cs1—O2xviii105.86 (3)O2xlix—O1—H1liv82.03 (3)
P1v—Cs1—O3v16.673 (19)O2xlix—O1—H1xliv149.75 (4)
P1v—Cs1—O3vi122.40 (4)O2xlix—O1—H1xlv121.27 (4)
P1v—Cs1—H1xix104.67 (2)O2l—O1—O3li168.45 (4)
P1v—Cs1—H1xx123.34 (3)O2l—O1—O3xxii85.89 (3)
P1v—Cs1—H1vii117.04 (3)O2l—O1—O3lii40.28 (2)
P1v—Cs1—H1viii67.36 (3)O2l—O1—H1127.08 (7)
P1v—Cs1—H1ix31.61 (3)O2l—O1—H1xliii94.43 (4)
P1v—Cs1—H1x92.81 (4)O2l—O1—H1liii118.28 (3)
P1v—Cs1—H1xi154.68 (3)O2l—O1—H1liv57.04 (3)
P1v—Cs1—H1xii85.41 (2)O2l—O1—H1xliv101.44 (4)
P1vi—Cs1—O1vii52.045 (16)O2l—O1—H1xlv15.62 (4)
P1vi—Cs1—O1viii133.79 (2)O3li—O1—O3xxii105.10 (3)
P1vi—Cs1—O1ix67.94 (2)O3li—O1—O3lii128.32 (3)
P1vi—Cs1—O1x54.31 (2)O3li—O1—H145.27 (6)
P1vi—Cs1—O1xi68.818 (18)O3li—O1—H1xliii90.92 (4)
P1vi—Cs1—O1xii161.38 (2)O3li—O1—H1liii67.52 (3)
P1vi—Cs1—O2xiii81.14 (2)O3li—O1—H1liv117.16 (4)
P1vi—Cs1—O2xiv101.91 (2)O3li—O1—H1xliv71.19 (3)
P1vi—Cs1—O2xv118.256 (18)O3li—O1—H1xlv159.91 (5)
P1vi—Cs1—O2xvi102.316 (18)O3xxii—O1—O3lii125.79 (3)
P1vi—Cs1—O2xvii105.86 (3)O3xxii—O1—H1138.66 (8)
P1vi—Cs1—O2xviii21.563 (16)O3xxii—O1—H1xliii45.64 (3)
P1vi—Cs1—O3v122.40 (4)O3xxii—O1—H1liii83.22 (3)
P1vi—Cs1—O3vi16.673 (19)O3xxii—O1—H1liv123.44 (3)
P1vi—Cs1—H1xix123.34 (3)O3xxii—O1—H1xliv113.35 (3)
P1vi—Cs1—H1xx104.67 (2)O3xxii—O1—H1xlv82.54 (4)
P1vi—Cs1—H1vii67.36 (3)O3lii—O1—H192.04 (7)
P1vi—Cs1—H1viii117.04 (3)O3lii—O1—H1xliii116.95 (4)
P1vi—Cs1—H1ix92.81 (4)O3lii—O1—H1liii122.11 (3)
P1vi—Cs1—H1x31.61 (3)O3lii—O1—H1liv41.87 (3)
P1vi—Cs1—H1xi85.41 (2)O3lii—O1—H1xliv80.24 (3)
P1vi—Cs1—H1xii154.68 (3)O3lii—O1—H1xlv44.15 (4)
O1vii—Cs1—O1viii171.39 (4)H1—O1—H1xliii135.34 (7)
O1vii—Cs1—O1ix112.25 (3)H1—O1—H1liii60.39 (7)
O1vii—Cs1—O1x76.20 (2)H1—O1—H1liv72.02 (7)
O1vii—Cs1—O1xi35.002 (19)H1—O1—H1xliv86.43 (7)
O1vii—Cs1—O1xii137.17 (4)H1—O1—H1xlv136.03 (8)
O1vii—Cs1—O2xiii37.60 (2)H1xliii—O1—H1liii117.76 (4)
O1vii—Cs1—O2xiv141.68 (2)H1xliii—O1—H1liv151.47 (5)
O1vii—Cs1—O2xv66.22 (2)H1xliii—O1—H1xliv67.71 (4)
O1vii—Cs1—O2xvi107.63 (3)H1xliii—O1—H1xlv81.19 (5)
O1vii—Cs1—O2xvii141.70 (3)H1liii—O1—H1liv80.32 (3)
O1vii—Cs1—O2xviii46.462 (16)H1liii—O1—H1xliv138.31 (4)
O1vii—Cs1—O3v121.27 (2)H1liii—O1—H1xlv132.42 (5)
O1vii—Cs1—O3vi62.778 (19)H1liv—O1—H1xliv114.72 (4)
O1vii—Cs1—H1xix71.77 (3)H1liv—O1—H1xlv70.62 (5)
O1vii—Cs1—H1xx101.27 (3)H1xliv—O1—H1xlv88.73 (5)
O1vii—Cs1—H1vii20.39 (3)S1lxxiii—O2—S1lxxiv124.84 (2)
O1vii—Cs1—H1viii158.00 (3)S1lxxiii—O2—P1lix73.77 (4)
O1vii—Cs1—H1ix132.47 (4)S1lxxiii—O2—O1lxii111.43 (3)
O1vii—Cs1—H1x56.09 (3)S1lxxiii—O2—O1lxxv109.21 (2)
O1vii—Cs1—H1xi52.90 (2)S1lxxiii—O2—O1lxiii20.398 (13)
O1vii—Cs1—H1xii118.87 (3)S1lxxiii—O2—O1lxiv18.015 (18)
O1viii—Cs1—O1ix76.20 (2)S1lxxiii—O2—O1lxv112.80 (2)
O1viii—Cs1—O1x112.25 (3)S1lxxiii—O2—O1lxvi143.85 (3)
O1viii—Cs1—O1xi137.17 (4)S1lxxiii—O2—O2lv55.60 (3)
O1viii—Cs1—O1xii35.002 (19)S1lxxiii—O2—O2lvi110.25 (3)
O1viii—Cs1—O2xiii141.68 (2)S1lxxiii—O2—O2lvii117.31 (2)
O1viii—Cs1—O2xiv37.60 (2)S1lxxiii—O2—O2lviii49.640 (15)
O1viii—Cs1—O2xv107.63 (3)S1lxxiii—O2—O3lix66.63 (3)
O1viii—Cs1—O2xvi66.22 (2)S1lxxiii—O2—O3lx109.32 (2)
O1viii—Cs1—O2xvii46.462 (16)S1lxxiii—O2—H1lxi105.07 (3)
O1viii—Cs1—O2xviii141.70 (3)S1lxxiii—O2—H1lxii111.87 (10)
O1viii—Cs1—O3v62.778 (19)S1lxxiii—O2—H1lxiii36.94 (3)
O1viii—Cs1—O3vi121.27 (2)S1lxxiii—O2—H1lxiv37.30 (3)
O1viii—Cs1—H1xix101.27 (3)S1lxxiii—O2—H1lxv117.03 (3)
O1viii—Cs1—H1xx71.77 (3)S1lxxiii—O2—H1lxvi135.35 (3)
O1viii—Cs1—H1vii158.00 (3)S1lxxiv—O2—P1lix100.38 (5)
O1viii—Cs1—H1viii20.39 (3)S1lxxiv—O2—O1lxii22.55 (2)
O1viii—Cs1—H1ix56.09 (3)S1lxxiv—O2—O1lxxv19.821 (14)
O1viii—Cs1—H1x132.47 (4)S1lxxiv—O2—O1lxiii134.13 (3)
O1viii—Cs1—H1xi118.87 (3)S1lxxiv—O2—O1lxiv125.62 (3)
O1viii—Cs1—H1xii52.90 (2)S1lxxiv—O2—O1lxv100.05 (2)
O1ix—Cs1—O1x41.88 (2)S1lxxiv—O2—O1lxvi25.043 (16)
O1ix—Cs1—O1xi136.70 (3)S1lxxiv—O2—O2lv138.55 (3)
O1ix—Cs1—O1xii109.81 (2)S1lxxiv—O2—O2lvi88.62 (3)
O1ix—Cs1—O2xiii113.66 (3)S1lxxiv—O2—O2lvii67.398 (19)
O1ix—Cs1—O2xiv72.18 (2)S1lxxiv—O2—O2lviii89.05 (2)
O1ix—Cs1—O2xv148.32 (3)S1lxxiv—O2—O3lix80.57 (3)
O1ix—Cs1—O2xvi113.48 (2)S1lxxiv—O2—O3lx125.80 (2)
O1ix—Cs1—O2xvii37.98 (2)S1lxxiv—O2—H1lxi86.16 (3)
O1ix—Cs1—O2xviii66.01 (3)S1lxxiv—O2—H1lxii21.99 (9)
O1ix—Cs1—O3v66.53 (3)S1lxxiv—O2—H1lxiii139.25 (4)
O1ix—Cs1—O3vi68.30 (3)S1lxxiv—O2—H1lxiv101.65 (3)
O1ix—Cs1—H1xix155.61 (3)S1lxxiv—O2—H1lxv79.84 (3)
O1ix—Cs1—H1xx123.35 (3)S1lxxiv—O2—H1lxvi35.30 (2)
O1ix—Cs1—H1vii114.51 (4)P1lix—O2—O1lxii116.06 (5)
O1ix—Cs1—H1viii73.24 (3)P1lix—O2—O1lxxv84.21 (4)
O1ix—Cs1—H1ix24.91 (3)P1lix—O2—O1lxiii57.08 (4)
O1ix—Cs1—H1x56.40 (3)P1lix—O2—O1lxiv91.50 (5)
O1ix—Cs1—H1xi150.99 (3)P1lix—O2—O1lxv148.25 (5)
O1ix—Cs1—H1xii128.65 (3)P1lix—O2—O1lxvi90.88 (5)
O1x—Cs1—O1xi109.81 (2)P1lix—O2—O2lv38.21 (4)
O1x—Cs1—O1xii136.70 (3)P1lix—O2—O2lvi38.21 (4)
O1x—Cs1—O2xiii72.18 (2)P1lix—O2—O2lvii166.59 (5)
O1x—Cs1—O2xiv113.66 (3)P1lix—O2—O2lviii113.94 (5)
O1x—Cs1—O2xv113.48 (2)P1lix—O2—O3lix31.51 (4)
O1x—Cs1—O2xvi148.32 (3)P1lix—O2—O3lx96.06 (5)
O1x—Cs1—O2xvii66.01 (3)P1lix—O2—H1lxi31.60 (4)
O1x—Cs1—O2xviii37.98 (2)P1lix—O2—H1lxii115.76 (11)
O1x—Cs1—O3v68.30 (3)P1lix—O2—H1lxiii46.40 (5)
O1x—Cs1—O3vi66.53 (3)P1lix—O2—H1lxiv106.64 (5)
O1x—Cs1—H1xix123.35 (3)P1lix—O2—H1lxv166.88 (6)
O1x—Cs1—H1xx155.61 (3)P1lix—O2—H1lxvi74.73 (5)
O1x—Cs1—H1vii73.24 (3)O1lxii—O2—O1lxxv32.31 (2)
O1x—Cs1—H1viii114.51 (4)O1lxii—O2—O1lxiii127.44 (4)
O1x—Cs1—H1ix56.40 (3)O1lxii—O2—O1lxiv106.78 (4)
O1x—Cs1—H1x24.91 (3)O1lxii—O2—O1lxv91.16 (3)
O1x—Cs1—H1xi128.65 (3)O1lxii—O2—O1lxvi46.35 (3)
