Figure 2
The integrated intensity for the measured reflections (grey central bars) displayed as a bar graph for an Si sample (Si crystallites immersed in a resin that occupy 50% of the volume), compared with the conventional theory: blue right-hand bars, include dynamical effects, cyan left-hand bars based purely on kinematical theory (large diamonds for B = 0.02 Å−2, small diamonds for B = 0.046 Å−2). The experimental data were collected on an instrument with R = 320 mm, divergence slit = 0.125°, a PIXcel detector with 255 strips of 0.055 mm and Soller slits of 0.04 radian and Cu Kα. The black diamond is the mean of six measurements on different samples, the `x' marks are the standard deviation points and `o' symbols the range. |