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Figure 1
(a) The experimental arrangement used to record diffuse scattering using high-energy X-rays ([\lambda = 0.30996] Å). (b) A single frame of data for PCNB recorded with a 2 s exposure using a Mar345 Image-plate detector. 500 frames, recorded at intervals of [0.36^{\circ}] of the crystal rotation, [\omega], were used for the complete three-dimensional set of data used in the study described in §3[link]. The dark region near the middle of the pattern is due to air scattering. This was subsequently subtracted during processing. The maximum [\sin\theta/\lambda] recorded was 0.85 Å−1.

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ISSN: 2053-2733
Volume 64| Part 1| January 2008| Pages 23-32
https://doi.org/10.1107/S0108767307041918
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