O1x—Cs1—H1xii150.99 (3)O1lxii—O2—O2lv150.44 (4)
O1xi—Cs1—O1xii110.35 (4)O1lxii—O2—O2lvi110.98 (4)
O1xi—Cs1—O2xiii60.94 (2)O1lxii—O2—O2lvii54.18 (3)
O1xi—Cs1—O2xiv115.31 (3)O1lxii—O2—O2lviii68.27 (3)
O1xi—Cs1—O2xv60.83 (3)O1lxii—O2—O3lix89.35 (4)
O1xi—Cs1—O2xvi73.94 (3)O1lxii—O2—O3lx133.45 (4)
O1xi—Cs1—O2xvii174.68 (3)O1lxii—O2—H1lxi107.88 (4)
O1xi—Cs1—O2xviii74.627 (19)O1lxii—O2—H1lxii0.56 (9)
O1xi—Cs1—O3v144.71 (3)O1lxii—O2—H1lxiii140.17 (5)
O1xi—Cs1—O3vi69.72 (2)O1lxii—O2—H1lxiv81.45 (4)
O1xi—Cs1—H1xix60.22 (3)O1lxii—O2—H1lxv68.38 (4)
O1xi—Cs1—H1xx66.65 (3)O1lxii—O2—H1lxvi57.85 (3)
O1xi—Cs1—H1vii47.49 (3)O1lxxv—O2—O1lxiii115.05 (3)
O1xi—Cs1—H1viii126.76 (4)O1lxxv—O2—O1lxiv115.17 (3)
O1xi—Cs1—H1ix161.61 (4)O1lxxv—O2—O1lxv119.44 (3)
O1xi—Cs1—H1x86.79 (3)O1lxxv—O2—O1lxvi35.41 (2)
O1xi—Cs1—H1xi18.96 (3)O1lxxv—O2—O2lv121.26 (3)
O1xi—Cs1—H1xii91.67 (4)O1lxxv—O2—O2lvi82.81 (3)
O1xii—Cs1—O2xiii115.31 (3)O1lxxv—O2—O2lvii84.80 (2)
O1xii—Cs1—O2xiv60.94 (2)O1lxxv—O2—O2lviii85.17 (2)
O1xii—Cs1—O2xv73.94 (3)O1lxxv—O2—O3lix61.17 (3)
O1xii—Cs1—O2xvi60.83 (3)O1lxxv—O2—O3lx139.88 (3)
O1xii—Cs1—O2xvii74.627 (19)O1lxxv—O2—H1lxi77.86 (3)
O1xii—Cs1—O2xviii174.68 (3)O1lxxv—O2—H1lxii31.93 (9)
O1xii—Cs1—O3v69.72 (2)O1lxxv—O2—H1lxiii119.49 (4)
O1xii—Cs1—O3vi144.71 (3)O1lxxv—O2—H1lxiv95.56 (3)
O1xii—Cs1—H1xix66.65 (3)O1lxxv—O2—H1lxv98.19 (3)
O1xii—Cs1—H1xx60.22 (3)O1lxxv—O2—H1lxvi36.58 (2)
O1xii—Cs1—H1vii126.76 (4)O1lxiii—O2—O1lxiv35.65 (2)
O1xii—Cs1—H1viii47.49 (3)O1lxiii—O2—O1lxv119.68 (3)
O1xii—Cs1—H1ix86.79 (3)O1lxiii—O2—O1lxvi142.74 (3)
O1xii—Cs1—H1x161.61 (4)O1lxiii—O2—O2lv35.31 (3)
O1xii—Cs1—H1xi91.67 (4)O1lxiii—O2—O2lvi91.12 (3)
O1xii—Cs1—H1xii18.96 (3)O1lxiii—O2—O2lvii135.37 (3)
O2xiii—Cs1—O2xiv174.15 (5)O1lxiii—O2—O2lviii70.00 (2)
O2xiii—Cs1—O2xv44.53 (2)O1lxiii—O2—O3lix59.68 (3)
O2xiii—Cs1—O2xvi130.14 (4)O1lxiii—O2—O3lx97.83 (2)
O2xiii—Cs1—O2xvii119.18 (3)O1lxiii—O2—H1lxi86.98 (3)
O2xiii—Cs1—O2xviii65.02 (2)O1lxiii—O2—H1lxii127.77 (10)
O2xiii—Cs1—O3v86.50 (2)O1lxiii—O2—H1lxiii16.62 (3)
O2xiii—Cs1—O3vi95.91 (2)O1lxiii—O2—H1lxiv57.67 (3)
O2xiii—Cs1—H1xix53.94 (3)O1lxiii—O2—H1lxv131.39 (3)
O2xiii—Cs1—H1xx120.58 (4)O1lxiii—O2—H1lxvi128.47 (3)
O2xiii—Cs1—H1vii17.22 (3)O1lxiv—O2—O1lxv96.05 (3)
O2xiii—Cs1—H1viii161.49 (3)O1lxiv—O2—O1lxvi149.89 (4)
O2xiii—Cs1—H1ix118.62 (4)O1lxiv—O2—O2lv68.51 (3)
O2xiii—Cs1—H1x66.47 (3)O1lxiv—O2—O2lvi126.75 (4)
O2xiii—Cs1—H1xi71.18 (3)O1lxiv—O2—O2lvii100.13 (3)
O2xiii—Cs1—H1xii103.93 (3)O1lxiv—O2—O2lviii39.07 (2)
O2xiv—Cs1—O2xv130.14 (4)O1lxiv—O2—O3lix83.42 (3)
O2xiv—Cs1—O2xvi44.53 (2)O1lxiv—O2—O3lx104.94 (3)
O2xiv—Cs1—O2xvii65.02 (2)O1lxiv—O2—H1lxi122.41 (4)
O2xiv—Cs1—O2xviii119.18 (3)O1lxiv—O2—H1lxii107.30 (10)
O2xiv—Cs1—O3v95.91 (2)O1lxiv—O2—H1lxiii50.80 (4)
O2xiv—Cs1—O3vi86.50 (2)O1lxiv—O2—H1lxiv25.66 (3)
O2xiv—Cs1—H1xix120.58 (4)O1lxiv—O2—H1lxv99.03 (3)
O2xiv—Cs1—H1xx53.94 (3)O1lxiv—O2—H1lxvi148.38 (3)
O2xiv—Cs1—H1vii161.49 (3)O1lxv—O2—O1lxvi97.56 (3)
O2xiv—Cs1—H1viii17.22 (3)O1lxv—O2—O2lv118.12 (4)
O2xiv—Cs1—H1ix66.47 (3)O1lxv—O2—O2lvi118.81 (4)
O2xiv—Cs1—H1x118.62 (4)O1lxv—O2—O2lvii37.425 (18)
O2xiv—Cs1—H1xi103.93 (3)O1lxv—O2—O2lviii90.43 (2)
O2xiv—Cs1—H1xii71.18 (3)O1lxv—O2—O3lix179.35 (4)
O2xv—Cs1—O2xvi96.04 (4)O1lxv—O2—O3lx52.190 (19)
O2xv—Cs1—O2xvii123.434 (18)O1lxv—O2—H1lxi127.30 (4)
O2xv—Cs1—O2xviii107.739 (18)O1lxv—O2—H1lxii91.31 (10)
O2xv—Cs1—O3v86.89 (2)O1lxv—O2—H1lxiii120.46 (4)
O2xv—Cs1—O3vi127.17 (2)O1lxv—O2—H1lxiv92.66 (3)
O2xv—Cs1—H1xix9.90 (3)O1lxv—O2—H1lxv23.03 (3)
O2xv—Cs1—H1xx86.51 (4)O1lxv—O2—H1lxvi110.71 (3)
O2xv—Cs1—H1vii52.84 (3)O1lxvi—O2—O2lv126.05 (4)
O2xv—Cs1—H1viii120.89 (4)O1lxvi—O2—O2lvi67.79 (3)
O2xv—Cs1—H1ix133.52 (3)O1lxvi—O2—O2lvii75.71 (2)
O2xv—Cs1—H1x110.93 (3)O1lxvi—O2—O2lviii114.05 (3)
O2xv—Cs1—H1xi55.24 (3)O1lxvi—O2—O3lix83.08 (3)
O2xv—Cs1—H1xii59.78 (3)O1lxvi—O2—O3lx104.64 (3)
O2xvi—Cs1—O2xvii107.739 (18)O1lxvi—O2—H1lxi67.66 (3)
O2xvi—Cs1—O2xviii123.434 (18)O1lxvi—O2—H1lxii45.79 (9)
O2xvi—Cs1—O3v127.17 (2)O1lxvi—O2—H1lxiii137.14 (4)
O2xvi—Cs1—O3vi86.89 (2)O1lxvi—O2—H1lxiv126.69 (4)
O2xvi—Cs1—H1xix86.51 (4)O1lxvi—O2—H1lxv83.94 (3)
O2xvi—Cs1—H1xx9.90 (3)O1lxvi—O2—H1lxvi16.20 (2)
O2xvi—Cs1—H1vii120.89 (4)O2lv—O2—O2lvi60.00 (3)
O2xvi—Cs1—H1viii52.84 (3)O2lv—O2—O2lvii153.87 (4)
O2xvi—Cs1—H1ix110.93 (3)O2lv—O2—O2lviii105.24 (3)
O2xvi—Cs1—H1x133.52 (3)O2lv—O2—O3lix61.34 (3)
O2xvi—Cs1—H1xi59.78 (3)O2lv—O2—O3lx73.80 (3)
O2xvi—Cs1—H1xii55.24 (3)O2lv—O2—H1lxi58.66 (4)
O2xvii—Cs1—O2xviii100.47 (3)O2lv—O2—H1lxii150.37 (11)
O2xvii—Cs1—O3v38.03 (2)O2lv—O2—H1lxiii18.69 (4)
O2xvii—Cs1—O3vi105.17 (3)O2lv—O2—H1lxiv92.58 (4)
O2xvii—Cs1—H1xix124.60 (2)O2lv—O2—H1lxv140.43 (4)
O2xvii—Cs1—H1xx115.62 (2)O2lv—O2—H1lxvi110.16 (4)
O2xvii—Cs1—H1vii131.33 (4)O2lvi—O2—O2lvii132.32 (4)
O2xvii—Cs1—H1viii54.99 (3)O2lvi—O2—O2lviii150.62 (4)
O2xvii—Cs1—H1ix13.07 (3)O2lvi—O2—O3lix61.34 (3)
O2xvii—Cs1—H1x88.51 (4)O2lvi—O2—O3lx73.80 (3)
O2xvii—Cs1—H1xi165.31 (3)O2lvi—O2—H1lxi8.55 (3)
O2xvii—Cs1—H1xii93.40 (2)O2lvi—O2—H1lxii110.44 (10)
O2xviii—Cs1—O3v105.17 (3)O2lvi—O2—H1lxiii76.34 (4)
O2xviii—Cs1—O3vi38.03 (2)O2lvi—O2—H1lxiv144.85 (4)
O2xviii—Cs1—H1xix115.62 (2)O2lvi—O2—H1lxv129.05 (4)
O2xviii—Cs1—H1xx124.60 (2)O2lvi—O2—H1lxvi53.64 (3)
O2xviii—Cs1—H1vii54.99 (3)O2lvii—O2—O2lviii72.68 (2)
O2xviii—Cs1—H1viii131.33 (4)O2lvii—O2—O3lix143.02 (4)
O2xviii—Cs1—H1ix88.51 (4)O2lvii—O2—O3lx87.43 (2)
O2xviii—Cs1—H1x13.07 (3)O2lvii—O2—H1lxi137.46 (4)
O2xviii—Cs1—H1xi93.40 (2)O2lvii—O2—H1lxii54.39 (9)
O2xviii—Cs1—H1xii165.31 (3)O2lvii—O2—H1lxiii146.97 (4)
