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Figure 7
(a) The number of independent observations and (b) the ratio of powder diffraction versus single-crystal observations as a function of reciprocal d spacing (1/d) (Å−1) and asymmetric unit-cell size (Å3) for a Δd/d resolution of 10−4.  (c) The number of independent observations and (d) the ratio of powder diffraction versus single-crystal observations as a function of reciprocal d spacing (1/d) (Å−1) and asymmetric unit-cell size (Å3) for a Δd/d resolution of 10−3. Note that an observation will generally consist of multiple Bragg reflections.

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