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Figure 2
High-resolution X-ray powder diffraction profiles from the final Rietveld refinement of the doubled-unit-cell T3R3 complex [(a) with λ = 1.401107 Å] and also the normal T3R3 complex [(b) with λ = 0.700233 Å]. Observed intensities are shown in red (+), calculated and difference curves as green and magenta lines and the reflection positions are shown in black (|). The background intensity found in the refinement has been subtracted from the observed and calculated intensities for clarity. [Reproduction of Fig. 2 in Von Dreele et al. (2000BB52).]

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