O3v—Cs1—O3vi131.44 (5)O2lvii—O2—H1lxiv82.06 (3)
O3v—Cs1—H1xix90.50 (3)O2lvii—O2—H1lxv14.40 (3)
O3v—Cs1—H1xx129.36 (3)O2lvii—O2—H1lxvi91.86 (3)
O3v—Cs1—H1vii102.58 (3)O2lviii—O2—O3lix89.40 (3)
O3v—Cs1—H1viii80.67 (3)O2lviii—O2—O3lx129.44 (3)
O3v—Cs1—H1ix46.63 (3)O2lviii—O2—H1lxi142.23 (4)
O3v—Cs1—H1x92.51 (4)O2lviii—O2—H1lxii68.81 (10)
O3v—Cs1—H1xi141.64 (3)O2lviii—O2—H1lxiii86.58 (4)
O3v—Cs1—H1xii82.87 (3)O2lviii—O2—H1lxiv13.40 (3)
O3vi—Cs1—H1xix129.36 (3)O2lviii—O2—H1lxv79.16 (3)
O3vi—Cs1—H1xx90.50 (3)O2lviii—O2—H1lxvi121.47 (3)
O3vi—Cs1—H1vii80.67 (3)O3lix—O2—O3lx127.57 (3)
O3vi—Cs1—H1viii102.58 (3)O3lix—O2—H1lxi52.86 (3)
O3vi—Cs1—H1ix92.51 (4)O3lix—O2—H1lxii89.21 (10)
O3vi—Cs1—H1x46.63 (3)O3lix—O2—H1lxiii58.91 (4)
O3vi—Cs1—H1xi82.87 (3)O3lix—O2—H1lxiv87.02 (4)
O3vi—Cs1—H1xii141.64 (3)O3lix—O2—H1lxv157.42 (4)
H1xix—Cs1—H1xx77.14 (4)O3lix—O2—H1lxvi69.90 (3)
H1xix—Cs1—H1vii60.70 (4)O3lx—O2—H1lxi81.79 (3)
H1xix—Cs1—H1viii112.55 (4)O3lx—O2—H1lxii133.26 (10)
H1xix—Cs1—H1ix136.26 (3)O3lx—O2—H1lxiii86.37 (4)
H1xix—Cs1—H1x120.00 (3)O3lx—O2—H1lxiv122.22 (3)
H1xix—Cs1—H1xi51.14 (3)O3lx—O2—H1lxv73.75 (3)
H1xix—Cs1—H1xii51.14 (3)O3lx—O2—H1lxvi104.73 (3)
H1xx—Cs1—H1vii112.55 (4)H1lxi—O2—H1lxii107.37 (10)
H1xx—Cs1—H1viii60.70 (4)H1lxi—O2—H1lxiii73.38 (4)
H1xx—Cs1—H1ix120.00 (3)H1lxi—O2—H1lxiv137.63 (4)
H1xx—Cs1—H1x136.26 (3)H1lxi—O2—H1lxv136.20 (4)
H1xx—Cs1—H1xi51.14 (3)H1lxi—O2—H1lxvi52.37 (3)
H1xx—Cs1—H1xii51.14 (3)H1lxii—O2—H1lxiii140.36 (11)
H1vii—Cs1—H1viii172.23 (5)H1lxii—O2—H1lxiv81.98 (10)
H1vii—Cs1—H1ix127.06 (4)H1lxii—O2—H1lxv68.56 (10)
H1vii—Cs1—H1x60.22 (4)H1lxii—O2—H1lxvi57.29 (10)
H1vii—Cs1—H1xi61.41 (3)H1lxiii—O2—H1lxiv74.07 (4)
H1vii—Cs1—H1xii111.70 (4)H1lxiii—O2—H1lxv138.36 (5)
H1viii—Cs1—H1ix60.22 (4)H1lxiii—O2—H1lxvi121.07 (4)
H1viii—Cs1—H1x127.06 (4)H1lxiv—O2—H1lxv86.03 (4)
H1viii—Cs1—H1xi111.70 (4)H1lxiv—O2—H1lxvi132.12 (4)
H1viii—Cs1—H1xii61.41 (3)H1lxv—O2—H1lxvi99.50 (4)
H1ix—Cs1—H1x77.15 (4)S1lxix—O3—S1lxx118.53 (2)
H1ix—Cs1—H1xi169.69 (3)S1lxix—O3—S1lxxi118.53 (2)
H1ix—Cs1—H1xii105.72 (3)S1lxix—O3—P182.98 (4)
H1x—Cs1—H1xi105.72 (3)S1lxix—O3—O1xxxi135.82 (3)
H1x—Cs1—H1xii169.69 (3)S1lxix—O3—O1xxxii115.40 (2)
H1xi—Cs1—H1xii73.26 (4)S1lxix—O3—O1xxxiii96.89 (2)
P1xxi—S1—P1xxii125.582 (16)S1lxix—O3—O1xxxiv126.07 (3)
P1xxi—S1—P1v102.068 (16)S1lxix—O3—O1xxxv21.881 (14)
P1xxi—S1—P1vi102.068 (16)S1lxix—O3—O1xxxvi21.910 (14)
P1xxi—S1—O1xxiii89.07 (4)S1lxix—O3—O1xxxvii21.576 (13)
P1xxi—S1—O1xxiv59.37 (3)S1lxix—O3—O1xxxviii129.75 (2)
P1xxi—S1—O1ix65.04 (4)S1lxix—O3—O1xxxix99.28 (2)
P1xxi—S1—O1x161.35 (3)S1lxix—O3—O2xl76.94 (3)
P1xxi—S1—O2xxv21.741 (16)S1lxix—O3—O2xli59.77 (2)
P1xxi—S1—O2xxvi144.290 (16)S1lxix—O3—O2xlii115.09 (3)
P1xxi—S1—O2xxvii22.301 (17)S1lxix—O3—O2lxxvi104.58 (2)
P1xxi—S1—O2xxviii124.666 (18)S1lxix—O3—O2lxxvii78.296 (18)
P1xxi—S1—O2xxix101.606 (16)S1lxix—O3—O2lxxviii107.37 (2)
P1xxi—S1—O2xxx85.164 (16)S1lxix—O3—H1xxxi127.56 (4)
P1xxi—S1—O2xvii80.930 (17)S1lxix—O3—H1xxxiii86.47 (4)
P1xxi—S1—O2xviii120.934 (17)S1lxix—O3—H1xxxv39.87 (3)
P1xxi—S1—O3xxi21.182 (16)S1lxix—O3—H1xxxvii35.89 (2)
P1xxi—S1—O3xxii107.920 (16)S1lxix—O3—H1xxxviii150.89 (3)
P1xxi—S1—O3v120.366 (16)S1lxix—O3—H1xxxix82.74 (3)
P1xxi—S1—O3vi96.848 (16)S1lxx—O3—S1lxxi118.53 (2)
P1xxi—S1—H1xxiii117.64 (4)S1lxx—O3—P182.98 (4)
P1xxi—S1—H1xxiv29.08 (4)S1lxx—O3—O1xxxi21.881 (14)
P1xxi—S1—H1ix77.02 (4)S1lxx—O3—O1xxxii21.910 (14)
P1xxi—S1—H1x129.39 (4)S1lxx—O3—O1xxxiii135.82 (3)
P1xxii—S1—P1v102.068 (16)S1lxx—O3—O1xxxiv115.40 (2)
P1xxii—S1—P1vi102.068 (16)S1lxx—O3—O1xxxv96.89 (2)
P1xxii—S1—O1xxiii59.37 (3)S1lxx—O3—O1xxxvi126.07 (3)
P1xxii—S1—O1xxiv89.07 (4)S1lxx—O3—O1xxxvii129.75 (2)
P1xxii—S1—O1ix161.35 (3)S1lxx—O3—O1xxxviii99.28 (2)
P1xxii—S1—O1x65.04 (4)S1lxx—O3—O1xxxix21.576 (13)
P1xxii—S1—O2xxv144.290 (16)S1lxx—O3—O2xl115.09 (3)
P1xxii—S1—O2xxvi21.741 (16)S1lxx—O3—O2xli76.94 (3)
P1xxii—S1—O2xxvii124.666 (18)S1lxx—O3—O2xlii59.77 (2)
P1xxii—S1—O2xxviii22.301 (17)S1lxx—O3—O2lxxvi78.296 (18)
P1xxii—S1—O2xxix85.164 (16)S1lxx—O3—O2lxxvii107.37 (2)
P1xxii—S1—O2xxx101.606 (16)S1lxx—O3—O2lxxviii104.58 (2)
P1xxii—S1—O2xvii120.934 (17)S1lxx—O3—H1xxxi39.87 (3)
P1xxii—S1—O2xviii80.930 (17)S1lxx—O3—H1xxxiii127.56 (4)
P1xxii—S1—O3xxi107.920 (16)S1lxx—O3—H1xxxv86.47 (4)
P1xxii—S1—O3xxii21.182 (16)S1lxx—O3—H1xxxvii150.89 (3)
P1xxii—S1—O3v96.848 (16)S1lxx—O3—H1xxxviii82.74 (3)
P1xxii—S1—O3vi120.366 (16)S1lxx—O3—H1xxxix35.89 (2)
P1xxii—S1—H1xxiii29.08 (4)S1lxxi—O3—P182.98 (4)
P1xxii—S1—H1xxiv117.64 (4)S1lxxi—O3—O1xxxi96.89 (2)
P1xxii—S1—H1ix129.39 (4)S1lxxi—O3—O1xxxii126.07 (3)
P1xxii—S1—H1x77.02 (4)S1lxxi—O3—O1xxxiii21.881 (14)
P1v—S1—P1vi125.582 (16)S1lxxi—O3—O1xxxiv21.910 (14)
P1v—S1—O1xxiii65.04 (4)S1lxxi—O3—O1xxxv135.82 (3)
P1v—S1—O1xxiv161.35 (3)S1lxxi—O3—O1xxxvi115.40 (2)
P1v—S1—O1ix59.37 (3)S1lxxi—O3—O1xxxvii99.28 (2)
P1v—S1—O1x89.07 (4)S1lxxi—O3—O1xxxviii21.576 (13)
P1v—S1—O2xxv85.164 (16)S1lxxi—O3—O1xxxix129.75 (2)
P1v—S1—O2xxvi101.606 (16)S1lxxi—O3—O2xl59.77 (2)
P1v—S1—O2xxvii120.934 (17)S1lxxi—O3—O2xli115.09 (3)
P1v—S1—O2xxviii80.930 (17)S1lxxi—O3—O2xlii76.94 (3)
P1v—S1—O2xxix21.741 (16)S1lxxi—O3—O2lxxvi107.37 (2)
P1v—S1—O2xxx144.290 (16)S1lxxi—O3—O2lxxvii104.58 (2)
P1v—S1—O2xvii22.301 (17)S1lxxi—O3—O2lxxviii78.296 (18)
P1v—S1—O2xviii124.666 (18)S1lxxi—O3—H1xxxi86.47 (4)
P1v—S1—O3xxi96.848 (16)S1lxxi—O3—H1xxxiii39.87 (3)
P1v—S1—O3xxii120.366 (16)S1lxxi—O3—H1xxxv127.56 (4)
P1v—S1—O3v21.182 (16)S1lxxi—O3—H1xxxvii82.74 (3)
P1v—S1—O3vi107.920 (16)S1lxxi—O3—H1xxxviii35.89 (2)
P1v—S1—H1xxiii77.02 (4)S1lxxi—O3—H1xxxix150.89 (3)
P1v—S1—H1xxiv129.39 (4)P1—O3—O1xxxi75.67 (5)
P1v—S1—H1ix29.08 (4)P1—O3—O1xxxii104.19 (5)
P1v—S1—H1x117.64 (4)P1—O3—O1xxxiii75.67 (5)
P1vi—S1—O1xxiii161.35 (3)P1—O3—O1xxxiv104.19 (5)
P1vi—S1—O1xxiv65.04 (4)P1—O3—O1xxxv75.67 (5)
P1vi—S1—O1ix89.07 (4)P1—O3—O1xxxvi104.19 (5)
P1vi—S1—O1x59.37 (3)P1—O3—O1xxxvii69.36 (4)
P1vi—S1—O2xxv101.606 (16)P1—O3—O1xxxviii69.36 (4)
P1vi—S1—O2xxvi85.164 (16)P1—O3—O1xxxix69.36 (4)
P1vi—S1—O2xxvii80.930 (17)P1—O3—O2xl33.63 (4)
P1vi—S1—O2xxviii120.934 (17)P1—O3—O2xli33.63 (4)
P1vi—S1—O2xxix144.290 (16)P1—O3—O2xlii33.63 (4)
P1vi—S1—O2xxx21.741 (16)P1—O3—O2lxxvi161.21 (5)
P1vi—S1—O2xvii124.666 (18)P1—O3—O2lxxvii161.21 (5)
P1vi—S1—O2xviii22.301 (17)P1—O3—O2lxxviii161.21 (5)
P1vi—S1—O3xxi120.366 (16)P1—O3—H1xxxi53.24 (5)
P1vi—S1—O3xxii96.848 (16)P1—O3—H1xxxiii53.24 (5)
P1vi—S1—O3v107.920 (16)P1—O3—H1xxxv53.24 (5)
P1vi—S1—O3vi21.182 (16)P1—O3—H1xxxvii80.15 (5)
P1vi—S1—H1xxiii129.39 (4)P1—O3—H1xxxviii80.15 (5)
P1vi—S1—H1xxiv77.02 (4)P1—O3—H1xxxix80.15 (5)
P1vi—S1—H1ix117.64 (4)O1xxxi—O3—O1xxxii38.756 (19)
P1vi—S1—H1x29.08 (4)O1xxxi—O3—O1xxxiii114.09 (3)
O1xxiii—S1—O1xxiv109.84 (5)O1xxxi—O3—O1xxxiv96.77 (3)
O1xxiii—S1—O1ix109.29 (5)O1xxxi—O3—O1xxxv114.09 (3)
O1xxiii—S1—O1x109.29 (5)O1xxxi—O3—O1xxxvi147.57 (3)
O1xxiii—S1—O2xxv94.27 (3)O1xxxi—O3—O1xxxvii139.04 (3)
O1xxiii—S1—O2xxvi77.21 (3)O1xxxi—O3—O1xxxviii77.40 (2)
O1xxiii—S1—O2xxvii107.44 (4)O1xxxi—O3—O1xxxix36.98 (2)
O1xxiii—S1—O2xxviii41.61 (3)O1xxxi—O3—O2xl102.54 (3)
O1xxiii—S1—O2xxix43.57 (4)O1xxxi—O3—O2xli82.42 (3)
O1xxiii—S1—O2xxx150.63 (4)O1xxxi—O3—O2xlii45.30 (3)
O1xxiii—S1—O2xvii71.46 (4)O1xxxi—O3—O2lxxvi87.33 (2)
O1xxiii—S1—O2xviii139.99 (3)O1xxxi—O3—O2lxxvii119.52 (3)
O1xxiii—S1—O3xxi68.50 (4)O1xxxi—O3—O2lxxviii104.89 (3)
O1xxiii—S1—O3xxii65.24 (3)O1xxxi—O3—H1xxxi23.58 (4)
O1xxiii—S1—O3v78.21 (4)O1xxxi—O3—H1xxxiii109.36 (4)
O1xxiii—S1—O3vi171.76 (4)O1xxxi—O3—H1xxxv98.09 (4)
O1xxiii—S1—H1xxiii33.06 (5)O1xxxi—O3—H1xxxvii155.66 (3)
O1xxiii—S1—H1xxiv108.83 (5)O1xxxi—O3—H1xxxviii61.40 (3)
O1xxiii—S1—H1ix79.20 (5)O1xxxi—O3—H1xxxix55.98 (3)
O1xxiii—S1—H1x134.65 (5)O1xxxii—O3—O1xxxiii147.57 (3)
O1xxiv—S1—O1ix109.29 (5)O1xxxii—O3—O1xxxiv114.19 (3)
O1xxiv—S1—O1x109.29 (5)O1xxxii—O3—O1xxxv96.77 (3)
O1xxiv—S1—O2xxv77.21 (3)O1xxxii—O3—O1xxxvi114.19 (3)
O1xxiv—S1—O2xxvi94.27 (3)O1xxxii—O3—O1xxxvii133.71 (3)
O1xxiv—S1—O2xxvii41.61 (3)O1xxxii—O3—O1xxxviii111.72 (3)
O1xxiv—S1—O2xxviii107.44 (4)O1xxxii—O3—O1xxxix36.71 (2)
O1xxiv—S1—O2xxix150.63 (4)O1xxxii—O3—O2xl136.92 (4)
O1xxiv—S1—O2xxx43.57 (4)O1xxxii—O3—O2xli91.90 (3)
O1xxiv—S1—O2xvii139.99 (3)O1xxxii—O3—O2xlii81.31 (3)
O1xxiv—S1—O2xviii71.46 (4)O1xxxii—O3—O2lxxvi57.01 (2)
O1xxiv—S1—O3xxi65.24 (3)O1xxxii—O3—O2lxxvii85.46 (2)
O1xxiv—S1—O3xxii68.50 (4)O1xxxii—O3—O2lxxviii85.82 (2)
O1xxiv—S1—O3v171.76 (4)O1xxxii—O3—H1xxxi60.52 (4)
O1xxiv—S1—O3vi78.21 (4)O1xxxii—O3—H1xxxiii148.08 (4)
O1xxiv—S1—H1xxiii108.83 (5)O1xxxii—O3—H1xxxv94.79 (4)
O1xxiv—S1—H1xxiv33.06 (5)O1xxxii—O3—H1xxxvii151.02 (3)
O1xxiv—S1—H1ix134.65 (5)O1xxxii—O3—H1xxxviii91.75 (3)
O1xxiv—S1—H1x79.20 (5)O1xxxii—O3—H1xxxix38.78 (3)
O1ix—S1—O1x109.84 (5)O1xxxiii—O3—O1xxxiv38.756 (19)
O1ix—S1—O2xxv43.57 (4)O1xxxiii—O3—O1xxxv114.09 (3)
O1ix—S1—O2xxvi150.63 (4)O1xxxiii—O3—O1xxxvi96.77 (3)
O1ix—S1—O2xxvii71.46 (4)O1xxxiii—O3—O1xxxvii77.40 (2)
O1ix—S1—O2xxviii139.99 (3)O1xxxiii—O3—O1xxxviii36.98 (2)
O1ix—S1—O2xxix77.21 (3)O1xxxiii—O3—O1xxxix139.04 (3)
O1ix—S1—O2xxx94.27 (3)O1xxxiii—O3—O2xl45.30 (3)
O1ix—S1—O2xvii41.61 (3)O1xxxiii—O3—O2xli102.54 (3)
O1ix—S1—O2xviii107.44 (4)O1xxxiii—O3—O2xlii82.42 (3)
O1ix—S1—O3xxi78.21 (4)O1xxxiii—O3—O2lxxvi119.52 (3)
O1ix—S1—O3xxii171.76 (4)O1xxxiii—O3—O2lxxvii104.89 (3)
O1ix—S1—O3v65.24 (3)O1xxxiii—O3—O2lxxviii87.33 (2)
O1ix—S1—O3vi68.50 (4)O1xxxiii—O3—H1xxxi98.09 (4)
O1ix—S1—H1xxiii134.65 (5)O1xxxiii—O3—H1xxxiii23.58 (4)
O1ix—S1—H1xxiv79.20 (5)O1xxxiii—O3—H1xxxv109.36 (4)
O1ix—S1—H1ix33.06 (5)O1xxxiii—O3—H1xxxvii61.40 (3)
O1ix—S1—H1x108.83 (5)O1xxxiii—O3—H1xxxviii55.98 (3)
O1x—S1—O2xxv150.63 (4)O1xxxiii—O3—H1xxxix155.66 (3)
O1x—S1—O2xxvi43.57 (4)O1xxxiv—O3—O1xxxv147.57 (3)
O1x—S1—O2xxvii139.99 (3)O1xxxiv—O3—O1xxxvi114.19 (3)
O1x—S1—O2xxviii71.46 (4)O1xxxiv—O3—O1xxxvii111.72 (3)
O1x—S1—O2xxix94.27 (3)O1xxxiv—O3—O1xxxviii36.71 (2)
O1x—S1—O2xxx77.21 (3)O1xxxiv—O3—O1xxxix133.71 (3)
O1x—S1—O2xvii107.44 (4)O1xxxiv—O3—O2xl81.31 (3)
O1x—S1—O2xviii41.61 (3)O1xxxiv—O3—O2xli136.92 (4)
O1x—S1—O3xxi171.76 (4)O1xxxiv—O3—O2xlii91.90 (3)
O1x—S1—O3xxii78.21 (4)O1xxxiv—O3—O2lxxvi85.46 (2)
O1x—S1—O3v68.50 (4)O1xxxiv—O3—O2lxxvii85.82 (2)
O1x—S1—O3vi65.24 (3)O1xxxiv—O3—O2lxxviii57.01 (2)
O1x—S1—H1xxiii79.20 (5)O1xxxiv—O3—H1xxxi94.79 (4)
O1x—S1—H1xxiv134.65 (5)O1xxxiv—O3—H1xxxiii60.52 (4)
O1x—S1—H1ix108.83 (5)O1xxxiv—O3—H1xxxv148.08 (4)
O1x—S1—H1x33.06 (5)O1xxxiv—O3—H1xxxvii91.75 (3)
O2xxv—S1—O2xxvi165.313 (15)O1xxxiv—O3—H1xxxviii38.78 (3)
O2xxv—S1—O2xxvii35.779 (18)O1xxxiv—O3—H1xxxix151.02 (3)
O2xxv—S1—O2xxviii135.369 (18)O1xxxv—O3—O1xxxvi38.756 (19)
O2xxv—S1—O2xxix90.936 (17)O1xxxv—O3—O1xxxvii36.98 (2)
O2xxv—S1—O2xxx90.936 (17)O1xxxv—O3—O1xxxviii139.04 (3)
O2xxv—S1—O2xvii62.962 (17)O1xxxv—O3—O1xxxix77.40 (2)
O2xxv—S1—O2xviii123.657 (17)O1xxxv—O3—O2xl82.42 (3)
O2xxv—S1—O3xxi36.433 (16)O1xxxv—O3—O2xli45.30 (3)
O2xxv—S1—O3xxii129.044 (16)O1xxxv—O3—O2xlii102.54 (3)
O2xxv—S1—O3v100.835 (16)O1xxxv—O3—O2lxxvi104.89 (3)
O2xxv—S1—O3vi89.236 (16)O1xxxv—O3—O2lxxvii87.33 (2)
O2xxv—S1—H1xxiii126.96 (4)O1xxxv—O3—O2lxxviii119.52 (3)
O2xxv—S1—H1xxiv44.28 (4)O1xxxv—O3—H1xxxi109.36 (4)
O2xxv—S1—H1ix57.58 (4)O1xxxv—O3—H1xxxiii98.09 (4)
O2xxv—S1—H1x130.60 (4)O1xxxv—O3—H1xxxv23.58 (4)
O2xxvi—S1—O2xxvii135.369 (18)O1xxxv—O3—H1xxxvii55.98 (3)
O2xxvi—S1—O2xxviii35.779 (18)O1xxxv—O3—H1xxxviii155.66 (3)
O2xxvi—S1—O2xxix90.936 (17)O1xxxv—O3—H1xxxix61.40 (3)
O2xxvi—S1—O2xxx90.936 (17)O1xxxvi—O3—O1xxxvii36.71 (2)
O2xxvi—S1—O2xvii123.657 (17)O1xxxvi—O3—O1xxxviii133.71 (3)
O2xxvi—S1—O2xviii62.962 (17)O1xxxvi—O3—O1xxxix111.72 (3)
O2xxvi—S1—O3xxi129.044 (16)O1xxxvi—O3—O2xl91.90 (3)
O2xxvi—S1—O3xxii36.433 (16)O1xxxvi—O3—O2xli81.31 (3)
O2xxvi—S1—O3v89.236 (16)O1xxxvi—O3—O2xlii136.92 (4)
O2xxvi—S1—O3vi100.835 (16)O1xxxvi—O3—O2lxxvi85.82 (2)
O2xxvi—S1—H1xxiii44.28 (4)O1xxxvi—O3—O2lxxvii57.01 (2)
O2xxvi—S1—H1xxiv126.96 (4)O1xxxvi—O3—O2lxxviii85.46 (2)
O2xxvi—S1—H1ix130.60 (4)O1xxxvi—O3—H1xxxi148.08 (4)
O2xxvi—S1—H1x57.58 (4)O1xxxvi—O3—H1xxxiii94.79 (4)
O2xxvii—S1—O2xxviii134.123 (19)O1xxxvi—O3—H1xxxv60.52 (4)
O2xxvii—S1—O2xxix123.657 (17)O1xxxvi—O3—H1xxxvii38.78 (3)
O2xxvii—S1—O2xxx62.962 (17)O1xxxvi—O3—H1xxxviii151.02 (3)
O2xxvii—S1—O2xvii98.737 (19)O1xxxvi—O3—H1xxxix91.75 (3)
O2xxvii—S1—O2xviii98.737 (19)O1xxxvii—O3—O1xxxviii108.28 (3)
O2xxvii—S1—O3xxi39.658 (18)O1xxxvii—O3—O1xxxix108.28 (3)
O2xxvii—S1—O3xxii103.729 (18)O1xxxvii—O3—O2xl56.27 (3)
O2xxvii—S1—O3v135.395 (18)O1xxxvii—O3—O2xli56.64 (3)
O2xxvii—S1—O3vi79.663 (18)O1xxxvii—O3—O2xlii102.99 (3)
O2xxvii—S1—H1xxiii129.75 (4)O1xxxvii—O3—O2lxxvi122.49 (3)
O2xxvii—S1—H1xxiv8.55 (4)O1xxxvii—O3—O2lxxvii92.25 (2)
O2xxvii—S1—H1ix93.04 (4)O1xxxvii—O3—O2lxxviii115.13 (2)
O2xxvii—S1—H1x107.24 (4)O1xxxvii—O3—H1xxxi121.20 (4)
O2xxviii—S1—O2xxix62.962 (17)O1xxxvii—O3—H1xxxiii64.96 (4)
O2xxviii—S1—O2xxx123.657 (17)O1xxxvii—O3—H1xxxv43.33 (4)
O2xxviii—S1—O2xvii98.737 (19)O1xxxvii—O3—H1xxxvii21.15 (2)
O2xxviii—S1—O2xviii98.737 (19)O1xxxvii—O3—H1xxxviii129.38 (3)
O2xxviii—S1—O3xxi103.729 (18)O1xxxvii—O3—H1xxxix96.74 (3)
O2xxviii—S1—O3xxii39.658 (18)O1xxxviii—O3—O1xxxix108.28 (3)
O2xxviii—S1—O3v79.663 (18)O1xxxviii—O3—O2xl56.64 (3)
O2xxviii—S1—O3vi135.395 (18)O1xxxviii—O3—O2xli102.99 (3)
O2xxviii—S1—H1xxiii8.55 (4)O1xxxviii—O3—O2xlii56.27 (3)
O2xxviii—S1—H1xxiv129.75 (4)O1xxxviii—O3—O2lxxvi115.13 (2)
O2xxviii—S1—H1ix107.24 (4)O1xxxviii—O3—O2lxxvii122.49 (3)
O2xxviii—S1—H1x93.04 (4)O1xxxviii—O3—O2lxxviii92.25 (2)
O2xxix—S1—O2xxx165.313 (15)O1xxxviii—O3—H1xxxi64.96 (4)
O2xxix—S1—O2xvii35.779 (18)O1xxxviii—O3—H1xxxiii43.33 (4)
O2xxix—S1—O2xviii135.369 (18)O1xxxviii—O3—H1xxxv121.20 (4)
O2xxix—S1—O3xxi89.236 (16)O1xxxviii—O3—H1xxxvii96.74 (3)
O2xxix—S1—O3xxii100.835 (16)O1xxxviii—O3—H1xxxviii21.15 (2)
O2xxix—S1—O3v36.433 (16)O1xxxviii—O3—H1xxxix129.38 (3)
O2xxix—S1—O3vi129.044 (16)O1xxxix—O3—O2xl102.99 (3)
O2xxix—S1—H1xxiii57.58 (4)O1xxxix—O3—O2xli56.27 (3)
O2xxix—S1—H1xxiv130.60 (4)O1xxxix—O3—O2xlii56.64 (3)
O2xxix—S1—H1ix44.28 (4)O1xxxix—O3—O2lxxvi92.25 (2)
O2xxix—S1—H1x126.96 (4)O1xxxix—O3—O2lxxvii115.13 (2)
O2xxx—S1—O2xvii135.369 (18)O1xxxix—O3—O2lxxviii122.49 (3)
O2xxx—S1—O2xviii35.779 (18)O1xxxix—O3—H1xxxi43.33 (4)
O2xxx—S1—O3xxi100.835 (16)O1xxxix—O3—H1xxxiii121.20 (4)
O2xxx—S1—O3xxii89.236 (16)O1xxxix—O3—H1xxxv64.96 (4)
O2xxx—S1—O3v129.044 (16)O1xxxix—O3—H1xxxvii129.38 (3)
O2xxx—S1—O3vi36.433 (16)O1xxxix—O3—H1xxxviii96.74 (3)
O2xxx—S1—H1xxiii130.60 (4)O1xxxix—O3—H1xxxix21.15 (2)
O2xxx—S1—H1xxiv57.58 (4)O2xl—O3—O2xli57.32 (3)
O2xxx—S1—H1ix126.96 (4)O2xl—O3—O2xlii57.32 (3)
O2xxx—S1—H1x44.28 (4)O2xl—O3—O2lxxvi164.30 (4)
O2xvii—S1—O2xviii134.123 (19)O2xl—O3—O2lxxvii137.17 (3)
O2xvii—S1—O3xxi79.663 (18)O2xl—O3—O2lxxviii131.96 (3)
O2xvii—S1—O3xxii135.395 (18)O2xl—O3—H1xxxi79.01 (4)
O2xvii—S1—O3v39.658 (18)O2xl—O3—H1xxxiii21.72 (4)
O2xvii—S1—O3vi103.729 (18)O2xl—O3—H1xxxv67.96 (4)
O2xvii—S1—H1xxiii93.04 (4)O2xl—O3—H1xxxvii56.23 (3)
O2xvii—S1—H1xxiv107.24 (4)O2xl—O3—H1xxxviii75.86 (3)
O2xvii—S1—H1ix8.55 (4)O2xl—O3—H1xxxix111.89 (4)
O2xvii—S1—H1x129.75 (4)O2xli—O3—O2xlii57.32 (3)
O2xviii—S1—O3xxi135.395 (18)O2xli—O3—O2lxxvi137.17 (3)
O2xviii—S1—O3xxii79.663 (18)O2xli—O3—O2lxxvii131.96 (3)
O2xviii—S1—O3v103.729 (18)O2xli—O3—O2lxxviii164.30 (4)
O2xviii—S1—O3vi39.658 (18)O2xli—O3—H1xxxi67.96 (4)
O2xviii—S1—H1xxiii107.24 (4)O2xli—O3—H1xxxiii79.01 (4)
O2xviii—S1—H1xxiv93.04 (4)O2xli—O3—H1xxxv21.72 (4)
O2xviii—S1—H1ix129.75 (4)O2xli—O3—H1xxxvii75.86 (3)
O2xviii—S1—H1x8.55 (4)O2xli—O3—H1xxxviii111.89 (4)
O3xxi—S1—O3xxii93.815 (17)O2xli—O3—H1xxxix56.23 (3)
O3xxi—S1—O3v117.822 (17)O2xlii—O3—O2lxxvi131.96 (3)
O3xxi—S1—O3vi117.822 (17)O2xlii—O3—O2lxxvii164.30 (4)
O3xxi—S1—H1xxiii96.50 (4)O2xlii—O3—O2lxxviii137.17 (3)
O3xxi—S1—H1xxiv43.46 (4)O2xlii—O3—H1xxxi21.72 (4)
O3xxi—S1—H1ix78.83 (4)O2xlii—O3—H1xxxiii67.96 (4)
O3xxi—S1—H1x143.75 (4)O2xlii—O3—H1xxxv79.01 (4)
O3xxii—S1—O3v117.822 (17)O2xlii—O3—H1xxxvii111.89 (4)
O3xxii—S1—O3vi117.822 (17)O2xlii—O3—H1xxxviii56.23 (3)
O3xxii—S1—H1xxiii43.46 (4)O2xlii—O3—H1xxxix75.86 (3)
O3xxii—S1—H1xxiv96.50 (4)O2lxxvi—O3—O2lxxvii32.402 (16)
O3xxii—S1—H1ix143.75 (4)O2lxxvi—O3—O2lxxviii32.402 (16)
O3xxii—S1—H1x78.83 (4)O2lxxvi—O3—H1xxxi110.64 (4)
O3v—S1—O3vi93.815 (17)O2lxxvi—O3—H1xxxiii142.99 (4)
O3v—S1—H1xxiii78.83 (4)O2lxxvi—O3—H1xxxv123.26 (4)
O3v—S1—H1xxiv143.75 (4)O2lxxvi—O3—H1xxxvii116.13 (3)
O3v—S1—H1ix43.46 (4)O2lxxvi—O3—H1xxxviii98.89 (3)
O3v—S1—H1x96.50 (4)O2lxxvi—O3—H1xxxix83.73 (3)
O3vi—S1—H1xxiii143.75 (4)O2lxxvii—O3—O2lxxviii32.402 (16)
O3vi—S1—H1xxiv78.83 (4)O2lxxvii—O3—H1xxxi142.99 (4)
O3vi—S1—H1ix96.50 (4)O2lxxvii—O3—H1xxxiii123.26 (4)
O3vi—S1—H1x43.46 (4)O2lxxvii—O3—H1xxxv110.64 (4)
H1xxiii—S1—H1xxiv126.72 (5)O2lxxvii—O3—H1xxxvii83.73 (3)
H1xxiii—S1—H1ix101.60 (5)O2lxxvii—O3—H1xxxviii116.13 (3)
H1xxiii—S1—H1x101.60 (5)O2lxxvii—O3—H1xxxix98.89 (3)
H1xxiv—S1—H1ix101.60 (5)O2lxxviii—O3—H1xxxi123.26 (4)
H1xxiv—S1—H1x101.60 (5)O2lxxviii—O3—H1xxxiii110.64 (4)
H1ix—S1—H1x126.72 (5)O2lxxviii—O3—H1xxxv142.99 (4)
S1lxix—P1—S1lxx114.220 (19)O2lxxviii—O3—H1xxxvii98.89 (3)
S1lxix—P1—S1lxxi114.220 (19)O2lxxviii—O3—H1xxxviii83.73 (3)
S1lxix—P1—O1xxxi134.66 (3)O2lxxviii—O3—H1xxxix116.13 (3)
S1lxix—P1—O1xxxii101.48 (2)H1xxxi—O3—H1xxxiii87.87 (5)
S1lxix—P1—O1xxxiii96.26 (2)H1xxxi—O3—H1xxxv87.87 (5)
S1lxix—P1—O1xxxiv109.46 (2)H1xxxi—O3—H1xxxvii133.13 (5)
S1lxix—P1—O1xxxv21.069 (14)H1xxxi—O3—H1xxxviii56.01 (4)
S1lxix—P1—O1xxxvi20.136 (13)H1xxxi—O3—H1xxxix64.43 (4)
S1lxix—P1—O1xxxvii21.335 (14)H1xxxiii—O3—H1xxxv87.87 (5)
S1lxix—P1—O1xxxviii134.94 (3)H1xxxiii—O3—H1xxxvii56.01 (4)
S1lxix—P1—O1xxxix101.97 (2)H1xxxiii—O3—H1xxxviii64.43 (4)
S1lxix—P1—O2xl84.49 (4)H1xxxiii—O3—H1xxxix133.13 (5)
S1lxix—P1—O2xli57.32 (4)H1xxxv—O3—H1xxxvii64.43 (4)
S1lxix—P1—O2xlii160.81 (5)H1xxxv—O3—H1xxxviii133.13 (5)
S1lxix—P1—O375.84 (4)H1xxxv—O3—H1xxxix56.01 (4)
S1lxix—P1—H1xxxi148.06 (5)H1xxxvii—O3—H1xxxviii117.14 (3)
S1lxix—P1—H1xxxiii91.86 (5)H1xxxvii—O3—H1xxxix117.14 (3)
S1lxix—P1—H1xxxv34.32 (4)H1xxxviii—O3—H1xxxix117.14 (3)
S1lxix—P1—H1xxxvii35.59 (2)S1lxxii—H1—P1li116.60 (7)
S1lxix—P1—H1xxxviii146.20 (3)S1lxxii—H1—P1lii67.38 (3)
S1lxix—P1—H1xxxix81.64 (3)S1lxxii—H1—O131.47 (5)
S1lxx—P1—S1lxxi114.220 (19)S1lxxii—H1—O1xliii24.76 (2)
S1lxx—P1—O1xxxi21.069 (14)S1lxxii—H1—O1liii146.04 (6)
S1lxx—P1—O1xxxii20.136 (13)S1lxxii—H1—O1liv115.75 (5)
S1lxx—P1—O1xxxiii134.66 (3)S1lxxii—H1—O1xliv32.50 (3)
S1lxx—P1—O1xxxiv101.48 (2)S1lxxii—H1—O1xlv16.303 (19)
S1lxx—P1—O1xxxv96.26 (2)S1lxxii—H1—O2lxxix138.40 (6)
S1lxx—P1—O1xxxvi109.46 (2)S1lxxii—H1—O2xlvi98.77 (5)
S1lxx—P1—O1xxxvii134.94 (3)S1lxxii—H1—O2i149.45 (12)
S1lxx—P1—O1xxxviii101.97 (2)S1lxxii—H1—O2xlviii85.12 (4)
S1lxx—P1—O1xxxix21.335 (14)S1lxxii—H1—O2xlix111.02 (5)
S1lxx—P1—O2xl160.81 (5)S1lxxii—H1—O2l51.66 (3)
S1lxx—P1—O2xli84.49 (4)S1lxxii—H1—O3li96.67 (5)
S1lxx—P1—O2xlii57.32 (4)S1lxxii—H1—O3lii65.28 (3)
S1lxx—P1—O375.84 (4)S1lxxii—H1—H1lxvii142.48 (6)
S1lxx—P1—H1xxxi34.32 (4)S1lxxii—H1—H1lxviii92.50 (5)
S1lxx—P1—H1xxxiii148.06 (5)S1lxxii—H1—H1liii125.07 (6)
S1lxx—P1—H1xxxv91.86 (5)S1lxxii—H1—H1liv98.33 (5)
S1lxx—P1—H1xxxvii146.20 (3)S1lxxii—H1—H1xliv39.20 (3)
S1lxx—P1—H1xxxviii81.64 (3)S1lxxii—H1—H1xlv39.20 (3)
S1lxx—P1—H1xxxix35.59 (2)P1li—H1—P1lii151.45 (6)
S1lxxi—P1—O1xxxi96.26 (2)P1li—H1—O1140.76 (10)
S1lxxi—P1—O1xxxii109.46 (2)P1li—H1—O1xliii99.43 (6)
S1lxxi—P1—O1xxxiii21.069 (14)P1li—H1—O1liii71.68 (5)
S1lxxi—P1—O1xxxiv20.136 (13)P1li—H1—O1liv112.25 (6)
S1lxxi—P1—O1xxxv134.66 (3)P1li—H1—O1xliv96.77 (6)
S1lxxi—P1—O1xxxvi101.48 (2)P1li—H1—O1xlv132.20 (6)
S1lxxi—P1—O1xxxvii101.97 (2)P1li—H1—O2lxxix21.83 (3)
S1lxxi—P1—O1xxxviii21.335 (14)P1li—H1—O2xlvi30.93 (3)
S1lxxi—P1—O1xxxix134.94 (3)P1li—H1—O2i39.73 (8)
S1lxxi—P1—O2xl57.32 (4)P1li—H1—O2xlviii150.73 (7)
S1lxxi—P1—O2xli160.81 (5)P1li—H1—O2xlix106.19 (6)
S1lxxi—P1—O2xlii84.49 (4)P1li—H1—O2l162.44 (6)
S1lxxi—P1—O375.84 (4)P1li—H1—O3li32.45 (3)
S1lxxi—P1—H1xxxi91.86 (5)P1li—H1—O3lii132.74 (6)
S1lxxi—P1—H1xxxiii34.32 (4)P1li—H1—H1lxvii30.28 (4)
S1lxxi—P1—H1xxxv148.06 (5)P1li—H1—H1lxviii30.28 (4)
S1lxxi—P1—H1xxxvii81.64 (3)P1li—H1—H1liii92.76 (6)
S1lxxi—P1—H1xxxviii35.59 (2)P1li—H1—H1liv134.36 (7)
S1lxxi—P1—H1xxxix146.20 (3)P1li—H1—H1xliv82.65 (5)
O1xxxi—P1—O1xxxii34.298 (18)P1li—H1—H1xlv153.08 (7)
O1xxxi—P1—O1xxxiii117.33 (3)P1lii—H1—O157.33 (6)
O1xxxi—P1—O1xxxiv87.61 (3)P1lii—H1—O1xliii91.01 (4)
O1xxxi—P1—O1xxxv117.33 (3)P1lii—H1—O1liii122.26 (4)
O1xxxi—P1—O1xxxvi126.37 (3)P1lii—H1—O1liv50.09 (2)
O1xxxi—P1—O1xxxvii155.79 (3)P1lii—H1—O1xliv71.89 (4)
O1xxxi—P1—O1xxxviii81.59 (3)P1lii—H1—O1xlv51.79 (3)
O1xxxi—P1—O1xxxix38.94 (2)P1lii—H1—O2lxxix143.53 (5)
O1xxxi—P1—O2xl140.82 (5)P1lii—H1—O2xlvi122.95 (5)
O1xxxi—P1—O2xli101.14 (5)P1lii—H1—O2i122.66 (11)
O1xxxi—P1—O2xlii40.54 (4)P1lii—H1—O2xlviii20.496 (19)
O1xxxi—P1—O380.49 (5)P1lii—H1—O2xlix97.40 (4)
O1xxxi—P1—H1xxxi16.03 (4)P1lii—H1—O2l20.643 (17)
O1xxxi—P1—H1xxxiii128.31 (5)P1lii—H1—O3li163.54 (6)
O1xxxi—P1—H1xxxv112.23 (5)P1lii—H1—O3lii19.865 (17)
O1xxxi—P1—H1xxxvii160.27 (3)P1lii—H1—H1lxvii149.14 (5)
O1xxxi—P1—H1xxxviii61.80 (3)P1lii—H1—H1lxviii127.30 (5)
O1xxxi—P1—H1xxxix56.29 (3)P1lii—H1—H1liii107.85 (5)
O1xxxii—P1—O1xxxiii126.37 (3)P1lii—H1—H1liv30.96 (3)
O1xxxii—P1—O1xxxiv92.24 (2)P1lii—H1—H1xliv87.59 (4)
O1xxxii—P1—O1xxxv87.61 (3)P1lii—H1—H1xlv30.71 (3)
O1xxxii—P1—O1xxxvi92.24 (2)O1—H1—O1xliii41.81 (5)
O1xxxii—P1—O1xxxvii122.75 (3)O1—H1—O1liii121.52 (8)
O1xxxii—P1—O1xxxviii104.28 (3)O1—H1—O1liv105.53 (7)
O1xxxii—P1—O1xxxix34.11 (2)O1—H1—O1xliv62.34 (6)
O1xxxii—P1—O2xl166.71 (5)O1—H1—O1xlv23.60 (5)
O1xxxii—P1—O2xli89.58 (5)O1—H1—O2lxxix159.03 (9)
O1xxxii—P1—O2xlii74.53 (4)O1—H1—O2xlvi130.02 (8)
O1xxxii—P1—O356.33 (4)O1—H1—O2i179.07 (15)
O1xxxii—P1—H1xxxi50.14 (4)O1—H1—O2xlviii67.46 (6)
O1xxxii—P1—H1xxxiii142.35 (5)O1—H1—O2xlix82.30 (7)
O1xxxii—P1—H1xxxv88.52 (5)O1—H1—O2l36.72 (5)
O1xxxii—P1—H1xxxvii128.18 (3)O1—H1—O3li111.16 (8)
O1xxxii—P1—H1xxxviii83.90 (3)O1—H1—O3lii66.81 (6)
O1xxxii—P1—H1xxxix36.75 (2)O1—H1—H1lxvii149.83 (9)
O1xxxiii—P1—O1xxxiv34.298 (18)O1—H1—H1lxviii122.96 (8)
O1xxxiii—P1—O1xxxv117.33 (3)O1—H1—H1liii97.48 (8)
O1xxxiii—P1—O1xxxvi87.61 (3)O1—H1—H1liv83.64 (7)
O1xxxiii—P1—O1xxxvii81.59 (3)O1—H1—H1xliv70.67 (7)
O1xxxiii—P1—O1xxxviii38.94 (2)O1—H1—H1xlv28.27 (6)
O1xxxiii—P1—O1xxxix155.79 (3)O1xliii—H1—O1liii126.41 (5)
O1xxxiii—P1—O2xl40.54 (4)O1xliii—H1—O1liv140.38 (5)
O1xxxiii—P1—O2xli140.82 (5)O1xliii—H1—O1xliv45.53 (3)
O1xxxiii—P1—O2xlii101.14 (5)O1xliii—H1—O1xlv39.26 (3)
O1xxxiii—P1—O380.49 (5)O1xliii—H1—O2lxxix120.27 (5)
O1xxxiii—P1—H1xxxi112.23 (5)O1xliii—H1—O2xlvi92.31 (4)
O1xxxiii—P1—H1xxxiii16.03 (4)O1xliii—H1—O2i138.82 (12)
O1xxxiii—P1—H1xxxv128.31 (5)O1xliii—H1—O2xlviii106.71 (5)
O1xxxiii—P1—H1xxxvii61.80 (3)O1xliii—H1—O2xlix101.89 (4)
O1xxxiii—P1—H1xxxviii56.29 (3)O1xliii—H1—O2l73.07 (3)
O1xxxiii—P1—H1xxxix160.27 (3)O1xliii—H1—O3li73.84 (4)
O1xxxiv—P1—O1xxxv126.37 (3)O1xliii—H1—O3lii90.01 (4)
O1xxxiv—P1—O1xxxvi92.24 (2)O1xliii—H1—H1lxvii119.75 (5)
O1xxxiv—P1—O1xxxvii104.28 (3)O1xliii—H1—H1lxviii83.56 (4)
O1xxxiv—P1—O1xxxviii34.11 (2)O1xliii—H1—H1liii112.17 (5)
O1xxxiv—P1—O1xxxix122.75 (3)O1xliii—H1—H1liv121.51 (5)
O1xxxiv—P1—O2xl74.53 (4)O1xliii—H1—H1xliv42.38 (3)
O1xxxiv—P1—O2xli166.71 (5)O1xliii—H1—H1xlv61.02 (4)
O1xxxiv—P1—O2xlii89.58 (5)O1liii—H1—O1liv87.13 (4)
O1xxxiv—P1—O356.33 (4)O1liii—H1—O1xliv165.68 (6)
O1xxxiv—P1—H1xxxi88.52 (5)O1liii—H1—O1xlv145.12 (5)
O1xxxiv—P1—H1xxxiii50.14 (4)O1liii—H1—O2lxxix55.31 (3)
O1xxxiv—P1—H1xxxv142.35 (5)O1liii—H1—O2xlvi100.14 (5)
O1xxxiv—P1—H1xxxvii83.90 (3)O1liii—H1—O2i57.61 (9)
O1xxxiv—P1—H1xxxviii36.75 (2)O1liii—H1—O2xlviii101.84 (4)
O1xxxiv—P1—H1xxxix128.18 (3)O1liii—H1—O2xlix39.72 (2)
O1xxxv—P1—O1xxxvi34.298 (18)O1liii—H1—O2l125.67 (4)
O1xxxv—P1—O1xxxvii38.94 (2)O1liii—H1—O3li73.18 (4)
O1xxxv—P1—O1xxxviii155.79 (3)O1liii—H1—O3lii135.49 (4)
O1xxxv—P1—O1xxxix81.59 (3)O1liii—H1—H1lxvii42.04 (3)
O1xxxv—P1—O2xl101.14 (5)O1liii—H1—H1lxviii101.86 (5)
O1xxxv—P1—O2xli40.54 (4)O1liii—H1—H1liii24.34 (3)
O1xxxv—P1—O2xlii140.82 (5)O1liii—H1—H1liv95.87 (5)
O1xxxv—P1—O380.49 (5)O1liii—H1—H1xliv150.07 (5)
O1xxxv—P1—H1xxxi128.31 (5)O1liii—H1—H1xlv134.24 (5)
O1xxxv—P1—H1xxxiii112.23 (5)O1liv—H1—O1xliv105.46 (5)
O1xxxv—P1—H1xxxv16.03 (4)O1liv—H1—O1xlv101.31 (4)
O1xxxv—P1—H1xxxvii56.29 (3)O1liv—H1—O2lxxix95.19 (4)
O1xxxv—P1—H1xxxviii160.27 (3)O1liv—H1—O2xlvi102.64 (5)
O1xxxv—P1—H1xxxix61.80 (3)O1liv—H1—O2i74.23 (9)
O1xxxvi—P1—O1xxxvii34.11 (2)O1liv—H1—O2xlviii38.52 (2)
O1xxxvi—P1—O1xxxviii122.75 (3)O1liv—H1—O2xlix91.79 (4)
O1xxxvi—P1—O1xxxix104.28 (3)O1liv—H1—O2l69.64 (3)
O1xxxvi—P1—O2xl89.58 (5)O1liv—H1—O3li143.30 (6)
O1xxxvi—P1—O2xli74.53 (4)O1liv—H1—O3lii51.07 (2)
O1xxxvi—P1—O2xlii166.71 (5)O1liv—H1—H1lxvii99.09 (4)
O1xxxvi—P1—O356.33 (4)O1liv—H1—H1lxviii112.27 (5)
O1xxxvi—P1—H1xxxi142.35 (5)O1liv—H1—H1liii90.12 (4)
O1xxxvi—P1—H1xxxiii88.52 (5)O1liv—H1—H1liv22.13 (3)
O1xxxvi—P1—H1xxxv50.14 (4)O1liv—H1—H1xliv117.41 (4)
O1xxxvi—P1—H1xxxvii36.75 (2)O1liv—H1—H1xlv80.76 (4)
O1xxxvi—P1—H1xxxviii128.18 (3)O1xliv—H1—O1xlv40.12 (3)
O1xxxvi—P1—H1xxxix83.90 (3)O1xliv—H1—O2lxxix115.52 (5)
O1xxxvii—P1—O1xxxviii119.94 (3)O1xliv—H1—O2xlvi70.83 (4)
O1xxxvii—P1—O1xxxix119.94 (3)O1xliv—H1—O2i118.59 (12)
O1xxxvii—P1—O2xl63.37 (4)O1xliv—H1—O2xlviii92.36 (5)
O1xxxvii—P1—O2xli63.99 (4)O1xliv—H1—O2xlix143.51 (6)
O1xxxvii—P1—O2xlii156.53 (5)O1xliv—H1—O2l66.50 (4)
O1xxxvii—P1—O388.61 (5)O1xliv—H1—O3li92.52 (5)
O1xxxvii—P1—H1xxxi166.16 (5)O1xliv—H1—O3lii58.68 (4)
O1xxxvii—P1—H1xxxiii73.71 (5)O1xliv—H1—H1lxvii127.04 (6)
O1xxxvii—P1—H1xxxv46.77 (4)O1xliv—H1—H1lxviii67.34 (4)
O1xxxvii—P1—H1xxxvii20.67 (3)O1xliv—H1—H1liii156.93 (7)
O1xxxvii—P1—H1xxxviii137.53 (3)O1xliv—H1—H1liv98.33 (5)
O1xxxvii—P1—H1xxxix100.68 (3)O1xliv—H1—H1xliv15.71 (3)
O1xxxviii—P1—O1xxxix119.94 (3)O1xliv—H1—H1xlv56.43 (4)
O1xxxviii—P1—O2xl63.99 (4)O1xlv—H1—O2lxxix153.66 (5)
O1xxxviii—P1—O2xli156.53 (5)O1xlv—H1—O2xlvi110.62 (5)
O1xxxviii—P1—O2xlii63.37 (4)O1xlv—H1—O2i157.26 (12)
O1xxxviii—P1—O388.61 (5)O1xlv—H1—O2xlviii68.89 (3)
O1xxxviii—P1—H1xxxi73.71 (5)O1xlv—H1—O2xlix105.70 (4)
O1xxxviii—P1—H1xxxiii46.77 (4)O1xlv—H1—O2l35.35 (2)
O1xxxviii—P1—H1xxxv166.16 (5)O1xlv—H1—O3li112.63 (5)
O1xxxviii—P1—H1xxxvii100.68 (3)O1xlv—H1—O3lii52.84 (3)
O1xxxviii—P1—H1xxxviii20.67 (3)O1xlv—H1—H1lxvii158.65 (5)
O1xxxviii—P1—H1xxxix137.53 (3)O1xlv—H1—H1lxviii105.84 (4)
O1xxxix—P1—O2xl156.53 (5)O1xlv—H1—H1liii120.98 (5)
O1xxxix—P1—O2xli63.37 (4)O1xlv—H1—H1liv82.56 (4)
O1xxxix—P1—O2xlii63.99 (4)O1xlv—H1—H1xliv51.27 (3)
O1xxxix—P1—O388.61 (5)O1xlv—H1—H1xlv22.90 (3)
O1xxxix—P1—H1xxxi46.77 (4)O2lxxix—H1—O2xlvi45.00 (3)
O1xxxix—P1—H1xxxiii166.16 (5)O2lxxix—H1—O2i21.09 (8)
O1xxxix—P1—H1xxxv73.71 (5)O2lxxix—H1—O2xlviii132.63 (5)
O1xxxix—P1—H1xxxvii137.53 (3)O2lxxix—H1—O2xlix94.05 (4)
O1xxxix—P1—H1xxxviii100.68 (3)O2lxxix—H1—O2l164.18 (5)
O1xxxix—P1—H1xxxix20.67 (3)O2lxxix—H1—O3li48.13 (3)
O2xl—P1—O2xli103.59 (6)O2lxxix—H1—O3lii131.76 (5)
O2xl—P1—O2xlii103.59 (6)O2lxxix—H1—H1lxvii14.75 (3)
O2xl—P1—O3114.86 (7)O2lxxix—H1—H1lxviii48.37 (3)
O2xl—P1—H1xxxi126.57 (7)O2lxxix—H1—H1liii78.98 (4)
O2xl—P1—H1xxxiii24.51 (5)O2lxxix—H1—H1liv116.80 (5)
O2xl—P1—H1xxxv102.67 (6)O2lxxix—H1—H1xliv102.80 (5)
O2xl—P1—H1xxxvii52.86 (4)O2lxxix—H1—H1xlv168.84 (5)
O2xl—P1—H1xxxviii84.63 (5)O2xlvi—H1—O2i50.87 (9)
O2xl—P1—H1xxxix156.45 (5)O2xlvi—H1—O2xlviii132.96 (5)
O2xli—P1—O2xlii103.59 (6)O2xlvi—H1—O2xlix137.02 (5)
O2xli—P1—O3114.86 (7)O2xlvi—H1—O2l131.95 (5)
O2xli—P1—H1xxxi102.67 (6)O2xlvi—H1—O3li53.12 (4)
O2xli—P1—H1xxxiii126.57 (7)O2xlvi—H1—O3lii103.19 (4)
O2xli—P1—H1xxxv24.51 (5)O2xlvi—H1—H1lxvii58.25 (4)
O2xli—P1—H1xxxvii84.63 (5)O2xlvi—H1—H1lxviii9.80 (3)
O2xli—P1—H1xxxviii156.45 (5)O2xlvi—H1—H1liii122.96 (6)
O2xli—P1—H1xxxix52.86 (4)O2xlvi—H1—H1liv120.73 (6)
O2xlii—P1—O3114.86 (7)O2xlvi—H1—H1xliv59.81 (4)
O2xlii—P1—H1xxxi24.51 (5)O2xlvi—H1—H1xlv125.53 (5)
O2xlii—P1—H1xxxiii102.67 (6)O2i—H1—O2xlviii112.21 (11)
O2xlii—P1—H1xxxv126.57 (7)O2i—H1—O2xlix96.79 (10)
O2xlii—P1—H1xxxvii156.45 (5)O2i—H1—O2l143.23 (11)
O2xlii—P1—H1xxxviii52.86 (4)O2i—H1—O3li69.07 (9)
O2xlii—P1—H1xxxix84.63 (5)O2i—H1—O3lii113.49 (11)
O3—P1—H1xxxi94.31 (6)O2i—H1—H1lxvii29.84 (8)
O3—P1—H1xxxiii94.31 (6)O2i—H1—H1lxviii57.88 (9)
O3—P1—H1xxxv94.31 (6)O2i—H1—H1liii81.63 (10)
O3—P1—H1xxxvii79.98 (5)O2i—H1—H1liv96.07 (10)
O3—P1—H1xxxviii79.98 (5)O2i—H1—H1xliv110.25 (11)
O3—P1—H1xxxix79.98 (5)O2i—H1—H1xlv151.96 (12)
H1xxxi—P1—H1xxxiii119.44 (7)O2xlviii—H1—O2xlix81.34 (4)
H1xxxi—P1—H1xxxv119.44 (7)O2xlviii—H1—O2l33.78 (2)
H1xxxi—P1—H1xxxvii172.21 (5)O2xlviii—H1—O3li173.41 (6)
H1xxxi—P1—H1xxxviii56.28 (5)O2xlviii—H1—O3lii36.74 (2)
H1xxxi—P1—H1xxxix66.64 (5)O2xlviii—H1—H1lxvii132.40 (5)
H1xxxiii—P1—H1xxxv119.44 (7)O2xlviii—H1—H1lxviii140.35 (5)
H1xxxiii—P1—H1xxxvii56.28 (5)O2xlviii—H1—H1liii89.44 (4)
H1xxxiii—P1—H1xxxviii66.64 (5)O2xlviii—H1—H1liv16.39 (3)
H1xxxiii—P1—H1xxxix172.21 (5)O2xlviii—H1—H1xliv108.06 (5)
H1xxxv—P1—H1xxxvii66.64 (5)O2xlviii—H1—H1xlv46.12 (3)
H1xxxv—P1—H1xxxviii172.21 (5)O2xlix—H1—O2l91.03 (4)
H1xxxv—P1—H1xxxix56.28 (5)O2xlix—H1—O3li92.11 (4)
H1xxxvii—P1—H1xxxviii117.04 (3)O2xlix—H1—O3lii116.98 (4)
H1xxxvii—P1—H1xxxix117.04 (3)O2xlix—H1—H1lxvii79.74 (4)
H1xxxviii—P1—H1xxxix117.04 (3)O2xlix—H1—H1lxviii135.07 (5)
S1lxxii—O1—P1li99.56 (4)O2xlix—H1—H1liii15.38 (3)
S1lxxii—O1—P1xxii70.79 (3)O2xlix—H1—H1liv85.64 (4)
S1lxxii—O1—P1lii93.62 (4)O2xlix—H1—H1xliv144.18 (5)
S1lxxii—O1—O1xliii35.08 (3)O2xlix—H1—H1xlv96.46 (4)
S1lxxii—O1—O1xliv35.36 (3)O2l—H1—O3li146.69 (5)
S1lxxii—O1—O1xlv35.36 (3)O2l—H1—O3lii34.233 (19)
S1lxxii—O1—O2xlvi82.39 (3)O2l—H1—H1lxvii165.37 (5)
S1lxxii—O1—O2i115.84 (5)O2l—H1—H1lxviii132.19 (5)
S1lxxii—O1—O2xlvii52.74 (3)O2l—H1—H1liii104.76 (4)
S1lxxii—O1—O2xlviii118.42 (5)O2l—H1—H1liv48.65 (3)
S1lxxii—O1—O2xlix155.46 (5)O2l—H1—H1xliv81.30 (4)
S1lxxii—O1—O2l83.50 (4)O2l—H1—H1xlv12.45 (3)
S1lxxii—O1—O3li92.88 (4)O3li—H1—O3lii149.38 (5)
S1lxxii—O1—O3xxii89.59 (4)O3li—H1—H1lxvii46.06 (4)
S1lxxii—O1—O3lii80.22 (4)O3li—H1—H1lxviii46.06 (4)
S1lxxii—O1—H1115.48 (8)O3li—H1—H1liii84.34 (5)
S1lxxii—O1—H1xliii46.41 (4)O3li—H1—H1liv164.63 (7)
S1lxxii—O1—H1liii156.29 (5)O3li—H1—H1xliv76.91 (4)
S1lxxii—O1—H1liv121.93 (5)O3li—H1—H1xlv134.86 (6)
S1lxxii—O1—H1xliv29.04 (3)O3lii—H1—H1lxvii143.32 (5)
S1lxxii—O1—H1xlv68.31 (5)O3lii—H1—H1lxviii107.49 (4)
P1li—O1—P1xxii133.89 (3)O3lii—H1—H1liii126.18 (5)
P1li—O1—P1lii121.63 (3)O3lii—H1—H1liv39.65 (3)
P1li—O1—O1xliii90.20 (3)O3lii—H1—H1xliv73.76 (4)
P1li—O1—O1xliv73.78 (3)O3lii—H1—H1xlv38.66 (3)
P1li—O1—O1xlv133.07 (4)H1lxvii—H1—H1lxviii60.00 (4)
P1li—O1—O2xlvi21.784 (18)H1lxvii—H1—H1liii64.93 (4)
P1li—O1—O2i23.40 (2)H1lxvii—H1—H1liv118.68 (5)
P1li—O1—O2xlvii119.89 (3)H1lxvii—H1—H1xliv112.78 (5)
P1li—O1—O2xlviii109.72 (3)H1lxvii—H1—H1xlv176.20 (6)
P1li—O1—O2xlix82.14 (3)H1lxviii—H1—H1liii122.73 (5)
P1li—O1—O2l146.16 (3)H1lxviii—H1—H1liv129.57 (6)
P1li—O1—O3li23.843 (19)H1lxviii—H1—H1xliv54.57 (4)
P1li—O1—O3xxii127.60 (3)H1lxviii—H1—H1xlv123.61 (5)
P1li—O1—O3lii106.61 (3)H1liii—H1—H1liv89.76 (5)
P1li—O1—H123.21 (6)H1liii—H1—H1xliv151.82 (6)
P1li—O1—H1xliii112.15 (4)H1liii—H1—H1xlv111.27 (5)
P1li—O1—H1liii68.11 (3)H1liv—H1—H1xliv113.29 (5)
P1li—O1—H1liv94.70 (3)H1liv—H1—H1xlv60.50 (4)
P1li—O1—H1xliv71.91 (3)H1xliv—H1—H1xlv70.44 (4)
P1li—O1—H1xlv148.51 (5)
Symmetry codes: (i) y, z, x; (ii) y, z1/2, x+1/2; (iii) x1, y1, z1; (iv) x1, y+1, z+3/2; (v) y3/4, x3/4, z3/4; (vi) y3/4, x+3/4, z+5/4; (vii) z, x1, y; (viii) z, x+1, y+1/2; (ix) y+1/4, x3/4, z+1/4; (x) y+1/4, x+3/4, z+1/4; (xi) x+3/4, z1/4, y+1/4; (xii) x+3/4, z+1/4, y+1/4; (xiii) x, y1, z; (xiv) x, y+1, z+1/2; (xv) y1, z, x; (xvi) y1, z, x+1/2; (xvii) z+1/4, y3/4, x+1/4; (xviii) z+1/4, y+3/4, x+1/4; (xix) x1, y, z; (xx) x1, y, z+1/2; (xxi) x+3/2, y+1, z1/2; (xxii) x+3/2, y1, z+1; (xxiii) y+1/2, z, x+1; (xxiv) y+1/2, z, x1/2; (xxv) x+1/2, y+1, z+1/2; (xxvi) x+1/2, y1, z; (xxvii) z+1/2, x, y1/2; (xxviii) z+1/2, x, y+1; (xxix) x+1/4, z+1/4, y3/4; (xxx) x+1/4, z1/4, y+5/4; (xxxi) x, y+1, z+1; (xxxii) x+3/2, y+1, z+1; (xxxiii) z+1, x, y+1; (xxxiv) z+1, x+3/2, y+1; (xxxv) y+1, z+1, x; (xxxvi) y+1, z+1, x+3/2; (xxxvii) y+5/4, x+7/4, z+3/4; (xxxviii) x+7/4, z+3/4, y+5/4; (xxxix) z+3/4, y+5/4, x+7/4; (xl) x+1, y, z+1; (xli) z+1, x+1, y; (xlii) y, z+1, x+1; (xliii) x+3/2, y, z; (xliv) z+3/4, y+1/4, x+3/4; (xlv) z+3/4, y+1/4, x3/4; (xlvi) z+1, x, y1; (xlvii) y+3/2, z, x; (xlviii) y+7/4, x+1/4, z+1/4; (xlix) y+7/4, x1/4, z+1/4; (l) x+3/4, z+1/4, y3/4; (li) x, y1, z1; (lii) y+7/4, x+5/4, z3/4; (liii) x+7/4, z1/4, y+1/4; (liv) x+7/4, z+1/4, y+1/4; (lv) z, x+1, y1; (lvi) y1, z+1, x; (lvii) z+1/4, y+7/4, x+1/4; (lviii) z+1/4, y+7/4, x1/4; (lix) x1, y, z1; (lx) y3/4, x+1/4, z3/4; (lxi) x1, y+1, z; (lxii) z, x, y; (lxiii) y, z+1, x1; (lxiv) y+1/4, x+7/4, z1/4; (lxv) y+1/4, x+7/4, z+1/4; (lxvi) x+3/4, z+3/4, y+1/4; (lxvii) z+1, x1, y; (lxviii) y+1, z, x1; (lxix) x+3/2, y+1, z+1/2; (lxx) z+1/2, x+3/2, y+1; (lxxi) y+1, z+1/2, x+3/2; (lxxii) z+1/2, x+1/2, y; (lxxiii) x+1/2, y+1, z1/2; (lxxiv) y, z+1/2, x+1/2; (lxxv) z, x+3/2, y; (lxxvi) y1/4, x+3/4, z+3/4; (lxxvii) x+3/4, z+3/4, y1/4; (lxxviii) z+3/4, y1/4, x+3/4; (lxxix) x+1, y1, z.
 

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